#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/02/2200214.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200214_Fobs loop_ _publ_author_name 'Arnold, Polly L.' 'Blake, Alexander J.' _publ_section_title ; Selective reduction in ring size of silsesquioxane oligomers mediated by potassium metal ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o131 _journal_page_last o133 _journal_volume 57 _journal_year 2001 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 75.182 _cell_angle_beta 89.959 _cell_angle_gamma 89.793 _cell_length_a 11.9992 _cell_length_b 14.6230 _cell_length_c 15.0146 _exptl_crystal_F_000 1040.00 _reflns_d_resolution_high 0.8108 _[local]_cod_data_source_file om6001Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' SI8OPE #2081 for /PLA, Soton kappaCCD data in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 236.13 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ 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31.66 o 8 1 0 113.09 106.78 37.56 o 9 1 0 27.82 11.54 23.07 o 10 1 0 10.30 17.44 46.14 o 11 1 0 163.17 280.62 72.44 o 12 1 0 4.45 34.88 81.02 o 13 1 0 343.18 296.18 104.63 o 14 1 0 85.96 218.11 99.00 o -14 2 0 418.98 386.59 104.63 o -13 2 0 133.65 136.56 69.75 o -10 2 0 54.44 84.24 40.78 o -9 2 0 212.59 250.04 52.31 o -8 2 0 359.00 374.70 26.85 o -7 2 0 1056.44 1139.80 55.62 o -6 2 0 3820.95 3867.00 327.30 o -5 2 0 826.70 868.37 47.91 o -4 2 0 143.93 147.96 13.13 o -3 2 0 2071.30 2178.50 106.57 o -2 2 0 10881.41 11132.65 633.05 o -1 2 0 3327.79 3274.61 196.13 o 1 2 0 126.78 159.32 11.14 o 2 2 0 5369.29 4878.16 423.86 o 3 2 0 6832.59 7206.98 311.90 o 4 2 0 994.72 1290.54 67.51 o 5 2 0 2.07 -5.66 5.77 o 6 2 0 2866.38 2998.53 119.74 o 7 2 0 1222.07 1265.49 92.29 o 8 2 0 2247.81 2347.48 177.30 o 9 2 0 1427.38 1867.50 150.51 o 10 2 0 10.92 -8.58 40.51 o 11 2 0 60.54 17.44 72.44 o 12 2 0 1.73 -26.02 60.90 o 13 2 0 6.25 28.97 78.34 o 14 2 0 117.35 136.82 119.39 o -14 3 0 5.04 -8.85 87.19 o 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1.62 -17.92 33.55 o 12 6 0 413.06 440.82 58.35 o 13 6 0 103.01 159.09 56.50 o -13 7 0 277.19 224.01 59.02 o -12 7 0 105.36 71.26 35.22 o -11 7 0 493.58 468.42 96.04 o -10 7 0 12.06 3.28 32.43 o -9 7 0 872.84 868.77 84.11 o -8 7 0 237.27 241.44 57.28 o -7 7 0 2286.71 2232.37 175.69 o -6 7 0 2655.66 2734.10 195.05 o -5 7 0 13.67 1.30 36.08 o -4 7 0 172.13 125.60 26.43 o -3 7 0 190.24 187.87 30.45 o -2 7 0 13.89 -5.19 45.07 o -1 7 0 3488.35 3321.20 309.19 o 0 7 0 354.70 349.88 32.90 o 1 7 0 3858.17 3932.59 289.34 o 2 7 0 236.32 215.16 25.64 o 3 7 0 239.47 199.07 25.56 o 4 7 0 2393.63 2373.02 147.35 o 5 7 0 58.24 55.98 19.25 o 6 7 0 1693.98 1802.03 120.12 o 7 7 0 688.83 715.00 57.15 o 8 7 0 657.73 680.61 46.61 o 9 7 0 74.01 95.61 27.57 o 11 7 0 1.10 40.85 40.91 o 12 7 0 0.29 55.53 90.41 o 13 7 0 91.76 -5.90 105.17 o -13 8 0 388.82 329.99 59.02 o -12 8 0 25.65 -4.21 33.74 o -11 8 0 9.19 72.44 66.80 o -10 8 0 182.44 164.51 36.58 o -9 8 0 779.00 632.58 84.11 o -8 8 0 1677.51 1535.37 161.51 o 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48.29 o 3 9 0 1032.76 1137.68 85.93 o 4 9 0 3151.47 2889.34 218.99 o 5 9 0 25.43 5.82 18.10 o 6 9 0 494.41 432.12 34.30 o 7 9 0 2388.99 2517.18 156.89 o 8 9 0 141.35 101.89 32.90 o 9 9 0 3.32 11.80 49.90 o 10 9 0 647.56 687.89 68.94 o 11 9 0 42.20 -2.95 44.80 o 12 9 0 33.63 -41.05 73.24 o -12 10 0 73.75 5.90 60.90 o -11 10 0 15.58 46.14 57.68 o -10 10 0 162.26 202.82 68.41 o -9 10 0 715.51 553.46 86.65 o -8 10 0 199.93 177.32 54.19 o -7 10 0 30.39 -14.37 36.42 o -6 10 0 1336.21 1472.82 116.04 o -5 10 0 63.64 61.36 26.53 o -4 10 0 26.38 -11.70 35.72 o -3 10 0 1672.59 1805.17 125.36 o -2 10 0 0.16 -5.01 22.23 o -1 10 0 41.97 10.19 53.92 o 0 10 0 2604.33 2599.32 364.46 o 1 10 0 581.48 619.45 76.06 o 2 10 0 2381.32 2285.31 147.58 o 3 10 0 4396.27 4897.11 300.44 o 4 10 0 354.14 324.89 60.90 o 5 10 0 1232.95 1184.35 76.87 o 6 10 0 282.13 232.18 34.22 o 7 10 0 104.67 79.15 29.21 o 8 10 0 2380.40 2356.30 213.48 o 9 10 0 285.65 230.33 40.97 o 10 10 0 309.68 192.36 65.19 o -11 11 0 153.33 40.24 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106.24 o -1 17 0 318.01 224.01 123.41 o 0 17 0 83.31 143.53 60.36 o 1 17 0 184.02 246.55 88.80 o 2 17 0 2.95 25.75 108.65 o 3 17 0 295.14 332.94 133.87 o -2 -17 1 106.82 122.60 102.48 o -1 -17 1 36.54 22.80 82.90 o 0 -17 1 9.41 -68.68 94.43 o 1 -17 1 132.78 100.34 111.87 o -5 -16 1 315.24 264.26 81.56 o -3 -16 1 223.14 141.92 88.00 o -2 -16 1 1.32 96.85 88.53 o -1 -16 1 145.41 77.26 88.80 o 0 -16 1 61.94 11.54 54.46 o 1 -16 1 3.23 -103.29 80.22 o 2 -16 1 24.53 -71.63 74.58 o 3 -16 1 2.73 57.14 100.07 o 4 -16 1 68.86 168.21 68.41 o -7 -15 1 5.99 -67.34 84.24 o -6 -15 1 280.75 235.82 106.78 o -5 -15 1 125.60 49.21 68.39 o -4 -15 1 8.67 40.31 92.56 o -3 -15 1 72.66 20.39 101.95 o -2 -15 1 10.33 12.54 48.70 o -1 -15 1 0.97 -108.92 80.22 o 0 -15 1 153.20 243.87 80.48 o 1 -15 1 308.70 332.94 77.53 o 2 -15 1 112.38 103.29 48.83 o 3 -15 1 3.84 -8.58 57.14 o 5 -15 1 352.74 471.64 108.12 o 6 -15 1 269.51 240.65 76.46 o 7 -15 1 171.06 313.62 110.26 o -8 -14 1 0.03 -76.46 56.61 o -7 -14 1 164.07 126.63 87.19 o -6 -14 1 506.62 494.35 138.57 o -5 -14 1 70.24 8.02 39.74 o -4 -14 1 0.33 -46.92 33.39 o -3 -14 1 114.88 98.85 105.30 o -2 -14 1 490.67 530.67 85.62 o -1 -14 1 417.80 323.78 70.52 o 0 -14 1 386.90 430.11 70.93 o 1 -14 1 261.56 269.44 64.90 o 2 -14 1 70.50 17.17 66.00 o 3 -14 1 11.56 -28.71 71.63 o 4 -14 1 600.07 658.90 128.51 o 5 -14 1 59.38 11.27 51.24 o 6 -14 1 97.69 59.56 87.73 o 7 -14 1 310.06 186.72 76.46 o 8 -14 1 123.47 90.41 67.88 o -9 -13 1 323.30 353.06 83.44 o -8 -13 1 588.97 602.29 127.97 o -7 -13 1 219.52 191.34 55.43 o -6 -13 1 82.16 90.38 39.39 o -5 -13 1 537.53 575.00 74.41 o -4 -13 1 133.23 149.68 50.59 o -3 -13 1 178.55 152.62 54.97 o -2 -13 1 780.50 934.43 94.31 o -1 -13 1 44.40 21.56 86.92 o 0 -13 1 1331.92 1255.61 143.26 o 1 -13 1 55.07 66.71 45.87 o 2 -13 1 292.20 310.23 87.33 o 3 -13 1 356.09 393.50 63.41 o 4 -13 1 69.54 14.22 51.24 o 5 -13 1 428.43 409.40 102.48 o 6 -13 1 470.69 461.98 107.85 o 7 -13 1 362.18 444.01 104.63 o 8 -13 1 79.90 8.58 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