#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2200303.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200303_Fobs loop_ _publ_author_name 'Bolte, Michael' 'Lerner, Hans-Wolfram' _publ_section_title ; Lithium trifluoromethanesulfonate ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m231 _journal_page_last m232 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.370 _cell_angle_gamma 90.000 _cell_length_a 10.0994 _cell_length_b 5.0410 _cell_length_c 9.5320 _exptl_crystal_F_000 304.00 _reflns_d_resolution_high 0.7220 _[local]_cod_data_source_file cv6022Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' wa75 in P21/c (Nr. 14)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 105.26 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2866.39 3147.92 31.49 o 3 0 0 1560.85 1922.75 19.82 o 4 0 0 9867.87 11997.84 175.53 o 5 0 0 1214.44 1416.12 17.15 o 6 0 0 1664.41 1961.73 18.35 o 7 0 0 122.85 128.58 2.80 o 8 0 0 1003.69 1186.57 21.79 o 9 0 0 31.85 43.65 2.66 o 10 0 0 0.16 1.04 1.54 o 11 0 0 700.42 839.48 14.03 o 12 0 0 474.91 587.07 12.70 o 13 0 0 95.46 105.70 5.72 o 1 1 0 5724.28 5433.96 60.77 o 2 1 0 512.40 520.59 4.07 o 3 1 0 2080.01 2182.82 19.07 o 4 1 0 0.16 1.91 0.54 o 5 1 0 703.96 690.24 5.88 o 6 1 0 100.11 90.47 1.43 o 7 1 0 94.88 88.32 2.03 o 8 1 0 6.48 4.06 0.99 o 9 1 0 25.39 24.51 1.32 o 10 1 0 153.12 166.00 2.65 o 11 1 0 154.76 172.72 3.25 o 12 1 0 99.33 114.63 3.70 o 13 1 0 104.13 103.25 8.27 o 0 2 0 1815.67 1772.59 17.31 o 1 2 0 0.06 0.22 0.61 o 2 2 0 381.54 389.81 3.00 o 3 2 0 641.02 696.39 8.05 o 4 2 0 123.27 136.75 1.62 o 5 2 0 258.32 281.22 4.07 o 6 2 0 419.72 423.94 4.43 o 7 2 0 213.82 216.76 3.24 o 8 2 0 97.63 105.34 2.37 o 9 2 0 23.07 21.44 1.68 o 10 2 0 18.21 17.12 1.73 o 11 2 0 3.10 1.75 1.46 o 12 2 0 5.79 2.89 2.04 o 1 3 0 705.02 675.41 4.85 o 2 3 0 117.15 118.86 1.66 o 3 3 0 137.36 135.21 2.15 o 4 3 0 634.62 646.09 6.63 o 5 3 0 224.48 226.58 3.46 o 6 3 0 17.03 16.61 1.76 o 7 3 0 297.88 313.42 4.27 o 8 3 0 252.56 258.09 4.39 o 9 3 0 8.71 12.15 2.02 o 10 3 0 126.07 125.57 3.13 o 11 3 0 124.34 112.43 3.47 o 0 4 0 1072.88 1057.23 13.58 o 1 4 0 81.00 83.79 2.34 o 2 4 0 56.40 53.25 2.13 o 3 4 0 662.35 703.65 7.45 o 4 4 0 57.39 55.97 2.54 o 5 4 0 482.44 479.38 5.89 o 6 4 0 26.03 22.06 2.43 o 7 4 0 20.74 20.26 2.40 o 8 4 0 187.91 184.60 3.91 o 9 4 0 172.54 170.76 4.09 o 10 4 0 69.21 67.37 6.88 o 1 5 0 3.56 6.38 3.61 o 2 5 0 165.65 155.96 4.18 o 3 5 0 4.41 2.60 2.35 o 4 5 0 52.20 50.43 3.40 o 5 5 0 1.99 1.95 2.33 o 6 5 0 14.67 16.10 2.87 o 7 5 0 8.26 10.34 2.86 o 8 5 0 6.05 3.66 4.06 o 0 6 0 146.62 137.64 10.53 o 1 6 0 2.40 2.71 10.09 o 2 6 0 98.21 105.64 17.26 o 3 6 0 69.32 67.98 9.24 o 4 6 0 0.16 2.70 4.88 o 5 6 0 162.99 154.04 8.05 o 6 6 0 161.85 160.29 16.35 o -12 1 1 25.09 24.07 2.09 o -11 1 1 132.13 133.60 3.59 o -10 1 1 86.71 85.11 2.17 o -9 1 1 108.39 116.06 2.15 o -8 1 1 2995.24 2996.64 34.39 o -7 1 1 253.77 276.62 2.99 o -6 1 1 770.69 773.16 7.01 o -5 1 1 1966.81 2016.21 14.89 o -4 1 1 5130.18 5135.99 56.50 o -3 1 1 8074.81 7751.78 50.59 o -2 1 1 4853.02 4736.81 23.54 o -1 1 1 96.95 122.85 1.06 o 0 1 1 963.52 931.54 5.19 o 1 1 1 1708.41 1728.34 31.60 o 2 1 1 310.03 322.15 3.28 o 3 1 1 2393.75 2315.64 19.41 o 4 1 1 1432.16 1463.94 14.07 o 5 1 1 1492.07 1534.96 12.32 o 6 1 1 143.74 139.99 1.60 o 7 1 1 492.26 495.61 6.22 o 8 1 1 61.49 59.47 2.63 o 9 1 1 347.17 376.56 3.81 o 10 1 1 21.95 22.52 1.83 o 11 1 1 3.35 1.14 1.71 o 12 1 1 126.89 139.18 3.51 o 13 1 1 21.29 14.80 11.20 o -12 2 1 92.70 90.33 4.49 o -11 2 1 18.69 17.08 2.03 o -10 2 1 19.11 22.68 1.92 o -9 2 1 487.03 495.44 5.07 o -8 2 1 35.17 42.85 1.83 o -7 2 1 1267.47 1240.37 11.37 o -6 2 1 60.79 66.62 1.95 o -5 2 1 1042.59 1055.88 9.23 o -4 2 1 1079.81 1032.84 7.21 o -3 2 1 1760.21 1809.48 17.46 o -2 2 1 305.33 260.60 2.39 o -1 2 1 119.70 165.81 1.77 o 0 2 1 467.92 458.04 3.36 o 1 2 1 9.23 18.88 0.73 o 2 2 1 663.54 579.02 3.82 o 3 2 1 494.10 488.50 3.56 o 4 2 1 1116.50 1112.01 7.21 o 5 2 1 666.10 642.87 4.80 o 6 2 1 487.89 467.97 4.61 o 7 2 1 78.11 73.72 2.50 o 8 2 1 1212.03 1239.14 12.79 o 9 2 1 17.66 19.73 1.69 o 10 2 1 7.34 8.99 1.72 o 11 2 1 296.75 285.19 4.63 o 12 2 1 0.15 0.73 2.38 o -11 3 1 0.04 0.62 2.27 o -10 3 1 2.89 0.32 1.94 o -9 3 1 0.32 1.42 1.78 o -8 3 1 95.71 94.22 2.56 o -7 3 1 1.00 0.73 1.67 o -6 3 1 155.95 147.29 3.03 o -5 3 1 181.24 167.61 3.27 o -4 3 1 231.63 248.34 4.05 o -3 3 1 51.46 44.86 1.80 o -2 3 1 0.33 1.03 0.85 o -1 3 1 18.43 20.56 1.16 o 0 3 1 172.65 176.08 2.12 o 1 3 1 5.77 5.38 0.87 o 2 3 1 870.00 860.61 6.51 o 3 3 1 441.79 447.35 4.21 o 4 3 1 303.90 322.00 3.98 o 5 3 1 100.85 102.43 2.58 o 6 3 1 646.58 609.05 5.98 o 7 3 1 287.63 281.57 3.87 o 8 3 1 252.10 241.99 3.83 o 9 3 1 64.10 66.75 2.66 o 10 3 1 51.45 45.44 2.55 o 11 3 1 1.16 -2.23 2.23 o -10 4 1 8.50 7.49 4.97 o -9 4 1 111.24 103.93 3.29 o -8 4 1 14.41 13.78 2.27 o -7 4 1 1.54 2.72 1.99 o -6 4 1 29.52 25.29 2.54 o -5 4 1 63.86 68.68 2.95 o -4 4 1 11.51 18.39 2.42 o -3 4 1 0.85 7.21 2.00 o -2 4 1 69.52 73.40 2.39 o -1 4 1 199.61 182.86 5.16 o 0 4 1 70.60 76.66 2.25 o 1 4 1 15.12 15.91 1.92 o 2 4 1 19.98 20.87 1.90 o 3 4 1 887.11 901.67 11.19 o 4 4 1 0.30 1.55 1.64 o 5 4 1 39.81 49.91 2.56 o 6 4 1 0.09 2.26 1.88 o 7 4 1 81.58 68.17 2.99 o 8 4 1 57.12 61.47 2.93 o 9 4 1 2.48 -0.96 2.22 o 10 4 1 49.41 57.39 9.32 o -9 5 1 0.39 1.08 8.67 o -8 5 1 319.30 302.00 8.16 o -7 5 1 54.60 62.21 3.81 o -6 5 1 83.35 89.62 3.59 o -5 5 1 252.35 268.52 5.13 o -4 5 1 11.67 13.92 2.65 o -3 5 1 506.35 507.11 7.25 o -2 5 1 231.45 229.10 6.08 o -1 5 1 0.20 4.28 3.77 o 0 5 1 700.66 667.33 17.96 o 1 5 1 353.07 356.41 7.06 o 2 5 1 66.78 74.54 4.28 o 3 5 1 385.52 373.55 5.49 o 4 5 1 108.57 97.48 3.82 o 5 5 1 155.48 147.60 3.85 o 6 5 1 210.28 219.84 4.46 o 7 5 1 52.56 62.39 3.85 o 8 5 1 276.24 298.80 8.69 o -6 6 1 57.07 33.03 12.11 o -5 6 1 4.57 -2.76 9.77 o -4 6 1 74.00 68.59 6.61 o -3 6 1 7.30 12.65 5.70 o -2 6 1 28.47 29.03 11.73 o -1 6 1 104.48 114.99 9.08 o 0 6 1 82.99 75.34 8.41 o 1 6 1 93.52 95.77 7.99 o 2 6 1 256.67 252.01 14.27 o 3 6 1 6.93 8.03 4.49 o 4 6 1 17.44 21.85 4.62 o 5 6 1 90.35 94.13 7.66 o 6 6 1 61.72 45.81 10.66 o -12 0 2 167.84 181.44 7.12 o -11 0 2 1971.69 2036.52 32.09 o -10 0 2 462.95 475.92 6.66 o -9 0 2 33.54 29.10 2.58 o -8 0 2 178.02 188.87 3.36 o -7 0 2 3759.18 3454.42 70.13 o -6 0 2 28.25 28.36 1.57 o -5 0 2 2381.00 2201.34 27.07 o -4 0 2 292.99 270.20 4.65 o -3 0 2 2108.66 2059.47 37.43 o -2 0 2 121.78 119.69 1.68 o -1 0 2 5182.39 4756.69 40.96 o 0 0 2 3089.01 2935.55 32.58 o 1 0 2 11080.20 9885.50 85.32 o 2 0 2 43.86 42.55 0.87 o 3 0 2 92.32 110.06 2.14 o 4 0 2 1803.01 1523.22 12.86 o 5 0 2 8.12 10.06 0.68 o 6 0 2 46.70 55.92 2.61 o 7 0 2 57.72 54.66 2.38 o 8 0 2 0.33 2.13 1.34 o 9 0 2 764.56 665.38 14.00 o 10 0 2 61.80 52.69 3.40 o 11 0 2 7.66 6.26 2.38 o 12 0 2 189.75 192.64 9.37 o 13 0 2 158.07 157.20 8.34 o -12 1 2 288.25 293.34 4.69 o -11 1 2 125.90 123.53 3.12 o -10 1 2 106.92 113.87 2.56 o -9 1 2 4.01 3.05 1.59 o -8 1 2 506.28 479.37 4.94 o -7 1 2 86.74 82.06 1.84 o -6 1 2 296.27 276.00 2.90 o -5 1 2 28.46 30.23 0.95 o -4 1 2 138.97 123.82 1.49 o -3 1 2 44.63 60.88 0.93 o -2 1 2 166.98 163.00 1.57 o -1 1 2 720.88 690.53 3.48 o 0 1 2 6045.94 5716.91 28.71 o 1 1 2 69.73 59.07 0.84 o 2 1 2 63.77 63.73 0.90 o 3 1 2 1953.05 1922.89 9.81 o 4 1 2 921.14 943.06 5.35 o 5 1 2 150.75 130.52 1.37 o 6 1 2 20.63 20.44 0.84 o 7 1 2 46.34 60.30 1.73 o 8 1 2 352.76 340.22 4.88 o 9 1 2 0.07 0.98 1.70 o 10 1 2 139.07 137.47 3.74 o 11 1 2 163.33 168.81 3.53 o 12 1 2 137.76 139.25 4.50 o -12 2 2 10.19 12.73 3.30 o -11 2 2 41.69 35.72 2.44 o -10 2 2 20.79 17.34 2.14 o -9 2 2 3.89 0.38 1.66 o -8 2 2 256.42 268.05 3.52 o -7 2 2 54.31 62.86 2.03 o -6 2 2 7.39 7.39 1.51 o -5 2 2 295.24 324.61 3.37 o -4 2 2 1642.87 1649.57 10.61 o -3 2 2 176.50 190.45 1.93 o -2 2 2 41.45 45.23 0.95 o -1 2 2 136.68 146.99 1.68 o 0 2 2 1231.17 1285.46 9.01 o 1 2 2 96.26 81.23 1.31 o 2 2 2 49.37 58.55 1.23 o 3 2 2 33.75 30.80 1.02 o 4 2 2 33.78 36.46 1.15 o 5 2 2 101.91 101.85 2.10 o 6 2 2 9.71 9.41 1.18 o 7 2 2 9.26 12.38 1.41 o 8 2 2 32.14 29.66 1.95 o 9 2 2 33.39 38.52 2.51 o 10 2 2 13.55 13.55 2.15 o 11 2 2 6.12 3.53 2.23 o 12 2 2 11.38 15.42 2.49 o -11 3 2 112.76 106.31 4.46 o -10 3 2 18.98 18.70 2.34 o -9 3 2 41.88 45.43 2.63 o -8 3 2 142.56 150.61 3.55 o -7 3 2 79.14 85.46 2.43 o -6 3 2 100.43 105.71 2.39 o -5 3 2 369.06 380.17 5.26 o -4 3 2 182.71 190.03 3.58 o -3 3 2 954.45 943.97 8.00 o -2 3 2 51.79 53.36 1.35 o -1 3 2 21.58 29.71 1.20 o 0 3 2 1726.66 1635.07 9.20 o 1 3 2 217.56 237.04 2.96 o 2 3 2 67.49 65.94 1.57 o 3 3 2 1015.76 1003.72 8.47 o 4 3 2 24.46 25.31 1.63 o 5 3 2 515.73 517.57 6.54 o 6 3 2 59.03 60.75 2.39 o 7 3 2 96.83 91.72 2.65 o 8 3 2 718.25 719.96 7.68 o 9 3 2 231.56 218.02 3.98 o 10 3 2 144.60 142.01 3.63 o 11 3 2 157.69 157.75 5.28 o -10 4 2 210.33 210.05 8.36 o -9 4 2 7.95 10.25 2.59 o -8 4 2 231.84 238.99 4.36 o -7 4 2 243.15 247.77 3.93 o -6 4 2 62.08 59.29 2.83 o -5 4 2 95.22 89.34 3.09 o -4 4 2 140.56 144.45 3.31 o -3 4 2 124.83 119.76 3.12 o -2 4 2 921.93 933.40 8.04 o -1 4 2 0.47 1.76 1.57 o 0 4 2 1074.39 1052.36 10.48 o 1 4 2 340.70 328.71 4.75 o 2 4 2 58.27 57.53 2.31 o 3 4 2 286.80 287.33 4.33 o 4 4 2 1601.41 1587.91 11.41 o 5 4 2 51.60 51.73 2.81 o 6 4 2 218.00 217.20 4.68 o 7 4 2 133.44 132.92 3.94 o 8 4 2 78.43 79.60 3.33 o 9 4 2 270.43 254.66 4.96 o 10 4 2 129.58 123.52 13.44 o -9 5 2 32.11 25.47 11.34 o -8 5 2 6.49 2.71 4.81 o -7 5 2 2.33 5.74 2.83 o -6 5 2 0.22 -0.79 2.73 o -5 5 2 48.56 40.00 3.55 o -4 5 2 2.23 4.39 3.16 o -3 5 2 33.69 31.40 3.34 o -2 5 2 2.16 3.00 4.64 o -1 5 2 480.13 461.61 7.80 o 0 5 2 1.77 7.55 6.05 o 1 5 2 0.05 0.55 3.63 o 2 5 2 0.33 0.02 2.21 o 3 5 2 260.22 263.17 4.94 o 4 5 2 2.67 -1.51 2.41 o 5 5 2 19.57 13.59 2.79 o 6 5 2 32.82 34.46 3.29 o 7 5 2 1.34 -1.74 2.83 o 8 5 2 0.05 -1.14 5.53 o -5 6 2 158.00 154.52 15.75 o -4 6 2 94.11 84.38 7.26 o -3 6 2 56.99 56.82 7.35 o -2 6 2 42.39 58.15 8.08 o -1 6 2 16.79 21.34 7.68 o 0 6 2 43.83 48.33 11.19 o 1 6 2 120.87 107.69 7.83 o 2 6 2 83.69 81.84 14.05 o 3 6 2 133.80 114.28 10.35 o 4 6 2 83.79 93.81 5.49 o 5 6 2 0.88 9.82 5.05 o -12 1 3 154.61 152.08 4.54 o -11 1 3 23.75 26.40 2.62 o -10 1 3 147.93 144.67 3.08 o -9 1 3 286.72 292.09 3.92 o -8 1 3 88.20 98.62 2.37 o -7 1 3 1112.20 1106.15 7.95 o -6 1 3 61.89 61.59 1.77 o -5 1 3 2.41 1.08 0.80 o -4 1 3 1057.86 1054.38 6.69 o -3 1 3 62.05 73.71 1.13 o -2 1 3 27.53 18.12 0.93 o -1 1 3 266.08 230.41 1.73 o 0 1 3 145.82 155.69 1.53 o 1 1 3 1281.23 1173.92 6.12 o 2 1 3 2137.34 2311.52 16.52 o 3 1 3 62.38 54.33 0.84 o 4 1 3 2.02 1.01 0.51 o 5 1 3 267.48 250.40 2.01 o 6 1 3 873.23 873.46 6.92 o 7 1 3 44.57 43.41 1.59 o 8 1 3 8.10 5.60 1.33 o 9 1 3 20.57 18.91 1.69 o 10 1 3 67.66 70.78 4.39 o 11 1 3 46.87 46.09 2.94 o 12 1 3 106.51 106.13 7.38 o -12 2 3 0.02 -2.48 5.29 o -11 2 3 103.62 100.21 3.61 o -10 2 3 6.35 5.16 1.91 o -9 2 3 77.63 90.08 3.00 o -8 2 3 534.77 533.77 5.94 o -7 2 3 43.18 50.55 2.07 o -6 2 3 507.59 484.51 5.35 o -5 2 3 1569.23 1503.08 10.30 o -4 2 3 360.61 394.78 4.18 o -3 2 3 1795.08 1709.49 10.89 o -2 2 3 825.51 851.77 5.56 o -1 2 3 2155.99 2256.52 16.48 o 0 2 3 1660.87 1617.62 8.95 o 1 2 3 406.59 418.32 3.37 o 2 2 3 581.70 574.90 3.95 o 3 2 3 12.50 9.21 0.97 o 4 2 3 866.49 840.95 6.15 o 5 2 3 1445.35 1389.52 8.65 o 6 2 3 2053.53 1928.04 14.05 o 7 2 3 15.57 16.60 1.57 o 8 2 3 389.73 388.89 5.04 o 9 2 3 746.19 729.83 7.99 o 10 2 3 158.34 163.53 4.60 o 11 2 3 197.80 196.25 8.76 o 12 2 3 201.78 176.23 12.66 o -11 3 3 12.85 -2.13 5.01 o -10 3 3 42.92 48.84 2.98 o -9 3 3 21.23 23.73 2.45 o -8 3 3 182.34 180.84 3.43 o -7 3 3 6.20 6.57 1.88 o -6 3 3 10.04 9.41 1.76 o -5 3 3 291.67 272.18 3.72 o -4 3 3 1188.04 1157.16 9.17 o -3 3 3 78.91 77.92 2.20 o -2 3 3 168.16 154.61 2.16 o -1 3 3 54.91 61.12 1.47 o 0 3 3 376.63 393.34 3.68 o 1 3 3 464.16 505.40 5.68 o 2 3 3 140.50 143.35 2.52 o 3 3 3 237.64 250.71 3.21 o 4 3 3 157.97 161.02 3.06 o 5 3 3 199.75 195.32 3.26 o 6 3 3 9.94 7.31 1.66 o 7 3 3 338.01 331.55 4.31 o 8 3 3 165.19 164.52 3.52 o 9 3 3 14.20 14.20 2.17 o 10 3 3 76.22 79.98 4.15 o 11 3 3 53.20 38.00 4.49 o -10 4 3 0.86 4.26 5.38 o -9 4 3 11.84 9.62 2.68 o -8 4 3 282.64 275.38 5.22 o -7 4 3 69.55 68.32 2.94 o -6 4 3 20.97 30.60 2.59 o -5 4 3 0.27 2.13 2.07 o -4 4 3 69.01 69.15 3.45 o -3 4 3 4.51 6.54 2.23 o -2 4 3 86.37 90.19 3.02 o -1 4 3 12.79 16.91 1.82 o 0 4 3 570.24 557.81 6.76 o 1 4 3 28.48 28.44 1.98 o 2 4 3 3.88 3.81 1.52 o 3 4 3 130.11 132.32 2.97 o 4 4 3 450.73 454.03 5.91 o 5 4 3 34.78 36.20 2.73 o 6 4 3 60.17 69.43 3.02 o 7 4 3 5.50 5.98 2.45 o 8 4 3 35.62 39.76 3.17 o 9 4 3 19.01 21.57 3.71 o -8 5 3 15.43 2.51 5.56 o -7 5 3 231.24 227.73 7.30 o -6 5 3 8.06 10.06 3.21 o -5 5 3 180.76 170.41 5.43 o -4 5 3 212.52 233.85 6.65 o -3 5 3 114.65 121.61 4.85 o -2 5 3 444.43 446.81 7.86 o -1 5 3 282.84 271.71 10.42 o 0 5 3 1.32 1.96 3.71 o 1 5 3 1020.33 976.20 17.66 o 2 5 3 307.26 313.17 5.97 o 3 5 3 0.03 3.71 2.18 o 4 5 3 181.42 177.84 4.42 o 5 5 3 223.62 211.96 5.04 o 6 5 3 0.01 1.84 3.02 o 7 5 3 96.54 104.63 7.62 o -4 6 3 4.88 1.38 5.21 o -3 6 3 124.17 126.43 9.41 o -2 6 3 28.59 31.53 31.87 o -1 6 3 1.70 18.62 9.05 o 0 6 3 161.31 172.27 7.99 o 1 6 3 120.03 126.46 21.97 o 2 6 3 87.28 75.78 9.05 o 3 6 3 136.95 120.74 13.16 o 4 6 3 24.47 32.78 6.73 o -12 0 4 505.62 506.21 14.60 o -11 0 4 2.21 2.77 2.71 o -10 0 4 391.03 373.44 11.63 o -9 0 4 148.99 154.71 4.87 o 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