#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:51:54 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180923 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/03/2200309.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200309_Fobs loop_ _publ_author_name 'Mentes, Ayfer' 'Fawcett, John' 'Kemmitt, Raymond D. W.' _publ_section_title ; 2,6-Bis[1-(phenylimino)ethyl]pyridine ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o424 _journal_page_last o425 _journal_volume 57 _journal_year 2001 _space_group_IT_number 36 _symmetry_space_group_name_Hall 'C 2c -2' _symmetry_space_group_name_H-M 'C m c 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 33.8052 _cell_length_b 7.1247 _cell_length_c 7.2074 _exptl_crystal_F_000 664.00 _reflns_d_resolution_high 0.8419 _cod_data_source_file na6065Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 9445 Cmc2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 239.73 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x, -y, z+1/2' '-x, y, z' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z+1/2' 'x+1/2, -y+1/2, z+1/2' '-x+1/2, y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 3738.85 3937.56 38.36 o 8 0 0 5522.98 5871.78 54.18 o 10 0 0 39.72 87.85 5.04 o 12 0 0 64.59 41.16 3.18 o 14 0 0 3717.64 4252.70 61.28 o 16 0 0 1311.37 1694.95 41.69 o 18 0 0 26.31 6.03 3.29 o 20 0 0 764.49 877.84 35.68 o 22 0 0 452.18 502.70 26.76 o 24 0 0 1.97 13.70 3.73 o 26 0 0 807.07 1053.26 44.01 o 28 0 0 3703.92 3924.11 91.64 o 30 0 0 2075.21 2350.26 74.82 o 32 0 0 274.13 300.98 16.33 o 34 0 0 83.19 97.32 7.73 o 36 0 0 13.05 4.71 6.36 o 38 0 0 5.73 16.55 6.08 o 40 0 0 1.26 4.93 5.37 o 1 1 0 472.03 425.47 8.42 o 3 1 0 8.85 8.33 1.92 o 5 1 0 0.00 1.86 1.92 o 7 1 0 2160.02 1976.49 33.59 o 9 1 0 3.01 0.00 2.30 o 11 1 0 0.51 3.29 2.41 o 13 1 0 297.64 261.12 12.89 o 15 1 0 40.27 64.77 4.71 o 17 1 0 180.16 127.23 6.80 o 19 1 0 115.64 106.21 6.36 o 21 1 0 1250.52 1146.38 46.75 o 23 1 0 250.59 269.10 14.03 o 25 1 0 0.34 0.82 4.27 o 27 1 0 478.84 483.93 20.62 o 29 1 0 255.01 230.77 11.95 o 31 1 0 69.81 66.91 7.89 o 33 1 0 51.99 75.23 7.89 o 35 1 0 28.28 11.67 7.12 o 37 1 0 30.60 22.08 6.47 o 39 1 0 0.38 -7.01 7.01 o 0 2 0 57468.15 59721.15 1140.32 o 2 2 0 14876.91 15375.14 101.19 o 4 2 0 895.06 931.80 25.63 o 6 2 0 1929.04 1709.96 36.28 o 8 2 0 109.68 103.43 5.54 o 10 2 0 10.95 2.63 2.68 o 12 2 0 25.97 35.51 3.73 o 14 2 0 662.94 690.36 30.30 o 16 2 0 237.47 207.73 10.31 o 18 2 0 16.54 17.59 3.84 o 20 2 0 13.33 4.66 3.62 o 22 2 0 17.76 15.62 4.49 o 24 2 0 36.05 25.75 5.10 o 26 2 0 213.19 218.59 11.51 o 28 2 0 3845.75 3563.21 109.88 o 30 2 0 1065.72 904.27 45.11 o 32 2 0 144.78 166.27 11.62 o 34 2 0 44.92 49.21 7.95 o 36 2 0 13.76 8.11 7.45 o 38 2 0 6.77 24.60 7.12 o 1 3 0 596.57 515.64 17.18 o 3 3 0 459.18 399.57 19.31 o 5 3 0 119.28 86.66 4.71 o 7 3 0 876.67 921.85 32.35 o 9 3 0 127.71 159.99 8.82 o 11 3 0 43.55 29.32 3.84 o 13 3 0 326.13 236.39 14.15 o 15 3 0 242.48 249.00 10.53 o 17 3 0 104.87 121.61 7.23 o 19 3 0 0.53 -3.56 4.22 o 21 3 0 772.24 710.46 37.70 o 23 3 0 9.06 13.64 5.53 o 25 3 0 5.96 23.01 6.14 o 27 3 0 274.40 327.02 16.23 o 29 3 0 20.86 21.20 7.78 o 31 3 0 61.90 59.56 9.37 o 33 3 0 35.64 39.51 7.62 o 35 3 0 2.54 4.16 6.41 o 37 3 0 37.21 38.47 8.71 o 0 4 0 3004.54 2615.64 62.48 o 2 4 0 3891.83 3973.16 76.49 o 4 4 0 212.11 221.08 9.48 o 6 4 0 1599.78 1667.10 50.10 o 8 4 0 745.19 915.24 39.52 o 10 4 0 19.74 19.84 4.16 o 12 4 0 91.20 124.23 7.40 o 14 4 0 162.13 170.95 9.32 o 16 4 0 34.67 34.74 4.93 o 18 4 0 3.02 0.55 4.27 o 20 4 0 172.80 180.97 9.59 o 22 4 0 207.92 207.78 13.65 o 24 4 0 84.87 96.12 8.27 o 26 4 0 39.97 56.71 8.22 o 28 4 0 1754.96 1750.66 82.06 o 30 4 0 208.96 180.75 13.87 o 32 4 0 52.21 76.16 9.26 o 34 4 0 17.22 31.72 7.56 o 1 5 0 220.56 217.34 7.24 o 3 5 0 91.00 101.87 7.29 o 5 5 0 98.95 83.57 6.80 o 7 5 0 43.91 54.74 6.03 o 9 5 0 121.79 143.64 8.17 o 11 5 0 18.79 24.99 4.44 o 13 5 0 307.72 330.57 18.64 o 15 5 0 212.45 210.47 13.81 o 17 5 0 54.27 62.91 6.79 o 19 5 0 45.81 32.55 6.14 o 21 5 0 0.02 -4.33 5.75 o 23 5 0 209.35 226.25 12.50 o 25 5 0 10.22 9.31 8.05 o 27 5 0 38.66 31.29 8.49 o 29 5 0 323.17 325.27 17.49 o 31 5 0 0.51 2.90 7.67 o 0 6 0 1600.07 1327.69 64.55 o 2 6 0 63.47 66.69 8.22 o 4 6 0 0.27 -0.66 4.93 o 6 6 0 0.51 -4.49 5.26 o 8 6 0 2.89 4.93 4.66 o 10 6 0 1.97 1.70 4.60 o 12 6 0 6.08 5.97 5.81 o 14 6 0 55.18 62.69 7.84 o 16 6 0 37.76 33.53 7.23 o 18 6 0 13.02 10.19 5.81 o 20 6 0 0.18 7.40 5.97 o 22 6 0 0.55 2.14 6.19 o 24 6 0 6.31 13.97 6.47 o 26 6 0 44.93 53.04 9.26 o 28 6 0 263.22 251.08 17.10 o 1 7 0 66.73 64.66 6.41 o 3 7 0 0.30 -7.34 7.34 o 5 7 0 13.97 18.30 7.01 o 7 7 0 32.43 38.25 7.12 o 9 7 0 1.63 6.03 5.97 o 11 7 0 10.36 9.48 6.25 o 13 7 0 49.27 63.73 8.77 o 15 7 0 113.50 102.69 11.18 o 17 7 0 38.87 24.27 7.89 o 19 7 0 3.38 6.03 6.96 o 21 7 0 1.23 -4.88 6.96 o 0 8 0 374.17 376.98 23.79 o 2 8 0 0.00 2.79 7.84 o 4 8 0 0.02 12.11 6.79 o 6 8 0 10.49 19.29 7.45 o 8 8 0 9.79 20.00 7.01 o 10 8 0 0.00 6.79 6.74 o 12 8 0 0.01 -4.44 7.12 o 1 1 1 27007.12 25839.03 431.21 o 3 1 1 16452.33 15251.88 339.01 o 5 1 1 68.79 101.73 3.73 o 7 1 1 6378.71 5997.09 95.92 o 9 1 1 162.82 164.81 7.07 o 11 1 1 102.93 95.48 3.84 o 13 1 1 3894.62 3865.03 49.42 o 15 1 1 4119.02 4147.88 56.20 o 17 1 1 906.37 860.88 27.57 o 19 1 1 366.94 402.23 13.44 o 21 1 1 230.00 239.99 10.36 o 23 1 1 390.40 341.39 12.72 o 25 1 1 244.36 220.03 8.55 o 27 1 1 440.50 437.40 15.46 o 29 1 1 1839.02 1931.45 50.17 o 31 1 1 70.71 72.22 6.58 o 33 1 1 91.17 95.18 6.36 o 35 1 1 176.08 179.59 8.28 o 37 1 1 6.64 5.04 5.15 o 39 1 1 21.23 23.23 5.26 o 0 2 1 1717.69 1580.65 25.28 o 2 2 1 4812.74 4949.84 43.61 o 4 2 1 1872.42 1834.40 26.78 o 6 2 1 3011.55 3014.97 35.63 o 8 2 1 930.11 854.91 20.72 o 10 2 1 385.91 428.28 14.59 o 12 2 1 100.43 175.88 6.69 o 14 2 1 133.75 124.47 4.28 o 16 2 1 24.26 39.23 3.12 o 18 2 1 365.29 306.92 11.13 o 20 2 1 258.17 209.36 6.96 o 22 2 1 109.77 105.71 5.64 o 24 2 1 746.93 701.39 23.54 o 26 2 1 205.22 183.12 7.45 o 28 2 1 313.54 299.20 12.55 o 30 2 1 277.95 272.54 10.74 o 32 2 1 84.77 86.58 6.58 o 34 2 1 56.86 50.52 5.59 o 36 2 1 19.94 18.63 5.26 o 38 2 1 6.36 2.79 4.71 o 1 3 1 4238.53 4505.18 35.91 o 3 3 1 1351.54 1312.10 26.96 o 5 3 1 1809.21 1791.12 32.61 o 7 3 1 741.03 695.26 20.97 o 9 3 1 837.63 834.67 23.50 o 11 3 1 110.51 171.76 6.03 o 13 3 1 1681.17 1680.04 35.64 o 15 3 1 398.78 493.88 16.51 o 17 3 1 387.20 414.61 14.15 o 19 3 1 116.48 97.33 5.10 o 21 3 1 632.88 607.46 21.78 o 23 3 1 128.59 118.16 5.86 o 25 3 1 474.62 479.85 16.61 o 27 3 1 983.77 990.94 32.82 o 29 3 1 531.72 465.54 20.29 o 31 3 1 130.58 112.51 7.67 o 33 3 1 41.46 30.41 5.81 o 35 3 1 19.40 18.14 5.42 o 37 3 1 29.69 37.97 6.14 o 0 4 1 1665.27 1660.59 36.58 o 2 4 1 395.24 472.14 16.40 o 4 4 1 115.79 140.80 4.99 o 6 4 1 43.63 41.86 3.51 o 8 4 1 47.57 56.22 3.67 o 10 4 1 24.54 37.42 3.45 o 12 4 1 98.54 106.10 5.04 o 14 4 1 131.72 138.00 5.32 o 16 4 1 86.22 80.83 4.49 o 18 4 1 34.12 27.07 3.95 o 20 4 1 5.70 2.74 3.51 o 22 4 1 9.66 3.23 4.05 o 24 4 1 11.34 15.51 3.95 o 26 4 1 140.47 127.69 7.40 o 28 4 1 118.71 113.05 8.06 o 30 4 1 86.49 87.84 6.90 o 32 4 1 93.65 82.96 7.56 o 34 4 1 2.00 -0.22 4.55 o 1 5 1 1140.00 1174.97 24.99 o 3 5 1 184.05 195.84 7.23 o 5 5 1 59.11 83.89 5.21 o 7 5 1 37.21 28.55 3.62 o 9 5 1 120.34 125.94 5.81 o 11 5 1 20.87 24.55 4.05 o 13 5 1 303.54 294.05 11.07 o 15 5 1 113.05 108.56 6.14 o 17 5 1 68.11 57.15 5.04 o 19 5 1 21.85 13.64 4.38 o 21 5 1 80.83 67.13 6.30 o 23 5 1 37.03 40.38 5.48 o 25 5 1 56.33 64.77 6.25 o 27 5 1 411.88 446.41 15.62 o 29 5 1 208.05 206.23 9.76 o 31 5 1 43.78 44.33 6.74 o 0 6 1 624.47 620.44 21.72 o 2 6 1 85.04 75.51 5.81 o 4 6 1 26.15 17.81 4.44 o 6 6 1 15.89 20.16 4.16 o 8 6 1 49.79 49.10 5.10 o 10 6 1 19.37 26.57 4.16 o 12 6 1 24.66 28.77 4.49 o 14 6 1 58.02 66.80 5.53 o 16 6 1 58.30 53.97 5.10 o 18 6 1 7.80 5.70 4.33 o 20 6 1 0.43 -4.71 4.71 o 22 6 1 15.10 18.03 4.88 o 24 6 1 19.05 22.63 5.37 o 26 6 1 122.09 131.63 8.71 o 1 7 1 430.56 423.09 9.59 o 3 7 1 44.51 35.62 6.08 o 5 7 1 65.85 67.56 5.92 o 7 7 1 0.26 5.59 4.27 o 9 7 1 2.24 3.89 4.05 o 11 7 1 0.32 -4.05 4.27 o 13 7 1 52.16 50.47 5.81 o 15 7 1 35.42 32.77 5.64 o 17 7 1 16.58 16.44 5.37 o 19 7 1 14.61 19.23 5.21 o 21 7 1 5.03 -1.81 5.26 o 0 8 1 30.36 32.05 6.63 o 2 8 1 24.37 21.48 6.36 o 4 8 1 13.69 7.94 5.59 o 6 8 1 5.08 -1.42 4.99 o 8 8 1 5.20 9.64 4.93 o 10 8 1 4.48 2.52 5.04 o 12 8 1 7.17 7.73 5.15 o 0 0 2 5916.35 6143.03 67.74 o 2 0 2 1584.44 1590.95 35.83 o 4 0 2 3026.94 2838.13 50.15 o 6 0 2 1406.66 1460.32 37.31 o 8 0 2 2967.43 2762.00 54.45 o 10 0 2 953.75 854.79 33.42 o 12 0 2 930.45 905.39 35.11 o 14 0 2 9137.62 10925.41 117.75 o 16 0 2 484.23 620.27 29.02 o 18 0 2 425.42 648.54 31.81 o 20 0 2 276.94 313.81 16.12 o 22 0 2 1.27 -3.01 4.11 o 24 0 2 201.34 162.57 8.61 o 26 0 2 522.17 484.08 23.86 o 28 0 2 384.07 383.61 20.50 o 30 0 2 690.50 762.35 37.19 o 32 0 2 875.56 864.06 45.10 o 34 0 2 68.79 80.39 8.49 o 36 0 2 36.30 70.03 7.95 o 38 0 2 33.69 53.26 9.26 o 1 1 2 1081.69 958.28 20.04 o 3 1 2 4789.09 4672.11 58.90 o 5 1 2 4259.52 4114.12 56.54 o 7 1 2 1619.39 1648.62 37.64 o 9 1 2 727.44 715.49 26.75 o 11 1 2 70.01 59.57 4.22 o 13 1 2 673.31 609.64 30.25 o 15 1 2 72.05 95.52 5.64 o 17 1 2 144.08 129.95 8.33 o 19 1 2 78.50 82.86 6.19 o 21 1 2 19.90 22.08 4.93 o 23 1 2 15.88 14.36 4.71 o 25 1 2 179.38 175.50 9.32 o 27 1 2 54.04 55.29 7.01 o 29 1 2 54.87 58.85 7.62 o 31 1 2 27.46 50.46 6.08 o 33 1 2 7.54 0.00 6.85 o 35 1 2 8.49 7.89 6.79 o 37 1 2 5.85 8.44 6.74 o 0 2 2 1786.41 1936.05 43.17 o 2 2 2 994.75 1002.62 30.84 o 4 2 2 2803.17 2893.84 52.70 o 6 2 2 442.53 375.62 19.48 o 8 2 2 1198.37 1286.01 37.56 o 10 2 2 275.97 319.35 15.57 o 12 2 2 488.45 484.25 24.25 o 14 2 2 3136.60 3556.96 72.26 o 16 2 2 440.14 483.08 22.38 o 18 2 2 189.49 174.80 8.66 o 20 2 2 554.96 539.18 26.33 o 22 2 2 151.82 141.62 9.87 o 24 2 2 185.40 171.06 10.19 o 26 2 2 10.48 4.88 5.37 o 28 2 2 229.33 213.43 12.17 o 30 2 2 151.77 144.85 10.74 o 32 2 2 94.23 109.87 10.47 o 34 2 2 2.10 -0.88 6.57 o 36 2 2 50.18 58.63 9.32 o 1 3 2 53.88 56.55 3.29 o 3 3 2 187.79 257.54 13.10 o 5 3 2 1646.85 1737.14 47.65 o 7 3 2 378.92 382.42 17.82 o 9 3 2 184.54 180.29 9.32 o 11 3 2 46.22 67.78 5.42 o 13 3 2 296.06 297.54 14.31 o 15 3 2 59.05 63.35 5.75 o 17 3 2 78.87 91.24 6.80 o 19 3 2 52.17 49.10 5.42 o 21 3 2 25.67 31.94 6.08 o 23 3 2 23.36 10.79 6.25 o 25 3 2 225.26 230.75 11.29 o 27 3 2 22.26 27.45 6.36 o 29 3 2 14.52 11.40 6.74 o 31 3 2 9.61 8.00 6.19 o 33 3 2 10.66 -2.25 6.79 o 35 3 2 28.49 20.16 8.99 o 0 4 2 655.49 829.91 37.70 o 2 4 2 654.78 706.67 34.07 o 4 4 2 295.84 287.34 16.72 o 6 4 2 26.68 35.94 5.26 o 8 4 2 189.69 185.32 9.59 o 10 4 2 19.12 15.73 4.71 o 12 4 2 184.77 189.54 9.10 o 14 4 2 483.90 568.53 26.16 o 16 4 2 330.29 345.88 18.09 o 18 4 2 281.72 257.48 11.46 o 20 4 2 381.62 388.00 19.13 o 22 4 2 166.42 189.02 10.85 o 24 4 2 412.40 422.21 20.07 o 26 4 2 332.85 339.92 16.06 o 28 4 2 135.76 157.94 11.23 o 30 4 2 27.86 29.20 7.01 o 32 4 2 15.79 14.14 7.40 o 34 4 2 34.57 37.53 8.88 o 1 5 2 127.14 103.20 5.64 o 3 5 2 656.30 575.51 29.51 o 5 5 2 25.01 25.42 6.03 o 7 5 2 43.39 41.81 6.03 o 9 5 2 86.69 86.25 7.45 o 11 5 2 108.08 78.15 7.29 o 13 5 2 9.40 1.26 5.53 o 15 5 2 144.68 145.39 10.30 o 17 5 2 10.68 1.75 5.92 o 19 5 2 14.06 21.09 6.36 o 21 5 2 6.39 3.07 6.30 o 23 5 2 123.36 127.79 10.41 o 25 5 2 4.32 -6.36 6.36 o 27 5 2 20.15 25.59 7.94 o 29 5 2 18.51 21.37 8.11 o 31 5 2 8.15 5.53 7.45 o 0 6 2 414.17 461.70 24.45 o 2 6 2 293.79 264.55 13.10 o 4 6 2 16.57 17.97 6.08 o 6 6 2 1.30 -0.71 5.42 o 8 6 2 9.34 13.64 5.37 o 10 6 2 1.32 7.23 5.37 o 12 6 2 29.88 31.18 5.97 o 14 6 2 243.13 226.42 12.83 o 16 6 2 15.04 19.45 6.30 o 18 6 2 17.25 14.85 6.85 o 20 6 2 3.54 7.34 6.41 o 22 6 2 1.89 -7.12 7.12 o 24 6 2 1.10 -7.12 7.12 o 26 6 2 16.55 17.75 9.21 o 1 7 2 19.08 16.44 5.31 o 3 7 2 56.89 53.15 9.10 o 5 7 2 5.31 9.42 6.14 o 7 7 2 3.02 7.07 6.14 o 9 7 2 1.59 4.66 5.81 o 11 7 2 2.28 -5.59 6.85 o 13 7 2 7.07 3.56 6.68 o 15 7 2 24.57 27.78 8.44 o 17 7 2 0.84 -4.22 6.96 o 19 7 2 3.35 11.18 7.23 o 0 8 2 160.34 166.27 13.43 o 2 8 2 70.58 67.12 10.79 o 4 8 2 2.67 6.79 8.11 o 6 8 2 2.32 2.47 5.86 o 8 8 2 2.76 5.48 6.74 o 1 1 3 5513.61 5213.45 58.68 o 3 1 3 518.09 514.26 25.08 o 5 1 3 354.54 365.56 18.98 o 7 1 3 898.95 901.40 33.67 o 9 1 3 3.73 -0.16 3.23 o 11 1 3 1528.23 1501.76 48.90 o 13 1 3 290.54 342.95 17.22 o 15 1 3 828.99 852.08 41.28 o 17 1 3 324.55 345.36 17.82 o 19 1 3 74.02 65.27 6.14 o 21 1 3 164.44 163.16 10.25 o 23 1 3 208.52 184.88 10.03 o 25 1 3 82.26 65.87 7.84 o 27 1 3 4.52 -5.75 5.75 o 29 1 3 1276.15 1076.77 58.74 o 31 1 3 229.37 246.69 12.77 o 33 1 3 92.21 76.00 9.81 o 35 1 3 195.58 168.53 13.70 o 37 1 3 22.79 37.64 8.27 o 0 2 3 1211.40 1118.68 40.95 o 2 2 3 1867.51 1912.25 49.45 o 4 2 3 346.93 314.30 15.96 o 6 2 3 906.04 940.27 37.29 o 8 2 3 319.94 336.68 18.42 o 10 2 3 1480.64 1495.37 47.45 o 12 2 3 347.01 378.13 16.83 o 14 2 3 11.81 -4.49 4.49 o 16 2 3 291.28 332.72 17.49 o 18 2 3 98.67 91.24 7.07 o 20 2 3 342.30 351.76 16.56 o 22 2 3 220.76 187.40 10.47 o 24 2 3 68.88 69.04 7.23 o 26 2 3 5.92 3.51 5.75 o 28 2 3 97.52 99.13 9.10 o 30 2 3 12.86 0.82 6.52 o 32 2 3 5.80 9.92 6.41 o 34 2 3 1.80 13.42 5.97 o 36 2 3 9.62 8.88 7.07 o 1 3 3 1815.98 1869.99 38.13 o 3 3 3 237.87 220.16 11.40 o 5 3 3 751.77 630.46 30.84 o 7 3 3 1211.98 1168.63 45.27 o 9 3 3 467.34 461.36 19.14 o 11 3 3 67.59 67.13 5.92 o 13 3 3 353.41 349.26 17.82 o 15 3 3 446.81 398.45 23.58 o 17 3 3 41.04 21.97 5.92 o 19 3 3 197.83 235.46 11.62 o 21 3 3 557.20 553.57 25.01 o 23 3 3 277.31 263.77 13.70 o 25 3 3 27.14 38.19 6.63 o 27 3 3 405.30 385.74 17.71 o 29 3 3 152.81 142.54 11.56 o 31 3 3 41.83 32.05 8.00 o 33 3 3 19.84 17.10 8.05 o 0 4 3 452.80 407.63 19.96 o 2 4 3 24.53 41.92 5.59 o 4 4 3 8.49 1.04 4.44 o 6 4 3 27.43 19.12 4.88 o 8 4 3 126.53 134.87 8.28 o 10 4 3 60.06 101.05 7.34 o 12 4 3 14.66 22.85 5.48 o 14 4 3 16.14 5.75 5.64 o 16 4 3 19.35 20.00 5.59 o 18 4 3 75.38 46.08 7.73 o 20 4 3 74.72 83.18 8.27 o 22 4 3 8.36 9.31 5.97 o 24 4 3 4.06 6.30 5.92 o 26 4 3 16.82 17.53 7.07 o 28 4 3 22.22 9.70 8.05 o 30 4 3 19.35 19.62 7.51 o 32 4 3 3.63 1.48 6.90 o 1 5 3 309.58 300.58 10.31 o 3 5 3 111.14 114.37 8.55 o 5 5 3 143.32 136.02 9.10 o 7 5 3 82.48 95.02 7.95 o 9 5 3 75.94 69.21 8.16 o 11 5 3 30.39 33.64 6.36 o 13 5 3 238.35 230.98 13.37 o 15 5 3 281.44 305.70 13.27 o 17 5 3 23.94 29.86 7.29 o 19 5 3 33.27 31.56 7.62 o 21 5 3 75.65 86.96 9.32 o 23 5 3 58.44 64.27 9.15 o 25 5 3 8.89 22.52 6.36 o 27 5 3 97.93 92.01 10.80 o 29 5 3 90.29 72.44 10.90 o 0 6 3 335.58 323.76 14.64 o 2 6 3 15.54 20.27 6.63 o 4 6 3 18.36 11.67 6.74 o 6 6 3 70.53 70.96 8.82 o 8 6 3 58.99 70.69 8.05 o 10 6 3 2.07 -2.68 6.25 o 12 6 3 35.84 33.70 7.67 o 14 6 3 24.31 22.47 7.18 o 16 6 3 43.64 39.73 8.44 o 18 6 3 68.40 78.47 9.48 o 20 6 3 16.95 7.73 7.73 o 22 6 3 12.75 13.75 6.85 o 24 6 3 3.91 20.33 7.29 o 1 7 3 65.39 62.41 6.36 o 3 7 3 5.68 15.51 6.41 o 5 7 3 15.78 20.00 7.18 o 7 7 3 2.20 0.44 6.57 o 9 7 3 5.01 10.30 5.75 o 11 7 3 12.21 0.44 7.18 o 13 7 3 117.36 125.22 11.51 o 15 7 3 150.91 152.13 13.48 o 17 7 3 6.99 15.83 7.94 o 0 0 4 8393.81 8561.82 117.60 o 2 0 4 198.33 230.73 9.26 o 4 0 4 33.37 31.89 4.16 o 6 0 4 106.28 99.85 6.25 o 8 0 4 1082.28 931.89 44.88 o 10 0 4 5.87 5.04 3.67 o 12 0 4 6.60 9.97 4.16 o 14 0 4 1936.73 1884.55 66.50 o 16 0 4 1858.86 1635.83 63.84 o 18 0 4 599.37 606.38 32.91 o 20 0 4 26.24 22.36 5.81 o 22 0 4 49.43 42.74 6.47 o 24 0 4 32.73 33.75 6.68 o 26 0 4 46.46 40.44 6.52 o 28 0 4 235.87 220.72 13.92 o 30 0 4 575.64 581.63 26.21 o 32 0 4 392.99 451.99 17.60 o 34 0 4 125.98 144.23 11.84 o 1 1 4 156.66 169.86 5.97 o 3 1 4 127.69 153.84 8.93 o 5 1 4 59.19 88.50 5.81 o 7 1 4 12.56 18.30 3.89 o 9 1 4 87.55 77.22 6.25 o 11 1 4 8.41 11.18 3.89 o 13 1 4 350.62 321.30 12.94 o 15 1 4 47.63 38.80 6.52 o 17 1 4 157.66 165.41 9.32 o 19 1 4 193.89 178.02 10.03 o 21 1 4 136.98 122.49 9.54 o 23 1 4 57.98 60.11 7.51 o 25 1 4 20.82 23.01 6.36 o 27 1 4 32.60 20.38 6.96 o 29 1 4 30.32 16.38 7.89 o 31 1 4 7.89 9.20 6.74 o 33 1 4 28.21 24.27 7.94 o 35 1 4 7.77 17.92 7.01 o 0 2 4 1946.46 1941.17 63.45 o 2 2 4 684.53 689.66 32.70 o 4 2 4 434.13 435.18 22.76 o 6 2 4 160.81 148.37 7.18 o 8 2 4 25.69 37.04 4.99 o 10 2 4 531.71 573.07 28.03 o 12 2 4 586.29 572.45 30.55 o 14 2 4 1188.90 1199.41 51.40 o 16 2 4 927.15 923.89 42.04 o 18 2 4 214.80 244.79 11.02 o 20 2 4 0.97 -0.66 5.26 o 22 2 4 37.77 51.29 7.07 o 24 2 4 31.40 40.05 6.47 o 26 2 4 72.63 69.37 8.99 o 28 2 4 281.28 239.42 13.98 o 30 2 4 178.55 151.10 12.11 o 32 2 4 104.38 95.84 10.69 o 34 2 4 8.70 13.92 7.40 o 1 3 4 108.53 121.50 5.48 o 3 3 4 3.15 4.05 4.49 o 5 3 4 36.75 54.30 5.59 o 7 3 4 15.13 22.85 4.49 o 9 3 4 128.33 119.91 7.51 o 11 3 4 64.59 45.21 6.30 o 13 3 4 371.99 361.91 19.35 o 15 3 4 69.13 71.46 7.45 o 17 3 4 161.07 177.79 9.81 o 19 3 4 117.30 142.65 9.86 o 21 3 4 84.28 77.10 8.22 o 23 3 4 21.90 18.30 6.19 o 25 3 4 11.07 10.08 6.85 o 27 3 4 23.35 29.92 7.73 o 29 3 4 29.24 33.10 8.00 o 31 3 4 3.35 -6.74 7.23 o 0 4 4 75.95 78.09 7.45 o 2 4 4 464.70 422.90 17.33 o 4 4 4 312.41 306.72 13.60 o 6 4 4 272.12 283.95 15.07 o 8 4 4 162.73 164.25 9.81 o 10 4 4 418.80 355.19 20.62 o 12 4 4 796.58 810.10 37.25 o 14 4 4 544.21 638.60 29.56 o 16 4 4 331.56 334.23 16.72 o 18 4 4 11.36 10.36 5.70 o 20 4 4 2.24 -2.74 6.03 o 22 4 4 4.49 -2.47 5.92 o 24 4 4 41.14 35.23 7.62 o 26 4 4 84.32 71.56 9.70 o 28 4 4 179.52 160.96 12.93 o 30 4 4 12.60 15.07 7.78 o 1 5 4 21.10 13.31 4.55 o 3 5 4 140.26 131.20 10.14 o 5 5 4 30.42 41.64 6.85 o 7 5 4 47.71 43.07 7.07 o 9 5 4 14.41 11.89 6.19 o 11 5 4 99.50 97.71 8.17 o 13 5 4 27.37 33.15 7.34 o 15 5 4 281.49 259.60 16.28 o 17 5 4 120.28 117.71 10.69 o 19 5 4 14.46 22.52 7.29 o 21 5 4 10.40 5.31 7.18 o 23 5 4 28.16 32.44 8.16 o 25 5 4 4.31 1.48 6.96 o 0 6 4 63.46 50.41 8.71 o 2 6 4 33.61 33.04 7.51 o 4 6 4 12.54 9.59 6.52 o 6 6 4 1.22 3.67 5.31 o 8 6 4 2.49 3.29 6.14 o 10 6 4 11.41 6.36 6.90 o 12 6 4 104.65 95.13 11.01 o 14 6 4 225.18 231.18 15.02 o 16 6 4 206.08 194.23 14.41 o 18 6 4 1.02 -5.21 7.07 o 20 6 4 2.11 6.85 6.85 o 1 7 4 21.64 34.30 5.81 o 3 7 4 8.06 4.16 7.51 o 5 7 4 1.40 5.15 6.90 o 7 7 4 2.27 1.92 6.25 o 9 7 4 0.75 -4.33 7.23 o 11 7 4 15.57 21.09 7.51 o 1 1 5 84.57 80.83 4.77 o 3 1 5 431.89 523.81 23.85 o 5 1 5 100.24 88.18 7.34 o 7 1 5 62.78 48.22 6.30 o 9 1 5 44.46 48.82 6.25 o 11 1 5 227.70 196.56 10.63 o 13 1 5 1424.03 1237.24 60.48 o 15 1 5 4495.70 4407.04 112.18 o 17 1 5 256.80 241.02 12.66 o 19 1 5 179.62 197.74 11.40 o 21 1 5 43.71 44.55 7.51 o 23 1 5 60.85 63.12 7.95 o 25 1 5 14.83 6.52 7.01 o 27 1 5 8.64 12.05 5.92 o 29 1 5 21.38 28.71 8.44 o 31 1 5 37.42 35.23 8.77 o 0 2 5 116.14 138.93 8.22 o 2 2 5 60.45 67.13 6.19 o 4 2 5 9.98 8.60 4.77 o 6 2 5 140.05 127.15 8.39 o 8 2 5 14.40 9.86 5.04 o 10 2 5 40.20 38.52 6.25 o 12 2 5 119.99 134.37 9.70 o 14 2 5 51.55 49.97 9.04 o 16 2 5 173.93 187.71 11.45 o 18 2 5 41.42 54.41 6.90 o 20 2 5 57.88 79.84 8.33 o 22 2 5 148.49 139.25 11.02 o 24 2 5 31.51 32.82 7.12 o 26 2 5 24.25 31.18 7.34 o 28 2 5 53.84 54.96 8.82 o 30 2 5 35.34 36.77 8.77 o 1 3 5 19.43 17.70 3.51 o 3 3 5 16.15 15.45 5.15 o 5 3 5 140.34 136.08 9.10 o 7 3 5 347.63 314.85 15.41 o 9 3 5 558.72 562.79 27.48 o 11 3 5 32.95 44.49 7.34 o 13 3 5 1938.60 2021.90 76.78 o 15 3 5 809.65 800.02 37.19 o 17 3 5 210.97 234.96 14.30 o 19 3 5 17.05 19.40 6.74 o 21 3 5 12.60 5.70 6.90 o 23 3 5 46.67 46.14 8.11 o 25 3 5 43.09 31.45 8.82 o 27 3 5 22.26 25.04 7.12 o 29 3 5 2.78 0.99 7.18 o 0 4 5 58.11 62.58 7.67 o 2 4 5 122.07 130.26 9.54 o 4 4 5 3.39 8.93 5.04 o 6 4 5 108.76 109.05 8.88 o 8 4 5 69.08 62.36 7.40 o 10 4 5 3.13 17.48 6.52 o 12 4 5 18.35 33.75 6.79 o 14 4 5 108.42 97.27 10.14 o 16 4 5 6.29 5.64 7.23 o 18 4 5 16.35 11.67 6.90 o 20 4 5 43.85 42.19 7.78 o 22 4 5 16.34 11.34 6.96 o 24 4 5 10.93 5.70 6.90 o 26 4 5 7.94 2.47 7.51 o 1 5 5 2.81 11.45 3.51 o 3 5 5 2.47 1.53 5.48 o 5 5 5 37.05 37.42 7.23 o 7 5 5 48.60 51.12 8.00 o 9 5 5 160.86 149.78 11.18 o 11 5 5 13.07 8.77 7.34 o 13 5 5 371.19 391.08 19.95 o 15 5 5 224.38 225.53 14.85 o 17 5 5 68.42 59.95 9.86 o 19 5 5 12.61 16.49 7.94 o 21 5 5 11.76 13.20 7.45 o 0 6 5 60.30 81.86 9.10 o 2 6 5 50.68 49.21 8.49 o 4 6 5 1.63 12.93 6.08 o 6 6 5 8.24 18.90 6.52 o 8 6 5 47.46 59.23 8.55 o 10 6 5 4.00 4.66 7.12 o 12 6 5 1.21 11.45 7.51 o 14 6 5 97.97 104.23 11.95 o 0 0 6 188.64 197.31 11.13 o 2 0 6 402.14 367.73 21.00 o 4 0 6 61.67 69.81 6.74 o 6 0 6 230.59 248.46 12.99 o 8 0 6 357.28 370.93 17.71 o 10 0 6 10.97 18.90 5.64 o 12 0 6 269.40 304.93 16.01 o 14 0 6 1650.94 1637.52 73.17 o 16 0 6 192.12 208.70 12.33 o 18 0 6 664.89 657.47 32.08 o 20 0 6 54.49 50.74 8.38 o 22 0 6 39.94 40.93 8.00 o 24 0 6 32.29 36.33 7.40 o 26 0 6 69.07 74.47 9.70 o 28 0 6 67.40 99.89 10.74 o 1 1 6 0.84 4.82 3.29 o 3 1 6 17.53 14.57 5.31 o 5 1 6 29.10 27.89 5.92 o 7 1 6 46.77 23.18 6.96 o 9 1 6 48.80 46.08 7.78 o 11 1 6 17.35 7.56 6.36 o 13 1 6 108.76 124.62 10.30 o 15 1 6 41.57 33.86 8.88 o 17 1 6 19.60 23.73 7.45 o 19 1 6 44.67 45.97 8.11 o 21 1 6 0.57 3.34 6.08 o 23 1 6 12.13 14.03 6.79 o 25 1 6 0.69 7.40 5.81 o 27 1 6 3.06 -6.85 6.85 o 0 2 6 130.88 118.43 8.60 o 2 2 6 201.53 185.09 10.63 o 4 2 6 5.11 1.70 5.26 o 6 2 6 40.17 52.33 6.36 o 8 2 6 109.82 124.94 9.26 o 10 2 6 261.70 264.69 13.32 o 12 2 6 55.19 61.43 8.16 o 14 2 6 868.03 945.04 44.88 o 16 2 6 117.17 121.44 10.36 o 18 2 6 139.38 163.25 11.45 o 20 2 6 55.23 59.01 8.49 o 22 2 6 84.03 74.20 10.52 o 24 2 6 2.68 1.37 6.52 o 26 2 6 46.21 37.59 8.77 o 1 3 6 6.02 8.55 3.84 o 3 3 6 39.09 32.11 7.01 o 5 3 6 32.44 39.73 5.97 o 7 3 6 36.38 21.86 6.58 o 9 3 6 47.85 63.84 8.33 o 11 3 6 4.34 0.77 6.85 o 13 3 6 152.03 160.46 11.40 o 15 3 6 98.21 108.94 11.01 o 17 3 6 16.93 7.29 7.78 o 19 3 6 16.73 20.00 6.74 o 21 3 6 4.05 6.96 6.96 o 23 3 6 6.98 7.73 7.07 o 0 4 6 55.23 44.49 7.45 o 2 4 6 95.44 87.24 9.15 o 4 4 6 30.23 31.73 7.56 o 6 4 6 33.39 30.52 6.47 o 8 4 6 10.30 10.30 7.07 o 10 4 6 256.63 247.96 14.96 o 12 4 6 122.94 115.30 12.00 o 14 4 6 253.16 278.32 14.85 o 16 4 6 106.56 110.69 11.89 o 18 4 6 6.41 2.36 7.94 o 20 4 6 46.36 62.74 9.48 o 1 5 6 16.76 17.97 5.26 o 3 5 6 4.81 -0.44 6.63 o 5 5 6 1.95 0.00 6.90 o 7 5 6 19.18 8.22 7.51 o 9 5 6 4.41 4.60 6.36 o 11 5 6 85.88 68.88 10.74 o 13 5 6 8.68 9.15 9.48 o 15 5 6 82.49 91.13 11.73 o 0 6 6 21.93 17.86 8.05 o 2 6 6 21.46 23.89 7.62 o 1 1 7 141.37 126.21 6.91 o 3 1 7 23.14 24.22 6.36 o 5 1 7 98.17 84.66 9.64 o 7 1 7 29.96 18.90 6.47 o 9 1 7 18.51 31.29 7.29 o 11 1 7 249.25 235.30 13.48 o 13 1 7 116.35 129.00 10.58 o 15 1 7 90.25 92.94 10.85 o 17 1 7 137.90 153.11 12.93 o 19 1 7 1.61 -7.23 7.23 o 21 1 7 4.69 -5.31 7.01 o 0 2 7 28.75 29.53 7.12 o 2 2 7 14.49 13.59 6.96 o 4 2 7 39.97 48.16 7.29 o 6 2 7 33.70 42.19 7.01 o 8 2 7 0.47 -6.25 6.79 o 10 2 7 235.60 236.12 13.76 o 12 2 7 62.44 66.47 8.93 o 14 2 7 12.67 4.44 8.00 o 16 2 7 44.32 53.86 8.77 o 18 2 7 20.49 20.93 7.23 o 20 2 7 24.90 16.27 8.49 o 1 3 7 101.13 86.64 6.80 o 3 3 7 1.98 0.00 6.68 o 5 3 7 72.89 74.52 8.60 o 7 3 7 20.05 18.74 7.40 o 9 3 7 12.85 8.44 7.78 o 11 3 7 13.27 9.53 7.56 o 13 3 7 36.56 37.53 9.31 o 15 3 7 90.22 96.11 10.52 o 17 3 7 5.32 11.34 7.62 o 0 4 7 24.18 32.44 7.84 o 2 4 7 6.34 7.45 7.51 o 4 4 7 1.76 4.66 6.57 o 6 4 7 4.95 15.12 6.68 o 8 4 7 33.15 27.29 8.27 o 10 4 7 18.12 3.89 7.67 o 12 4 7 6.43 8.93 8.00 o 0 0 8 133.85 123.25 11.12 o 2 0 8 21.84 19.45 7.45 o 4 0 8 27.77 21.81 7.07 o 6 0 8 27.84 17.48 7.73 o 8 0 8 51.29 60.05 8.71 o 10 0 8 8.32 -7.78 7.78 o 12 0 8 11.03 15.45 8.99 o 14 0 8 415.41 518.54 28.07 o 1 1 8 5.27 7.07 4.55 o 3 1 8 2.24 -6.79 6.79 o 5 1 8 10.91 11.12 7.34 o 7 1 8 37.20 24.38 8.27 o 9 1 8 24.95 34.79 7.56 o 11 1 8 0.15 0.49 7.18 o 13 1 8 51.09 63.51 10.19 o 0 2 8 127.24 106.31 10.41 o 2 2 8 14.38 11.94 6.63 o 4 2 8 16.10 15.89 7.78 o 6 2 8 19.22 14.08 7.67 o 8 2 8 4.86 4.93 7.18 o 10 2 8 5.18 -1.48 7.51 o 1 3 8 6.88 7.84 5.26 o