#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/03/2200353.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200353_Fobs loop_ _publ_author_name 'Staples, Richard J.' 'Segal, Brent M.' _publ_section_title ; Triisopropylphosphine sulfide ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o432 _journal_page_last o433 _journal_volume 57 _journal_year 2001 _space_group_IT_number 72 _symmetry_space_group_name_Hall '-I 2 2c' _symmetry_space_group_name_H-M 'I b a m' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.5730 _cell_length_b 13.8717 _cell_length_c 12.6880 _exptl_crystal_F_000 848.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file wn6010Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' rjs12 in Ibam' _shelx_refln_list_code 4 _shelx_f_calc_maximum 234.70 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' '-x+1/2, y+1/2, -z' 'x+1/2, -y+1/2, -z' 'x+1/2, y+1/2, z+1/2' '-x+1/2, -y+1/2, z+1/2' '-x+1, y+1, -z+1/2' 'x+1, -y+1, -z+1/2' '-x, -y, -z' 'x, y, -z' 'x-1/2, -y-1/2, z' '-x-1/2, y-1/2, z' '-x+1/2, -y+1/2, -z+1/2' 'x+1/2, y+1/2, -z+1/2' 'x, -y, z+1/2' '-x, y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 26198.51 27580.58 403.75 o 4 0 0 1554.13 1667.56 52.65 o 6 0 0 108.81 53.98 28.88 o 8 0 0 21902.89 19042.53 441.65 o 10 0 0 3035.20 2812.26 70.71 o 12 0 0 53.69 86.71 102.61 o 14 0 0 53.95 45.82 115.87 o 16 0 0 520.15 500.20 148.43 o 1 1 0 272.82 313.34 10.64 o 3 1 0 6575.90 7100.05 79.22 o 5 1 0 171.87 196.42 20.57 o 7 1 0 44.55 57.60 21.28 o 9 1 0 124.39 104.33 25.31 o 11 1 0 511.32 566.36 52.58 o 13 1 0 167.62 126.51 75.34 o 15 1 0 22.91 46.76 92.08 o 0 2 0 51505.46 44940.73 654.62 o 2 2 0 12162.51 10867.20 143.02 o 4 2 0 18.08 62.62 28.61 o 6 2 0 7123.20 7225.14 111.26 o 8 2 0 10447.58 9631.61 146.18 o 10 2 0 1531.23 1414.44 58.09 o 12 2 0 2.06 8.15 55.56 o 14 2 0 160.96 122.45 83.53 o 16 2 0 389.16 320.89 124.95 o 1 3 0 79.39 62.78 13.09 o 3 3 0 22929.31 20836.13 243.27 o 5 3 0 13165.69 12969.52 181.16 o 7 3 0 445.42 434.47 36.65 o 9 3 0 209.58 192.87 39.19 o 11 3 0 940.96 901.27 48.23 o 13 3 0 781.94 937.63 88.42 o 15 3 0 141.76 118.11 91.12 o 0 4 0 19971.18 21641.30 324.49 o 2 4 0 566.69 554.37 18.93 o 4 4 0 1746.19 1535.18 25.72 o 6 4 0 6701.95 6364.07 153.55 o 8 4 0 229.26 233.97 37.71 o 10 4 0 167.31 151.26 39.90 o 12 4 0 236.94 299.73 48.05 o 14 4 0 492.68 545.36 89.97 o 1 5 0 252.60 250.01 20.20 o 3 5 0 8698.23 7880.29 105.81 o 5 5 0 12420.56 11806.83 177.77 o 7 5 0 592.68 624.75 39.14 o 9 5 0 0.03 12.77 39.74 o 11 5 0 141.12 144.07 43.34 o 13 5 0 614.11 629.05 56.08 o 15 5 0 79.22 -7.73 89.68 o 0 6 0 216.88 115.39 26.50 o 2 6 0 115.30 139.40 19.99 o 4 6 0 346.93 325.03 23.14 o 6 6 0 13.14 -7.37 37.55 o 8 6 0 280.03 231.61 44.49 o 10 6 0 78.17 56.26 43.78 o 12 6 0 627.39 518.27 53.26 o 14 6 0 457.30 450.84 67.97 o 1 7 0 336.92 358.88 23.34 o 3 7 0 235.10 236.18 19.31 o 5 7 0 102.88 70.90 21.70 o 7 7 0 1.88 47.67 39.91 o 9 7 0 142.03 165.08 45.07 o 11 7 0 94.44 122.18 63.29 o 13 7 0 125.86 208.96 55.60 o 0 8 0 305.83 315.30 65.57 o 2 8 0 4.31 23.35 21.35 o 4 8 0 18.08 24.94 21.25 o 6 8 0 1.78 -7.72 39.41 o 8 8 0 1.72 2.02 43.50 o 10 8 0 123.68 173.57 49.27 o 12 8 0 171.32 87.89 52.60 o 14 8 0 145.01 48.94 64.08 o 1 9 0 45.98 109.77 24.90 o 3 9 0 259.25 230.03 27.41 o 5 9 0 562.79 471.68 59.21 o 7 9 0 355.52 410.22 49.96 o 9 9 0 224.73 168.03 48.17 o 11 9 0 74.01 90.06 53.06 o 13 9 0 0.05 1.71 59.91 o 0 10 0 327.82 200.99 40.50 o 2 10 0 309.54 326.66 29.33 o 4 10 0 0.01 -24.92 41.38 o 6 10 0 536.66 635.75 51.76 o 8 10 0 225.84 203.21 45.29 o 10 10 0 42.68 -19.30 52.82 o 12 10 0 2.25 26.49 59.18 o 1 11 0 22.40 9.05 30.48 o 3 11 0 20.89 -18.32 35.46 o 5 11 0 33.95 88.81 45.22 o 7 11 0 71.65 67.24 41.98 o 9 11 0 55.98 52.71 49.17 o 11 11 0 8.59 30.62 53.00 o 0 12 0 792.07 893.58 105.08 o 2 12 0 731.96 765.27 61.49 o 4 12 0 0.90 -24.60 75.69 o 6 12 0 441.93 512.98 79.30 o 8 12 0 293.77 128.98 79.36 o 10 12 0 204.74 245.40 129.31 o 1 13 0 71.47 115.77 49.70 o 3 13 0 151.25 110.68 79.12 o 5 13 0 135.60 22.57 76.50 o 7 13 0 83.45 142.06 131.20 o 9 13 0 2.51 -73.80 84.96 o 0 14 0 619.67 761.50 79.94 o 2 14 0 344.18 488.48 148.43 o 4 14 0 7.22 56.45 80.38 o 6 14 0 119.85 149.94 88.99 o 8 14 0 176.47 278.80 94.07 o 1 15 0 96.94 65.40 82.59 o 3 15 0 247.19 286.22 91.70 o 5 15 0 220.72 278.39 93.57 o 2 16 0 12.49 -25.81 91.26 o 2 1 1 21511.41 20246.05 173.45 o 4 1 1 3407.44 3640.37 37.18 o 6 1 1 136.03 235.36 16.45 o 8 1 1 1747.57 1493.16 30.27 o 10 1 1 3611.59 3043.81 48.65 o 12 1 1 108.59 102.51 50.27 o 14 1 1 11.20 3.87 58.75 o 16 1 1 256.99 256.55 78.92 o 1 2 1 634.35 898.73 25.81 o 3 2 1 1354.14 1363.76 19.00 o 5 2 1 1584.52 1518.77 49.09 o 7 2 1 717.70 661.07 32.02 o 9 2 1 388.46 483.12 28.74 o 11 2 1 207.86 190.75 30.19 o 13 2 1 658.18 712.48 60.21 o 15 2 1 14.89 24.43 64.05 o 2 3 1 386.45 684.75 17.26 o 4 3 1 12146.33 11223.59 123.59 o 6 3 1 1363.54 1372.48 33.74 o 8 3 1 91.15 161.50 24.76 o 10 3 1 543.01 468.65 31.07 o 12 3 1 358.40 380.30 35.80 o 14 3 1 10.78 14.40 57.92 o 1 4 1 4051.87 4553.42 40.10 o 3 4 1 89.25 196.12 13.81 o 5 4 1 2595.44 2968.66 44.40 o 7 4 1 19.17 67.64 20.52 o 9 4 1 767.45 630.23 30.41 o 11 4 1 266.61 391.54 32.90 o 13 4 1 405.38 395.76 42.12 o 15 4 1 49.46 78.43 62.54 o 2 5 1 2518.92 2277.88 28.14 o 4 5 1 11762.12 10496.60 104.72 o 6 5 1 1831.80 1565.90 43.31 o 8 5 1 506.22 516.97 29.42 o 10 5 1 96.64 82.54 30.18 o 12 5 1 901.83 902.05 38.42 o 14 5 1 159.33 186.61 51.20 o 1 6 1 120.30 162.86 13.89 o 3 6 1 102.51 165.21 13.39 o 5 6 1 143.08 142.98 15.11 o 7 6 1 196.21 209.01 27.47 o 9 6 1 24.06 31.75 29.01 o 11 6 1 0.21 2.60 31.43 o 13 6 1 10.38 -9.82 36.59 o 2 7 1 3050.00 2974.38 48.44 o 4 7 1 4184.57 3906.14 72.16 o 6 7 1 2339.70 2330.33 81.88 o 8 7 1 156.80 172.38 29.98 o 10 7 1 300.27 323.05 34.07 o 12 7 1 840.88 825.64 72.33 o 14 7 1 291.94 341.29 44.18 o 1 8 1 2175.09 1951.41 31.23 o 3 8 1 547.74 614.57 18.93 o 5 8 1 44.39 107.13 21.68 o 7 8 1 213.22 301.93 30.47 o 9 8 1 439.43 479.36 34.95 o 11 8 1 275.70 339.58 36.77 o 13 8 1 40.48 34.92 40.52 o 2 9 1 821.48 689.91 20.22 o 4 9 1 1986.73 1861.94 29.06 o 6 9 1 764.35 821.03 32.97 o 8 9 1 55.81 23.50 32.15 o 10 9 1 294.27 260.06 36.27 o 12 9 1 444.60 520.55 53.21 o 1 10 1 2131.67 1951.28 36.16 o 3 10 1 952.49 972.58 29.04 o 5 10 1 9.27 -3.81 25.57 o 7 10 1 521.73 501.88 31.72 o 9 10 1 740.91 803.41 40.10 o 11 10 1 316.46 402.19 41.21 o 2 11 1 103.22 120.89 23.56 o 4 11 1 480.58 488.34 52.24 o 6 11 1 0.07 -41.23 38.05 o 8 11 1 176.90 156.67 38.63 o 10 11 1 157.14 158.96 43.50 o 1 12 1 630.80 596.56 29.43 o 3 12 1 70.16 -11.75 33.41 o 5 12 1 76.48 94.88 39.35 o 7 12 1 463.77 431.70 45.28 o 9 12 1 383.49 391.40 44.91 o 11 12 1 48.83 64.46 53.37 o 2 13 1 1.91 -38.72 39.61 o 4 13 1 7.30 -49.40 48.48 o 6 13 1 56.00 47.72 53.36 o 8 13 1 129.68 133.65 59.54 o 1 14 1 110.38 122.42 40.82 o 3 14 1 8.44 -24.68 51.04 o 5 14 1 32.20 -53.36 54.84 o 7 14 1 142.45 90.12 63.38 o 2 15 1 1.74 16.66 56.06 o 4 15 1 2.65 -53.44 63.92 o 6 15 1 5.19 -110.88 71.27 o 1 16 1 18.71 12.50 76.27 o 3 16 1 2.54 -2.05 67.44 o 0 0 2 55082.30 54457.85 1372.61 o 2 0 2 6401.95 5818.00 184.91 o 4 0 2 262.21 218.21 31.89 o 6 0 2 3814.14 3371.03 82.53 o 8 0 2 11278.98 11019.28 188.13 o 10 0 2 2788.55 2857.38 77.36 o 12 0 2 288.98 191.00 68.81 o 14 0 2 33.42 -42.40 82.83 o 1 1 2 457.35 391.03 12.78 o 3 1 2 2687.58 2990.49 59.24 o 5 1 2 2096.19 2509.77 40.03 o 7 1 2 230.54 273.17 17.24 o 9 1 2 209.34 275.56 22.34 o 11 1 2 34.74 -9.65 45.73 o 13 1 2 91.17 104.20 53.38 o 15 1 2 34.38 33.82 65.14 o 0 2 2 29064.46 25488.71 464.50 o 2 2 2 7809.50 6910.40 74.47 o 4 2 2 183.76 182.73 16.27 o 6 2 2 2218.53 2255.95 29.22 o 8 2 2 5531.50 5180.34 57.78 o 10 2 2 1436.77 1353.27 34.95 o 12 2 2 8.35 -15.24 48.40 o 14 2 2 122.44 138.83 59.46 o 1 3 2 192.84 236.17 14.70 o 3 3 2 8302.79 8714.92 179.84 o 5 3 2 8543.18 8560.54 73.83 o 7 3 2 971.03 897.56 33.99 o 9 3 2 501.49 522.68 29.41 o 11 3 2 161.04 259.27 30.84 o 13 3 2 537.69 516.94 48.97 o 15 3 2 159.34 130.58 65.29 o 0 4 2 4478.35 4483.94 94.88 o 2 4 2 1517.74 1668.95 37.63 o 4 4 2 170.36 364.69 19.36 o 6 4 2 745.14 742.49 22.96 o 8 4 2 679.88 622.46 31.45 o 10 4 2 101.70 52.99 28.51 o 12 4 2 390.72 447.92 47.55 o 14 4 2 386.38 299.62 61.54 o 1 5 2 323.38 343.54 15.26 o 3 5 2 2806.10 2574.39 42.83 o 5 5 2 3168.98 2883.24 76.75 o 7 5 2 432.46 418.99 27.70 o 9 5 2 25.93 -14.63 26.70 o 11 5 2 226.84 299.27 33.33 o 13 5 2 532.57 524.71 42.57 o 15 5 2 71.76 92.20 66.86 o 0 6 2 5.00 31.19 19.04 o 2 6 2 208.16 206.28 14.43 o 4 6 2 587.84 511.74 19.58 o 6 6 2 716.17 802.51 25.66 o 8 6 2 48.03 86.23 27.41 o 10 6 2 88.54 76.78 31.12 o 12 6 2 564.09 497.32 38.85 o 14 6 2 420.35 457.08 51.00 o 1 7 2 37.19 96.11 15.24 o 3 7 2 136.65 163.94 15.84 o 5 7 2 93.86 118.77 19.79 o 7 7 2 14.38 -1.70 25.44 o 9 7 2 142.15 166.37 31.09 o 11 7 2 179.79 238.91 34.63 o 13 7 2 129.01 75.75 39.95 o 0 8 2 36.22 65.35 22.43 o 2 8 2 0.81 72.64 16.79 o 4 8 2 93.93 89.90 15.81 o 6 8 2 699.96 665.84 28.66 o 8 8 2 14.08 9.08 30.52 o 10 8 2 55.01 36.42 33.08 o 12 8 2 134.36 145.60 38.91 o 1 9 2 48.57 49.46 17.66 o 3 9 2 7.45 17.93 18.00 o 5 9 2 25.76 49.34 23.93 o 7 9 2 248.97 277.10 29.92 o 9 9 2 213.65 174.89 31.20 o 11 9 2 52.11 19.79 37.59 o 13 9 2 1.28 24.62 43.54 o 0 10 2 472.97 431.16 35.44 o 2 10 2 598.25 556.96 24.64 o 4 10 2 4.11 11.15 28.30 o 6 10 2 321.16 350.39 34.77 o 8 10 2 62.64 37.23 35.17 o 10 10 2 46.32 50.00 40.97 o 12 10 2 0.07 29.58 48.79 o 1 11 2 2.87 20.98 23.22 o 3 11 2 4.26 -12.98 25.04 o 5 11 2 3.10 -14.28 35.37 o 7 11 2 25.83 35.11 35.01 o 9 11 2 69.61 68.04 41.58 o 11 11 2 12.97 -33.99 45.18 o 0 12 2 895.21 888.84 65.91 o 2 12 2 669.93 690.89 28.55 o 4 12 2 24.97 0.95 35.02 o 6 12 2 175.44 149.64 41.13 o 8 12 2 209.88 236.81 46.85 o 10 12 2 142.49 129.58 46.18 o 1 13 2 82.00 74.05 29.09 o 3 13 2 102.08 111.50 36.62 o 5 13 2 65.16 52.39 40.69 o 7 13 2 57.95 13.99 47.24 o 9 13 2 10.86 -31.62 55.22 o 0 14 2 372.06 401.45 51.94 o 2 14 2 165.74 129.40 48.26 o 4 14 2 1.65 -30.49 50.72 o 6 14 2 103.67 131.01 70.07 o 8 14 2 172.97 231.14 65.80 o 1 15 2 59.75 76.93 52.70 o 3 15 2 173.52 176.80 57.24 o 5 15 2 163.96 220.73 65.12 o 0 16 2 52.30 120.79 106.40 o 2 16 2 5.52 40.56 65.29 o 2 1 3 550.19 1043.99 34.28 o 4 1 3 74.32 250.15 22.87 o 6 1 3 27.39 -6.48 17.77 o 8 1 3 567.66 581.60 30.50 o 10 1 3 469.97 502.47 39.46 o 12 1 3 42.26 8.86 49.79 o 14 1 3 20.41 23.78 63.94 o 1 2 3 27319.49 27054.18 283.60 o 3 2 3 2290.13 2095.60 38.03 o 5 2 3 715.36 911.10 23.80 o 7 2 3 76.16 66.52 16.12 o 9 2 3 795.03 775.89 34.99 o 11 2 3 208.30 218.28 35.12 o 13 2 3 86.87 95.28 53.74 o 15 2 3 14.75 -7.06 64.43 o 2 3 3 5264.52 4971.20 66.07 o 4 3 3 11.16 1.48 15.08 o 6 3 3 235.79 169.93 17.82 o 8 3 3 5.17 51.99 23.88 o 10 3 3 1199.47 981.10 33.41 o 12 3 3 350.46 410.76 46.47 o 14 3 3 20.95 41.53 58.31 o 1 4 3 3715.80 4300.51 107.93 o 3 4 3 406.77 494.59 18.87 o 5 4 3 32.39 27.16 15.26 o 7 4 3 907.03 936.08 25.21 o 9 4 3 824.51 774.35 31.20 o 11 4 3 160.24 161.17 30.31 o 13 4 3 176.99 138.69 48.43 o 15 4 3 14.98 -37.59 72.09 o 2 5 3 6833.78 6843.73 230.36 o 4 5 3 4630.86 4448.21 78.82 o 6 5 3 3371.57 3073.67 47.64 o 8 5 3 64.95 56.86 27.20 o 10 5 3 843.19 730.81 44.96 o 12 5 3 655.27 733.19 38.92 o 14 5 3 197.66 238.90 63.66 o 1 6 3 458.45 352.27 16.61 o 3 6 3 448.10 421.55 19.84 o 5 6 3 39.90 44.25 19.80 o 7 6 3 60.06 87.07 26.45 o 9 6 3 9.66 -9.85 28.84 o 11 6 3 12.10 23.92 32.61 o 13 6 3 28.45 44.64 38.12 o 2 7 3 2660.44 2412.98 38.01 o 4 7 3 9698.77 9034.67 120.00 o 6 7 3 3219.62 3091.21 61.20 o 8 7 3 18.03 29.95 28.45 o 10 7 3 190.67 155.23 32.49 o 12 7 3 701.70 822.78 46.18 o 14 7 3 210.33 272.16 52.23 o 1 8 3 1002.85 1197.43 26.58 o 3 8 3 909.95 775.16 26.26 o 5 8 3 232.42 222.28 22.72 o 7 8 3 787.18 841.75 30.71 o 9 8 3 422.35 607.22 36.49 o 11 8 3 274.00 242.10 37.29 o 13 8 3 17.42 10.89 42.19 o 2 9 3 711.16 690.02 26.13 o 4 9 3 3026.30 2635.43 53.09 o 6 9 3 326.69 329.69 33.60 o 8 9 3 16.03 -9.65 31.46 o 10 9 3 141.21 145.04 39.71 o 12 9 3 487.74 442.75 59.66 o 1 10 3 1523.72 1591.43 31.90 o 3 10 3 307.20 372.63 26.52 o 5 10 3 158.16 145.07 35.31 o 7 10 3 881.45 867.76 41.19 o 9 10 3 684.08 639.37 43.63 o 11 10 3 203.04 245.50 46.05 o 2 11 3 35.09 26.55 23.51 o 4 11 3 89.76 11.10 33.79 o 6 11 3 25.68 39.24 37.90 o 8 11 3 142.90 170.87 38.51 o 10 11 3 160.94 172.90 44.86 o 1 12 3 945.28 859.24 30.04 o 3 12 3 42.78 54.25 31.87 o 5 12 3 7.22 20.16 36.14 o 7 12 3 301.81 284.26 48.41 o 9 12 3 301.78 269.04 49.02 o 2 13 3 1.21 48.41 32.84 o 4 13 3 11.67 25.22 36.76 o 6 13 3 33.60 -11.10 41.85 o 8 13 3 103.05 67.44 49.33 o 1 14 3 103.82 105.24 31.44 o 3 14 3 0.00 4.76 39.51 o 5 14 3 9.80 2.84 42.06 o 7 14 3 82.45 25.13 55.36 o 2 15 3 2.33 12.15 51.92 o 4 15 3 0.43 13.29 54.86 o 1 16 3 0.87 -39.90 66.81 o 0 0 4 265.84 372.59 56.42 o 2 0 4 4551.33 4569.25 72.56 o 4 0 4 133.56 292.32 54.26 o 6 0 4 3065.23 2751.31 66.48 o 8 0 4 2610.49 2777.36 91.05 o 10 0 4 1653.34 1971.45 94.66 o 12 0 4 163.79 100.11 107.54 o 14 0 4 27.02 -29.20 81.45 o 1 1 4 19.03 96.83 24.57 o 3 1 4 189.50 199.06 20.76 o 5 1 4 1433.42 1557.25 51.47 o 7 1 4 497.57 475.70 23.72 o 9 1 4 92.08 95.85 27.32 o 11 1 4 43.19 5.97 46.62 o 13 1 4 27.16 44.07 55.35 o 15 1 4 36.21 36.50 63.76 o 0 2 4 13488.77 15211.19 936.21 o 2 2 4 2513.21 2648.93 48.35 o 4 2 4 18.41 35.53 20.62 o 6 2 4 557.84 492.44 32.94 o 8 2 4 2585.50 2378.44 46.03 o 10 2 4 991.22 893.83 38.25 o 12 2 4 2.03 -39.72 48.30 o 14 2 4 69.81 62.76 60.46 o 1 3 4 166.59 143.29 20.52 o 3 3 4 848.08 1006.29 28.13 o 5 3 4 2127.68 2076.32 35.24 o 7 3 4 1342.06 1129.89 30.67 o 9 3 4 330.63 326.43 32.63 o 11 3 4 1.11 64.30 32.60 o 13 3 4 227.89 287.58 57.48 o 15 3 4 121.56 143.32 66.89 o 0 4 4 19454.58 17030.69 807.47 o 2 4 4 482.37 411.59 30.11 o 4 4 4 15.86 27.64 19.06 o 6 4 4 209.70 363.23 22.01 o 8 4 4 1932.99 1491.42 34.59 o 10 4 4 46.74 24.26 33.78 o 12 4 4 224.16 217.34 39.85 o 14 4 4 218.13 218.75 63.77 o 1 5 4 1.08 14.45 29.71 o 3 5 4 760.46 967.39 40.54 o 5 5 4 450.86 598.00 24.81 o 7 5 4 103.00 99.00 22.63 o 9 5 4 46.85 53.23 28.38 o 11 5 4 223.43 247.40 34.31 o 13 5 4 310.17 308.07 53.43 o 0 6 4 118.12 532.95 49.18 o 2 6 4 44.45 39.62 20.04 o 4 6 4 224.89 302.10 21.26 o 6 6 4 1783.31 1816.07 35.03 o 8 6 4 389.43 435.81 31.33 o 10 6 4 59.65 32.30 30.51 o 12 6 4 308.77 357.78 41.60 o 14 6 4 354.40 368.41 66.97 o 1 7 4 169.27 162.05 26.96 o 3 7 4 399.33 405.20 21.51 o 5 7 4 478.42 461.89 24.06 o 7 7 4 150.13 142.71 26.97 o 9 7 4 63.66 64.75 30.28 o 11 7 4 180.49 149.50 35.89 o 13 7 4 114.08 87.66 46.00 o 0 8 4 94.95 56.87 32.68 o 2 8 4 110.11 110.98 25.94 o 4 8 4 239.32 279.13 36.15 o 6 8 4 980.01 1008.95 37.05 o 8 8 4 0.04 27.90 32.10 o 10 8 4 0.23 -1.17 33.23 o 12 8 4 126.85 70.59 50.61 o 1 9 4 0.51 19.80 23.65 o 3 9 4 152.76 110.78 28.17 o 5 9 4 84.37 31.32 28.43 o 7 9 4 79.41 42.44 32.12 o 9 9 4 133.35 235.79 37.22 o 11 9 4 49.39 14.65 40.67 o 0 10 4 369.18 401.84 36.11 o 2 10 4 416.87 434.58 26.92 o 4 10 4 1.43 -21.93 25.51 o 6 10 4 103.17 84.17 36.54 o 8 10 4 18.87 43.01 36.48 o 10 10 4 47.04 25.17 41.38 o 12 10 4 4.28 -36.95 47.44 o 1 11 4 128.91 127.92 24.23 o 3 11 4 26.20 31.75 26.38 o 5 11 4 2.10 32.25 36.77 o 7 11 4 1.27 21.35 40.63 o 9 11 4 93.28 154.43 41.16 o 11 11 4 24.71 -0.12 46.51 o 0 12 4 495.88 593.61 45.82 o 2 12 4 297.71 324.22 31.44 o 4 12 4 39.41 69.52 45.69 o 6 12 4 70.55 114.55 42.27 o 8 12 4 150.35 214.84 46.03 o 10 12 4 53.56 57.84 46.31 o 1 13 4 46.36 12.97 30.16 o 3 13 4 35.83 75.36 36.86 o 5 13 4 26.71 31.92 41.06 o 7 13 4 27.24 66.38 46.32 o 0 14 4 180.88 143.41 49.43 o 2 14 4 60.69 16.53 41.48 o 4 14 4 0.21 -34.12 41.42 o 6 14 4 65.08 82.87 46.84 o 1 15 4 16.48 47.29 46.01 o 3 15 4 98.25 111.51 49.06 o 5 15 4 103.18 17.81 57.10 o 2 1 5 32.91 230.10 20.34 o 4 1 5 99.74 125.82 20.41 o 6 1 5 74.30 70.57 24.98 o 8 1 5 228.24 282.90 38.73 o 10 1 5 493.07 462.51 33.20 o 12 1 5 79.92 54.16 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