#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/03/2200356.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200356_Fobs loop_ _publ_author_name 'Howie, R. Alan' 'McQuillan, Geoffrey P.' 'Thompson, David W.' _publ_section_title ; Dichlorobis(\h^5^-1,2,4-trimethylcyclopentadienyl)titanium(IV) ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m181 _journal_page_last m182 _journal_volume 57 _journal_year 2001 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 119.890 _cell_angle_gamma 90.000 _cell_length_a 16.7880 _cell_length_b 6.7910 _cell_length_c 15.8140 _exptl_crystal_F_000 696.00 _reflns_d_resolution_high 0.7093 _[local]_cod_data_source_file wn6013Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C16H22TiCl2 (C2/c, Z=4)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 202.64 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z+1/2' '-x, -y, -z' '-x, y, -z-1/2' '-x+1/2, -y+1/2, -z' '-x+1/2, y+1/2, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 2397.91 2558.51 12.12 o 6 0 0 416.82 383.67 4.91 o 8 0 0 5265.76 5411.45 17.55 o 10 0 0 3318.17 3203.75 13.54 o 12 0 0 37.85 45.49 2.26 o 14 0 0 109.47 141.83 3.24 o 16 0 0 817.00 809.67 6.95 o 18 0 0 435.36 386.53 4.93 o 20 0 0 224.84 170.02 3.48 o 1 1 0 15550.94 12932.55 27.06 o 3 1 0 5349.80 5973.10 18.43 o 5 1 0 16034.58 17224.88 31.22 o 7 1 0 455.91 657.60 6.30 o 9 1 0 835.77 850.39 7.11 o 11 1 0 411.18 435.24 5.20 o 13 1 0 849.38 889.50 7.26 o 15 1 0 73.70 58.24 2.41 o 17 1 0 120.16 118.00 3.03 o 19 1 0 155.51 151.85 3.33 o 0 2 0 771.34 830.17 7.03 o 2 2 0 4300.47 4046.61 15.20 o 4 2 0 3138.01 3039.74 13.19 o 6 2 0 1668.81 1802.56 10.21 o 8 2 0 373.83 408.36 5.06 o 10 2 0 2.54 10.41 1.77 o 12 2 0 1027.34 1040.00 7.83 o 14 2 0 596.30 580.16 5.94 o 16 2 0 53.95 51.26 2.33 o 18 2 0 0.73 2.48 1.63 o 1 3 0 2224.11 1832.54 10.29 o 3 3 0 9980.82 9990.56 23.80 o 5 3 0 6691.09 6983.01 19.91 o 7 3 0 3726.79 3960.43 15.03 o 9 3 0 325.86 380.02 4.90 o 11 3 0 549.76 600.75 6.04 o 13 3 0 1006.74 970.81 7.57 o 15 3 0 139.45 112.01 2.97 o 17 3 0 148.47 139.06 3.22 o 19 3 0 73.90 77.00 2.62 o 0 4 0 2421.57 2133.00 11.09 o 2 4 0 596.87 654.70 6.28 o 4 4 0 42.96 38.31 2.17 o 6 4 0 1925.94 1900.93 10.48 o 8 4 0 3340.34 3362.68 13.86 o 12 4 0 73.05 75.31 2.60 o 14 4 0 44.19 55.12 2.38 o 16 4 0 147.12 127.07 3.11 o 1 5 0 3517.07 3305.30 13.75 o 3 5 0 6.48 11.96 1.79 o 5 5 0 212.33 237.38 3.99 o 7 5 0 150.91 127.24 3.11 o 9 5 0 1102.45 1118.30 8.10 o 11 5 0 0.76 0.82 1.60 o 13 5 0 107.02 118.95 3.04 o 15 5 0 417.13 384.47 4.92 o 17 5 0 617.74 641.20 6.22 o 0 6 0 331.06 267.25 4.20 o 2 6 0 1260.91 1159.04 8.24 o 4 6 0 2631.55 2639.95 12.31 o 6 6 0 344.54 428.16 5.17 o 8 6 0 53.69 48.01 2.29 o 10 6 0 90.47 69.94 2.54 o 12 6 0 675.52 640.85 6.22 o 14 6 0 600.28 597.11 6.02 o 1 7 0 727.68 744.29 6.68 o 3 7 0 13.82 12.78 1.80 o 5 7 0 87.42 119.18 3.04 o 7 7 0 4.40 16.67 1.86 o 9 7 0 353.22 402.91 5.03 o 11 7 0 87.11 105.16 2.91 o 13 7 0 19.17 45.98 2.26 o 0 8 0 61.71 79.27 2.65 o 2 8 0 156.89 168.09 3.46 o 4 8 0 136.78 138.49 3.22 o 6 8 0 7.03 6.22 1.70 o 8 8 0 15.07 17.59 1.88 o 10 8 0 190.42 187.41 3.62 o 1 9 0 175.06 165.41 3.44 o 3 9 0 44.66 54.46 2.36 o 5 9 0 59.66 61.64 2.45 o 7 9 0 235.73 227.57 3.92 o -19 1 1 210.97 187.29 3.62 o -17 1 1 900.24 858.82 7.14 o -15 1 1 633.44 604.93 6.05 o -13 1 1 768.52 788.52 6.86 o -11 1 1 2758.89 2760.54 12.58 o -9 1 1 4471.76 4679.37 16.32 o -7 1 1 926.81 1011.05 7.72 o -5 1 1 184.29 161.15 3.41 o -3 1 1 8384.81 8911.76 22.48 o -1 1 1 19645.26 13846.80 28.00 o 1 1 1 10409.15 10212.21 24.06 o 3 1 1 37.11 43.93 2.24 o 5 1 1 420.61 656.41 6.29 o 7 1 1 3706.23 3831.91 14.79 o 9 1 1 1837.29 1865.28 10.38 o 11 1 1 81.71 84.50 2.70 o 15 1 1 739.32 792.62 6.87 o 17 1 1 640.47 649.45 6.26 o 19 1 1 140.74 123.29 3.08 o -20 2 1 161.44 173.47 3.51 o -18 2 1 83.25 93.57 2.79 o -16 2 1 54.58 44.53 2.25 o -14 2 1 2022.04 1932.69 10.56 o -12 2 1 4694.77 4755.30 16.46 o -10 2 1 458.04 433.08 5.19 o -8 2 1 31.81 38.17 2.16 o -6 2 1 7694.19 7771.41 21.00 o -4 2 1 13314.67 13188.11 27.33 o -2 2 1 1673.40 1703.26 9.93 o 0 2 1 2033.25 1994.46 10.73 o 2 2 1 21149.42 19541.71 33.25 o 4 2 1 9415.84 10042.73 23.86 o 6 2 1 445.56 576.91 5.92 o 8 2 1 593.11 638.43 6.21 o 10 2 1 198.48 195.60 3.68 o 12 2 1 1338.17 1472.94 9.25 o 14 2 1 313.24 314.70 4.50 o 16 2 1 7.10 23.79 1.97 o 18 2 1 181.21 201.24 3.72 o -19 3 1 93.45 67.02 2.51 o -17 3 1 298.98 291.89 4.36 o -15 3 1 218.07 217.38 3.85 o -13 3 1 645.50 699.99 6.48 o -11 3 1 175.45 184.33 3.59 o -9 3 1 2571.98 2677.87 12.40 o -7 3 1 11.06 0.43 1.60 o -5 3 1 4310.74 4382.52 15.81 o -3 3 1 1462.30 1433.60 9.14 o -1 3 1 415.82 351.22 4.73 o 1 3 1 293.55 341.13 4.67 o 3 3 1 3709.09 3916.49 14.95 o 5 3 1 4371.31 4728.67 16.41 o 7 3 1 964.44 937.80 7.45 o 9 3 1 807.83 776.49 6.81 o 11 3 1 705.97 701.01 6.49 o 13 3 1 311.90 290.65 4.35 o 15 3 1 59.36 44.36 2.25 o 17 3 1 52.54 37.46 2.16 o -18 4 1 263.98 261.58 4.16 o -16 4 1 299.66 308.03 4.46 o -14 4 1 30.50 50.56 2.32 o -12 4 1 254.31 297.01 4.39 o -10 4 1 2315.23 2319.30 11.55 o -8 4 1 1991.67 1961.91 10.64 o -6 4 1 402.29 395.76 4.99 o -4 4 1 386.50 412.91 5.08 o -2 4 1 5324.03 5158.44 17.14 o 0 4 1 10527.49 9193.18 22.83 o 2 4 1 2248.56 2304.56 11.51 o 4 4 1 479.40 592.40 6.00 o 6 4 1 982.17 1017.25 7.74 o 8 4 1 699.97 780.35 6.82 o 10 4 1 210.10 238.23 4.00 o 12 4 1 5.15 1.89 1.63 o 14 4 1 131.94 138.76 3.22 o 16 4 1 836.29 841.14 7.07 o 18 4 1 314.69 312.33 4.49 o -17 5 1 87.59 88.04 2.74 o -15 5 1 551.69 574.17 5.91 o -13 5 1 301.97 301.77 4.42 o -11 5 1 89.19 90.63 2.76 o -9 5 1 132.04 138.93 3.22 o -7 5 1 1193.30 1194.19 8.36 o -5 5 1 2537.27 2433.75 11.83 o -3 5 1 1090.76 1086.00 7.99 o -1 5 1 762.71 746.89 6.68 o 1 5 1 783.61 810.52 6.95 o 3 5 1 774.54 809.29 6.94 o 5 5 1 863.77 924.29 7.40 o 7 5 1 39.74 50.25 2.31 o 9 5 1 12.68 25.00 1.99 o 11 5 1 38.37 43.91 2.24 o 13 5 1 291.17 282.70 4.30 o 15 5 1 435.41 386.18 4.93 o -16 6 1 91.20 91.08 2.77 o -12 6 1 78.01 80.00 2.65 o -10 6 1 59.08 55.49 2.38 o -8 6 1 614.85 598.36 6.03 o -6 6 1 53.16 59.71 2.43 o -4 6 1 498.43 444.16 5.25 o -2 6 1 110.68 97.26 2.83 o 0 6 1 608.06 571.02 5.90 o 2 6 1 174.65 174.04 3.52 o 4 6 1 74.69 92.47 2.78 o 6 6 1 453.46 448.91 5.28 o 8 6 1 163.78 170.96 3.49 o 10 6 1 56.27 27.18 2.01 o 14 6 1 56.20 54.07 2.36 o -13 7 1 691.26 680.08 6.39 o -11 7 1 316.55 284.76 4.31 o -9 7 1 48.25 52.67 2.35 o -7 7 1 256.24 285.09 4.32 o -5 7 1 827.04 846.14 7.09 o -3 7 1 798.42 787.25 6.85 o -1 7 1 223.64 207.21 3.77 o 1 7 1 675.90 646.95 6.25 o 3 7 1 2056.19 2045.60 10.86 o 5 7 1 834.21 909.43 7.34 o 7 7 1 23.70 40.88 2.20 o 9 7 1 83.13 65.79 2.50 o 11 7 1 609.81 588.96 5.98 o 13 7 1 190.11 202.24 3.74 o -10 8 1 442.63 494.12 5.51 o -8 8 1 592.10 560.76 5.85 o -6 8 1 3.30 5.81 1.69 o -2 8 1 621.42 591.58 5.99 o 0 8 1 891.38 894.61 7.28 o 2 8 1 85.27 75.14 2.60 o 4 8 1 0.47 3.01 1.64 o 6 8 1 266.54 259.57 4.14 o 8 8 1 540.74 585.83 5.96 o 10 8 1 78.85 100.73 2.87 o -7 9 1 3.89 1.22 1.61 o -5 9 1 4.51 12.94 1.81 o -3 9 1 43.11 58.06 2.41 o -1 9 1 183.03 225.86 3.91 o 1 9 1 50.46 61.44 2.45 o 3 9 1 18.07 25.91 2.00 o 5 9 1 8.61 8.80 1.74 o -20 0 2 316.42 254.70 4.11 o -18 0 2 791.60 724.49 6.59 o -16 0 2 700.94 740.84 6.66 o -14 0 2 303.24 267.14 4.20 o -12 0 2 58.17 66.61 2.51 o -10 0 2 19284.91 20562.25 34.10 o -8 0 2 9693.14 10235.51 24.08 o -6 0 2 56.16 104.77 2.91 o -4 0 2 1582.25 1684.72 9.88 o 0 0 2 19089.71 20478.47 34.03 o 2 0 2 1730.03 2142.62 11.11 o 4 0 2 6230.29 7351.35 20.43 o 6 0 2 6417.73 6198.06 18.77 o 8 0 2 3489.69 3638.46 14.42 o 10 0 2 1236.68 1156.56 8.23 o 12 0 2 15.16 19.68 1.91 o 14 0 2 1215.45 1367.36 8.93 o 16 0 2 1483.91 1477.48 9.27 o 18 0 2 199.37 163.34 3.43 o -21 1 2 203.00 225.53 3.90 o -19 1 2 5.11 14.86 1.83 o -17 1 2 39.83 49.66 2.31 o -15 1 2 480.80 471.04 5.39 o -13 1 2 64.36 97.21 2.83 o -11 1 2 44.39 46.95 2.27 o -9 1 2 291.96 373.99 4.86 o -7 1 2 1838.41 1999.72 10.74 o -5 1 2 11526.56 12220.29 26.31 o -3 1 2 139.42 161.18 3.41 o -1 1 2 1.92 1.42 1.61 o 1 1 2 3517.30 4049.64 15.20 o 3 1 2 11442.22 12782.63 26.90 o 5 1 2 672.01 580.49 5.94 o 7 1 2 5226.16 5815.93 18.19 o 9 1 2 752.12 817.25 6.97 o 11 1 2 4514.42 4540.09 16.08 o 13 1 2 537.44 544.45 5.77 o 19 1 2 170.63 159.02 3.39 o -20 2 2 47.11 51.34 2.33 o -18 2 2 44.38 38.24 2.17 o -16 2 2 662.04 642.43 6.23 o -14 2 2 2436.90 2373.49 11.68 o -12 2 2 1407.18 1410.22 9.06 o -10 2 2 86.03 99.93 2.86 o -8 2 2 530.75 485.22 5.47 o -6 2 2 2190.38 2100.27 11.00 o -4 2 2 1665.77 1660.43 9.81 o -2 2 2 128.86 173.08 3.50 o 0 2 2 2932.85 2754.10 12.57 o 2 2 2 7200.26 6802.91 19.66 o 4 2 2 7412.85 7769.70 21.00 o 6 2 2 2533.65 2946.33 12.99 o 8 2 2 14.10 6.20 1.70 o 10 2 2 306.57 242.98 4.03 o 12 2 2 106.63 110.72 2.96 o 14 2 2 46.78 56.37 2.39 o 16 2 2 68.59 78.17 2.64 o 18 2 2 221.97 231.44 3.95 o -19 3 2 33.19 45.13 2.25 o -17 3 2 202.78 171.67 3.49 o -15 3 2 872.51 809.86 6.95 o -13 3 2 3876.87 3834.82 14.80 o -11 3 2 2697.45 2709.65 12.46 o -9 3 2 753.68 715.18 6.55 o -7 3 2 491.23 467.22 5.38 o -5 3 2 725.13 677.57 6.38 o -3 3 2 3842.97 3398.74 13.94 o -1 3 2 1194.55 904.67 7.32 o 1 3 2 3260.84 3193.94 13.52 o 3 3 2 7941.68 8133.97 21.48 o 5 3 2 2315.47 2513.92 12.01 o 7 3 2 1179.98 1185.19 8.33 o 9 3 2 518.40 585.91 5.96 o 11 3 2 439.46 478.28 5.43 o 13 3 2 81.94 55.13 2.38 o 15 3 2 75.86 92.94 2.79 o 17 3 2 811.07 822.21 7.00 o -18 4 2 169.42 176.56 3.53 o -16 4 2 254.25 264.27 4.18 o -14 4 2 11.01 18.20 1.88 o -12 4 2 28.03 34.86 2.12 o -10 4 2 1029.11 1047.92 7.85 o -8 4 2 466.94 452.38 5.30 o -6 4 2 1180.65 1297.65 8.70 o -2 4 2 4599.92 4028.90 15.16 o 0 4 2 649.05 618.14 6.12 o 2 4 2 62.82 52.74 2.35 o 4 4 2 219.08 243.47 4.03 o 6 4 2 2654.87 2677.15 12.39 o 8 4 2 893.11 954.50 7.51 o 10 4 2 118.30 93.76 2.80 o 12 4 2 16.22 19.48 1.91 o 14 4 2 110.50 91.20 2.77 o 16 4 2 295.47 292.72 4.36 o -17 5 2 222.44 221.76 3.88 o -13 5 2 8.60 15.52 1.85 o -11 5 2 1960.26 1916.27 10.52 o -9 5 2 3219.84 2976.17 13.06 o -7 5 2 142.26 122.77 3.08 o -5 5 2 318.42 310.73 4.48 o -3 5 2 203.07 194.60 3.67 o -1 5 2 4433.05 4081.23 15.26 o 1 5 2 590.25 612.19 6.09 o 3 5 2 1306.35 1310.09 8.75 o 5 5 2 16.16 31.59 2.08 o 7 5 2 905.57 917.28 7.37 o 9 5 2 153.00 196.28 3.69 o 11 5 2 94.58 89.97 2.76 o 13 5 2 95.78 76.05 2.61 o 15 5 2 456.53 423.95 5.14 o -16 6 2 204.76 203.57 3.74 o -14 6 2 881.07 891.94 7.27 o -12 6 2 530.52 457.39 5.32 o -10 6 2 194.07 186.18 3.61 o -8 6 2 938.51 984.75 7.62 o -6 6 2 3364.71 3272.22 13.68 o -4 6 2 1140.24 1047.63 7.85 o -2 6 2 28.04 29.71 2.05 o 0 6 2 99.89 96.72 2.83 o 2 6 2 1260.84 1222.43 8.46 o 4 6 2 774.64 824.99 7.01 o 6 6 2 11.01 3.63 1.65 o 8 6 2 43.35 53.58 2.36 o 10 6 2 380.67 378.70 4.89 o 12 6 2 857.04 882.21 7.23 o 14 6 2 223.94 229.31 3.93 o -11 7 2 225.05 212.36 3.81 o -9 7 2 235.67 226.60 3.92 o -7 7 2 17.09 23.61 1.96 o -5 7 2 42.13 44.47 2.25 o -3 7 2 200.02 225.02 3.90 o -1 7 2 249.00 274.97 4.25 o 1 7 2 4.32 13.81 1.82 o 3 7 2 129.70 148.35 3.30 o 5 7 2 27.50 29.03 2.04 o 7 7 2 66.46 85.84 2.71 o 9 7 2 144.62 176.49 3.53 o 11 7 2 12.83 13.62 1.82 o -12 8 2 416.21 423.78 5.14 o -10 8 2 113.99 124.13 3.09 o -8 8 2 26.14 12.50 1.80 o -6 8 2 98.37 83.17 2.69 o -4 8 2 89.30 89.74 2.75 o -2 8 2 23.24 37.30 2.15 o 0 8 2 70.49 73.05 2.58 o 2 8 2 180.57 152.55 3.33 o 4 8 2 64.45 59.90 2.43 o 6 8 2 41.56 65.97 2.50 o 8 8 2 103.36 111.64 2.97 o 10 8 2 31.51 37.84 2.16 o -7 9 2 199.49 207.73 3.77 o -5 9 2 48.83 52.35 2.34 o -3 9 2 99.33 100.12 2.86 o -1 9 2 199.53 171.48 3.49 o 1 9 2 51.04 57.76 2.40 o 3 9 2 5.79 12.53 1.80 o 5 9 2 109.70 100.67 2.87 o -21 1 3 150.12 123.42 3.08 o -19 1 3 692.45 674.80 6.37 o -17 1 3 650.96 629.80 6.17 o -15 1 3 312.04 312.65 4.49 o -13 1 3 1139.20 1142.76 8.19 o -11 1 3 5134.13 5213.22 17.23 o -9 1 3 10959.88 11884.04 25.95 o -7 1 3 3454.70 3536.09 14.21 o -5 1 3 971.72 1231.82 8.49 o -3 1 3 18.36 20.46 1.92 o -1 1 3 2830.74 2818.72 12.71 o 1 1 3 382.36 340.31 4.66 o 3 1 3 383.09 364.79 4.81 o 5 1 3 4748.99 5287.47 17.35 o 7 1 3 3273.43 3575.55 14.29 o 9 1 3 1.09 4.72 1.67 o 11 1 3 13.71 15.47 1.85 o 13 1 3 891.96 888.73 7.26 o 15 1 3 585.03 503.15 5.56 o 17 1 3 161.39 157.16 3.37 o -20 2 3 99.72 98.14 2.84 o -18 2 3 20.17 15.97 1.85 o -16 2 3 1072.76 981.09 7.61 o -14 2 3 5350.34 5237.40 17.27 o -12 2 3 1118.96 1249.84 8.55 o -10 2 3 5.17 13.15 1.81 o -8 2 3 6306.80 6810.67 19.67 o -6 2 3 11802.12 11801.94 25.86 o -4 2 3 75.40 46.37 2.27 o -2 2 3 1006.10 1149.09 8.21 o 0 2 3 755.36 764.11 6.75 o 2 2 3 6271.48 6133.33 18.67 o 4 2 3 945.89 928.83 7.41 o 6 2 3 62.65 103.60 2.89 o 8 2 3 121.84 134.75 3.18 o 10 2 3 1528.74 1533.04 9.43 o 12 2 3 1012.96 1065.48 7.92 o 14 2 3 2.05 9.58 1.75 o 18 2 3 561.02 535.14 5.72 o -19 3 3 289.82 295.58 4.38 o -17 3 3 10.94 14.69 1.83 o -15 3 3 302.40 311.20 4.48 o -11 3 3 487.09 504.04 5.56 o -9 3 3 602.87 624.46 6.14 o -7 3 3 1227.66 1179.57 8.31 o -5 3 3 2457.10 2318.93 11.55 o -3 3 3 4109.13 3727.18 14.59 o -1 3 3 5994.25 5344.83 17.44 o 1 3 3 2460.70 2311.98 11.53 o 3 3 3 4968.78 5208.62 17.22 o 5 3 3 43.45 34.29 2.11 o 7 3 3 990.56 982.98 7.62 o 9 3 3 664.00 637.64 6.21 o 11 3 3 1029.70 1007.34 7.70 o 13 3 3 4.75 11.45 1.78 o 15 3 3 41.18 50.16 2.31 o 17 3 3 0.08 1.57 1.62 o -20 4 3 253.18 232.16 3.96 o -18 4 3 143.25 143.68 3.26 o -16 4 3 69.01 65.09 2.49 o -14 4 3 147.53 164.50 3.44 o -12 4 3 2445.95 2571.68 12.15 o -10 4 3 3587.90 3416.93 13.98 o -8 4 3 85.24 50.15 2.31 o -6 4 3 38.29 32.34 2.09 o -4 4 3 1363.12 1177.92 8.31 o -2 4 3 3333.13 2796.22 12.66 o 0 4 3 472.89 404.97 5.04 o 2 4 3 436.57 429.85 5.17 o 4 4 3 321.96 294.40 4.37 o 6 4 3 4375.38 4301.81 15.66 o 8 4 3 3190.10 3242.94 13.62 o 10 4 3 329.17 297.51 4.40 o 12 4 3 0.46 1.78 1.62 o 14 4 3 458.10 452.12 5.29 o 16 4 3 660.00 687.78 6.43 o -17 5 3 259.07 262.41 4.16 o -15 5 3 579.92 620.50 6.13 o -13 5 3 201.39 223.47 3.89 o -11 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