#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/03/2200384.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200384_Fobs loop_ _publ_author_name 'Filippou, Alexander C.' 'Philippopoulos, Athanassios I.' 'Ziemer, Burkhard' _publ_section_title ; cis-Dicarbonylbis[1,2-ethanediylbis(diphenylphosphine)-P,P']tungsten(0) benzene sesquisolvate ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m338 _journal_page_last m340 _journal_volume 57 _journal_year 2001 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 89.154 _cell_angle_beta 87.729 _cell_angle_gamma 77.309 _cell_length_a 12.6751 _cell_length_b 18.2592 _cell_length_c 22.8639 _exptl_crystal_F_000 2340.00 _reflns_d_resolution_high 0.8255 _[local]_cod_data_source_file bt6052Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' PHILI19' _shelx_refln_list_code 4 _shelx_f_calc_maximum 391.67 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l 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o 3 1 0 40163.45 37876.75 1885.83 o 4 1 0 21390.10 21339.82 702.46 o 5 1 0 8138.43 7248.68 297.35 o 6 1 0 3751.50 3993.97 167.34 o 7 1 0 177.28 245.79 112.80 o 8 1 0 2592.31 2638.05 128.20 o 9 1 0 5828.50 5861.35 135.18 o 10 1 0 9844.30 10771.19 346.85 o 11 1 0 3705.54 3951.77 136.56 o 12 1 0 520.05 660.99 136.80 o 13 1 0 674.73 601.89 136.72 o 14 1 0 3097.00 2892.91 180.56 o 15 1 0 1432.29 1210.88 215.66 o -14 2 0 3101.09 3172.71 173.97 o -13 2 0 5529.80 5140.40 166.42 o -12 2 0 6689.96 6670.47 156.85 o -11 2 0 3297.58 3252.73 126.23 o -10 2 0 466.86 488.68 131.17 o -9 2 0 516.50 653.10 118.94 o -8 2 0 7803.45 7893.28 124.24 o -7 2 0 11860.02 11565.00 139.00 o -6 2 0 17111.57 16530.61 198.15 o -5 2 0 26913.66 26696.86 533.35 o -4 2 0 28937.93 29430.74 264.77 o -3 2 0 30.91 111.15 92.75 o -2 2 0 14420.86 13473.74 178.74 o -1 2 0 89256.85 82536.84 433.47 o 2 2 0 42299.75 37679.43 771.13 o 3 2 0 1957.46 1843.89 152.73 o 4 2 0 5866.40 5879.92 201.30 o 5 2 0 22461.57 21132.64 458.16 o 6 2 0 24423.08 24110.07 558.26 o 7 2 0 16626.31 15692.83 524.85 o 8 2 0 8039.10 7757.04 195.71 o 9 2 0 7403.43 6829.36 152.76 o 10 2 0 438.72 347.58 122.73 o 11 2 0 3774.99 3982.48 178.13 o 12 2 0 1845.16 1787.52 112.65 o 13 2 0 1784.61 1809.37 157.60 o 14 2 0 186.83 244.04 149.33 o 15 2 0 88.21 -34.61 134.03 o -14 3 0 1266.96 1107.52 143.99 o -13 3 0 1786.66 1748.07 153.78 o -12 3 0 256.08 50.20 127.54 o -11 3 0 52.58 90.59 133.09 o -10 3 0 4872.69 4986.75 147.34 o -9 3 0 9031.38 8997.01 186.08 o -8 3 0 5026.81 4945.14 110.93 o -7 3 0 8126.42 8720.45 126.54 o -6 3 0 203.09 182.43 84.22 o -5 3 0 19223.47 18522.21 196.17 o -4 3 0 18735.63 17347.25 183.12 o -3 3 0 2118.59 1754.33 89.85 o -2 3 0 3090.20 2998.97 109.77 o -1 3 0 52939.45 47454.79 906.16 o 0 3 0 6877.15 5362.69 170.68 o 1 3 0 2471.89 2238.11 144.89 o 2 3 0 35772.55 32617.65 729.25 o 3 3 0 1463.44 1734.64 127.17 o 4 3 0 607.99 636.75 129.68 o 5 3 0 13650.78 11426.80 914.44 o 6 3 0 3478.07 3243.77 155.97 o 7 3 0 6571.93 6969.85 156.35 o 8 3 0 39012.37 41042.84 1307.27 o 9 3 0 12895.33 13055.41 329.90 o 10 3 0 5901.89 6407.66 184.88 o 11 3 0 3628.54 3694.26 159.21 o 12 3 0 996.37 908.21 129.55 o 13 3 0 55.16 86.79 171.32 o 14 3 0 833.41 823.04 196.45 o 15 3 0 313.10 264.52 182.02 o -14 4 0 186.03 9.69 155.98 o -13 4 0 568.75 429.20 163.84 o -12 4 0 898.63 918.25 165.01 o -11 4 0 1645.94 1676.14 148.82 o -10 4 0 34.75 57.70 107.27 o -9 4 0 1132.97 1270.74 132.34 o -8 4 0 1496.16 1530.25 88.71 o -7 4 0 22569.90 21950.27 229.38 o -6 4 0 50094.05 50597.68 409.84 o -5 4 0 83980.59 88668.05 567.67 o -4 4 0 17617.44 17681.63 245.52 o -3 4 0 809.25 978.86 81.69 o -2 4 0 481.39 482.81 80.34 o -1 4 0 39369.69 37645.42 263.55 o 0 4 0 4034.99 3731.32 137.61 o 1 4 0 6568.93 5511.49 158.00 o 2 4 0 39513.53 36657.68 355.61 o 3 4 0 5872.30 5142.03 148.15 o 4 4 0 484.36 304.70 116.57 o 5 4 0 14584.57 13840.96 428.12 o 6 4 0 80451.37 80995.44 4782.72 o 7 4 0 93732.73 99578.60 510.00 o 8 4 0 35290.46 34344.78 1319.17 o 9 4 0 8564.33 8339.72 327.42 o 10 4 0 283.72 288.68 144.37 o 11 4 0 25.46 56.35 118.83 o 12 4 0 324.13 321.32 127.03 o 13 4 0 168.98 173.30 169.99 o 14 4 0 182.07 243.10 171.04 o 15 4 0 592.80 530.80 144.48 o -13 5 0 9.33 -184.22 148.29 o -12 5 0 29.33 -38.98 117.74 o -11 5 0 1419.03 1361.78 112.70 o -10 5 0 4528.13 4793.60 125.89 o -9 5 0 10160.99 10173.02 231.29 o -8 5 0 25671.36 26340.04 323.94 o -7 5 0 14695.68 15113.42 249.87 o -6 5 0 398.43 385.65 83.11 o -5 5 0 18072.56 18223.05 282.37 o -4 5 0 35123.15 34762.88 672.34 o -3 5 0 46569.03 46548.33 831.00 o -2 5 0 41986.03 41016.25 686.95 o -1 5 0 19548.21 18191.85 577.91 o 0 5 0 2466.06 2469.94 116.53 o 1 5 0 51.43 122.66 101.71 o 2 5 0 20368.09 19492.21 242.50 o 3 5 0 17636.94 16030.74 409.18 o 4 5 0 26492.62 23805.78 257.44 o 5 5 0 33352.77 30388.53 1483.57 o 6 5 0 23696.64 22245.71 254.92 o 7 5 0 6528.45 6790.68 518.21 o 8 5 0 3536.76 3446.51 169.63 o 9 5 0 29833.92 30947.22 1193.35 o 10 5 0 23406.63 25037.56 981.90 o 11 5 0 1975.28 2128.80 138.34 o 12 5 0 38.99 -3.47 112.52 o 13 5 0 659.60 487.19 149.66 o 14 5 0 120.14 139.75 172.44 o 15 5 0 14.60 93.83 151.74 o -13 6 0 372.17 407.64 153.07 o -12 6 0 334.93 190.50 136.81 o -11 6 0 474.57 496.32 126.49 o -10 6 0 55.76 -32.78 92.42 o -9 6 0 6.91 21.39 97.19 o -8 6 0 559.27 590.99 116.18 o -7 6 0 18824.86 18928.81 156.81 o -6 6 0 49063.37 49967.36 542.14 o -5 6 0 84215.30 87553.48 1569.15 o -4 6 0 38651.27 39333.94 1202.72 o -3 6 0 10230.06 10607.24 224.64 o -2 6 0 17205.71 17378.30 213.63 o -1 6 0 3916.06 3441.88 101.80 o 0 6 0 26359.02 25724.37 236.29 o 1 6 0 24481.44 23468.58 239.43 o 2 6 0 42498.89 41349.98 317.66 o 3 6 0 3375.54 3255.06 129.04 o 4 6 0 27227.83 26335.98 428.61 o 5 6 0 2012.26 1897.10 141.87 o 6 6 0 34139.75 33519.88 1008.46 o 7 6 0 55325.74 55138.23 365.43 o 8 6 0 19994.66 18982.89 958.12 o 9 6 0 3177.53 2885.92 140.50 o 10 6 0 70.16 -56.80 117.65 o 11 6 0 453.73 460.13 116.54 o 12 6 0 2568.37 2595.37 128.34 o 13 6 0 1731.69 1630.35 156.05 o 14 6 0 215.54 157.39 171.64 o 15 6 0 1768.79 2099.46 193.28 o -13 7 0 24.35 -22.82 136.25 o -12 7 0 243.11 426.91 129.82 o -11 7 0 893.93 699.61 116.06 o -10 7 0 3976.96 3869.31 128.06 o -9 7 0 7075.20 7229.40 134.61 o -8 7 0 22662.67 22866.45 161.67 o -7 7 0 7523.78 7799.36 157.99 o -6 7 0 392.79 491.76 79.71 o -5 7 0 478.27 307.91 84.74 o -4 7 0 16348.08 16286.84 360.08 o -3 7 0 84531.22 87917.77 877.00 o -2 7 0 18061.19 16386.33 192.96 o -1 7 0 12167.48 11457.86 153.49 o 0 7 0 28808.85 27725.73 378.54 o 1 7 0 331.70 334.96 88.91 o 2 7 0 24355.30 22635.97 230.75 o 3 7 0 20128.19 18221.12 202.54 o 4 7 0 10920.09 9200.35 177.05 o 5 7 0 46846.03 44248.57 312.28 o 6 7 0 41184.36 41760.14 307.58 o 7 7 0 2573.46 2474.76 148.62 o 8 7 0 350.97 305.55 107.25 o 9 7 0 2581.94 2456.43 125.04 o 10 7 0 12192.58 12267.23 289.05 o 11 7 0 9110.70 9478.09 410.76 o 12 7 0 1014.41 461.32 1144.05 o 13 7 0 9.50 -373.74 307.59 o 14 7 0 328.20 -433.96 525.02 o 15 7 0 1445.29 1272.75 172.73 o -12 8 0 1698.81 1498.62 131.45 o -11 8 0 1653.75 1525.77 114.33 o -10 8 0 627.72 430.55 107.77 o -9 8 0 334.07 313.14 105.63 o -8 8 0 21.41 62.19 97.28 o -7 8 0 787.68 728.74 102.86 o -6 8 0 8068.80 8078.58 192.32 o -5 8 0 16643.58 16795.93 257.10 o -4 8 0 19318.34 18828.18 455.04 o -3 8 0 9845.36 9960.10 171.10 o -2 8 0 4.11 30.79 95.93 o -1 8 0 15039.95 14641.57 207.90 o 0 8 0 37538.56 37526.34 625.81 o 1 8 0 79010.98 80788.71 868.76 o 2 8 0 63309.62 64214.33 655.15 o 3 8 0 20655.44 20354.33 290.13 o 4 8 0 4272.85 4210.96 129.54 o 5 8 0 2207.31 2151.52 162.79 o 6 8 0 11184.38 10867.70 188.05 o 7 8 0 18409.79 18354.39 463.14 o 8 8 0 8456.79 7986.26 238.98 o 9 8 0 1732.54 1683.67 123.54 o 10 8 0 502.22 462.90 135.67 o 11 8 0 1155.32 1184.17 143.95 o 12 8 0 1932.72 1933.65 180.00 o 13 8 0 3984.20 4191.85 150.63 o 14 8 0 4673.80 4814.48 176.10 o 15 8 0 1406.84 1280.82 190.57 o -12 9 0 1077.27 785.88 141.95 o -11 9 0 688.92 968.02 149.30 o -10 9 0 2406.05 2100.84 134.46 o -9 9 0 5956.47 5909.54 203.30 o 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o -4 10 0 9738.01 10144.86 125.78 o -3 10 0 5696.93 5572.60 169.49 o -2 10 0 6521.16 6722.48 142.60 o -1 10 0 1167.87 815.74 94.44 o 0 10 0 41826.52 40182.60 1630.09 o 1 10 0 76143.52 77077.11 399.15 o 2 10 0 69732.73 71360.59 405.38 o 3 10 0 24498.93 23752.16 612.33 o 4 10 0 513.63 648.78 100.98 o 5 10 0 7587.33 7685.34 161.06 o 6 10 0 13304.22 12758.79 175.41 o 7 10 0 16820.82 15028.11 1069.55 o 8 10 0 6776.89 7113.50 196.16 o 9 10 0 9212.56 9768.08 212.74 o 10 10 0 2153.55 2210.00 161.55 o 11 10 0 0.90 -29.55 155.79 o 12 10 0 312.99 223.57 157.48 o 13 10 0 2743.66 2835.99 143.39 o 14 10 0 4995.19 5234.20 195.03 o -11 11 0 617.89 478.41 152.64 o -10 11 0 3948.83 3666.61 202.90 o -9 11 0 7780.68 8032.30 161.36 o -8 11 0 7685.25 7997.90 194.11 o -7 11 0 12945.30 12659.29 151.11 o -6 11 0 7578.75 7816.75 134.45 o -5 11 0 7.30 60.00 117.36 o -4 11 0 7469.70 7543.98 136.87 o -3 11 0 7227.26 7070.60 121.07 o -2 11 0 31597.96 31149.50 377.96 o -1 11 0 69521.22 72529.01 512.63 o 0 11 0 51524.60 53187.91 584.92 o 1 11 0 7951.88 7733.63 158.92 o 2 11 0 3257.43 3128.99 148.60 o 3 11 0 30001.69 29206.41 253.81 o 4 11 0 69287.59 71008.21 444.61 o 5 11 0 35189.75 34503.43 240.47 o 6 11 0 15104.32 14812.56 194.40 o 7 11 0 2149.05 2117.19 132.02 o 8 11 0 5.86 36.36 123.65 o 9 11 0 86.50 97.37 125.93 o 10 11 0 3455.12 3551.20 145.92 o 11 11 0 7727.69 7432.68 224.75 o 12 11 0 10067.20 10291.17 212.93 o 13 11 0 4402.55 4345.13 226.76 o 14 11 0 1254.86 1339.82 173.88 o -10 12 0 4387.07 4056.68 387.43 o -9 12 0 1557.49 1497.02 134.05 o -8 12 0 0.70 -87.79 122.10 o -7 12 0 588.16 601.71 137.56 o -6 12 0 12566.24 12635.09 147.44 o -5 12 0 23571.18 24195.14 259.47 o -4 12 0 13342.40 13259.62 213.06 o -3 12 0 5284.32 5571.24 148.96 o -2 12 0 6707.95 6969.53 111.01 o -1 12 0 255.72 190.18 82.29 o 0 12 0 6867.60 6828.68 115.91 o 1 12 0 26274.00 26390.32 400.06 o 2 12 0 34044.72 33306.62 501.06 o 3 12 0 7124.91 7108.98 152.87 o 4 12 0 728.76 740.01 89.52 o 5 12 0 3676.99 3418.44 120.18 o 6 12 0 16691.05 16860.75 199.22 o 7 12 0 20504.76 21065.72 235.69 o 8 12 0 23119.86 22713.45 219.92 o 9 12 0 15086.69 15154.40 465.89 o 10 12 0 2234.33 2244.15 160.46 o 11 12 0 1757.04 1842.25 189.85 o 12 12 0 522.04 407.21 148.61 o 13 12 0 2298.19 2214.94 227.03 o 14 12 0 1184.59 1179.68 183.86 o -10 13 0 3324.74 2805.24 172.29 o -9 13 0 8278.95 7864.67 256.86 o -8 13 0 10686.09 10422.70 306.04 o -7 13 0 6265.16 6575.18 139.58 o -6 13 0 10521.99 10967.37 168.38 o -5 13 0 1481.79 1502.51 107.51 o -4 13 0 1536.80 1663.80 106.11 o -3 13 0 16857.13 16979.39 296.37 o -2 13 0 26776.30 27571.06 584.38 o -1 13 0 38601.27 39543.42 518.00 o 0 13 0 22381.00 22962.22 167.35 o 1 13 0 5704.06 5646.46 129.38 o 2 13 0 12.70 14.11 81.80 o 3 13 0 6246.67 6060.33 132.03 o 4 13 0 14110.24 13989.18 215.69 o 5 13 0 28293.49 28647.51 576.55 o 6 13 0 25073.83 26317.65 244.57 o 7 13 0 11531.91 11370.77 218.84 o 8 13 0 3677.34 3687.03 168.11 o 9 13 0 1801.28 1867.62 117.43 o 10 13 0 8285.45 8467.88 216.31 o 11 13 0 6012.75 5763.31 252.18 o 12 13 0 4408.39 4371.25 170.97 o 13 13 0 1372.81 1428.91 217.83 o 14 13 0 385.18 476.88 226.37 o -9 14 0 240.59 239.16 145.32 o -8 14 0 92.19 120.90 151.68 o -7 14 0 623.21 646.23 133.21 o -6 14 0 9489.52 9871.62 215.77 o -5 14 0 21518.36 22268.14 190.01 o -4 14 0 10238.00 10567.60 277.24 o -3 14 0 11798.65 11899.76 238.96 o -2 14 0 1975.19 1966.57 133.96 o -1 14 0 137.18 184.44 108.96 o 0 14 0 1870.01 1910.54 103.00 o 1 14 0 12555.01 13054.14 172.26 o 2 14 0 12865.83 13524.66 227.64 o 3 14 0 6870.58 7041.95 289.67 o 4 14 0 1226.16 1284.74 108.64 o 5 14 0 977.81 988.41 147.67 o 6 14 0 2437.68 2547.90 131.57 o 7 14 0 15714.83 16881.83 216.99 o 8 14 0 15724.99 16062.00 200.37 o 9 14 0 12016.32 12653.76 203.73 o 10 14 0 3268.99 3207.17 144.26 o 11 14 0 13.94 -25.34 146.12 o 12 14 0 3518.61 3835.08 225.34 o 13 14 0 4210.29 3934.33 189.24 o -8 15 0 5784.83 5156.54 153.30 o -7 15 0 9553.13 9746.01 201.53 o -6 15 0 6675.59 6695.23 139.62 o -5 15 0 1329.56 1339.95 122.09 o -4 15 0 1302.11 1476.16 110.26 o -3 15 0 8307.15 8230.17 156.98 o -2 15 0 16125.18 16905.00 150.70 o -1 15 0 28543.32 29696.78 570.05 o 0 15 0 16131.32 16912.43 186.00 o 1 15 0 6666.04 6961.59 129.45 o 2 15 0 282.00 210.81 117.13 o 3 15 0 807.25 1004.83 120.44 o 4 15 0 4340.47 4707.54 185.76 o 5 15 0 12473.73 12716.89 162.68 o 6 15 0 34357.75 34881.54 619.71 o 7 15 0 18277.66 18092.28 226.77 o 8 15 0 3255.37 3323.23 160.14 o 9 15 0 563.59 644.62 145.93 o 10 15 0 6460.59 6935.80 204.55 o 11 15 0 5827.90 5749.74 174.86 o 12 15 0 2818.67 2847.42 182.16 o 13 15 0 625.87 600.24 163.12 o -7 16 0 164.86 89.73 132.07 o -6 16 0 2795.25 2708.10 142.09 o -5 16 0 5928.26 6081.75 134.11 o -4 16 0 12676.68 12904.42 179.79 o -3 16 0 7472.20 8397.39 138.07 o -2 16 0 583.92 709.88 105.22 o -1 16 0 800.09 813.38 104.43 o 0 16 0 1789.25 1882.15 90.84 o 1 16 0 9649.69 10071.52 135.35 o 2 16 0 23424.50 24647.05 209.60 o 3 16 0 27944.36 27981.68 310.90 o 4 16 0 11231.40 11668.77 186.59 o 5 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