#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:52:14 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180924 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/04/2200436.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200436_Fobs loop_ _publ_author_name 'Srinivasan, N.' 'Sridhar, B.' 'Rajaram, R. K.' _publ_section_title ; Bis(D-phenylglycinium) sulfate monohydrate ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o754 _journal_page_last o756 _journal_volume 57 _journal_year 2001 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 111.369 _cell_angle_gamma 90.000 _cell_length_a 12.3201 _cell_length_b 5.9377 _cell_length_c 14.2908 _exptl_crystal_F_000 440.00 _reflns_d_resolution_high 0.8407 _cod_data_source_file ci6028Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' D-PHENYL GLYCINE SULPHATE' _shelx_refln_list_code 4 _shelx_f_calc_maximum 93.25 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4008.08 3699.84 23.07 o 3 0 0 1098.79 1168.17 16.21 o 4 0 0 1.04 1.48 0.46 o 5 0 0 534.36 583.74 3.54 o 6 0 0 285.38 301.47 2.84 o 7 0 0 33.44 37.31 1.11 o 8 0 0 321.45 343.88 3.68 o 9 0 0 11.79 8.72 0.69 o 10 0 0 43.01 44.07 1.37 o 11 0 0 87.31 90.42 2.46 o 12 0 0 8.92 9.34 0.84 o 13 0 0 1.66 1.74 1.18 o 1 1 0 230.51 192.77 1.32 o 2 1 0 1414.51 1390.59 17.04 o 3 1 0 598.95 606.88 2.97 o 4 1 0 944.23 909.95 4.16 o 5 1 0 1202.56 1251.82 5.19 o 6 1 0 372.96 416.24 3.34 o 7 1 0 26.05 24.96 0.69 o 8 1 0 675.69 711.95 5.29 o 9 1 0 232.68 234.83 3.30 o 10 1 0 188.29 195.54 3.26 o 11 1 0 128.05 126.38 2.91 o 12 1 0 88.12 93.06 2.33 o 13 1 0 25.36 24.32 1.06 o 0 2 0 2113.76 1984.67 24.20 o 1 2 0 161.49 130.19 1.57 o 2 2 0 325.36 292.11 2.36 o 3 2 0 644.70 753.01 4.02 o 4 2 0 277.06 322.79 2.79 o 5 2 0 121.04 119.40 1.88 o 6 2 0 258.10 280.01 3.03 o 7 2 0 137.25 147.76 2.41 o 8 2 0 612.95 619.90 5.15 o 9 2 0 129.01 128.13 2.63 o 10 2 0 62.76 59.34 1.86 o 11 2 0 137.08 141.03 3.07 o 12 2 0 17.80 19.75 0.92 o 13 2 0 17.47 20.96 1.11 o 1 3 0 235.90 203.08 2.33 o 2 3 0 265.27 258.10 2.77 o 3 3 0 169.98 191.94 2.39 o 4 3 0 197.73 222.32 2.70 o 5 3 0 211.04 253.14 3.02 o 6 3 0 22.66 25.52 0.83 o 7 3 0 130.90 123.78 2.49 o 8 3 0 122.44 131.67 2.67 o 9 3 0 39.59 40.21 1.15 o 10 3 0 63.31 71.16 2.11 o 11 3 0 33.55 33.91 1.10 o 12 3 0 54.94 59.20 1.79 o 0 4 0 153.11 154.33 2.46 o 1 4 0 215.77 233.24 3.03 o 2 4 0 55.80 53.95 1.39 o 3 4 0 116.13 122.15 2.38 o 4 4 0 13.61 21.83 0.72 o 5 4 0 84.06 94.15 2.26 o 6 4 0 52.48 62.02 1.70 o 7 4 0 127.08 133.36 2.79 o 8 4 0 171.32 181.34 3.37 o 9 4 0 103.57 100.44 2.76 o 10 4 0 27.84 25.65 1.01 o 11 4 0 69.15 82.10 2.50 o 1 5 0 82.94 78.93 2.14 o 2 5 0 69.39 71.60 1.90 o 3 5 0 75.87 60.60 1.81 o 4 5 0 57.64 56.58 1.75 o 5 5 0 58.03 68.28 1.92 o 6 5 0 17.97 21.63 0.92 o 7 5 0 195.71 234.83 3.96 o 8 5 0 47.98 53.38 1.64 o 9 5 0 8.05 15.76 0.96 o 0 6 0 273.08 271.28 4.26 o 1 6 0 11.62 13.61 0.86 o 2 6 0 49.40 47.27 1.42 o 3 6 0 166.71 158.86 3.37 o 4 6 0 33.61 32.18 1.12 o 5 6 0 58.04 61.55 1.76 o 6 6 0 62.82 65.60 1.95 o 7 6 0 1.21 2.96 1.35 o 1 7 0 46.60 50.40 1.53 o -13 0 1 3.11 5.04 0.75 o -12 0 1 54.70 53.26 1.51 o -11 0 1 0.11 -0.63 0.85 o -10 0 1 0.04 0.30 0.66 o -9 0 1 277.71 274.84 3.43 o -8 0 1 6.35 8.02 0.54 o -7 0 1 1129.98 1193.05 5.96 o -6 0 1 704.29 748.05 4.24 o -5 0 1 738.99 836.59 3.99 o -4 0 1 1460.52 1492.38 20.65 o -3 0 1 28.71 21.47 0.64 o -2 0 1 375.40 335.93 1.58 o 1 0 1 138.22 180.99 1.04 o 2 0 1 2353.29 2509.31 21.59 o 3 0 1 5230.30 5277.43 36.95 o 4 0 1 4.95 7.12 0.35 o 5 0 1 665.50 719.33 3.93 o 6 0 1 63.05 76.04 1.58 o 7 0 1 53.26 54.97 1.53 o 8 0 1 16.63 15.56 0.65 o 9 0 1 239.72 231.80 3.28 o 10 0 1 340.91 327.61 4.21 o 11 0 1 129.58 129.99 3.05 o 12 0 1 27.72 29.78 0.99 o 13 0 1 5.25 4.23 1.40 o -13 1 1 98.46 99.41 2.92 o -12 1 1 35.35 32.57 1.08 o -11 1 1 775.77 798.63 6.58 o -10 1 1 147.58 156.48 2.91 o -9 1 1 205.86 201.73 3.06 o -8 1 1 41.64 44.64 1.38 o -7 1 1 185.09 180.18 2.43 o -6 1 1 315.36 344.04 3.04 o -5 1 1 143.88 172.06 2.03 o -4 1 1 183.75 182.73 1.87 o -3 1 1 7504.33 6508.00 40.34 o -2 1 1 348.28 384.00 2.03 o -1 1 1 672.43 568.43 2.26 o 0 1 1 3087.48 2800.93 108.39 o 1 1 1 3881.25 4133.47 28.27 o 2 1 1 984.08 1085.41 16.19 o 3 1 1 149.92 171.04 1.69 o 4 1 1 1759.97 1874.48 26.13 o 5 1 1 171.91 194.69 2.29 o 6 1 1 22.60 24.40 0.72 o 7 1 1 1076.74 1162.87 6.17 o 8 1 1 276.51 281.46 3.47 o 9 1 1 136.76 135.86 2.71 o 10 1 1 0.64 2.37 1.03 o 11 1 1 198.31 209.77 3.62 o 12 1 1 115.50 121.11 3.13 o 13 1 1 15.54 16.11 0.97 o -13 2 1 28.61 36.37 1.14 o -12 2 1 16.81 16.95 0.89 o -11 2 1 14.31 17.74 0.87 o -10 2 1 202.28 213.41 3.40 o -9 2 1 400.95 410.10 4.36 o -8 2 1 158.63 160.61 2.62 o -7 2 1 255.90 268.03 3.10 o -6 2 1 20.82 24.27 0.72 o -5 2 1 23.04 31.84 0.92 o -4 2 1 279.29 350.63 2.91 o -3 2 1 485.64 533.03 3.18 o -2 2 1 160.43 195.78 1.93 o -1 2 1 1334.67 1321.08 20.68 o 0 2 1 125.99 117.78 5.89 o 1 2 1 1877.57 1875.60 24.27 o 2 2 1 14.19 20.60 0.59 o 3 2 1 801.09 832.11 4.23 o 4 2 1 788.77 782.87 4.34 o 5 2 1 161.21 142.57 2.16 o 6 2 1 21.60 20.92 0.63 o 7 2 1 116.48 118.75 2.35 o 8 2 1 88.25 83.43 2.05 o 9 2 1 238.57 262.27 3.77 o 10 2 1 37.28 41.42 1.33 o 11 2 1 52.03 53.95 1.58 o 12 2 1 27.82 33.81 1.15 o -12 3 1 42.64 49.31 1.45 o -11 3 1 94.81 100.01 2.84 o -10 3 1 8.41 8.59 0.76 o -9 3 1 94.06 106.05 2.58 o -8 3 1 244.98 268.73 3.68 o -7 3 1 15.74 15.69 0.72 o -6 3 1 127.24 136.66 2.42 o -5 3 1 193.78 211.40 2.76 o -4 3 1 49.22 59.07 1.52 o -3 3 1 523.99 537.61 4.00 o -2 3 1 2904.11 2832.18 37.62 o -1 3 1 510.14 497.03 3.65 o 0 3 1 44.22 32.66 1.60 o 1 3 1 462.01 472.36 3.56 o 2 3 1 126.45 99.75 1.81 o 3 3 1 105.99 121.30 1.99 o 4 3 1 224.76 274.84 3.00 o 5 3 1 42.87 43.67 1.31 o 6 3 1 57.73 40.64 1.21 o 7 3 1 136.72 125.99 2.52 o 8 3 1 49.45 45.57 1.40 o 9 3 1 123.56 133.26 2.89 o 10 3 1 34.88 41.97 1.34 o 11 3 1 163.76 185.66 3.64 o -11 4 1 19.28 22.48 1.06 o -10 4 1 116.02 138.79 3.25 o -9 4 1 31.09 32.87 1.04 o -8 4 1 124.29 120.63 2.84 o -7 4 1 96.21 100.70 2.42 o -6 4 1 8.82 8.52 0.68 o -5 4 1 162.01 191.94 2.99 o -4 4 1 178.53 176.27 2.75 o -3 4 1 140.77 122.92 2.29 o -2 4 1 79.17 73.14 1.84 o -1 4 1 226.04 200.14 2.81 o 0 4 1 125.00 121.58 4.80 o 1 4 1 133.19 143.60 2.38 o 2 4 1 265.06 283.78 3.34 o 3 4 1 61.93 61.48 1.76 o 4 4 1 428.81 485.57 4.56 o 5 4 1 138.82 158.21 2.93 o 6 4 1 124.61 126.96 2.72 o 7 4 1 162.53 150.71 3.07 o 8 4 1 22.73 17.52 0.87 o 9 4 1 13.43 11.68 0.85 o 10 4 1 65.05 75.44 2.32 o -9 5 1 36.01 35.44 1.13 o -8 5 1 63.71 71.16 1.96 o -7 5 1 18.40 18.92 0.94 o -6 5 1 198.68 224.12 3.74 o -5 5 1 5.73 3.61 1.23 o -4 5 1 1.43 2.70 0.62 o -3 5 1 111.60 123.30 2.68 o -2 5 1 180.43 187.31 3.19 o -1 5 1 56.40 62.16 1.77 o 0 5 1 335.09 332.49 11.40 o 1 5 1 93.62 93.40 2.42 o 2 5 1 224.13 202.71 3.31 o 3 5 1 141.47 127.16 2.82 o 4 5 1 1.24 1.54 1.11 o 5 5 1 41.28 42.70 1.30 o 6 5 1 148.09 151.98 3.29 o 7 5 1 56.18 52.38 1.62 o 8 5 1 65.21 65.12 1.95 o 9 5 1 30.95 26.76 1.07 o -7 6 1 73.50 83.75 2.53 o -6 6 1 28.76 37.68 1.17 o -5 6 1 25.21 23.52 1.05 o -4 6 1 89.16 96.25 2.45 o -3 6 1 33.00 32.47 1.08 o -2 6 1 4.56 5.36 0.74 o -1 6 1 89.75 84.54 2.22 o 0 6 1 102.87 91.27 2.76 o 1 6 1 11.17 9.21 0.81 o 2 6 1 23.32 20.84 0.94 o 3 6 1 34.57 31.26 1.06 o 4 6 1 75.45 80.47 2.32 o 5 6 1 39.93 44.12 1.32 o 6 6 1 19.72 24.49 1.11 o -1 7 1 9.51 12.37 0.94 o 0 7 1 38.88 43.57 0.97 o 1 7 1 5.80 7.45 0.85 o -14 0 2 177.46 188.37 4.02 o -13 0 2 11.29 11.83 0.86 o -12 0 2 51.89 58.48 1.71 o -11 0 2 32.38 31.50 0.92 o -10 0 2 181.02 177.87 2.99 o -9 0 2 322.84 299.83 3.43 o -8 0 2 5.15 4.61 0.46 o -7 0 2 708.29 801.07 4.88 o -6 0 2 1213.40 1306.70 5.61 o -5 0 2 87.09 68.28 1.21 o -4 0 2 4.87 6.29 0.30 o -3 0 2 46.80 40.64 0.77 o -2 0 2 2602.59 2138.08 18.34 o -1 0 2 149.64 141.95 1.03 o 0 0 2 385.83 303.50 1.06 o 1 0 2 1223.84 1370.73 15.64 o 2 0 2 3055.17 3287.77 27.68 o 3 0 2 137.55 130.48 1.58 o 4 0 2 63.45 63.73 1.24 o 5 0 2 399.34 405.06 3.30 o 6 0 2 58.51 56.97 1.43 o 7 0 2 62.67 64.01 1.66 o 8 0 2 733.80 794.49 5.83 o 9 0 2 321.61 293.74 3.84 o 10 0 2 1.08 3.34 1.14 o 11 0 2 2.40 4.18 1.23 o 12 0 2 0.03 -0.49 0.87 o -14 1 2 34.51 36.63 1.20 o -13 1 2 13.88 17.19 0.89 o -12 1 2 89.01 91.41 2.31 o -11 1 2 55.79 56.19 1.61 o -10 1 2 212.15 205.18 3.21 o -9 1 2 199.45 199.66 2.92 o -8 1 2 82.61 92.15 1.99 o -7 1 2 905.21 949.64 5.31 o -6 1 2 188.99 207.16 2.36 o -5 1 2 125.21 128.82 1.66 o -4 1 2 1561.33 1449.72 21.34 o -3 1 2 225.94 222.57 1.80 o -2 1 2 122.67 138.48 1.32 o -1 1 2 6040.43 5269.29 31.92 o 0 1 2 5430.42 5098.58 199.64 o 1 1 2 4872.90 5218.10 34.87 o 2 1 2 6985.33 7370.82 45.89 o 3 1 2 1241.29 1315.76 5.00 o 4 1 2 74.92 60.00 1.34 o 5 1 2 215.72 234.83 2.51 o 6 1 2 10.55 9.90 0.51 o 7 1 2 204.39 218.09 2.93 o 8 1 2 24.24 27.12 0.81 o 9 1 2 33.54 29.55 0.89 o 10 1 2 111.18 117.72 2.71 o 11 1 2 39.71 35.69 1.08 o 12 1 2 9.50 9.05 0.86 o -13 2 2 31.89 34.98 1.12 o -12 2 2 12.30 11.77 0.83 o -11 2 2 79.12 86.13 2.48 o -10 2 2 299.76 302.97 4.05 o -9 2 2 8.78 11.25 0.67 o -8 2 2 157.68 167.12 2.68 o -7 2 2 13.84 16.56 0.60 o -6 2 2 162.33 159.63 2.29 o -5 2 2 69.03 78.77 1.53 o -4 2 2 521.04 542.02 3.61 o -3 2 2 477.86 479.51 3.21 o -2 2 2 716.34 637.41 3.48 o -1 2 2 442.72 347.89 2.57 o 0 2 2 1559.92 1507.15 41.99 o 1 2 2 445.81 454.36 2.94 o 2 2 2 349.73 402.98 2.94 o 3 2 2 267.58 294.33 2.66 o 4 2 2 2186.84 2061.84 32.10 o 5 2 2 23.39 13.36 0.57 o 6 2 2 76.47 69.64 1.73 o 7 2 2 137.56 112.17 2.28 o 8 2 2 158.92 129.21 2.65 o 9 2 2 326.84 342.29 4.31 o 10 2 2 95.54 104.72 2.65 o 11 2 2 145.51 164.23 3.54 o 12 2 2 3.12 2.01 1.35 o -12 3 2 69.34 71.67 2.19 o -11 3 2 0.72 1.43 1.10 o -10 3 2 41.32 43.90 1.26 o -9 3 2 220.04 247.68 3.66 o -8 3 2 150.99 146.72 2.71 o -7 3 2 124.98 128.33 2.44 o -6 3 2 289.34 329.64 3.44 o -5 3 2 139.24 155.51 2.37 o -4 3 2 37.45 45.28 1.22 o -3 3 2 81.62 64.84 1.53 o -2 3 2 548.35 550.28 4.05 o -1 3 2 592.72 678.54 4.27 o 0 3 2 274.10 291.86 17.30 o 1 3 2 402.68 395.23 3.26 o 2 3 2 36.31 31.26 0.87 o 3 3 2 16.53 12.49 0.55 o 4 3 2 109.59 80.23 1.85 o 5 3 2 77.04 59.87 1.73 o 6 3 2 13.36 8.02 0.64 o 8 3 2 87.33 54.40 1.65 o 9 3 2 138.72 152.09 3.19 o 10 3 2 86.97 108.28 2.96 o 11 3 2 12.92 13.11 0.94 o -11 4 2 14.49 14.26 0.94 o -10 4 2 15.96 15.35 0.88 o -9 4 2 118.23 133.56 2.99 o -8 4 2 106.46 118.18 2.72 o -7 4 2 0.78 1.23 0.99 o -6 4 2 124.30 133.36 2.69 o -5 4 2 290.65 294.33 3.70 o -4 4 2 175.29 158.21 2.71 o -3 4 2 30.74 29.87 0.85 o -2 4 2 57.73 51.39 1.42 o -1 4 2 61.53 58.80 1.65 o 0 4 2 372.06 381.97 22.71 o 1 4 2 279.74 318.01 3.54 o 2 4 2 223.83 223.60 2.97 o 3 4 2 139.96 122.25 2.57 o 4 4 2 444.88 357.28 4.07 o 7 4 2 101.51 68.00 1.99 o 8 4 2 23.23 20.06 0.93 o 9 4 2 29.16 17.56 0.94 o 10 4 2 48.84 48.94 1.57 o -10 5 2 20.97 20.02 1.04 o -9 5 2 8.87 10.90 0.85 o -8 5 2 23.57 28.75 1.06 o -7 5 2 195.96 196.87 3.63 o -6 5 2 16.31 17.66 0.87 o -5 5 2 55.16 57.75 1.77 o -4 5 2 102.88 108.55 2.61 o -3 5 2 13.38 10.93 0.74 o -2 5 2 32.40 34.52 1.11 o -1 5 2 319.50 299.23 3.88 o 0 5 2 36.35 35.83 1.45 o 1 5 2 719.73 780.46 6.02 o 2 5 2 215.30 257.82 3.74 o 3 5 2 63.63 62.36 1.84 o 4 5 2 113.70 84.22 2.21 o 5 5 2 37.32 29.83 0.99 o 6 5 2 1.89 1.46 1.20 o 7 5 2 86.04 62.23 1.70 o 8 5 2 32.68 23.27 1.04 o -7 6 2 26.48 25.83 1.09 o -6 6 2 28.44 32.33 1.13 o -5 6 2 18.24 24.23 1.02 o -4 6 2 6.84 6.56 0.82 o -3 6 2 29.20 31.31 1.06 o -2 6 2 6.57 9.85 0.81 o -1 6 2 2.99 3.58 1.35 o 0 6 2 17.37 20.04 0.65 o 1 6 2 61.65 61.82 1.76 o 2 6 2 29.27 29.41 1.03 o 3 6 2 27.86 25.18 0.99 o 4 6 2 8.28 7.92 0.85 o 5 6 2 43.69 38.37 1.17 o 6 6 2 11.65 10.12 0.93 o -1 7 2 26.36 20.41 1.01 o 0 7 2 10.13 10.20 0.88 o -14 0 3 27.05 31.26 1.11 o -13 0 3 0.44 1.19 1.04 o -12 0 3 320.10 324.81 4.51 o -11 0 3 0.04 -1.19 1.19 o -10 0 3 764.92 738.88 5.62 o -9 0 3 55.49 54.97 1.47 o -8 0 3 9.19 6.10 0.47 o -7 0 3 196.74 202.10 2.45 o -6 0 3 476.03 530.84 3.57 o -5 0 3 204.61 208.77 2.12 o -4 0 3 531.52 484.43 2.85 o -3 0 3 7894.44 5715.81 36.50 o -2 0 3 1549.62 1313.57 15.94 o -1 0 3 2516.50 2373.02 20.58 o 0 0 3 97.12 83.29 2.28 o 1 0 3 7393.03 7197.91 41.69 o 2 0 3 296.17 243.36 2.02 o 3 0 3 2307.34 2753.81 31.67 o 4 0 3 547.73 481.02 3.40 o 5 0 3 130.02 167.45 2.23 o 6 0 3 104.34 116.97 2.05 o 7 0 3 0.14 0.00 0.02 o 8 0 3 237.57 255.48 3.44 o 9 0 3 0.27 0.14 0.57 o 10 0 3 563.89 549.88 5.66 o 11 0 3 35.04 29.26 1.03 o 12 0 3 35.79 37.84 1.22 o -14 1 3 7.91 10.17 0.88 o -13 1 3 16.55 16.11 0.90 o -12 1 3 14.60 15.97 0.83 o -11 1 3 148.92 149.65 2.95 o -10 1 3 43.03 38.26 1.07 o -9 1 3 5.30 5.76 0.58 o -8 1 3 1032.94 1090.82 6.26 o -7 1 3 334.25 341.01 3.18 o -6 1 3 564.52 616.68 3.85 o -5 1 3 23.17 36.21 1.04 o -4 1 3 976.87 909.43 3.90 o -3 1 3 799.30 774.21 3.36 o -2 1 3 7076.85 5700.17 37.75 o -1 1 3 433.08 372.09 2.16 o 0 1 3 1044.09 1014.41 70.21 o 1 1 3 1217.54 1425.53 20.18 o 2 1 3 2042.53 2380.17 28.18 o 3 1 3 1081.26 1325.16 5.33 o 4 1 3 147.11 171.94 2.15 o 5 1 3 1382.61 1492.71 6.66 o 6 1 3 397.47 395.57 3.77 o 7 1 3 61.19 66.02 1.89 o 8 1 3 111.95 116.78 2.52 o 9 1 3 65.72 54.84 1.60 o 10 1 3 147.90 146.19 3.23 o 11 1 3 20.04 23.73 0.97 o 12 1 3 21.72 26.14 1.01 o -13 2 3 35.50 38.69 1.18 o -12 2 3 132.98 154.44 3.32 o -11 2 3 54.53 62.43 1.70 o -10 2 3 150.92 156.16 3.02 o -9 2 3 217.21 214.29 3.16 o -8 2 3 46.35 51.32 1.42 o -7 2 3 198.38 205.05 2.72 o -6 2 3 47.33 50.77 1.41 o -5 2 3 298.31 306.88 2.87 o -4 2 3 494.00 440.32 3.26 o -3 2 3 581.26 576.06 3.52 o -2 2 3 591.18 572.34 3.51 o -1 2 3 2061.86 1972.40 26.80 o 0 2 3 2647.22 2829.51 109.98 o 1 2 3 804.19 960.03 4.54 o 2 2 3 233.28 240.27 2.41 o 3 2 3 16.23 17.99 0.55 o 4 2 3 501.08 496.65 3.84 o 5 2 3 114.11 90.34 1.88 o 7 2 3 141.40 115.85 2.41 o 8 2 3 64.75 48.40 1.50 o 9 2 3 44.23 46.97 1.42 o 10 2 3 204.93 206.91 3.72 o 11 2 3 28.67 29.92 1.09 o -13 3 3 46.61 51.45 1.55 o -12 3 3 22.39 23.94 1.01 o -11 3 3 76.39 89.93 2.53 o -10 3 3 104.16 120.16 2.84 o -9 3 3 496.10 494.15 4.98 o -8 3 3 103.43 102.00 2.35 o 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