#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/04/2200446.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200446_Fobs loop_ _publ_author_name 'Skakle, J. M. S.' 'Foreman, M. R. St J.' 'Plater, M. J.' _publ_section_title ; catena-Poly[[[(1,10-phenanthroline)manganese(II)]-\m-(1-hydroxybenzene-3,5-dicarboxylato)] hydrate] ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m373 _journal_page_last m375 _journal_volume 57 _journal_year 2001 _space_group_IT_number 13 _symmetry_space_group_name_Hall '-P 2yac' _symmetry_space_group_name_H-M 'P 1 2/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.860 _cell_angle_gamma 90.000 _cell_length_a 8.6089 _cell_length_b 12.2249 _cell_length_c 17.3057 _exptl_crystal_F_000 884.00 _reflns_d_resolution_high 0.7103 _[local]_cod_data_source_file ci6041Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' js035' _shelx_refln_list_code 4 _shelx_f_calc_maximum 316.81 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 20416.54 20876.36 141.46 o 4 0 0 4308.05 4500.51 112.52 o 6 0 0 500.73 496.71 26.28 o 8 0 0 2079.56 2144.26 81.19 o 10 0 0 23.05 37.72 36.32 o 1 1 0 1664.88 1681.04 24.92 o 2 1 0 483.55 500.36 16.92 o 3 1 0 1614.01 1635.99 25.12 o 4 1 0 699.81 729.60 20.86 o 5 1 0 2667.22 2788.82 40.50 o 6 1 0 126.88 131.15 17.27 o 7 1 0 196.35 223.61 26.50 o 8 1 0 845.29 836.54 40.17 o 9 1 0 54.16 34.94 23.98 o 10 1 0 2.18 -1.50 23.17 o 11 1 0 2.67 -27.17 32.33 o 0 2 0 245.29 232.70 14.11 o 1 2 0 143.71 162.39 11.04 o 2 2 0 187.37 244.76 12.54 o 3 2 0 5101.41 5361.58 94.18 o 4 2 0 575.55 605.67 20.10 o 5 2 0 2801.62 2882.86 47.63 o 6 2 0 3.79 4.51 16.79 o 7 2 0 11.59 8.98 20.42 o 8 2 0 726.00 730.86 41.79 o 9 2 0 34.28 27.88 23.59 o 10 2 0 143.19 142.70 36.34 o 11 2 0 21.75 -19.39 44.69 o 0 3 0 14936.89 15258.42 233.96 o 1 3 0 59.08 63.55 10.64 o 2 3 0 71.97 64.92 10.42 o 3 3 0 10.49 -0.97 10.03 o 4 3 0 1467.15 1579.27 37.64 o 5 3 0 2.31 -4.42 14.49 o 6 3 0 220.90 241.79 20.54 o 7 3 0 304.67 309.31 27.76 o 8 3 0 941.88 977.95 42.21 o 9 3 0 83.01 84.23 31.22 o 10 3 0 207.66 191.37 45.92 o 11 3 0 38.50 -3.12 39.96 o 0 4 0 3831.20 4109.08 46.40 o 1 4 0 414.77 394.16 14.09 o 2 4 0 1534.93 1548.37 27.12 o 3 4 0 1348.25 1273.38 25.94 o 4 4 0 6.06 1.48 12.14 o 5 4 0 4242.11 4240.04 72.89 o 6 4 0 133.17 138.52 19.77 o 7 4 0 155.45 136.95 24.00 o 8 4 0 51.09 39.83 26.82 o 9 4 0 43.28 27.12 37.53 o 10 4 0 0.60 -36.09 36.09 o 11 4 0 38.56 -38.06 38.06 o 0 5 0 1792.16 1736.61 41.25 o 1 5 0 231.52 254.94 13.67 o 2 5 0 6.53 5.70 12.94 o 3 5 0 1867.05 1851.95 26.99 o 4 5 0 36.02 52.29 14.44 o 5 5 0 669.00 701.51 24.40 o 6 5 0 408.72 411.08 24.78 o 7 5 0 107.33 96.26 24.57 o 8 5 0 556.97 527.13 53.70 o 9 5 0 8.37 6.32 36.22 o 10 5 0 101.27 104.88 43.83 o 11 5 0 0.15 -23.90 42.40 o 0 6 0 59.41 50.47 16.71 o 1 6 0 405.51 411.13 17.22 o 2 6 0 7.01 -4.54 14.00 o 3 6 0 1353.99 1248.30 36.75 o 4 6 0 120.51 116.56 16.13 o 5 6 0 92.49 82.64 19.29 o 6 6 0 9.18 -9.76 17.70 o 7 6 0 729.06 748.75 64.17 o 8 6 0 83.89 60.63 36.46 o 9 6 0 12.85 26.40 58.83 o 10 6 0 6.55 18.49 38.54 o 11 6 0 35.51 -12.93 43.13 o 0 7 0 6774.50 6760.65 210.46 o 1 7 0 23.13 25.29 13.03 o 2 7 0 5078.58 4918.49 91.91 o 3 7 0 546.44 570.37 26.65 o 4 7 0 284.53 285.11 23.36 o 5 7 0 480.59 468.55 27.18 o 6 7 0 10.16 11.11 22.45 o 7 7 0 54.89 52.96 35.68 o 8 7 0 126.46 87.69 41.01 o 9 7 0 2.80 2.10 39.62 o 10 7 0 136.17 130.98 49.60 o 0 8 0 3576.62 3404.48 58.97 o 1 8 0 550.65 586.27 23.44 o 2 8 0 3201.97 3126.90 57.63 o 3 8 0 753.87 716.30 30.01 o 4 8 0 38.71 42.38 19.78 o 5 8 0 278.59 269.25 29.39 o 6 8 0 161.19 150.08 26.71 o 7 8 0 293.47 283.21 50.04 o 8 8 0 44.27 18.91 37.23 o 9 8 0 4.82 12.20 40.65 o 10 8 0 170.82 196.72 53.50 o 0 9 0 9150.32 8974.79 87.80 o 1 9 0 735.35 755.35 27.08 o 2 9 0 745.73 720.60 27.08 o 3 9 0 1681.15 1611.10 42.60 o 4 9 0 93.54 111.14 26.95 o 5 9 0 1001.43 1000.05 43.98 o 6 9 0 10.00 8.24 23.59 o 7 9 0 426.44 430.22 41.97 o 8 9 0 10.15 -2.58 39.06 o 9 9 0 0.56 -37.74 42.64 o 10 9 0 5.44 -34.43 44.27 o 0 10 0 705.12 707.64 40.59 o 1 10 0 29.58 30.35 18.36 o 2 10 0 1812.89 1723.53 39.86 o 3 10 0 284.81 314.70 27.06 o 4 10 0 99.45 94.84 27.01 o 5 10 0 2.59 11.65 24.68 o 6 10 0 211.66 226.91 30.74 o 7 10 0 1.47 -1.82 29.55 o 8 10 0 226.83 237.27 54.60 o 9 10 0 22.24 31.82 45.68 o 0 11 0 3143.49 3030.00 81.05 o 1 11 0 35.14 39.26 20.07 o 2 11 0 3174.86 3120.55 53.87 o 3 11 0 327.83 353.79 34.09 o 4 11 0 2.83 8.76 25.15 o 5 11 0 354.69 359.21 35.58 o 6 11 0 18.72 38.45 25.34 o 7 11 0 142.30 168.20 38.33 o 8 11 0 13.85 -29.37 43.51 o 9 11 0 22.84 12.57 46.75 o 0 12 0 723.28 656.61 42.38 o 1 12 0 5.67 2.06 17.38 o 2 12 0 36.61 69.52 33.90 o 3 12 0 26.25 -4.26 29.93 o 4 12 0 96.52 104.67 29.63 o 5 12 0 1.90 40.65 28.24 o 6 12 0 6.58 -23.87 29.09 o 7 12 0 52.10 43.63 36.08 o 8 12 0 79.61 138.14 51.33 o 0 13 0 123.24 148.66 30.89 o 1 13 0 136.54 150.15 29.49 o 2 13 0 422.40 432.21 44.64 o 3 13 0 148.63 145.89 36.70 o 4 13 0 20.38 19.15 32.91 o 5 13 0 449.36 440.26 41.66 o 6 13 0 0.63 33.78 34.67 o 7 13 0 17.14 44.98 40.08 o 0 14 0 623.03 435.47 92.44 o 1 14 0 13.35 -0.24 25.68 o 2 14 0 56.95 90.06 29.12 o 3 14 0 59.10 62.33 35.49 o 4 14 0 0.80 8.10 35.04 o 5 14 0 23.93 21.87 37.87 o 6 14 0 33.00 30.22 42.96 o 0 15 0 265.64 347.61 91.68 o 1 15 0 96.58 93.28 30.48 o 2 15 0 271.72 339.19 38.53 o 3 15 0 8.85 3.28 24.92 o 4 15 0 6.38 -24.33 35.63 o 5 15 0 0.05 30.76 37.80 o 0 16 0 160.52 190.99 86.33 o 1 16 0 115.44 168.04 57.77 o 2 16 0 4.37 21.17 31.10 o 3 16 0 346.89 350.09 43.01 o 4 16 0 0.68 -28.78 37.68 o 0 17 0 181.75 249.82 93.21 o 1 17 0 7.53 61.03 56.11 o -11 0 1 10.74 -0.38 39.47 o -9 0 1 71.76 19.43 32.83 o -7 0 1 246.32 255.45 39.39 o -5 0 1 1045.12 1014.88 34.29 o -3 0 1 2312.90 2297.56 126.44 o -1 0 1 15349.11 16653.05 262.81 o 1 0 1 34.85 119.18 12.99 o 3 0 1 4391.11 4360.79 90.15 o 5 0 1 370.00 379.05 25.24 o 7 0 1 21.39 51.34 31.28 o 9 0 1 472.38 462.28 64.17 o 11 0 1 232.80 165.02 71.05 o -11 1 1 8.00 12.77 32.35 o -10 1 1 89.50 60.48 25.52 o -9 1 1 448.31 444.58 36.30 o -8 1 1 823.40 900.14 41.55 o -7 1 1 1.79 -12.77 20.45 o -6 1 1 103.36 101.89 21.42 o -5 1 1 1.19 -0.37 12.43 o -4 1 1 434.32 415.44 16.22 o -3 1 1 3954.96 4112.27 40.28 o -2 1 1 1502.68 1575.29 45.61 o -1 1 1 1601.77 1566.76 31.91 o 0 1 1 13174.88 14097.72 97.79 o 1 1 1 1601.85 1540.80 40.73 o 2 1 1 2654.86 2626.72 88.63 o 3 1 1 5505.41 6252.99 98.82 o 4 1 1 4419.29 4411.49 46.43 o 5 1 1 350.18 335.16 18.66 o 6 1 1 2.04 5.23 15.43 o 7 1 1 106.53 125.96 24.43 o 8 1 1 58.83 52.64 22.72 o 9 1 1 10.34 23.89 22.45 o 10 1 1 60.82 52.09 30.99 o 11 1 1 0.37 -33.38 33.38 o -11 2 1 93.24 92.24 44.76 o -10 2 1 7.60 13.01 25.41 o -9 2 1 0.70 -3.31 21.48 o -8 2 1 263.77 281.62 28.67 o -7 2 1 65.17 87.76 23.76 o -6 2 1 97.53 77.91 20.77 o -5 2 1 987.14 937.98 28.55 o -4 2 1 0.62 15.05 12.39 o -3 2 1 3267.72 3373.54 32.01 o -2 2 1 722.68 732.25 16.53 o -1 2 1 3.03 7.18 9.44 o 0 2 1 1227.46 1247.63 21.94 o 1 2 1 2349.52 2597.20 36.13 o 2 2 1 669.95 710.15 19.10 o 3 2 1 2726.44 2746.62 80.83 o 4 2 1 860.14 806.42 22.04 o 5 2 1 1769.38 1798.17 34.51 o 6 2 1 0.20 -3.19 15.93 o 7 2 1 714.20 749.23 52.75 o 8 2 1 52.27 53.61 22.23 o 9 2 1 178.84 158.15 32.41 o 10 2 1 11.77 9.28 28.82 o 11 2 1 92.91 80.32 47.37 o -11 3 1 38.36 5.62 42.10 o -10 3 1 129.01 101.11 38.83 o -9 3 1 2.11 -1.24 22.60 o -8 3 1 1162.85 1097.47 43.84 o -7 3 1 76.46 74.67 23.21 o -6 3 1 78.16 75.31 21.63 o -5 3 1 1060.22 1008.07 27.94 o -4 3 1 2039.80 2238.04 30.73 o -3 3 1 637.58 600.60 17.29 o -2 3 1 656.50 655.65 16.57 o -1 3 1 2.90 10.60 10.94 o 0 3 1 552.19 572.22 40.72 o 1 3 1 526.89 542.47 14.39 o 2 3 1 1102.83 1033.98 34.74 o 3 3 1 122.08 134.02 11.81 o 4 3 1 3950.96 4187.42 47.04 o 5 3 1 788.03 779.84 25.97 o 6 3 1 28.12 21.23 16.46 o 7 3 1 596.47 595.99 33.08 o 8 3 1 36.40 39.76 21.68 o 9 3 1 205.59 205.94 33.40 o 10 3 1 270.05 277.84 48.24 o 11 3 1 1.27 -2.73 40.73 o -11 4 1 94.62 79.82 44.59 o -10 4 1 242.07 245.37 47.42 o -9 4 1 2.60 -31.57 31.57 o -8 4 1 1526.99 1579.77 51.63 o -7 4 1 49.19 52.44 21.48 o -6 4 1 951.09 966.12 37.35 o -5 4 1 750.29 762.75 24.88 o -4 4 1 5390.17 5504.23 63.00 o -3 4 1 1658.74 1718.19 26.67 o -2 4 1 486.34 436.97 17.86 o -1 4 1 2531.94 2652.58 66.11 o 0 4 1 2252.78 2197.30 32.08 o 1 4 1 3.26 21.54 9.95 o 2 4 1 518.11 447.07 18.92 o 3 4 1 2263.68 2385.02 29.78 o 4 4 1 5033.26 5248.80 70.72 o 5 4 1 223.52 240.08 19.12 o 6 4 1 425.53 426.34 24.75 o 7 4 1 173.46 177.97 23.71 o 8 4 1 264.76 289.86 34.61 o 9 4 1 1.39 -2.84 33.22 o 10 4 1 201.82 258.13 48.62 o 11 4 1 44.04 50.80 56.92 o -11 5 1 109.69 121.34 48.00 o -10 5 1 0.80 59.15 52.33 o -9 5 1 1.02 -12.65 33.41 o -8 5 1 57.89 38.61 35.24 o -7 5 1 661.10 660.86 39.27 o -6 5 1 265.24 298.26 22.99 o -5 5 1 2900.33 2929.86 41.64 o -4 5 1 2282.64 2498.84 35.79 o -3 5 1 4495.12 4493.14 76.80 o -2 5 1 704.38 766.94 23.36 o -1 5 1 11.87 5.54 10.69 o 0 5 1 963.29 978.24 22.57 o 1 5 1 176.00 194.47 12.40 o 2 5 1 101.36 122.68 14.15 o 3 5 1 4858.79 4997.90 75.39 o 4 5 1 6.98 1.79 12.47 o 5 5 1 2247.93 2111.93 58.37 o 6 5 1 269.65 252.56 21.86 o 7 5 1 687.90 663.62 54.73 o 8 5 1 73.23 30.94 35.65 o 9 5 1 72.74 76.21 39.10 o 10 5 1 12.81 -7.37 38.01 o 11 5 1 33.05 9.77 46.06 o -11 6 1 0.35 -21.63 43.86 o -10 6 1 141.17 105.77 45.53 o -9 6 1 0.11 8.25 40.11 o -8 6 1 368.21 377.41 76.40 o -7 6 1 396.20 407.96 73.34 o -6 6 1 191.65 184.79 21.70 o -5 6 1 402.30 419.12 25.63 o -4 6 1 106.69 97.93 15.46 o -3 6 1 100.09 114.66 17.61 o -2 6 1 820.04 773.08 25.10 o -1 6 1 741.87 790.64 23.86 o 0 6 1 1809.72 1740.73 26.63 o 1 6 1 1720.77 1795.29 28.80 o 2 6 1 6840.64 6884.99 78.40 o 3 6 1 785.32 810.94 26.05 o 4 6 1 1552.36 1550.63 35.11 o 5 6 1 169.65 170.92 20.38 o 6 6 1 549.72 570.05 40.35 o 7 6 1 0.86 -11.68 30.52 o 8 6 1 0.53 -31.19 32.90 o 9 6 1 7.49 27.47 38.34 o 10 6 1 171.77 183.55 49.79 o 11 6 1 0.79 -8.85 43.46 o -10 7 1 108.70 71.05 45.51 o -9 7 1 0.12 1.20 38.89 o -8 7 1 54.09 46.87 41.55 o -7 7 1 0.20 -30.74 30.74 o -6 7 1 412.46 416.55 31.30 o -5 7 1 83.26 103.61 21.33 o -4 7 1 223.33 256.18 23.02 o -3 7 1 2962.90 2958.79 66.84 o -2 7 1 5.60 -8.64 16.27 o -1 7 1 1189.03 1157.68 24.97 o 0 7 1 240.04 195.76 14.38 o 1 7 1 1160.88 1119.63 25.52 o 2 7 1 1451.87 1462.63 37.34 o 3 7 1 1828.94 1794.31 37.45 o 4 7 1 415.82 408.90 25.20 o 5 7 1 445.92 473.47 34.20 o 6 7 1 151.59 152.05 26.37 o 7 7 1 334.28 308.16 45.88 o 8 7 1 123.72 105.44 42.04 o 9 7 1 151.87 179.09 48.00 o 10 7 1 12.78 14.18 42.51 o -10 8 1 1.84 -9.15 43.06 o -9 8 1 21.38 24.61 41.86 o -8 8 1 169.24 257.70 50.16 o -7 8 1 166.22 127.62 40.42 o -6 8 1 70.27 82.79 24.35 o -5 8 1 554.01 596.44 31.38 o -4 8 1 163.06 147.15 23.19 o -3 8 1 391.87 419.41 26.39 o -2 8 1 1124.14 1175.44 31.10 o -1 8 1 391.42 363.23 20.35 o 0 8 1 1449.86 1488.73 28.81 o 1 8 1 13.51 3.81 13.71 o 2 8 1 1918.69 1802.68 48.30 o 3 8 1 986.73 991.10 32.51 o 4 8 1 280.35 260.33 28.77 o 5 8 1 261.55 250.94 28.69 o 6 8 1 16.73 9.71 22.28 o 7 8 1 387.71 428.59 76.40 o 8 8 1 15.18 -20.73 34.56 o 9 8 1 52.34 69.73 44.55 o 10 8 1 39.41 61.58 47.75 o -10 9 1 23.68 -2.77 47.63 o -9 9 1 4.10 -14.32 43.51 o -8 9 1 213.74 233.50 49.73 o -7 9 1 18.48 40.31 37.95 o -6 9 1 630.08 627.84 38.56 o -5 9 1 7.34 8.88 24.08 o -4 9 1 295.50 328.71 27.27 o -3 9 1 915.96 874.89 35.04 o -2 9 1 803.60 815.58 29.35 o -1 9 1 1531.02 1546.00 35.72 o 0 9 1 1759.09 1678.84 40.57 o 1 9 1 896.89 986.64 29.42 o 2 9 1 2531.35 2462.15 42.79 o 3 9 1 393.63 384.94 26.90 o 4 9 1 219.17 217.75 28.69 o 5 9 1 94.87 130.88 26.35 o 6 9 1 54.32 43.39 24.41 o 7 9 1 70.86 58.69 39.68 o 8 9 1 11.90 5.60 39.64 o 9 9 1 46.17 50.36 47.21 o 10 9 1 7.29 5.47 44.37 o -9 10 1 240.33 279.37 58.52 o -8 10 1 2.46 7.36 41.45 o -7 10 1 12.85 8.66 37.06 o -6 10 1 22.58 15.23 28.71 o -5 10 1 421.60 417.43 35.93 o -4 10 1 0.25 30.48 24.70 o -3 10 1 2382.22 2426.14 52.85 o -2 10 1 80.28 89.31 20.38 o -1 10 1 62.08 64.39 19.40 o 0 10 1 43.29 43.94 17.81 o 1 10 1 266.63 261.59 21.35 o 2 10 1 413.82 437.33 25.00 o 3 10 1 54.28 68.20 25.80 o 4 10 1 27.96 29.74 24.12 o 5 10 1 427.37 484.50 36.64 o 6 10 1 41.14 46.58 26.88 o 7 10 1 543.17 552.75 47.12 o 8 10 1 42.99 34.36 43.94 o 9 10 1 21.11 -24.13 44.57 o -9 11 1 56.31 47.95 50.28 o -8 11 1 280.92 261.86 93.21 o -7 11 1 1.40 -27.05 36.03 o -6 11 1 700.97 780.11 54.00 o -5 11 1 66.08 54.38 27.82 o -4 11 1 79.74 71.66 27.60 o -3 11 1 8.36 -14.00 24.85 o -2 11 1 2.98 5.51 18.76 o -1 11 1 585.09 532.28 30.67 o 0 11 1 41.84 62.21 18.55 o 1 11 1 3.86 -7.06 17.10 o 2 11 1 1403.02 1546.33 77.19 o 3 11 1 729.20 751.92 41.41 o 4 11 1 286.69 300.85 32.79 o 5 11 1 111.46 86.54 28.36 o 6 11 1 30.76 48.29 28.18 o 7 11 1 23.31 38.66 32.88 o 8 11 1 173.05 214.79 61.88 o 9 11 1 0.16 -4.63 46.54 o -8 12 1 0.71 42.20 51.00 o -7 12 1 124.19 87.82 47.06 o -6 12 1 237.29 230.16 41.22 o -5 12 1 71.45 46.00 29.07 o -4 12 1 5.07 -20.39 26.74 o -3 12 1 988.34 1061.68 58.04 o -2 12 1 45.58 37.17 24.90 o -1 12 1 895.87 869.74 36.74 o 0 12 1 127.92 123.10 20.33 o 1 12 1 36.70 34.79 20.42 o 2 12 1 1429.01 1413.82 64.27 o 3 12 1 7.49 -9.84 28.85 o 4 12 1 6.94 10.17 27.14 o 5 12 1 993.96 955.94 51.23 o 6 12 1 204.81 170.99 33.58 o 7 12 1 264.66 239.62 44.35 o 8 12 1 43.20 40.27 73.72 o -7 13 1 46.52 41.76 50.11 o -6 13 1 299.05 261.73 45.23 o -5 13 1 25.06 10.77 30.31 o -4 13 1 26.55 23.00 32.54 o -3 13 1 540.61 554.43 48.85 o -2 13 1 42.91 60.94 32.96 o -1 13 1 643.27 629.52 31.28 o 0 13 1 553.86 516.89 29.81 o 1 13 1 37.62 49.13 27.31 o 2 13 1 452.58 523.46 34.83 o 3 13 1 3.56 -0.36 32.09 o 4 13 1 62.71 59.36 35.12 o 5 13 1 550.31 561.26 47.67 o 6 13 1 26.39 10.27 35.87 o 7 13 1 216.63 259.60 46.26 o -6 14 1 306.72 355.02 62.65 o -5 14 1 134.89 163.03 41.44 o -4 14 1 78.07 67.94 38.09 o -3 14 1 232.58 254.70 43.00 o -2 14 1 0.36 -20.57 29.91 o -1 14 1 184.86 164.11 33.37 o 0 14 1 438.41 447.72 38.82 o 1 14 1 22.08 33.24 26.46 o 2 14 1 1134.09 1163.57 54.58 o 3 14 1 227.41 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