#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/04/2200490.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200490_Fobs loop_ _publ_author_name 'Srinivasan, N.' 'Sridhar, B.' 'Rajaram, R. K.' _publ_section_title ; Bis(L-histidinium sulfate) trihydrate ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o607 _journal_page_last o609 _journal_volume 57 _journal_year 2001 _space_group_IT_number 1 _symmetry_space_group_name_Hall 'P 1' _symmetry_space_group_name_H-M 'P 1' _cell_angle_alpha 102.576 _cell_angle_beta 107.704 _cell_angle_gamma 119.667 _cell_length_a 8.3400 _cell_length_b 8.9291 _cell_length_c 10.7239 _exptl_crystal_F_000 294.00 _reflns_d_resolution_high 0.8318 _[local]_cod_data_source_file na6086Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' HISTIDINE SULFATE' _shelx_refln_list_code 4 _shelx_f_calc_maximum 87.38 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 -1 -12 22.80 27.67 0.53 o 5 -1 -12 3.71 4.32 0.20 o 6 -1 -12 0.84 1.97 0.16 o 2 0 -12 5.29 3.46 0.18 o 3 0 -12 4.45 5.44 0.20 o 4 0 -12 3.46 5.43 0.21 o 5 0 -12 54.54 62.20 0.81 o 6 0 -12 9.17 6.32 0.24 o 1 1 -12 23.07 23.37 0.46 o 2 1 -12 12.41 10.40 0.32 o 3 1 -12 15.62 16.58 0.48 o 4 1 -12 23.64 25.08 0.57 o 5 1 -12 3.47 3.11 0.19 o 6 1 -12 2.57 3.82 0.20 o 1 2 -12 39.43 41.03 0.64 o 2 2 -12 2.79 1.94 0.17 o 3 2 -12 7.93 9.75 0.30 o 4 2 -12 37.35 43.67 0.74 o 5 2 -12 20.71 19.04 0.49 o 0 3 -12 11.24 13.02 0.37 o 1 3 -12 16.83 16.21 0.45 o 2 3 -12 27.55 25.71 0.57 o 3 3 -12 7.66 8.15 0.25 o 4 3 -12 17.60 17.06 0.47 o 5 3 -12 7.15 9.15 0.29 o 0 4 -12 10.63 9.88 0.30 o 1 4 -12 24.83 26.55 0.54 o 2 4 -12 7.26 6.94 0.23 o 3 4 -12 17.73 18.99 0.49 o 4 4 -12 32.42 38.26 0.62 o 0 5 -12 16.40 18.06 0.43 o 1 5 -12 8.40 6.38 0.22 o 2 5 -12 1.22 1.23 0.15 o 3 5 -12 23.20 21.54 0.46 o 4 -3 -11 0.33 -0.01 0.06 o 5 -3 -11 12.93 13.60 0.39 o 6 -3 -11 4.33 4.70 0.20 o 3 -2 -11 40.28 43.39 0.66 o 4 -2 -11 13.68 13.68 0.37 o 5 -2 -11 23.00 23.21 0.56 o 6 -2 -11 83.25 88.54 1.00 o 7 -2 -11 4.76 2.88 0.19 o 1 -1 -11 1.91 1.54 0.15 o 2 -1 -11 11.12 12.45 0.35 o 3 -1 -11 4.94 5.79 0.23 o 4 -1 -11 54.30 54.58 0.87 o 5 -1 -11 25.77 22.30 0.57 o 6 -1 -11 33.23 31.96 0.66 o 7 -1 -11 5.63 8.06 0.24 o 0 0 -11 34.65 35.32 0.53 o 1 0 -11 8.89 7.67 0.24 o 2 0 -11 55.27 57.02 0.86 o 3 0 -11 67.52 70.76 0.99 o 4 0 -11 12.71 11.12 0.32 o 5 0 -11 44.74 55.53 0.92 o 6 0 -11 7.10 9.89 0.31 o 7 0 -11 4.98 3.60 0.18 o 0 1 -11 25.27 27.49 0.55 o 1 1 -11 14.43 16.09 0.42 o 2 1 -11 22.59 28.99 0.66 o 3 1 -11 67.45 67.35 1.03 o 4 1 -11 1.95 2.21 0.18 o 5 1 -11 6.77 6.37 0.25 o 6 1 -11 11.33 14.08 0.39 o 7 1 -11 2.78 2.06 0.17 o 0 2 -11 2.22 1.87 0.18 o 1 2 -11 11.84 12.95 0.37 o 2 2 -11 22.70 28.12 0.68 o 3 2 -11 5.31 4.23 0.23 o 4 2 -11 3.27 5.66 0.24 o 5 2 -11 11.97 18.31 0.54 o 6 2 -11 2.62 4.24 0.21 o 0 3 -11 79.17 87.06 1.07 o 1 3 -11 66.50 76.73 1.08 o 2 3 -11 98.82 104.79 1.26 o 3 3 -11 2.34 4.30 0.22 o 4 3 -11 33.41 34.24 0.72 o 5 3 -11 24.13 25.86 0.60 o 0 4 -11 7.74 9.16 0.26 o 1 4 -11 7.62 7.11 0.26 o 2 4 -11 18.05 18.52 0.48 o 3 4 -11 4.51 3.42 0.19 o 4 4 -11 21.36 25.03 0.59 o 5 4 -11 48.92 58.18 0.76 o 0 5 -11 1.32 1.54 0.17 o 1 5 -11 71.62 74.43 1.01 o 2 5 -11 3.12 2.86 0.20 o 3 5 -11 1.26 1.07 0.16 o 4 5 -11 6.65 4.84 0.23 o 0 6 -11 7.82 9.37 0.26 o 1 6 -11 35.08 36.91 0.66 o 2 6 -11 16.60 15.29 0.44 o 3 6 -11 6.18 5.91 0.22 o 0 7 -11 9.95 10.48 0.31 o 1 7 -11 5.48 6.80 0.23 o 4 -4 -10 21.94 22.72 0.49 o 5 -4 -10 20.57 24.63 0.54 o 6 -4 -10 1.22 1.22 0.15 o 7 -4 -10 53.52 56.60 0.73 o 2 -3 -10 27.38 30.12 0.53 o 3 -3 -10 12.63 14.84 0.39 o 4 -3 -10 51.22 49.86 0.81 o 5 -3 -10 65.24 61.14 0.92 o 6 -3 -10 31.16 25.11 0.60 o 7 -3 -10 27.16 26.35 0.57 o 8 -3 -10 29.39 31.69 0.56 o 1 -2 -10 32.44 30.15 0.55 o 2 -2 -10 7.05 7.83 0.26 o 3 -2 -10 21.28 19.38 0.55 o 4 -2 -10 54.70 57.94 0.96 o 5 -2 -10 26.95 33.32 0.73 o 6 -2 -10 0.33 0.82 0.16 o 7 -2 -10 13.66 15.16 0.42 o 8 -2 -10 23.09 24.44 0.52 o 0 -1 -10 6.51 6.93 0.22 o 1 -1 -10 50.63 49.29 0.80 o 2 -1 -10 133.14 128.62 1.40 o 3 -1 -10 40.81 43.85 0.83 o 4 -1 -10 171.92 193.38 1.76 o 5 -1 -10 11.41 9.77 0.30 o 6 -1 -10 1.66 2.89 0.19 o 7 -1 -10 28.21 34.56 0.69 o 8 -1 -10 0.09 0.21 0.16 o 0 0 -10 5.69 4.46 0.22 o 1 0 -10 7.91 8.54 0.28 o 2 0 -10 29.65 22.87 0.63 o 3 0 -10 8.84 13.69 0.40 o 4 0 -10 9.40 6.51 0.26 o 5 0 -10 10.41 11.06 0.31 o 6 0 -10 0.87 0.90 0.25 o 7 0 -10 26.41 31.03 0.65 o 0 1 -10 6.23 11.54 0.36 o 1 1 -10 81.87 100.97 1.27 o 2 1 -10 16.94 20.07 0.54 o 3 1 -10 95.94 126.50 1.45 o 4 1 -10 4.64 5.87 0.26 o 5 1 -10 35.89 31.54 0.75 o 6 1 -10 0.92 0.42 0.23 o 7 1 -10 1.01 0.83 0.14 o 0 2 -10 85.70 80.33 1.10 o 1 2 -10 47.10 50.79 0.92 o 2 2 -10 58.24 65.15 1.06 o 3 2 -10 55.73 54.12 0.97 o 4 2 -10 48.73 62.79 1.04 o 5 2 -10 2.70 2.78 0.20 o 6 2 -10 88.79 92.36 1.10 o 7 2 -10 0.87 2.88 0.17 o 0 3 -10 54.61 76.76 1.10 o 1 3 -10 5.15 6.54 0.26 o 2 3 -10 47.83 58.53 1.01 o 3 3 -10 91.38 87.26 1.23 o 4 3 -10 9.56 8.96 0.29 o 5 3 -10 12.64 9.23 0.27 o 6 3 -10 17.88 18.24 0.48 o 0 4 -10 164.71 196.16 1.77 o 1 4 -10 8.81 9.39 0.30 o 2 4 -10 94.88 103.88 1.31 o 3 4 -10 112.77 115.76 1.36 o 4 4 -10 16.69 17.64 0.48 o 5 4 -10 25.61 23.74 0.56 o 0 5 -10 49.62 53.70 0.94 o 1 5 -10 28.43 29.40 0.71 o 2 5 -10 4.22 4.70 0.23 o 3 5 -10 112.69 112.41 1.28 o 4 5 -10 6.40 6.25 0.24 o 0 6 -10 16.94 17.25 0.48 o 1 6 -10 9.68 10.00 0.29 o 2 6 -10 100.64 94.63 1.14 o 3 6 -10 5.32 5.62 0.22 o 0 7 -10 22.49 25.30 0.59 o 1 7 -10 1.17 1.26 0.16 o 2 7 -10 35.84 35.19 0.61 o 0 8 -10 3.32 2.49 0.18 o 4 -5 -9 21.05 21.69 0.48 o 5 -5 -9 27.57 29.66 0.59 o 6 -5 -9 16.82 13.90 0.38 o 7 -5 -9 9.59 6.27 0.23 o 8 -5 -9 17.02 17.02 0.41 o 2 -4 -9 9.22 8.99 0.26 o 3 -4 -9 40.15 37.87 0.69 o 4 -4 -9 10.91 12.95 0.36 o 5 -4 -9 18.83 18.07 0.50 o 6 -4 -9 92.33 96.76 1.16 o 7 -4 -9 4.53 4.83 0.23 o 8 -4 -9 82.66 75.75 0.92 o 1 -3 -9 8.10 9.61 0.27 o 2 -3 -9 0.22 0.59 0.14 o 3 -3 -9 24.14 25.84 0.65 o 4 -3 -9 14.48 19.09 0.51 o 5 -3 -9 1.46 2.58 0.21 o 6 -3 -9 8.63 7.79 0.28 o 7 -3 -9 0.38 0.64 0.26 o 8 -3 -9 41.42 41.74 0.74 o 0 -2 -9 11.23 12.55 0.35 o 1 -2 -9 34.26 33.92 0.70 o 2 -2 -9 25.58 24.89 0.66 o 3 -2 -9 163.01 181.70 1.70 o 4 -2 -9 94.36 98.11 1.28 o 5 -2 -9 77.15 80.89 1.18 o 6 -2 -9 20.10 20.67 0.55 o 7 -2 -9 53.86 48.37 0.88 o 8 -2 -9 0.99 1.41 0.17 o 0 -1 -9 2.87 3.47 0.19 o 1 -1 -9 9.86 11.66 0.34 o 2 -1 -9 41.85 48.66 0.90 o 3 -1 -9 7.65 8.90 0.29 o 4 -1 -9 5.72 7.06 0.27 o 5 -1 -9 109.83 127.79 1.49 o 6 -1 -9 8.68 11.49 0.36 o 7 -1 -9 36.53 29.63 0.70 o 8 -1 -9 49.88 45.98 0.76 o 0 0 -9 47.86 50.21 0.89 o 1 0 -9 11.87 16.87 0.49 o 2 0 -9 184.50 187.94 1.73 o 3 0 -9 3.22 5.98 0.24 o 4 0 -9 139.69 137.48 1.51 o 5 0 -9 31.69 37.32 0.82 o 6 0 -9 3.04 2.33 0.21 o 7 0 -9 6.75 5.82 0.23 o 8 0 -9 15.33 16.41 0.45 o 0 1 -9 49.40 52.67 0.93 o 1 1 -9 126.87 141.07 1.50 o 2 1 -9 156.77 179.47 1.69 o 3 1 -9 22.75 18.06 0.50 o 4 1 -9 55.59 63.69 1.05 o 5 1 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0 8 -9 36.05 35.34 0.65 o 1 8 -9 2.01 2.54 0.17 o 4 -6 -8 19.09 17.32 0.43 o 5 -6 -8 11.19 8.91 0.26 o 6 -6 -8 7.64 8.17 0.25 o 7 -6 -8 45.37 49.51 0.75 o 8 -6 -8 4.46 3.78 0.20 o 2 -5 -8 33.66 34.53 0.57 o 3 -5 -8 7.59 7.00 0.25 o 4 -5 -8 4.40 7.00 0.25 o 5 -5 -8 122.06 122.42 1.33 o 6 -5 -8 29.85 32.72 0.72 o 7 -5 -8 26.89 23.87 0.60 o 8 -5 -8 17.32 19.58 0.51 o 9 -5 -8 13.91 10.93 0.30 o 1 -4 -8 23.46 25.08 0.53 o 2 -4 -8 6.16 7.49 0.24 o 3 -4 -8 6.13 5.88 0.24 o 4 -4 -8 6.81 10.76 0.33 o 5 -4 -8 64.88 68.27 1.06 o 6 -4 -8 21.56 21.79 0.64 o 7 -4 -8 18.54 15.95 0.47 o 8 -4 -8 21.95 25.07 0.60 o 9 -4 -8 35.36 31.54 0.58 o 0 -3 -8 0.29 0.47 0.17 o 1 -3 -8 3.72 3.61 0.20 o 2 -3 -8 94.04 109.38 1.32 o 3 -3 -8 132.23 148.41 1.57 o 4 -3 -8 387.43 414.89 2.66 o 5 -3 -8 7.47 7.83 0.28 o 6 -3 -8 409.10 419.82 2.67 o 7 -3 -8 11.79 12.43 0.38 o 8 -3 -8 5.08 3.13 0.20 o 9 -3 -8 63.73 61.66 0.81 o 0 -2 -8 34.41 38.55 0.76 o 1 -2 -8 27.01 25.41 0.68 o 2 -2 -8 39.44 35.04 0.78 o 3 -2 -8 48.61 53.80 0.94 o 4 -2 -8 181.62 191.41 1.75 o 5 -2 -8 65.69 65.21 1.06 o 6 -2 -8 158.70 130.10 1.51 o 7 -2 -8 76.48 76.32 1.13 o 8 -2 -8 1.74 1.79 0.16 o 9 -2 -8 69.52 65.85 0.79 o 0 -1 -8 13.51 16.24 0.48 o 1 -1 -8 140.26 152.88 1.56 o 2 -1 -8 1.37 3.56 0.20 o 3 -1 -8 614.31 651.46 3.13 o 4 -1 -8 193.66 188.33 1.70 o 5 -1 -8 65.58 68.87 1.07 o 6 -1 -8 30.43 25.49 0.69 o 7 -1 -8 11.58 9.62 0.31 o 8 -1 -8 32.37 30.80 0.67 o 0 0 -8 100.81 101.98 1.27 o 1 0 -8 342.73 368.32 2.33 o 2 0 -8 23.37 17.60 0.46 o 3 0 -8 296.85 328.98 2.15 o 4 0 -8 17.41 20.74 0.59 o 5 0 -8 13.23 14.52 0.41 o 6 0 -8 4.04 4.69 0.24 o 7 0 -8 60.94 57.75 0.98 o 8 0 -8 20.10 15.41 0.40 o 0 1 -8 6.03 5.48 0.21 o 1 1 -8 26.56 33.04 0.69 o 2 1 -8 50.74 57.69 0.91 o 3 1 -8 147.56 161.22 1.50 o 4 1 -8 58.55 66.23 1.03 o 5 1 -8 77.98 68.05 1.06 o 6 1 -8 0.82 1.07 0.17 o 7 1 -8 24.02 27.73 0.65 o 8 1 -8 17.92 16.65 0.42 o 0 2 -8 340.83 379.50 2.37 o 1 2 -8 8.99 7.53 0.23 o 2 2 -8 122.61 126.69 1.32 o 3 2 -8 20.15 19.58 0.49 o 4 2 -8 25.32 23.32 0.63 o 5 2 -8 9.75 11.35 0.35 o 6 2 -8 15.90 19.51 0.51 o 7 2 -8 38.59 33.32 0.64 o 0 3 -8 33.97 32.18 0.70 o 1 3 -8 40.79 44.56 0.82 o 2 3 -8 93.34 90.26 1.17 o 3 3 -8 81.34 89.95 1.20 o 4 3 -8 32.68 25.13 0.69 o 5 3 -8 70.44 65.45 1.04 o 6 3 -8 1.07 0.65 0.22 o 0 4 -8 197.62 206.71 1.74 o 1 4 -8 163.68 154.62 1.54 o 2 4 -8 501.34 498.60 2.79 o 3 4 -8 55.17 56.22 0.99 o 4 4 -8 108.16 116.04 1.39 o 5 4 -8 36.04 38.93 0.77 o 6 4 -8 0.32 0.45 0.17 o 0 5 -8 4.57 4.52 0.21 o 1 5 -8 66.36 64.68 1.04 o 2 5 -8 73.89 77.40 1.16 o 3 5 -8 54.18 64.14 1.03 o 4 5 -8 30.77 24.08 0.63 o 5 5 -8 18.26 14.69 0.43 o 0 6 -8 25.90 30.52 0.73 o 1 6 -8 46.65 45.61 0.87 o 2 6 -8 235.48 237.29 1.95 o 3 6 -8 8.74 8.14 0.25 o 4 6 -8 3.12 2.62 0.17 o 0 7 -8 4.68 5.21 0.24 o 1 7 -8 23.29 24.26 0.63 o 2 7 -8 33.24 32.64 0.69 o 3 7 -8 0.80 0.98 0.14 o 0 8 -8 2.99 2.99 0.20 o 1 8 -8 27.79 26.15 0.57 o 0 9 -8 17.12 17.32 0.42 o 5 -7 -7 0.31 0.18 0.16 o 6 -7 -7 82.89 83.72 0.94 o 7 -7 -7 4.02 3.73 0.19 o 8 -7 -7 79.72 87.39 0.88 o 3 -6 -7 14.69 16.86 0.47 o 4 -6 -7 45.44 46.89 0.80 o 5 -6 -7 28.92 32.05 0.70 o 6 -6 -7 7.62 7.44 0.26 o 7 -6 -7 24.94 27.00 0.64 o 8 -6 -7 46.41 39.77 0.70 o 9 -6 -7 36.32 35.34 0.58 o 1 -5 -7 22.53 19.21 0.46 o 2 -5 -7 17.92 17.36 0.51 o 3 -5 -7 5.97 5.80 0.25 o 4 -5 -7 54.59 56.76 0.99 o 5 -5 -7 98.51 106.32 1.36 o 6 -5 -7 12.83 8.75 0.30 o 7 -5 -7 84.18 91.42 1.21 o 8 -5 -7 18.87 16.79 0.44 o 9 -5 -7 7.49 10.03 0.30 o 0 -4 -7 11.20 14.18 0.42 o 1 -4 -7 7.48 4.56 0.23 o 2 -4 -7 41.20 47.60 0.89 o 3 -4 -7 194.07 205.87 1.86 o 4 -4 -7 0.55 0.62 0.25 o 5 -4 -7 454.73 471.76 2.84 o 6 -4 -7 7.52 7.55 0.29 o 7 -4 -7 123.33 111.92 1.40 o 8 -4 -7 100.96 87.62 1.18 o 9 -4 -7 13.10 8.08 0.26 o 0 -3 -7 6.96 6.74 0.24 o 1 -3 -7 37.87 35.17 0.78 o 2 -3 -7 60.63 72.50 1.10 o 3 -3 -7 41.23 45.94 0.87 o 4 -3 -7 378.59 383.79 2.44 o 5 -3 -7 76.56 63.55 1.03 o 6 -3 -7 88.17 82.96 1.20 o 7 -3 -7 16.81 16.38 0.51 o 8 -3 -7 74.90 63.55 1.00 o 9 -3 -7 0.50 0.51 0.20 o 0 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372.59 352.70 1.80 o 3 1 2 29.65 31.21 0.65 o 4 1 2 5.55 2.68 0.21 o 5 1 2 27.06 18.93 0.51 o 6 1 2 1.11 1.72 0.16 o 0 2 2 1255.07 1189.40 14.85 o 1 2 2 299.29 307.06 1.62 o 2 2 2 232.05 217.98 1.62 o 3 2 2 5.90 7.36 0.25 o 4 2 2 213.09 204.74 1.85 o 5 2 2 0.39 1.39 0.17 o 0 3 2 38.90 33.44 0.55 o 1 3 2 103.56 103.43 1.11 o 2 3 2 42.79 44.22 0.84 o 3 3 2 10.01 11.06 0.32 o 4 3 2 0.74 0.35 0.22 o 0 4 2 188.47 195.43 1.53 o 1 4 2 37.22 38.40 0.78 o 2 4 2 10.53 11.17 0.32 o 3 4 2 56.20 52.32 0.89 o 0 5 2 82.68 77.21 1.11 o 1 5 2 103.46 90.75 1.26 o 2 5 2 0.54 1.74 0.17 o 3 5 2 12.57 13.15 0.38 o 0 6 2 46.76 50.53 0.92 o 1 6 2 2.45 2.66 0.20 o 0 7 2 15.00 14.75 0.39 o 2 -10 3 3.86 4.49 0.21 o 3 -10 3 2.25 3.20 0.18 o 4 -10 3 13.61 8.82 0.26 o 5 -10 3 8.38 9.80 0.28 o 6 -10 3 29.97 28.24 0.56 o 7 -10 3 15.35 16.73 0.40 o 0 -9 3 19.18 18.60 0.43 o 1 -9 3 1.47 1.60 0.17 o 2 -9 3 123.48 115.89 1.30 o 3 -9 3 7.20 7.09 0.25 o 4 -9 3 59.79 59.83 0.97 o 5 -9 3 82.70 94.06 1.19 o 6 -9 3 0.13 0.59 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17.26 0.49 o 3 2 6 3.01 3.73 0.19 o 0 3 6 13.67 12.17 0.35 o 1 3 6 4.34 2.61 0.20 o 2 3 6 12.41 12.98 0.35 o 0 4 6 5.97 6.12 0.23 o 1 4 6 1.59 1.57 0.16 o 0 5 6 14.42 12.08 0.34 o 3 -10 7 7.43 8.53 0.27 o 0 -9 7 3.04 4.25 0.21 o 1 -9 7 4.70 5.50 0.22 o 2 -9 7 72.88 69.90 0.93 o 3 -9 7 49.03 43.18 0.75 o 4 -9 7 24.54 26.36 0.59 o 5 -9 7 41.90 43.46 0.68 o 0 -8 7 50.39 51.99 0.87 o 1 -8 7 25.78 27.22 0.66 o 2 -8 7 154.96 138.35 1.49 o 3 -8 7 15.52 15.09 0.46 o 4 -8 7 7.89 9.08 0.28 o 5 -8 7 0.83 1.68 0.17 o 6 -8 7 8.44 7.70 0.24 o 0 -7 7 25.84 23.53 0.65 o 1 -7 7 26.94 32.32 0.75 o 2 -7 7 6.55 7.51 0.27 o 3 -7 7 173.64 161.30 1.64 o 4 -7 7 11.52 12.84 0.39 o 5 -7 7 13.12 11.02 0.34 o 6 -7 7 77.15 87.03 0.94 o 0 -6 7 153.45 145.18 1.52 o 1 -6 7 37.42 34.19 0.77 o 2 -6 7 151.15 143.70 1.51 o 3 -6 7 28.00 25.61 0.69 o 4 -6 7 58.47 66.17 1.07 o 5 -6 7 11.74 10.48 0.31 o 6 -6 7 3.25 4.10 0.19 o 0 -5 7 122.35 107.53 1.25 o 1 -5 7 13.25 12.35 0.36 o 2 -5 7 173.36 163.16 1.58 o 3 -5 7 186.64 190.34 1.79 o 4 -5 7 5.23 6.05 0.25 o 5 -5 7 148.93 150.75 1.45 o 6 -5 7 7.56 9.01 0.27 o 0 -4 7 179.24 168.85 1.46 o 1 -4 7 31.80 29.54 0.65 o 2 -4 7 116.34 119.06 1.35 o 3 -4 7 116.63 139.64 1.52 o 4 -4 7 18.25 20.58 0.53 o 5 -4 7 9.33 10.84 0.33 o 0 -3 7 22.37 24.56 0.57 o 1 -3 7 49.54 40.35 0.75 o 2 -3 7 58.68 56.10 0.92 o 3 -3 7 50.24 52.80 0.96 o 4 -3 7 3.11 3.96 0.21 o 5 -3 7 3.41 3.47 0.19 o 0 -2 7 194.55 188.15 1.50 o 1 -2 7 48.12 46.23 0.80 o 2 -2 7 187.41 188.01 1.70 o 3 -2 7 13.09 18.14 0.51 o 4 -2 7 20.40 17.55 0.47 o 5 -2 7 25.20 22.52 0.47 o 0 -1 7 20.12 26.46 0.59 o 1 -1 7 60.97 50.71 0.88 o 2 -1 7 29.33 33.18 0.76 o 3 -1 7 11.15 10.76 0.34 o 4 -1 7 4.55 4.72 0.22 o 0 0 7 0.40 0.03 0.11 o 1 0 7 85.28 76.82 1.10 o 2 0 7 24.79 17.16 0.50 o 3 0 7 12.91 11.59 0.35 o 0 1 7 145.45 119.94 1.35 o 1 1 7 78.28 68.93 1.07 o 2 1 7 1.88 2.29 0.18 o 3 1 7 5.81 4.49 0.19 o 0 2 7 39.96 35.84 0.79 o 1 2 7 5.08 4.01 0.21 o 2 2 7 18.19 15.51 0.44 o 0 3 7 7.92 5.98 0.23 o 1 3 7 5.84 5.02 0.21 o 0 4 7 14.17 15.34 0.44 o 0 -9 8 17.47 16.62 0.40 o 1 -9 8 27.81 22.39 0.50 o 2 -9 8 14.73 12.76 0.36 o 3 -9 8 0.64 0.91 0.16 o 4 -9 8 27.69 24.29 0.51 o 0 -8 8 2.66 2.59 0.19 o 1 -8 8 11.46 10.17 0.31 o 2 -8 8 10.23 7.95 0.26 o 3 -8 8 0.53 0.11 0.17 o 4 -8 8 33.22 29.55 0.62 o 5 -8 8 16.31 15.76 0.41 o 0 -7 8 4.39 4.56 0.23 o 1 -7 8 109.53 103.77 1.29 o 2 -7 8 47.80 45.69 0.87 o 3 -7 8 99.57 86.72 1.17 o 4 -7 8 94.76 89.38 1.11 o 5 -7 8 1.39 0.20 0.18 o 0 -6 8 25.21 27.30 0.70 o 1 -6 8 187.50 183.43 1.75 o 2 -6 8 13.47 13.88 0.40 o 3 -6 8 32.52 34.00 0.77 o 4 -6 8 166.46 163.48 1.54 o 5 -6 8 23.39 27.45 0.57 o 0 -5 8 5.51 5.37 0.22 o 1 -5 8 104.09 97.91 1.25 o 2 -5 8 0.74 1.70 0.18 o 3 -5 8 10.84 9.09 0.29 o 4 -5 8 3.78 3.81 0.22 o 5 -5 8 8.54 7.00 0.23 o 0 -4 8 195.43 172.37 1.62 o 1 -4 8 135.08 120.60 1.39 o 2 -4 8 1.83 0.55 0.24 o 3 -4 8 27.07 29.56 0.73 o 4 -4 8 9.35 7.45 0.24 o 5 -4 8 1.12 1.90 0.16 o 0 -3 8 26.04 20.97 0.58 o 1 -3 8 87.64 91.49 1.18 o 2 -3 8 12.73 14.30 0.44 o 3 -3 8 53.44 48.66 0.90 o 4 -3 8 63.96 62.20 0.90 o 0 -2 8 342.97 313.53 2.15 o 1 -2 8 280.44 223.59 1.86 o 2 -2 8 17.05 23.14 0.65 o 3 -2 8 1.00 0.62 0.21 o 4 -2 8 14.69 15.44 0.44 o 0 -1 8 9.47 5.23 0.22 o 1 -1 8 89.95 85.15 1.19 o 2 -1 8 108.59 99.49 1.26 o 3 -1 8 57.65 53.80 0.84 o 0 0 8 96.45 80.80 1.13 o 1 0 8 16.49 16.08 0.48 o 2 0 8 3.13 3.41 0.19 o 3 0 8 14.91 11.87 0.31 o 0 1 8 9.14 9.55 0.29 o 1 1 8 1.33 1.97 0.17 o 2 1 8 29.29 28.93 0.57 o 0 2 8 35.73 33.02 0.72 o 1 2 8 0.72 1.29 0.16 o 0 3 8 0.46 -0.11 0.15 o 1 -9 9 0.14 0.28 0.16 o 2 -9 9 1.32 1.39 0.15 o 0 -8 9 37.15 31.89 0.63 o 1 -8 9 15.75 15.75 0.41 o 2 -8 9 122.83 114.19 1.17 o 3 -8 9 40.92 42.92 0.71 o 4 -8 9 0.66 0.38 0.17 o 0 -7 9 75.47 74.44 1.04 o 1 -7 9 30.81 29.21 0.68 o 2 -7 9 35.89 30.32 0.71 o 3 -7 9 53.10 44.04 0.78 o 4 -7 9 0.16 1.50 0.16 o 0 -6 9 11.73 11.13 0.33 o 1 -6 9 42.04 37.62 0.81 o 2 -6 9 45.55 48.32 0.87 o 3 -6 9 1.37 2.53 0.19 o 4 -6 9 1.41 1.29 0.16 o 0 -5 9 17.79 16.76 0.49 o 1 -5 9 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10 24.22 21.10 0.56 o 3 -5 10 29.70 29.16 0.56 o 0 -4 10 157.85 162.18 1.61 o 1 -4 10 30.48 31.85 0.73 o 2 -4 10 135.17 131.30 1.32 o 3 -4 10 26.30 22.02 0.48 o 0 -3 10 55.18 65.44 1.02 o 1 -3 10 24.91 27.67 0.68 o 2 -3 10 5.66 4.96 0.22 o 3 -3 10 2.88 1.75 0.16 o 0 -2 10 85.50 65.78 1.02 o 1 -2 10 52.34 39.06 0.73 o 2 -2 10 9.41 10.79 0.32 o 0 -1 10 4.16 6.78 0.25 o 1 -1 10 4.97 5.04 0.22 o 0 0 10 4.69 2.95 0.19 o 1 0 10 3.75 3.29 0.19 o 0 1 10 5.82 4.45 0.19 o 0 -7 11 10.36 10.45 0.30 o 1 -7 11 35.91 32.37 0.57 o 0 -6 11 7.44 7.81 0.25 o 1 -6 11 57.58 52.38 0.77 o 2 -6 11 16.90 18.07 0.41 o 0 -5 11 0.87 1.00 0.16 o 1 -5 11 51.59 55.07 0.81 o 2 -5 11 26.02 26.74 0.52 o 0 -4 11 9.41 8.58 0.25 o 1 -4 11 4.31 3.45 0.19 o 2 -4 11 3.50 5.46 0.21 o 0 -3 11 78.40 69.37 0.95 o 1 -3 11 11.46 14.72 0.37 o 0 -2 11 1.55 0.37 0.21 o 1 -2 11 29.18 24.16 0.49 o 0 -1 11 24.55 21.67 0.49 o 0 0 11 33.37 27.96 0.48 o 0 -5 12 14.61 14.18 0.38 o 0 -4 12 10.75 7.61 0.22 o 0 -3 12 11.07 10.92 0.29 o