#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:52:33 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180925 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/05/2200501.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200501_Fobs loop_ _publ_author_name 'Srinivasan, N.' 'Sridhar, B.' 'Rajaram, R. K.' _publ_section_title ; Bis(DL-aspartic acid) sulfate ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o679 _journal_page_last o681 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.660 _cell_angle_gamma 90.000 _cell_length_a 16.7738 _cell_length_b 5.9697 _cell_length_c 14.5276 _exptl_crystal_F_000 760.00 _reflns_d_resolution_high 0.8419 _cod_data_source_file ob6050Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ASSUL' _shelx_refln_list_code 4 _shelx_f_calc_maximum 218.74 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3353.45 3805.69 32.96 o 3 0 0 330.20 369.86 4.23 o 4 0 0 1307.98 1596.97 9.82 o 5 0 0 1457.76 1712.03 15.12 o 6 0 0 5289.77 5724.12 22.99 o 7 0 0 6918.18 7737.67 54.29 o 8 0 0 130.39 163.83 4.06 o 9 0 0 6562.18 7184.11 32.32 o 10 0 0 304.43 288.39 9.06 o 11 0 0 5456.13 5643.42 32.44 o 12 0 0 1766.11 1827.54 21.15 o 13 0 0 60.54 51.00 2.98 o 14 0 0 299.61 302.17 7.29 o 15 0 0 17.33 26.94 7.89 o 16 0 0 174.42 180.38 4.27 o 17 0 0 31.79 29.53 3.75 o 18 0 0 78.16 61.98 4.02 o 19 0 0 776.50 775.05 26.30 o 1 1 0 165.66 210.69 3.59 o 2 1 0 788.04 825.07 13.28 o 3 1 0 8823.19 9091.88 131.69 o 4 1 0 169.64 181.92 4.74 o 5 1 0 4723.42 4919.49 20.46 o 6 1 0 993.80 1032.90 10.30 o 7 1 0 844.42 879.06 10.28 o 8 1 0 1692.79 1850.74 21.50 o 9 1 0 1837.33 2120.45 19.75 o 10 1 0 2521.04 2682.18 33.74 o 11 1 0 34.79 34.24 2.15 o 12 1 0 930.53 965.87 14.78 o 13 1 0 106.09 99.78 6.15 o 14 1 0 1044.89 1086.42 39.75 o 15 1 0 1124.16 1101.02 18.81 o 16 1 0 192.25 200.21 9.70 o 17 1 0 4.38 0.00 0.12 o 18 1 0 116.57 114.27 4.32 o 19 1 0 92.82 82.50 4.19 o 0 2 0 6839.44 7035.04 32.16 o 1 2 0 1689.62 1685.70 26.74 o 2 2 0 6520.12 6525.42 134.73 o 3 2 0 740.55 833.25 15.82 o 4 2 0 131.01 125.69 8.61 o 5 2 0 165.65 200.74 14.78 o 6 2 0 3053.72 3353.78 56.49 o 7 2 0 93.30 132.44 3.12 o 8 2 0 639.98 736.17 12.77 o 9 2 0 529.07 613.52 13.17 o 10 2 0 26.35 24.87 2.39 o 11 2 0 125.17 123.18 4.27 o 12 2 0 197.27 165.15 5.95 o 13 2 0 474.62 478.39 10.17 o 14 2 0 238.28 204.97 5.26 o 15 2 0 188.35 200.22 9.40 o 16 2 0 12.61 0.37 7.09 o 17 2 0 10.48 7.00 5.41 o 18 2 0 63.05 66.38 3.60 o 1 3 0 9.88 42.70 5.61 o 2 3 0 4.20 9.23 1.12 o 3 3 0 1108.43 1078.81 26.47 o 4 3 0 399.37 391.07 12.20 o 5 3 0 1388.71 1378.12 26.34 o 6 3 0 106.50 104.80 6.11 o 7 3 0 2977.45 3003.98 58.14 o 8 3 0 352.34 353.47 7.44 o 9 3 0 558.65 546.22 10.75 o 10 3 0 339.23 356.77 8.00 o 11 3 0 0.31 0.00 0.12 o 12 3 0 366.57 369.66 8.54 o 13 3 0 155.34 159.43 3.92 o 14 3 0 3.85 0.36 7.39 o 15 3 0 145.80 126.29 4.79 o 16 3 0 315.87 307.30 7.08 o 17 3 0 19.54 16.19 3.64 o 0 4 0 680.27 729.69 15.75 o 1 4 0 73.53 77.61 3.52 o 2 4 0 2323.74 2449.15 20.06 o 3 4 0 2814.00 2836.73 92.61 o 4 4 0 12.01 17.85 2.18 o 5 4 0 12.73 22.85 1.68 o 6 4 0 958.99 947.51 28.02 o 7 4 0 303.04 258.14 7.59 o 8 4 0 722.38 693.97 13.05 o 9 4 0 339.67 322.80 31.22 o 10 4 0 601.90 568.10 15.03 o 11 4 0 17.87 24.01 2.86 o 12 4 0 199.09 200.27 8.56 o 13 4 0 823.71 814.15 24.23 o 14 4 0 25.10 21.20 5.38 o 15 4 0 202.32 231.20 5.56 o 16 4 0 0.78 0.12 2.55 o 1 5 0 106.07 108.12 3.00 o 2 5 0 206.81 215.10 4.88 o 3 5 0 234.88 226.37 5.24 o 4 5 0 1087.44 1052.23 22.42 o 5 5 0 797.22 777.48 35.57 o 6 5 0 298.75 341.98 8.05 o 7 5 0 144.24 145.04 3.73 o 8 5 0 137.25 127.90 3.59 o 9 5 0 9.13 11.44 4.96 o 10 5 0 211.65 213.85 5.09 o 11 5 0 82.38 67.66 3.36 o 12 5 0 0.24 3.48 4.30 o 13 5 0 1.79 7.59 4.46 o 0 6 0 3.74 6.04 6.04 o 1 6 0 5.60 0.46 8.33 o 2 6 0 153.05 141.63 3.88 o 3 6 0 109.37 104.54 3.55 o 4 6 0 75.38 61.62 5.81 o 5 6 0 131.58 129.65 3.79 o 6 6 0 27.98 26.63 3.31 o 7 6 0 72.71 82.38 3.51 o 8 6 0 39.46 42.58 4.94 o 9 6 0 2.73 0.08 1.58 o 10 6 0 0.17 0.14 2.66 o 1 7 0 51.57 62.98 3.43 o 2 7 0 0.07 0.26 4.41 o 3 7 0 74.61 74.73 3.80 o -19 1 1 40.20 33.87 4.73 o -18 1 1 158.22 158.72 6.57 o -17 1 1 1.86 13.36 6.51 o -16 1 1 550.96 575.20 17.39 o -15 1 1 3009.95 2921.58 41.38 o -14 1 1 65.97 68.99 4.19 o -13 1 1 533.39 517.59 16.08 o -12 1 1 3.15 5.22 3.95 o -11 1 1 330.85 341.05 10.58 o -10 1 1 142.63 162.96 5.52 o -9 1 1 2202.71 2385.86 27.10 o -8 1 1 1888.66 2019.51 23.26 o -7 1 1 714.18 629.12 12.28 o -6 1 1 1647.63 1812.98 19.01 o -4 1 1 1273.01 1402.18 14.14 o -3 1 1 1041.71 1172.69 11.73 o -2 1 1 2.02 4.84 1.90 o -1 1 1 2749.46 2759.05 14.93 o 0 1 1 45.81 40.74 1.27 o 1 1 1 1568.99 1738.74 12.12 o 2 1 1 956.86 1005.66 10.18 o 3 1 1 19930.01 19975.71 13.24 o 4 1 1 1.14 1.87 2.15 o 5 1 1 303.82 227.95 6.76 o 6 1 1 162.30 155.19 4.82 o 7 1 1 276.04 221.06 6.86 o 8 1 1 223.29 273.11 7.91 o 9 1 1 580.12 672.51 15.00 o 10 1 1 381.29 478.45 13.32 o 11 1 1 1933.26 1988.96 27.87 o 12 1 1 1489.61 1568.58 26.40 o 13 1 1 81.79 86.03 4.14 o 14 1 1 629.96 623.37 19.05 o 15 1 1 1056.73 1068.56 26.17 o 16 1 1 11.81 7.18 6.72 o 17 1 1 46.94 51.95 4.57 o 18 1 1 140.77 129.35 7.07 o 19 1 1 345.27 342.34 11.38 o -19 2 1 36.72 37.00 4.66 o -18 2 1 40.95 27.29 9.20 o -17 2 1 0.96 0.00 0.17 o -16 2 1 140.85 116.59 5.76 o -15 2 1 984.36 993.19 25.53 o -14 2 1 5.63 15.49 5.80 o -13 2 1 1090.30 1162.67 24.79 o -12 2 1 849.31 808.44 20.01 o -11 2 1 349.54 404.97 11.56 o -10 2 1 146.98 156.05 5.03 o -9 2 1 1990.37 2025.05 26.51 o -8 2 1 88.24 75.19 2.79 o -7 2 1 298.77 288.98 8.21 o -6 2 1 686.74 610.42 12.47 o -5 2 1 168.46 107.19 3.39 o -4 2 1 59.84 49.20 1.94 o -3 2 1 281.60 329.87 7.86 o -2 2 1 437.15 414.84 8.36 o -1 2 1 107.93 99.16 3.20 o 0 2 1 10286.42 9767.90 38.26 o 1 2 1 3065.37 2962.93 21.51 o 2 2 1 2728.84 2666.39 21.08 o 3 2 1 340.06 391.54 8.66 o 4 2 1 1838.91 1894.77 19.66 o 5 2 1 2.12 1.73 3.06 o 6 2 1 197.82 186.22 6.36 o 7 2 1 284.05 274.21 8.08 o 8 2 1 732.16 711.74 15.23 o 9 2 1 1065.08 1075.28 19.75 o 10 2 1 2589.69 2756.78 32.69 o 11 2 1 337.77 330.74 10.95 o 12 2 1 491.58 510.35 16.01 o 13 2 1 323.28 325.70 10.76 o 14 2 1 572.38 555.80 16.13 o 15 2 1 18.35 22.93 3.82 o 16 2 1 23.57 20.67 6.95 o 17 2 1 399.23 370.97 11.84 o 18 2 1 0.75 0.00 0.17 o -17 3 1 48.60 57.46 4.84 o -16 3 1 136.86 116.83 5.92 o -15 3 1 39.87 42.19 3.86 o -14 3 1 129.88 131.22 5.54 o -13 3 1 67.49 72.13 4.35 o -12 3 1 108.49 97.43 4.42 o -11 3 1 278.33 252.15 8.50 o -10 3 1 162.74 175.92 5.97 o -9 3 1 202.99 223.33 7.35 o -8 3 1 0.98 0.68 3.61 o -7 3 1 77.62 77.18 2.92 o -6 3 1 132.34 128.72 4.37 o -5 3 1 139.35 115.05 3.67 o -4 3 1 289.99 259.77 7.49 o -3 3 1 57.02 38.41 2.03 o -2 3 1 1.14 2.53 2.79 o -1 3 1 543.93 551.26 11.79 o 0 3 1 7083.89 7609.17 41.92 o 1 3 1 310.13 317.67 9.04 o 2 3 1 370.69 302.09 8.96 o 3 3 1 122.28 122.86 3.86 o 4 3 1 18.50 16.75 1.89 o 5 3 1 5962.32 5983.51 41.82 o 6 3 1 392.60 383.23 11.75 o 7 3 1 881.30 968.98 18.54 o 8 3 1 149.77 185.78 6.02 o 9 3 1 1518.39 1617.54 25.96 o 10 3 1 5.23 7.09 4.54 o 11 3 1 23.01 30.00 3.02 o 12 3 1 125.22 127.26 4.89 o 13 3 1 14.85 8.52 6.62 o 14 3 1 1236.72 1207.21 28.46 o 15 3 1 117.58 127.53 5.73 o 16 3 1 98.66 92.37 5.54 o 17 3 1 263.91 272.90 9.34 o -16 4 1 31.67 33.07 4.54 o -15 4 1 40.20 33.61 4.47 o -14 4 1 179.65 149.83 6.18 o -13 4 1 1145.03 1042.87 27.06 o -12 4 1 106.31 85.14 4.91 o -11 4 1 47.71 48.21 3.75 o -10 4 1 2.30 3.32 4.96 o -9 4 1 64.32 65.22 3.72 o -8 4 1 221.96 218.45 6.70 o -7 4 1 4.77 2.34 5.15 o -6 4 1 0.20 0.00 0.17 o -5 4 1 149.47 139.25 4.92 o -4 4 1 722.14 638.48 15.63 o -3 4 1 1293.78 1250.18 21.06 o -2 4 1 106.58 95.65 3.46 o -1 4 1 1572.01 1661.65 23.47 o 0 4 1 29.00 11.31 4.98 o 1 4 1 25.24 33.00 2.43 o 2 4 1 97.18 106.06 3.79 o 3 4 1 192.86 186.85 6.22 o 4 4 1 9.40 5.41 4.57 o 5 4 1 17.07 15.24 4.85 o 6 4 1 298.47 285.22 10.07 o 7 4 1 1.50 3.98 5.22 o 8 4 1 187.02 194.15 6.46 o 9 4 1 1065.90 1054.01 22.82 o 10 4 1 336.40 333.31 10.06 o 11 4 1 189.55 192.96 5.87 o 12 4 1 99.55 110.61 5.26 o 13 4 1 26.05 22.75 7.53 o 14 4 1 31.69 47.63 4.30 o 15 4 1 123.51 137.99 6.36 o 16 4 1 5.10 0.00 0.17 o -14 5 1 90.49 86.61 5.69 o -13 5 1 139.93 142.22 6.48 o -12 5 1 4.73 6.30 6.67 o -11 5 1 41.26 48.05 4.37 o -10 5 1 767.14 715.71 22.21 o -9 5 1 325.89 317.86 10.62 o -8 5 1 592.39 552.57 16.26 o -7 5 1 870.13 851.59 22.51 o -6 5 1 223.20 196.23 6.30 o -5 5 1 931.03 888.27 21.48 o -4 5 1 158.01 147.34 4.94 o -3 5 1 928.82 896.13 20.66 o -2 5 1 65.22 55.86 3.72 o -1 5 1 224.86 225.11 7.14 o 0 5 1 4.06 4.40 5.26 o 1 5 1 557.49 541.18 15.92 o 2 5 1 43.05 56.89 3.42 o 3 5 1 794.38 798.71 19.47 o 4 5 1 139.61 166.79 5.62 o 5 5 1 279.66 287.91 9.59 o 6 5 1 801.46 815.98 20.71 o 7 5 1 92.57 104.84 4.71 o 8 5 1 106.49 125.74 5.01 o 9 5 1 95.75 79.81 4.59 o 10 5 1 33.27 14.84 8.19 o 11 5 1 232.14 242.11 7.44 o 12 5 1 164.07 159.14 6.83 o 13 5 1 55.32 52.82 4.94 o -10 6 1 52.74 42.95 4.96 o -9 6 1 14.16 16.43 6.81 o -8 6 1 21.50 22.40 7.44 o -7 6 1 306.18 290.18 9.64 o -6 6 1 50.58 51.27 4.05 o -5 6 1 19.90 31.73 3.54 o -4 6 1 264.50 249.71 7.81 o -3 6 1 575.06 566.73 16.85 o -2 6 1 229.56 226.50 7.35 o -1 6 1 98.67 88.86 4.85 o 0 6 1 617.66 632.29 19.54 o 1 6 1 265.23 260.59 8.87 o 2 6 1 380.07 398.82 13.93 o 3 6 1 314.42 328.86 11.23 o 4 6 1 229.51 242.32 8.08 o 5 6 1 53.03 59.26 4.10 o 6 6 1 185.74 190.66 6.79 o 7 6 1 229.82 221.49 7.21 o 8 6 1 387.72 387.65 12.34 o 9 6 1 20.03 14.77 8.59 o 10 6 1 106.71 103.07 5.80 o -3 7 1 42.52 37.23 4.38 o -2 7 1 7.42 8.24 7.14 o -1 7 1 28.76 5.66 7.79 o 0 7 1 0.46 0.00 0.17 o 1 7 1 0.02 6.30 6.67 o 2 7 1 19.32 24.97 4.23 o -19 0 2 62.36 76.58 5.26 o -18 0 2 41.34 40.68 4.40 o -17 0 2 171.69 169.27 6.27 o -16 0 2 1399.18 1354.43 29.79 o -15 0 2 2666.15 2656.21 38.90 o -14 0 2 1125.46 1149.12 24.95 o -13 0 2 479.14 515.74 16.27 o -12 0 2 1559.76 1593.69 25.89 o -11 0 2 1700.46 1790.90 26.02 o -10 0 2 108.60 118.65 3.74 o -9 0 2 132.40 148.77 5.10 o -8 0 2 96.30 57.45 2.34 o -7 0 2 457.38 423.93 9.90 o -6 0 2 206.73 154.25 5.01 o -5 0 2 6879.88 7004.69 32.72 o -4 0 2 33147.04 32644.06 16.92 o -3 0 2 4974.89 4988.31 21.76 o -2 0 2 538.84 389.08 5.45 o -1 0 2 108.13 116.01 2.79 o 0 0 2 2468.57 2223.11 10.62 o 1 0 2 52.45 48.89 1.66 o 3 0 2 91.13 92.07 3.09 o 4 0 2 23840.17 22532.29 14.93 o 5 0 2 1608.44 1716.88 17.15 o 7 0 2 2052.44 2171.89 22.65 o 8 0 2 6776.97 7087.13 43.81 o 9 0 2 113.19 137.85 4.54 o 10 0 2 45.62 52.98 2.65 o 11 0 2 122.75 131.25 4.52 o 12 0 2 537.31 598.79 16.76 o 13 0 2 229.95 243.60 7.87 o 14 0 2 8319.98 8023.36 65.74 o 15 0 2 1403.83 1369.36 29.42 o 16 0 2 68.85 73.95 4.49 o 17 0 2 992.68 1014.64 27.95 o 18 0 2 0.27 7.79 6.90 o 19 0 2 931.24 890.98 28.81 o -19 1 2 0.88 2.23 7.18 o -18 1 2 24.80 19.94 7.68 o -17 1 2 6.14 15.84 7.30 o -16 1 2 1.14 7.56 6.55 o -14 1 2 163.10 188.74 6.44 o -13 1 2 85.35 102.11 4.19 o -12 1 2 138.26 145.10 4.80 o -11 1 2 0.08 0.00 0.17 o -10 1 2 216.41 232.84 7.42 o -9 1 2 345.53 425.89 11.72 o -8 1 2 445.84 473.14 11.66 o -7 1 2 1260.13 1430.66 18.28 o -6 1 2 3938.46 4110.13 28.78 o -5 1 2 711.25 620.33 10.56 o -4 1 2 5365.45 5501.06 28.23 o -3 1 2 1182.19 1004.46 11.23 o -2 1 2 1824.44 1720.41 13.43 o -1 1 2 19429.35 18881.99 11.17 o 0 1 2 2261.85 2156.37 13.97 o 1 1 2 979.96 735.10 8.66 o 2 1 2 1420.94 1329.86 12.40 o 3 1 2 2913.65 3120.07 20.62 o 4 1 2 50.51 44.21 1.66 o 5 1 2 13715.35 14734.61 14.14 o 6 1 2 961.13 1023.05 15.14 o 7 1 2 3262.36 3494.54 29.56 o 8 1 2 1272.68 1303.51 19.38 o 9 1 2 473.79 520.00 13.25 o 10 1 2 316.14 335.69 10.06 o 11 1 2 182.55 171.29 5.40 o 12 1 2 1697.35 1840.63 29.25 o 13 1 2 40.54 39.78 3.54 o 14 1 2 360.22 377.05 11.87 o 15 1 2 172.42 175.22 5.80 o 16 1 2 160.26 147.11 5.94 o 17 1 2 104.38 109.62 5.66 o 18 1 2 35.33 38.19 4.59 o 19 1 2 96.52 106.48 6.32 o -19 2 2 3.56 0.00 0.17 o -18 2 2 1.55 0.00 0.17 o -17 2 2 162.67 173.56 6.48 o -16 2 2 570.69 584.36 18.16 o -15 2 2 107.36 115.24 5.20 o -14 2 2 114.76 118.37 4.85 o -13 2 2 296.88 303.31 10.34 o -12 2 2 230.71 201.36 7.23 o -11 2 2 186.69 172.04 5.48 o -10 2 2 2081.43 2335.43 30.02 o -9 2 2 147.05 178.76 6.01 o -8 2 2 1096.23 1123.47 18.74 o -7 2 2 184.65 186.06 5.64 o -6 2 2 2841.01 3077.38 27.57 o -5 2 2 1073.36 1087.22 15.63 o -4 2 2 5048.32 4887.05 31.20 o -3 2 2 496.10 493.66 9.74 o -2 2 2 66.84 61.20 2.10 o -1 2 2 425.52 462.12 8.77 o 0 2 2 5329.07 5639.18 30.00 o 1 2 2 2.40 2.06 2.20 o 2 2 2 1136.39 1293.96 15.21 o 3 2 2 1759.95 1844.29 18.95 o 4 2 2 1168.35 1110.18 15.49 o 5 2 2 1122.46 1225.39 17.13 o 6 2 2 1485.00 1559.80 20.39 o 7 2 2 5.05 0.84 3.23 o 8 2 2 418.24 415.08 11.94 o 9 2 2 107.30 98.04 3.35 o 10 2 2 312.87 312.95 10.56 o 11 2 2 17.08 6.60 4.71 o 12 2 2 39.24 37.91 3.42 o 13 2 2 154.13 166.30 5.40 o 14 2 2 600.60 583.06 19.03 o 15 2 2 19.63 21.74 6.93 o 16 2 2 10.28 5.74 6.53 o 17 2 2 262.83 260.92 8.97 o 18 2 2 57.44 63.70 5.40 o -18 3 2 1.46 0.00 0.17 o -17 3 2 35.72 39.72 4.85 o -16 3 2 134.33 133.14 6.22 o -15 3 2 6.90 0.61 6.84 o -14 3 2 281.99 265.60 8.64 o -13 3 2 396.22 390.08 12.34 o -12 3 2 1288.73 1218.55 25.35 o -11 3 2 377.52 381.42 12.33 o -10 3 2 1048.97 1037.53 21.49 o -9 3 2 241.77 251.49 8.52 o -8 3 2 557.29 590.63 15.31 o -7 3 2 0.08 0.00 0.17 o -6 3 2 60.17 72.74 2.92 o -5 3 2 1.04 1.38 3.42 o -4 3 2 20.71 23.00 1.85 o -3 3 2 336.49 358.47 9.94 o -2 3 2 734.89 652.36 13.13 o -1 3 2 2706.99 2686.57 25.53 o 0 3 2 440.80 407.61 10.34 o 1 3 2 218.91 161.76 5.40 o 2 3 2 1867.86 2090.09 23.05 o 3 3 2 480.20 451.16 11.26 o 4 3 2 3585.25 3846.38 32.76 o 5 3 2 473.34 468.69 12.40 o 6 3 2 525.48 577.71 14.32 o 7 3 2 492.64 499.92 14.07 o 8 3 2 225.94 218.96 7.28 o 9 3 2 141.28 133.33 4.38 o 10 3 2 476.46 536.09 16.13 o 11 3 2 1334.01 1336.58 26.44 o 12 3 2 1507.13 1482.05 28.72 o 13 3 2 511.04 526.36 15.73 o 14 3 2 284.19 284.05 9.06 o 15 3 2 109.47 115.38 5.59 o 16 3 2 0.24 0.00 0.17 o 17 3 2 39.83 28.74 9.64 o -16 4 2 9.05 0.00 0.17 o -15 4 2 276.52 268.81 9.03 o -14 4 2 0.13 0.00 0.17 o -13 4 2 190.67 200.49 6.48 o -12 4 2 18.56 14.74 6.62 o -11 4 2 345.07 351.56 11.65 o -10 4 2 255.24 228.62 7.37 o -9 4 2 7.64 16.47 5.88 o -8 4 2 27.41 34.03 3.09 o -7 4 2 619.08 638.67 16.99 o -6 4 2 108.75 96.94 3.67 o -5 4 2 1270.57 1262.93 22.44 o -4 4 2 132.20 122.37 3.96 o -3 4 2 13.42 23.89 2.43 o -2 4 2 1426.49 1315.02 21.35 o -1 4 2 94.52 73.27 3.02 o 0 4 2 179.10 172.85 5.95 o 1 4 2 1940.44 1925.68 25.62 o 2 4 2 2931.53 2991.96 32.02 o 3 4 2 29.33 33.32 2.53 o 4 4 2 670.54 684.24 16.17 o 5 4 2 1.64 0.00 0.17 o 6 4 2 1452.56 1573.28 25.30 o 7 4 2 436.58 412.72 12.28 o 8 4 2 99.91 109.81 4.35 o 9 4 2 656.08 627.34 18.19 o 10 4 2 291.90 300.96 9.76 o 11 4 2 2.11 0.52 5.83 o 12 4 2 423.09 435.67 15.33 o 13 4 2 10.18 13.10 3.32 o 14 4 2 263.21 244.00 8.21 o 15 4 2 129.75 136.28 6.39 o -14 5 2 58.32 62.37 4.80 o -13 5 2 8.13 9.36 6.62 o -12 5 2 88.54 75.27 5.26 o -11 5 2 5.32 8.33 7.18 o -10 5 2 129.96 133.23 5.59 o 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