#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2200513.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200513_Fobs loop_ _publ_author_name 'Breneman, Gary L.' 'Howald, Carl W.' 'Parker, O. Jerry' _publ_section_title ; Second crystal form of dinitrito(1,10-phenanthroline)copper(II) ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m286 _journal_page_last m287 _journal_volume 57 _journal_year 2001 _space_group_IT_number 60 _symmetry_space_group_name_Hall '-P 2n 2ab' _symmetry_space_group_name_H-M 'P b c n' _exptl_absorpt_correction_type 'psi scan' _refine_ls_extinction_method none _[local]_cod_data_source_file om6023Isup2.hkl _[local]_cod_data_source_block I loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma 2 0 0 8370.03 8758.59 149.94 4 0 0 54.62 36.17 0.60 6 0 0 2174.99 1969.11 6.19 8 0 0 2694.76 2537.04 8.56 10 0 0 9.81 16.41 1.16 1 1 0 7551.26 7900.45 390.58 3 1 0 2719.99 3045.58 5.08 5 1 0 1232.41 1607.12 4.99 7 1 0 232.90 252.85 2.51 9 1 0 0.33 -0.40 1.11 0 2 0 4836.02 3738.88 18.53 2 2 0 22533.17 20475.81 3345.22 4 2 0 3851.41 4097.72 7.00 6 2 0 3449.55 3430.35 8.23 8 2 0 1808.21 1760.89 7.27 10 2 0 449.62 415.63 4.16 1 3 0 13.69 20.65 0.59 3 3 0 4695.31 5412.33 316.87 5 3 0 5013.93 4916.18 50.18 7 3 0 426.55 426.29 3.54 9 3 0 365.18 346.42 3.47 0 4 0 11618.66 9200.72 121.91 2 4 0 5387.99 5781.04 399.46 4 4 0 1895.21 1976.84 5.29 6 4 0 2175.25 2295.79 7.05 8 4 0 116.80 122.64 1.40 10 4 0 146.95 142.51 1.77 1 5 0 464.18 545.11 2.85 3 5 0 10714.31 11294.78 2109.13 5 5 0 6130.36 6057.72 299.42 7 5 0 1480.74 1495.31 6.45 9 5 0 246.34 250.71 2.50 0 6 0 841.05 927.52 4.25 2 6 0 5158.32 6284.09 35.29 4 6 0 204.26 236.57 2.36 6 6 0 31.25 33.24 0.95 8 6 0 189.12 190.12 1.86 10 6 0 2.88 3.79 1.23 1 7 0 430.77 390.79 3.00 3 7 0 16972.39 18789.38 3368.91 5 7 0 4673.21 4602.65 175.19 7 7 0 129.28 123.25 1.42 9 7 0 567.65 571.99 5.12 0 8 0 754.08 784.40 4.47 2 8 0 3941.70 4331.83 50.60 4 8 0 78.02 75.41 1.00 6 8 0 290.15 307.26 3.06 8 8 0 99.84 98.60 1.51 1 9 0 1563.39 1507.01 6.39 3 9 0 647.19 455.21 3.54 5 9 0 928.31 905.57 5.15 7 9 0 2151.53 2097.34 8.58 9 9 0 129.72 132.80 1.77 0 10 0 7579.55 7503.51 55.80 2 10 0 1245.00 1049.53 5.59 4 10 0 387.70 410.79 3.73 6 10 0 882.14 883.08 5.63 8 10 0 960.44 899.40 6.38 1 11 0 298.85 309.67 3.04 3 11 0 115.73 127.19 1.39 5 11 0 21.77 20.78 1.08 7 11 0 30.13 24.09 1.31 0 12 0 8091.87 8109.03 222.94 2 12 0 1707.23 1452.39 7.26 4 12 0 408.45 407.52 4.05 6 12 0 951.42 949.93 6.37 8 12 0 1119.45 1075.44 7.42 1 13 0 25.57 32.92 1.29 3 13 0 54.66 47.51 1.30 5 13 0 152.12 161.05 1.77 7 13 0 16.66 24.30 1.40 0 14 0 4568.24 4881.39 96.45 2 14 0 1105.14 1061.53 6.87 4 14 0 746.28 673.33 5.79 6 14 0 762.33 780.63 6.45 1 15 0 426.32 466.81 4.73 3 15 0 1025.96 922.51 6.81 5 15 0 192.78 220.80 2.25 0 16 0 10.28 10.48 1.24 2 16 0 1117.44 1046.43 7.33 4 16 0 593.84 504.77 5.03 1 17 0 666.44 730.79 6.28 3 17 0 1076.27 1084.60 7.80 0 18 0 47.81 39.31 1.49 2 18 0 17.42 26.90 1.47 1 19 0 484.65 522.04 5.17 1 1 1 17229.09 16617.27 285.96 2 1 1 4300.85 4967.69 105.16 3 1 1 1435.99 1430.66 3.74 4 1 1 604.32 651.72 2.98 5 1 1 1391.22 1322.04 4.68 6 1 1 96.47 117.67 1.19 7 1 1 3455.93 3439.96 9.24 8 1 1 10.53 11.58 1.05 9 1 1 771.59 730.31 5.29 10 1 1 15.35 12.60 1.15 0 2 1 9273.12 9464.64 111.39 1 2 1 245.90 286.45 2.06 2 2 1 135.08 125.99 1.25 3 2 1 1032.66 1088.87 3.42 4 2 1 1779.00 1757.16 4.82 5 2 1 6.40 7.92 0.66 6 2 1 443.64 432.39 3.26 7 2 1 0.64 -1.67 1.32 8 2 1 514.72 515.01 4.30 9 2 1 8.59 8.49 1.07 10 2 1 16.31 18.71 1.19 1 3 1 8637.24 8995.97 161.62 2 3 1 3403.52 3722.68 5.93 3 3 1 940.23 1024.02 3.48 4 3 1 45.98 42.11 0.73 5 3 1 2448.36 2598.12 6.70 6 3 1 9.11 13.46 0.78 7 3 1 1299.63 1254.59 5.84 8 3 1 49.96 46.47 1.20 9 3 1 196.30 194.94 1.93 10 3 1 0.18 -1.79 1.71 0 4 1 1250.67 1265.07 3.93 1 4 1 2263.34 2411.26 5.77 2 4 1 5836.40 6698.24 33.35 3 4 1 1895.67 2118.74 5.19 4 4 1 8802.36 9980.73 45.85 5 4 1 213.84 228.95 2.31 6 4 1 1149.72 1159.66 5.20 7 4 1 2.90 2.77 0.81 8 4 1 756.08 761.62 5.10 9 4 1 1.97 0.80 0.85 10 4 1 303.94 300.59 3.04 1 5 1 107.27 97.93 1.06 2 5 1 120.61 171.28 1.70 3 5 1 1952.98 2175.38 5.65 4 5 1 200.62 219.83 2.22 5 5 1 533.88 565.49 3.56 6 5 1 206.72 226.60 2.24 7 5 1 60.39 65.50 1.16 8 5 1 20.98 24.19 1.08 9 5 1 58.23 54.68 1.33 10 5 1 6.52 6.95 1.23 0 6 1 354.94 305.24 2.67 1 6 1 2461.67 2512.90 6.89 2 6 1 16628.28 17846.14 477.87 3 6 1 250.09 251.08 2.41 4 6 1 8833.88 9916.97 3352.07 5 6 1 2.18 3.37 0.73 6 6 1 1729.13 1722.34 6.70 7 6 1 163.24 156.06 1.58 8 6 1 8.37 7.30 1.01 9 6 1 85.51 85.29 1.47 10 6 1 461.39 450.64 4.45 1 7 1 955.15 1056.42 4.92 2 7 1 24.82 20.12 0.94 3 7 1 1511.07 1853.55 6.12 4 7 1 4.24 6.06 0.80 5 7 1 63.95 62.35 1.03 6 7 1 9.07 9.48 0.92 7 7 1 273.57 270.20 2.71 8 7 1 74.45 74.99 1.37 9 7 1 8.33 8.11 1.16 0 8 1 1690.62 1611.86 6.16 1 8 1 150.43 154.57 1.55 2 8 1 2670.52 2448.33 7.61 3 8 1 364.79 359.14 3.20 4 8 1 4238.29 4177.36 381.46 5 8 1 1.74 2.64 0.83 6 8 1 1719.69 1758.17 7.29 7 8 1 8.27 9.41 1.09 8 8 1 936.67 935.37 6.17 9 8 1 0.04 -1.55 1.62 1 9 1 1747.81 1718.86 6.88 2 9 1 228.61 199.35 1.97 3 9 1 631.26 625.01 4.38 4 9 1 3.78 3.84 0.86 5 9 1 810.19 788.73 5.06 6 9 1 110.40 107.58 1.46 7 9 1 870.79 838.41 5.76 8 9 1 2.18 -0.31 1.11 9 9 1 194.97 201.97 2.06 0 10 1 2272.95 2289.69 8.25 1 10 1 9.68 12.78 1.02 2 10 1 2111.13 1938.29 7.77 3 10 1 19.72 19.34 1.00 4 10 1 1345.70 1422.94 6.79 5 10 1 2.85 3.86 0.99 6 10 1 85.62 89.08 1.44 7 10 1 68.76 73.63 1.52 8 10 1 303.02 297.98 2.92 9 10 1 0.04 -0.73 1.43 1 11 1 4984.80 5148.08 54.11 2 11 1 423.57 420.03 4.16 3 11 1 856.79 799.11 5.49 4 11 1 21.45 27.63 1.11 5 11 1 1041.50 1079.68 6.47 6 11 1 48.84 49.64 1.34 7 11 1 1095.02 1119.00 7.09 8 11 1 2.70 -0.34 1.16 0 12 1 2143.24 2220.02 8.96 1 12 1 300.13 302.23 3.07 2 12 1 111.41 111.98 1.48 3 12 1 9.57 11.12 1.06 4 12 1 0.72 4.67 1.07 5 12 1 45.54 45.78 1.37 6 12 1 0.16 1.90 1.04 7 12 1 22.05 22.60 1.41 8 12 1 9.91 10.61 1.43 1 13 1 6503.32 6587.39 180.76 2 13 1 69.79 63.81 1.42 3 13 1 1026.13 927.23 6.41 4 13 1 13.36 9.48 1.16 5 13 1 244.61 285.56 2.85 6 13 1 44.96 37.48 1.42 7 13 1 815.20 782.73 6.57 0 14 1 3309.16 3613.21 12.13 1 14 1 101.30 72.61 2.15 2 14 1 99.35 111.22 1.64 3 14 1 25.17 24.92 1.34 4 14 1 37.72 52.60 1.44 5 14 1 38.90 30.98 1.42 6 14 1 0.59 3.54 1.22 7 14 1 1.79 0.69 1.08 1 15 1 200.72 204.04 2.04 2 15 1 20.16 18.41 1.30 3 15 1 747.49 664.01 5.97 4 15 1 30.20 26.17 1.42 5 15 1 1389.75 1178.76 8.06 6 15 1 24.12 18.04 1.51 0 16 1 30.93 33.70 1.37 1 16 1 87.12 92.79 1.83 2 16 1 508.08 517.23 5.14 3 16 1 8.73 7.85 1.31 4 16 1 1013.39 891.81 7.19 5 16 1 17.12 12.92 1.47 1 17 1 395.38 423.33 4.19 2 17 1 4.70 4.45 1.29 3 17 1 125.16 125.09 1.92 4 17 1 0.03 -3.29 1.70 0 18 1 336.63 356.66 3.56 1 18 1 6.15 5.07 1.38 2 18 1 681.38 706.41 6.48 3 18 1 0.05 -2.41 1.69 0 0 2 38826.23 38337.80 475.81 1 0 2 28369.17 21821.56 889.50 2 0 2 3657.70 3742.06 6.08 3 0 2 17.49 17.50 0.59 4 0 2 451.84 380.94 2.58 5 0 2 570.85 531.87 3.31 6 0 2 1239.66 1154.54 5.20 7 0 2 150.65 157.63 1.59 8 0 2 1155.74 1135.18 6.13 9 0 2 148.27 122.36 1.56 10 0 2 63.25 70.58 1.47 1 1 2 13171.56 11446.82 1700.01 2 1 2 30.66 23.69 0.70 3 1 2 33.53 24.19 0.64 4 1 2 1232.69 1445.24 4.70 5 1 2 246.28 305.43 2.66 6 1 2 291.13 340.44 3.10 7 1 2 88.90 81.49 1.20 8 1 2 14.70 18.37 1.10 9 1 2 0.42 2.94 1.01 10 1 2 0.45 2.63 1.05 0 2 2 542.68 697.85 2.72 1 2 2 2207.75 1962.39 5.69 2 2 2 812.56 770.72 3.33 3 2 2 28.14 23.84 0.65 4 2 2 3189.97 3313.61 7.14 5 2 2 166.69 170.01 1.70 6 2 2 2625.32 2637.53 7.82 7 2 2 52.04 56.93 1.11 8 2 2 858.21 833.36 5.40 9 2 2 0.45 -3.28 1.74 10 2 2 273.62 258.67 2.60 1 3 2 4663.54 3791.18 7.97 2 3 2 173.12 195.41 1.96 3 3 2 3214.11 3347.53 6.93 4 3 2 58.23 58.00 0.84 5 3 2 1384.90 1337.70 5.26 6 3 2 184.38 183.18 1.81 7 3 2 622.54 618.81 4.43 8 3 2 3.54 3.36 0.97 9 3 2 401.32 387.94 3.95 10 3 2 0.22 0.73 0.96 0 4 2 17.66 12.77 0.68 1 4 2 10.07 10.90 0.92 2 4 2 197.51 186.16 1.84 3 4 2 38.87 54.79 0.88 4 4 2 570.23 575.41 3.42 5 4 2 228.31 268.58 2.65 6 4 2 883.22 904.17 4.94 7 4 2 28.80 31.28 1.11 8 4 2 126.82 141.30 1.56 9 4 2 17.59 20.61 1.20 10 4 2 79.42 71.65 1.63 1 5 2 4751.52 4270.05 215.56 2 5 2 934.77 972.31 4.61 3 5 2 5937.78 6090.49 258.15 4 5 2 18.74 20.76 0.80 5 5 2 3063.65 3068.39 8.41 6 5 2 30.50 31.76 0.97 7 5 2 1193.18 1206.09 6.20 8 5 2 34.57 35.84 1.19 9 5 2 443.43 445.99 4.48 0 6 2 77.47 71.50 0.92 1 6 2 420.52 455.88 3.62 2 6 2 216.95 248.86 2.45 3 6 2 101.61 118.52 1.25 4 6 2 20.24 18.01 0.87 5 6 2 43.64 49.91 1.06 6 6 2 119.80 112.94 1.30 7 6 2 45.41 51.15 1.23 8 6 2 41.49 39.07 1.25 9 6 2 13.76 12.03 1.24 1 7 2 8632.41 8302.75 179.36 2 7 2 1327.04 1429.60 6.17 3 7 2 9715.25 11359.66 62.11 4 7 2 268.90 302.69 3.07 5 7 2 2439.45 2492.96 8.33 6 7 2 770.50 785.10 5.10 7 7 2 56.31 60.30 1.30 8 7 2 254.93 260.07 2.62 9 7 2 206.95 208.63 2.10 0 8 2 143.18 122.00 1.25 1 8 2 135.08 158.16 1.57 2 8 2 2945.46 3045.91 9.40 3 8 2 946.29 1035.84 5.68 4 8 2 1639.57 1815.78 7.33 5 8 2 91.68 94.98 1.34 6 8 2 72.02 74.49 1.38 7 8 2 162.48 162.30 1.72 8 8 2 37.26 34.38 1.35 9 8 2 55.07 50.06 1.52 1 9 2 3092.63 3034.97 9.64 2 9 2 141.03 174.47 1.75 3 9 2 1974.55 1739.81 7.61 4 9 2 0.07 1.35 0.88 5 9 2 1213.93 1241.17 6.61 6 9 2 82.09 84.38 1.49 7 9 2 1182.48 1158.73 6.95 8 9 2 143.15 142.70 1.80 9 9 2 269.52 273.95 2.77 0 10 2 2906.82 2680.21 9.19 1 10 2 217.63 236.35 2.38 2 10 2 1587.48 1475.90 7.23 3 10 2 11.60 6.51 1.02 4 10 2 1250.16 1232.19 6.88 5 10 2 2.65 2.01 1.03 6 10 2 1168.82 1206.31 7.09 7 10 2 19.14 16.16 1.30 8 10 2 449.71 461.58 4.69 1 11 2 667.63 685.88 5.23 2 11 2 19.38 13.19 1.13 3 11 2 712.81 643.83 5.27 4 11 2 31.31 34.96 1.34 5 11 2 240.19 253.57 2.54 6 11 2 2.31 3.10 1.16 7 11 2 60.71 63.27 1.54 8 11 2 29.97 34.07 1.51 0 12 2 3864.70 3826.93 12.02 1 12 2 213.29 231.44 2.32 2 12 2 1617.32 1680.24 8.22 3 12 2 25.17 23.92 1.26 4 12 2 820.33 787.88 6.03 5 12 2 27.44 26.25 1.32 6 12 2 808.69 801.25 6.43 7 12 2 28.94 31.96 1.47 1 13 2 4.72 6.22 1.26 2 13 2 8.13 6.26 1.23 3 13 2 60.29 60.66 1.47 4 13 2 36.24 31.67 1.39 5 13 2 8.37 5.89 1.21 6 13 2 0.45 1.96 1.19 7 13 2 26.08 26.84 1.50 0 14 2 2363.25 2491.77 10.51 1 14 2 164.67 179.49 1.99 2 14 2 1224.65 1308.60 7.73 3 14 2 0.33 0.95 0.96 4 14 2 560.16 517.19 5.10 5 14 2 9.21 9.98 1.29 6 14 2 458.84 449.87 4.50 1 15 2 445.45 501.83 5.01 2 15 2 49.96 48.67 1.52 3 15 2 116.12 113.90 1.77 4 15 2 16.30 12.30 1.37 5 15 2 67.35 68.77 1.68 6 15 2 8.93 4.89 1.44 0 16 2 378.13 416.16 4.09 1 16 2 202.24 201.94 2.20 2 16 2 489.15 527.72 5.23 3 16 2 4.49 3.49 1.28 4 16 2 277.94 259.81 2.58 5 16 2 0.01 -1.06 1.41 1 17 2 357.53 394.18 3.88 2 17 2 7.93 8.98 1.37 3 17 2 659.24 686.35 6.48 4 17 2 14.16 13.20 1.50 0 18 2 84.67 97.27 1.82 1 18 2 2.87 -2.86 1.88 2 18 2 22.81 22.70 1.58 1 1 3 10009.05 10353.69 1285.33 2 1 3 10.24 11.72 1.01 3 1 3 3351.51 3188.12 7.45 4 1 3 118.70 112.21 1.14 5 1 3 2377.83 2327.19 7.25 6 1 3 220.38 236.45 2.35 7 1 3 1252.61 1223.22 6.26 8 1 3 11.36 13.19 1.09 9 1 3 315.91 316.68 3.14 0 2 3 625.46 608.09 3.01 1 2 3 1399.68 1489.55 5.24 2 2 3 1239.71 1190.64 5.61 3 2 3 5.21 13.74 0.85 4 2 3 206.45 188.73 1.89 5 2 3 3.06 4.72 0.83 6 2 3 219.65 220.21 2.21 7 2 3 53.06 56.01 1.25 8 2 3 244.60 247.12 2.46 9 2 3 34.77 35.31 1.32 1 3 3 3668.62 3484.16 8.25 2 3 3 6.82 16.29 1.05 3 3 3 4362.17 4567.07 92.36 4 3 3 279.44 315.69 2.97 5 3 3 1457.91 1440.38 6.04 6 3 3 0.87 1.14 0.79 7 3 3 434.58 438.90 4.08 8 3 3 13.93 13.81 1.16 9 3 3 230.29 229.44 2.29 0 4 3 4104.14 4165.93 90.75 1 4 3 0.00 2.72 0.83 2 4 3 2229.31 1955.18 7.41 3 4 3 1.17 3.13 0.85 4 4 3 1080.97 1058.64 5.17 5 4 3 162.61 159.21 1.58 6 4 3 1411.79 1382.80 6.48 7 4 3 21.44 18.43 1.13 8 4 3 426.09 425.87 4.23 9 4 3 1.40 2.10 1.07 1 5 3 2095.30 2017.31 7.11 2 5 3 211.63 208.58 2.06 3 5 3 774.43 784.00 4.86 4 5 3 6.37 9.50 0.95 5 5 3 271.55 257.82 2.52 6 5 3 76.00 78.31 1.33 7 5 3 17.72 20.93 1.14 8 5 3 99.04 104.75 1.56 9 5 3 6.48 4.80 1.19 0 6 3 2213.36 2249.42 7.03 1 6 3 967.94 958.26 5.30 2 6 3 3764.37 3625.47 10.51 3 6 3 249.82 273.00 2.72 4 6 3 4086.05 4184.13 258.68 5 6 3 105.32 109.43 1.34 6 6 3 313.38 306.36 3.05 7 6 3 187.40 178.18 1.75 8 6 3 185.54 189.22 1.88 9 6 3 167.59 164.29 1.92 1 7 3 15.17 18.18 0.99 2 7 3 216.15 235.65 2.37 3 7 3 279.68 289.61 2.84 4 7 3 102.68 128.68 1.53 5 7 3 47.38 56.41 1.22 6 7 3 266.57 272.24 2.70 7 7 3 40.00 37.59 1.30 8 7 3 50.47 50.38 1.45 9 7 3 19.29 22.03 1.44 0 8 3 701.85 619.78 4.47 1 8 3 0.12 -0.18 0.61 2 8 3 1009.92 938.30 5.93 3 8 3 24.95 24.89 1.15 4 8 3 1264.26 1260.92 6.98 5 8 3 8.51 7.57 1.13 6 8 3 1185.31 1178.36 6.88 7 8 3 1.31 -1.15 1.44 8 8 3 542.48 556.69 5.41 1 9 3 215.24 187.60 1.89 2 9 3 30.04 28.76 1.19 3 9 3 378.28 315.69 3.17 4 9 3 30.52 24.25 1.23 5 9 3 673.43 687.42 5.60 6 9 3 1.02 2.61 1.16 7 9 3 382.52 387.33 3.88 8 9 3 14.00 11.63 1.35 0 10 3 753.00 713.77 5.27 1 10 3 1.04 2.03 0.98 2 10 3 603.62 617.62 5.17 3 10 3 0.02 -1.60 1.19 4 10 3 357.63 333.64 3.32 5 10 3 127.72 127.52 1.80 6 10 3 253.40 273.13 2.77 7 10 3 12.26 8.76 1.35 8 10 3 97.06 98.75 1.89 1 11 3 1141.41 1113.49 6.85 2 11 3 37.85 34.96 1.35 3 11 3 1179.92 1158.28 7.24 4 11 3 24.26 27.16 1.32 5 11 3 593.43 599.80 5.70 6 11 3 4.11 5.71 1.27 7 11 3 403.92 432.20 4.40 0 12 3 1.84 17.56 1.26 1 12 3 140.64 150.71 1.95 2 12 3 108.67 125.92 1.77 3 12 3 0.90 -3.59 1.47 4 12 3 12.02 13.16 1.29 5 12 3 5.44 4.53 1.28 6 12 3 0.94 -0.46 0.71 7 12 3 0.21 -0.39 1.18 1 13 3 3230.00 3293.74 12.12 2 13 3 279.03 290.07 2.87 3 13 3 517.32 520.45 5.12 4 13 3 24.23 18.01 1.32 5 13 3 322.26 313.21 3.14 6 13 3 94.34 82.87 1.81 0 14 3 1178.75 1207.73 7.79 1 14 3 620.79 649.58 6.02 2 14 3 601.72 659.44 6.05 3 14 3 15.45 16.04 1.35 4 14 3 1.89 3.36 1.21 5 14 3 0.40 -0.40 1.05 6 14 3 3.41 3.62 1.39 1 15 3 138.66 134.95 1.95 2 15 3 34.45 34.91 1.54 3 15 3 539.59 520.98 5.22 4 15 3 57.37 52.64 1.66 5 15 3 464.52 402.05 3.97 0 16 3 108.67 123.38 1.92 1 16 3 127.40 131.56 1.92 2 16 3 246.97 263.05 2.65 3 16 3 26.41 20.65 1.50 4 16 3 511.62 486.44 4.91 1 17 3 291.91 298.86 2.98 2 17 3 36.75 29.75 1.72 0 0 4 5737.52 5703.66 257.40 1 0 4 3560.15 3536.66 8.14 2 0 4 11385.72 9615.49 388.73 3 0 4 734.72 779.80 4.80 4 0 4 400.38 344.03 3.31 5 0 4 1.94 2.52 0.86 6 0 4 488.48 487.79 4.21 7 0 4 31.86 31.98 1.21 8 0 4 272.25 271.42 2.74 9 0 4 100.67 94.95 1.64 1 1 4 2237.77 2219.91 6.77 2 1 4 1389.72 1274.08 6.85 3 1 4 42.44 46.02 1.18 4 1 4 119.91 132.44 1.35 5 1 4 112.16 108.39 1.31 6 1 4 171.36 169.68 1.69 7 1 4 5.98 3.99 1.06 8 1 4 18.17 17.18 1.21 9 1 4 0.92 -1.13 1.00 0 2 4 5387.40 5198.26 9.78 1 2 4 156.13 165.49 1.61 2 2 4 956.96 698.31 5.25 3 2 4 3.09 6.39 1.07 4 2 4 1679.80 1634.22 6.91 5 2 4 3.77 3.48 0.92 6 2 4 1211.81 1225.33 6.44 7 2 4 31.03 33.05 1.24 8 2 4 439.37 415.62 4.05 9 2 4 2.71 4.54 1.23 1 3 4 246.78 221.48 2.24 2 3 4 56.56 55.48 1.31 3 3 4 1498.05 1492.54 7.46 4 3 4 3.13 4.83 1.00 5 3 4 525.88 520.68 4.36 6 3 4 0.20 0.15 0.87 7 3 4 370.20 363.89 3.68 8 3 4 12.53 11.60 1.23 9 3 4 115.34 119.63 1.85 0 4 4 905.71 889.14 4.59 1 4 4 6.93 8.38 0.88 2 4 4 983.15 841.52 5.79 3 4 4 35.00 37.33 1.32 4 4 4 720.89 736.89 5.31 5 4 4 2.82 6.35 1.13 6 4 4 238.03 237.77 2.41 7 4 4 60.23 60.21 1.40 8 4 4 160.88 162.20 1.86 9 4 4 1.26 3.25 1.23 1 5 4 450.47 421.99 3.88 2 5 4 226.88 202.62 2.08 3 5 4 1567.46 1475.80 7.78 4 5 4 20.64 27.14 1.25 5 5 4 1663.70 1694.70 7.87 6 5 4 1.91 1.49 0.99 7 5 4 354.50 371.93 3.74 8 5 4 0.01 -1.00 1.50 0 6 4 457.03 513.62 4.03 1 6 4 12.12 15.96 1.07 2 6 4 81.05 86.39 1.49 3 6 4 206.42 200.96 1.99 4 6 4 273.16 286.62 2.81 5 6 4 135.08 146.75 1.80 6 6 4 63.20 65.28 1.46 7 6 4 3.83 3.58 1.14 8 6 4 3.32 3.91 1.18 1 7 4 2046.59 1906.82 8.39 2 7 4 266.66 261.76 2.62 3 7 4 1774.74 1604.27 8.46 4 7 4 65.79 64.49 1.54 5 7 4 654.31 676.82 5.70 6 7 4 236.51 243.07 2.35 7 7 4 321.36 350.08 3.46 8 7 4 81.58 82.33 1.70 0 8 4 941.83 940.54 5.79 1 8 4 540.49 506.91 4.80 2 8 4 176.74 170.79 1.82 3 8 4 0.30 5.32 1.21 4 8 4 590.93 569.42 5.47 5 8 4 67.82 75.26 1.67 6 8 4 70.59 65.18 1.60 7 8 4 23.80 25.42 1.44 8 8 4 20.88 24.86 1.53 1 9 4 372.27 303.56 3.08 2 9 4 10.10 8.31 1.21 3 9 4 575.30 553.50 5.41 4 9 4 43.03 42.50 1.49 5 9 4 523.57 538.01 5.34 6 9 4 95.48 100.78 1.80 7 9 4 176.48 183.10 2.14 0 10 4 1238.10 1136.85 7.05 1 10 4 42.01 44.56 1.40 2 10 4 758.88 726.79 6.07 3 10 4 7.21 8.51 1.28 4 10 4 178.28 177.41 2.01 5 10 4 54.16 57.90 1.62 6 10 4 487.83 498.41 4.90 7 10 4 0.29 -0.74 1.37 1 11 4 181.64 180.25 1.99 2 11 4 21.14 24.30 1.48 3 11 4 44.07 48.60 1.52 4 11 4 1.07 1.19 1.06 5 11 4 16.62 21.35 1.41 6 11 4 0.99 0.22 1.17 0 12 4 1254.11 1095.48 7.39 1 12 4 105.88 97.15 1.72 2 12 4 880.76 922.30 6.97 3 12 4 6.71 6.18 1.25 4 12 4 331.00 316.64 3.15 5 12 4 24.68 23.45 1.45 6 12 4 356.49 352.27 3.56 1 13 4 0.99 3.17 1.25 2 13 4 29.21 29.51 1.63 3 13 4 25.76 27.26 1.42 4 13 4 0.95 1.32 1.13 5 13 4 6.33 6.63 1.37 0 14 4 461.94 477.99 4.78 1 14 4 44.23 39.71 1.59 2 14 4 807.35 851.24 7.03 3 14 4 15.59 15.64 1.42 4 14 4 328.65 323.09 3.29 1 15 4 231.59 246.93 2.56 2 15 4 30.88 36.36 1.61 3 15 4 85.57 91.30 1.84 0 16 4 397.42 423.42 4.17 1 16 4 11.51 11.61 1.46 2 16 4 73.75 88.62 1.94 1 1 5 971.93 892.23 5.02 2 1 5 517.26 508.82 4.61 3 1 5 397.45 333.95 3.26 4 1 5 7.43 8.55 1.23 5 1 5 441.23 469.12 4.51 6 1 5 77.38 78.83 1.48 7 1 5 271.05 283.00 2.80 8 1 5 6.76 8.37 1.25 0 2 5 23.52 22.55 0.87 1 2 5 5.56 6.55 0.91 2 2 5 765.57 719.74 5.56 3 2 5 0.35 2.20 1.30 4 2 5 140.50 149.35 1.87 5 2 5 0.03 4.29 1.15 6 2 5 158.46 165.09 1.81 7 2 5 18.63 20.52 1.30 8 2 5 13.97 15.06 1.32 1 3 5 254.92 249.31 2.46 2 3 5 2.14 8.11 1.23 3 3 5 478.13 376.34 3.73 4 3 5 4.96 7.40 1.36 5 3 5 199.06 211.49 2.10 6 3 5 0.70 4.56 1.17 7 3 5 154.25 158.89 1.86 8 3 5 0.08 2.32 1.20 0 4 5 815.02 780.10 4.88 1 4 5 8.02 9.28 0.99 2 4 5 952.24 895.33 6.53 3 4 5 40.01 37.31 1.56 4 4 5 630.88 635.48 5.94 5 4 5 7.42 10.72 1.28 6 4 5 588.51 589.81 5.41 7 4 5 20.49 20.98 1.33 8 4 5 112.08 123.19 1.93 1 5 5 44.37 48.87 1.26 2 5 5 2.20 5.87 1.24 3 5 5 23.97 29.37 1.55 4 5 5 3.21 11.75 1.54 5 5 5 23.52 21.97 1.44 6 5 5 50.51 46.83 1.53 7 5 5 34.64 40.75 1.48 0 6 5 2375.93 2444.44 9.09 1 6 5 445.42 456.65 4.42 2 6 5 995.10 836.84 6.52 3 6 5 70.49 59.06 1.66 4 6 5 1605.71 1484.91 8.94 5 6 5 355.60 369.82 3.73 6 6 5 105.32 117.17 1.85 7 6 5 11.66 11.57 1.37 1 7 5 462.54 460.72 4.51 2 7 5 0.06 5.42 1.33 3 7 5 68.60 65.51 1.71 4 7 5 61.47 59.22 1.80 5 7 5 0.22 -0.03 0.39 6 7 5 62.22 65.71 1.73 7 7 5 5.29 5.79 1.35 0 8 5 631.18 590.40 5.24 1 8 5 14.68 19.60 1.39 2 8 5 756.73 703.86 6.28 3 8 5 58.22 57.34 1.67 4 8 5 471.46 424.50 4.29 5 8 5 18.82 13.78 1.44 6 8 5 443.61 458.97 4.62 7 8 5 0.01 1.30 1.25 1 9 5 371.00 325.79 3.22 2 9 5 26.34 26.77 1.54 3 9 5 197.34 194.24 2.17 4 9 5 23.64 19.41 1.50 5 9 5 169.94 165.38 2.19 6 9 5 17.47 15.07 1.65 0 10 5 677.52 693.76 6.03 1 10 5 6.55 3.44 1.26 2 10 5 484.08 474.86 4.76 3 10 5 5.89 6.13 1.34 4 10 5 87.69 99.13 1.88 5 10 5 1.39 -0.09 0.67 6 10 5 129.21 138.45 2.27 1 11 5 557.81 519.71 5.08 2 11 5 11.12 23.00 1.50 3 11 5 440.47 460.67 4.66 4 11 5 3.51 2.49 1.25 5 11 5 204.28 194.11 2.38 0 12 5 84.34 67.96 1.65 1 12 5 15.19 10.50 1.51 2 12 5 207.23 214.12 2.36 3 12 5 59.96 59.99 1.82 4 12 5 1.08 1.59 1.19 5 12 5 0.15 3.29 1.45 1 13 5 782.68 814.11 7.19 2 13 5 409.86 448.10 4.47 3 13 5 348.86 386.51 3.79 4 13 5 2.80 -1.95 1.63 0 14 5 0.65 -0.70 0.76 1 14 5 57.79 52.91 1.81 2 14 5 233.82 243.24 2.54 3 14 5 80.58 80.02 2.01 0 0 6 245.08 245.70 2.41 1 0 6 98.37 100.62 1.40 2 0 6 1603.51 1509.48 7.54 3 0 6 796.21 665.63 6.49 4 0 6 375.30 398.56 4.02 5 0 6 86.52 85.68 1.68 6 0 6 155.42 174.95 1.97 7 0 6 45.66 34.61 1.54 1 1 6 145.59 144.95 1.57 2 1 6 667.44 629.80 5.39 3 1 6 83.49 70.46 2.01 4 1 6 0.00 3.41 1.56 5 1 6 24.54 28.30 1.49 6 1 6 0.44 -0.48 1.35 7 1 6 28.10 23.02 1.49 0 2 6 379.78 377.36 3.71 1 2 6 10.87 11.15 1.13 2 2 6 179.44 196.88 2.05 3 2 6 138.95 119.71 2.13 4 2 6 399.64 403.68 4.04 5 2 6 33.75 39.62 1.63 6 2 6 217.66 233.19 2.38 7 2 6 0.09 -2.06 1.89 1 3 6 353.56 355.27 3.48 2 3 6 161.72 157.91 1.94 3 3 6 153.80 119.78 2.08 4 3 6 7.95 13.40 1.64 5 3 6 103.59 115.76 2.01 6 3 6 2.92 2.72 1.28 7 3 6 140.56 138.64 2.08 0 4 6 100.79 105.52 1.49 1 4 6 4.29 11.44 1.22 2 4 6 122.70 132.81 1.89 3 4 6 8.85 11.16 1.54 4 4 6 195.23 183.63 2.38 5 4 6 12.35 17.44 1.60 6 4 6 19.51 28.44 1.54 1 5 6 495.26 510.98 5.03 2 5 6 104.45 106.23 1.83 3 5 6 269.60 249.28 2.55 4 5 6 14.82 9.84 1.52 5 5 6 276.62 282.67 2.85 6 5 6 28.32 31.93 1.61 0 6 6 238.49 239.09 2.34 1 6 6 1.55 9.98 1.37 2 6 6 3.58 6.60 1.32 3 6 6 9.44 12.52 1.53 4 6 6 0.17 2.11 1.31 5 6 6 104.74 97.15 2.06 6 6 6 1.30 1.56 1.34 1 7 6 915.42 937.11 6.99 2 7 6 24.15 21.61 1.44 3 7 6 324.11 322.01 3.20 4 7 6 96.50 95.81 1.98 5 7 6 95.47 89.35 2.03 6 7 6 74.52 73.59 2.04 0 8 6 413.45 427.71 4.25 1 8 6 0.97 6.64 1.38 2 8 6 10.29 10.82 1.36 3 8 6 0.33 1.37 1.24 4 8 6 91.32 82.17 1.90 5 8 6 233.76 204.04 2.54 1 9 6 184.59 187.33 2.20 2 9 6 1.48 2.28 1.23 3 9 6 152.31 150.41 2.19 4 9 6 4.32 5.69 1.47 5 9 6 194.38 187.20 2.54 0 10 6 41.15 48.14 1.51 1 10 6 28.84 31.04 1.55 2 10 6 193.57 185.67 2.27 3 10 6 15.69 16.48 1.54 4 10 6 179.35 185.63 2.46 1 11 6 50.07 48.28 1.68 2 11 6 26.84 23.16 1.65 3 11 6 33.47 35.58 1.72 0 12 6 95.81 105.12 1.92 1 12 6 20.92 23.41 1.50 2 12 6 245.36 259.71 2.77 1 1 7 198.67 226.67 2.23 2 1 7 31.52 35.19 1.42 3 1 7 463.33 469.87 4.66 4 1 7 0.43 0.54 1.21 5 1 7 202.92 230.91 2.82 0 2 7 75.73 71.86 1.41 1 2 7 4.42 4.11 1.16 2 2 7 54.27 58.41 1.57 3 2 7 26.86 27.73 1.79 4 2 7 8.75 6.95 1.76 5 2 7 7.16 5.43 1.83 1 3 7 209.48 228.30 2.26 2 3 7 8.43 7.99 1.38 3 3 7 135.37 141.61 2.30 4 3 7 1.80 0.36 1.04 5 3 7 109.91 109.13 2.41 0 4 7 125.76 136.16 1.74 1 4 7 0.04 0.00 0.04 2 4 7 137.93 147.37 2.03 3 4 7 0.32 0.09 0.90 4 4 7 68.29 66.78 2.03 1 5 7 103.39 110.44 1.80 2 5 7 0.02 1.67 1.24 3 5 7 44.59 47.86 1.79 4 5 7 13.59 13.04 1.70 0 6 7 724.76 762.93 6.30 1 6 7 0.32 3.58 1.23 2 6 7 107.49 122.13 2.06 3 6 7 13.25 8.56 1.51 4 6 7 29.48 35.62 1.87 1 7 7 6.72 5.34 1.34 2 7 7 1.48 6.05 1.44 3 7 7 1.99 0.97 1.18 0 8 7 52.61 60.97 1.67 1 8 7 0.82 -0.43 0.73 2 8 7 75.75 85.07 1.91 3 8 7 4.67 4.73 1.54 1 9 7 3.84 5.77 1.47 2 9 7 4.18 2.49 1.40 0 0 8 52.21 60.87 1.52 1 0 8 2.04 2.26 1.16 2 0 8 69.96 88.02 1.82 1 1 8 0.47 -1.09 1.57 0 2 8 32.41 40.21 1.46 1 2 8 4.64 3.88 1.27 1 3 8 72.70 75.64 1.75