#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/05/2200514.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200514_Fobs loop_ _publ_author_name 'Robinson, Paul D.' 'Parady, Thomas E.' 'Hou, Yuqing' 'Meyers, Cal Y.' _publ_section_title ; 2-Bromo-2-propyl phenyl sulfone ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o584 _journal_page_last o586 _journal_volume 57 _journal_year 2001 _space_group_IT_number 33 _symmetry_space_group_name_Hall 'P 2c -2n' _symmetry_space_group_name_H-M 'P n a 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 21.1338 _cell_length_b 6.2537 _cell_length_c 7.9792 _exptl_crystal_F_000 528.00 _reflns_d_resolution_high 0.8398 _[local]_cod_data_source_file om6024Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 2-Bromo-2-propyl phenyl sulfone' _shelx_refln_list_code 4 _shelx_f_calc_maximum 165.76 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' '-x+1/2, y+1/2, z+1/2' 'x+1/2, -y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1076.47 1057.65 11.60 o 4 0 0 8423.61 8206.21 71.65 o 6 0 0 27477.29 26064.92 184.18 o 8 0 0 176.12 208.51 16.62 o 10 0 0 19380.31 19243.99 134.81 o 12 0 0 1351.44 1300.09 34.78 o 14 0 0 1072.38 975.33 36.45 o 16 0 0 1008.70 1140.47 41.59 o 18 0 0 41.18 48.85 16.70 o 20 0 0 802.18 891.40 48.05 o 22 0 0 104.52 177.21 21.97 o 24 0 0 137.38 155.39 23.95 o 1 1 0 4631.13 4771.19 97.85 o 2 1 0 16814.77 15650.44 143.12 o 3 1 0 16342.70 15251.04 122.29 o 4 1 0 9287.60 8993.68 48.65 o 5 1 0 305.47 323.56 19.22 o 6 1 0 934.30 852.97 15.07 o 7 1 0 14032.65 14124.54 70.41 o 8 1 0 7449.86 7257.19 161.36 o 9 1 0 3404.34 3293.36 31.78 o 10 1 0 1590.60 1637.29 25.25 o 11 1 0 1450.35 1478.70 26.83 o 12 1 0 658.61 656.64 20.95 o 13 1 0 2888.71 2769.93 35.59 o 14 1 0 888.71 894.64 29.56 o 15 1 0 75.43 89.26 18.95 o 16 1 0 150.20 147.07 11.27 o 17 1 0 1269.83 1319.70 78.07 o 18 1 0 304.18 326.73 19.33 o 19 1 0 200.79 199.52 19.80 o 20 1 0 75.29 85.39 27.13 o 21 1 0 0.01 15.06 36.13 o 22 1 0 49.26 35.39 19.76 o 23 1 0 80.48 7.58 32.60 o 24 1 0 46.70 57.78 21.38 o 0 2 0 306.79 349.81 16.15 o 1 2 0 14324.40 13196.06 223.29 o 2 2 0 254.03 224.25 16.61 o 3 2 0 213.33 198.52 10.77 o 4 2 0 79.02 87.05 5.43 o 5 2 0 8606.23 8114.06 48.45 o 6 2 0 368.92 371.13 14.17 o 7 2 0 868.23 779.64 26.54 o 8 2 0 968.32 1024.19 20.45 o 9 2 0 2791.43 2906.57 32.40 o 10 2 0 1.53 -3.91 15.35 o 11 2 0 4640.14 4533.88 46.16 o 12 2 0 30.10 14.13 25.35 o 13 2 0 25.16 26.70 18.72 o 14 2 0 21.19 17.60 19.61 o 15 2 0 1819.12 1842.34 49.80 o 16 2 0 71.11 33.15 30.48 o 17 2 0 46.28 60.63 24.58 o 18 2 0 121.40 112.28 13.34 o 19 2 0 28.94 51.56 26.40 o 20 2 0 4.78 -23.18 28.47 o 21 2 0 487.68 476.51 28.13 o 22 2 0 1.63 8.11 31.41 o 23 2 0 2.26 -10.53 53.83 o 24 2 0 2.55 -34.48 34.48 o 1 3 0 2876.64 3293.97 48.04 o 2 3 0 1911.88 1917.78 47.17 o 3 3 0 4354.01 4516.67 37.43 o 4 3 0 612.59 647.90 17.61 o 5 3 0 360.61 380.78 16.32 o 6 3 0 697.31 695.56 19.23 o 7 3 0 2222.82 2165.66 79.51 o 8 3 0 2298.18 2236.20 36.53 o 9 3 0 1071.89 1058.52 25.15 o 10 3 0 51.42 27.35 18.07 o 11 3 0 4.08 7.52 12.74 o 12 3 0 743.59 783.77 26.26 o 13 3 0 425.39 452.12 25.83 o 14 3 0 287.94 281.67 17.49 o 15 3 0 2.03 20.47 23.08 o 16 3 0 112.58 110.57 13.04 o 17 3 0 162.63 164.57 13.98 o 18 3 0 388.12 397.30 55.27 o 19 3 0 34.95 64.36 19.06 o 20 3 0 0.83 31.65 24.21 o 21 3 0 5.71 2.22 42.05 o 22 3 0 38.41 69.73 32.51 o 23 3 0 15.56 -35.47 35.47 o 0 4 0 3829.93 3747.99 70.55 o 1 4 0 93.55 101.07 8.41 o 2 4 0 122.33 101.48 8.22 o 3 4 0 2.68 2.85 25.03 o 4 4 0 1912.28 1984.92 30.27 o 5 4 0 65.52 60.81 10.88 o 6 4 0 1072.11 1115.49 65.08 o 7 4 0 50.04 36.24 19.04 o 8 4 0 645.87 639.95 24.52 o 9 4 0 335.38 299.08 16.48 o 10 4 0 2785.13 2731.75 72.10 o 11 4 0 37.70 25.10 37.13 o 12 4 0 36.70 53.95 14.61 o 13 4 0 4.08 -12.99 24.17 o 14 4 0 371.89 346.85 23.27 o 15 4 0 133.18 114.33 30.17 o 16 4 0 382.55 423.79 43.91 o 17 4 0 0.02 -12.18 29.41 o 18 4 0 20.95 1.75 39.76 o 19 4 0 9.62 -32.24 32.24 o 20 4 0 170.90 205.31 31.12 o 21 4 0 0.39 -8.85 36.10 o 1 5 0 372.98 380.65 24.14 o 2 5 0 50.13 74.27 10.43 o 3 5 0 1027.92 980.56 87.07 o 4 5 0 79.33 79.99 14.73 o 5 5 0 2.59 -42.29 50.76 o 6 5 0 291.77 307.46 18.81 o 7 5 0 1368.87 1371.07 34.54 o 8 5 0 148.93 164.58 19.01 o 9 5 0 15.76 25.84 23.97 o 10 5 0 0.26 -19.18 24.79 o 11 5 0 145.79 154.22 30.36 o 12 5 0 85.56 58.49 18.08 o 13 5 0 299.38 322.64 32.22 o 14 5 0 110.39 133.52 47.24 o 15 5 0 6.72 -16.49 43.67 o 16 5 0 32.87 31.00 30.71 o 17 5 0 189.47 157.20 17.28 o 18 5 0 34.67 77.98 21.08 o 0 6 0 114.90 95.64 38.72 o 1 6 0 185.88 199.22 34.86 o 2 6 0 0.08 45.81 24.74 o 3 6 0 0.12 39.61 24.31 o 4 6 0 38.64 25.82 25.47 o 5 6 0 346.42 334.35 29.94 o 6 6 0 40.37 9.53 26.68 o 7 6 0 0.38 7.46 26.74 o 8 6 0 11.82 42.92 27.07 o 9 6 0 107.90 140.02 14.81 o 10 6 0 35.96 4.67 29.56 o 11 6 0 88.15 60.88 30.82 o 12 6 0 6.97 9.61 30.34 o 13 6 0 5.85 5.03 32.54 o 14 6 0 7.94 -25.22 33.09 o 1 7 0 0.09 -17.22 29.04 o 2 7 0 61.88 44.79 32.80 o 3 7 0 19.61 -29.94 29.94 o 4 7 0 2.52 44.92 16.19 o 5 7 0 4.86 -33.58 36.19 o 6 7 0 13.87 -31.36 32.77 o 7 7 0 37.59 24.43 32.36 o 8 7 0 56.44 50.94 33.27 o 2 0 1 6320.26 7613.40 58.38 o 4 0 1 6563.90 7335.60 50.92 o 6 0 1 520.89 641.66 17.15 o 8 0 1 2651.25 2796.28 36.61 o 10 0 1 502.62 498.51 23.01 o 12 0 1 50.18 30.81 10.71 o 14 0 1 2035.83 1947.77 45.24 o 16 0 1 786.97 754.81 38.44 o 18 0 1 351.47 331.43 27.03 o 20 0 1 584.47 586.79 45.84 o 22 0 1 66.94 24.54 42.47 o 24 0 1 168.91 186.48 24.86 o 0 1 1 11165.01 12733.89 138.87 o 1 1 1 1958.85 2124.94 22.68 o 2 1 1 1887.21 1948.55 24.02 o 3 1 1 329.71 359.59 9.05 o 4 1 1 1438.37 1437.70 19.02 o 5 1 1 1246.95 1107.06 14.85 o 6 1 1 1795.99 1743.63 32.56 o 7 1 1 989.18 999.31 16.49 o 8 1 1 463.60 512.94 14.71 o 9 1 1 2015.59 2278.39 28.96 o 10 1 1 490.16 519.49 34.77 o 11 1 1 1750.96 1705.72 26.26 o 12 1 1 576.77 549.98 20.21 o 13 1 1 139.84 124.73 8.85 o 14 1 1 21.62 15.98 18.20 o 15 1 1 360.52 428.77 22.77 o 16 1 1 613.69 593.44 27.57 o 17 1 1 987.13 943.01 30.63 o 18 1 1 88.10 12.12 25.26 o 19 1 1 8.85 0.98 20.77 o 20 1 1 87.66 107.05 39.40 o 21 1 1 147.39 153.93 15.08 o 22 1 1 110.22 116.34 15.44 o 23 1 1 132.51 125.28 16.52 o 24 1 1 49.47 46.25 34.27 o 1 2 1 2451.56 2509.00 86.77 o 2 2 1 870.08 960.83 15.13 o 3 2 1 2933.15 2807.39 24.65 o 4 2 1 413.72 471.80 12.99 o 5 2 1 259.10 267.16 12.47 o 6 2 1 7.40 -10.18 11.08 o 7 2 1 1912.00 1898.22 32.58 o 8 2 1 492.39 486.29 17.16 o 9 2 1 2314.85 2260.82 28.52 o 10 2 1 84.43 80.79 7.68 o 11 2 1 62.05 51.18 9.93 o 12 2 1 27.82 9.23 17.57 o 13 2 1 876.10 829.78 31.95 o 14 2 1 150.26 128.39 14.78 o 15 2 1 586.23 575.32 29.61 o 16 2 1 28.26 13.65 34.83 o 17 2 1 215.39 214.48 13.03 o 18 2 1 17.56 22.93 25.21 o 19 2 1 575.52 550.27 32.54 o 20 2 1 40.39 41.28 28.90 o 21 2 1 31.02 53.12 30.19 o 22 2 1 6.94 32.27 31.44 o 23 2 1 43.84 66.86 33.27 o 24 2 1 2.60 21.67 33.62 o 0 3 1 2402.02 2444.46 56.44 o 1 3 1 1071.98 1234.96 39.67 o 2 3 1 951.06 940.23 20.53 o 3 3 1 85.95 93.25 6.97 o 4 3 1 1448.96 1345.90 22.89 o 5 3 1 191.64 203.15 12.96 o 6 3 1 1585.15 1573.96 25.46 o 7 3 1 274.10 281.80 14.82 o 8 3 1 250.80 283.91 17.61 o 9 3 1 13.01 -24.59 24.59 o 10 3 1 812.73 740.13 60.38 o 11 3 1 114.68 150.09 9.76 o 12 3 1 835.96 761.96 46.99 o 13 3 1 380.45 412.78 24.00 o 14 3 1 43.67 30.09 34.41 o 15 3 1 23.60 17.22 30.06 o 16 3 1 305.77 340.85 19.34 o 17 3 1 237.72 256.26 16.23 o 18 3 1 151.19 161.82 14.27 o 19 3 1 23.83 -29.32 29.32 o 20 3 1 21.51 9.79 30.05 o 21 3 1 23.94 19.70 31.63 o 22 3 1 130.95 142.89 16.99 o 1 4 1 245.64 255.27 15.25 o 2 4 1 222.67 252.07 15.89 o 3 4 1 88.65 85.44 8.72 o 4 4 1 235.52 232.45 29.34 o 5 4 1 7.51 -2.60 17.58 o 6 4 1 554.67 622.59 26.92 o 7 4 1 145.20 166.14 21.84 o 8 4 1 368.39 445.99 49.20 o 9 4 1 138.29 131.18 13.87 o 10 4 1 629.36 681.57 41.12 o 11 4 1 46.08 24.53 23.31 o 12 4 1 124.18 137.31 15.65 o 13 4 1 114.06 98.61 12.54 o 14 4 1 282.50 339.22 30.00 o 15 4 1 22.05 49.69 25.93 o 16 4 1 251.74 241.95 15.83 o 17 4 1 13.75 23.44 37.01 o 18 4 1 47.75 41.19 36.74 o 19 4 1 21.35 12.11 52.08 o 20 4 1 153.41 188.56 17.21 o 21 4 1 10.81 -34.59 35.02 o 0 5 1 19.21 17.61 21.21 o 1 5 1 162.70 164.73 11.20 o 2 5 1 1.15 -4.31 20.87 o 3 5 1 5.23 -1.16 21.58 o 4 5 1 14.26 22.22 22.05 o 5 5 1 230.87 288.04 17.10 o 6 5 1 41.98 50.83 13.62 o 7 5 1 174.19 163.14 22.28 o 8 5 1 52.92 80.73 14.74 o 9 5 1 166.47 184.65 12.87 o 10 5 1 84.13 77.43 18.18 o 11 5 1 97.93 108.84 45.75 o 12 5 1 38.20 53.51 27.52 o 13 5 1 49.80 59.33 15.79 o 14 5 1 35.72 13.42 29.04 o 15 5 1 23.64 72.28 18.27 o 16 5 1 9.96 64.11 30.82 o 17 5 1 76.55 63.49 20.48 o 18 5 1 30.41 30.61 49.09 o 1 6 1 6.96 25.08 25.12 o 2 6 1 39.29 35.94 25.81 o 3 6 1 34.02 56.26 24.92 o 4 6 1 9.97 54.30 25.74 o 5 6 1 6.00 -12.96 27.29 o 6 6 1 7.66 -16.84 48.28 o 7 6 1 68.44 71.95 28.36 o 8 6 1 21.64 32.53 27.48 o 9 6 1 59.37 61.95 17.60 o 10 6 1 17.89 24.58 28.96 o 11 6 1 11.30 56.79 29.35 o 12 6 1 3.55 -10.53 46.99 o 13 6 1 3.01 22.83 32.12 o 14 6 1 6.17 -14.90 32.47 o 0 7 1 2.64 -46.37 63.52 o 1 7 1 1.51 -10.21 73.39 o 2 7 1 0.29 32.52 21.91 o 3 7 1 0.70 -3.47 31.19 o 4 7 1 3.59 24.87 31.23 o 5 7 1 9.10 -26.33 31.86 o 6 7 1 2.44 22.28 32.31 o 7 7 1 8.53 18.46 57.70 o 8 7 1 12.93 -33.69 33.69 o 0 0 2 14045.62 14286.20 105.47 o 2 0 2 5732.92 6046.68 45.82 o 4 0 2 15530.08 16489.04 125.17 o 6 0 2 12261.42 12235.88 85.08 o 8 0 2 589.87 621.63 21.85 o 10 0 2 6877.90 6453.46 65.66 o 12 0 2 2877.96 2791.62 47.73 o 14 0 2 1773.30 1811.80 44.90 o 16 0 2 2458.08 2263.98 54.36 o 18 0 2 493.78 453.08 38.76 o 20 0 2 230.12 236.01 23.45 o 22 0 2 182.00 177.58 22.66 o 24 0 2 74.80 42.64 48.41 o 1 1 2 436.68 402.70 21.13 o 2 1 2 7664.67 7686.12 79.83 o 3 1 2 18439.83 19510.97 100.97 o 4 1 2 1502.23 1524.70 17.38 o 5 1 2 251.28 260.42 10.82 o 6 1 2 385.52 406.42 12.69 o 7 1 2 2912.14 2833.39 26.68 o 8 1 2 4565.94 4540.29 46.26 o 9 1 2 1915.72 1893.25 24.68 o 10 1 2 329.24 289.21 16.31 o 11 1 2 335.22 311.54 16.84 o 12 1 2 1967.41 1946.10 29.38 o 13 1 2 1831.16 1740.22 36.63 o 14 1 2 1032.75 1012.53 26.97 o 15 1 2 223.73 234.80 14.83 o 16 1 2 266.29 261.10 32.12 o 17 1 2 210.06 200.67 13.39 o 18 1 2 407.85 457.40 27.65 o 19 1 2 296.37 311.77 20.73 o 20 1 2 100.60 96.28 20.42 o 21 1 2 47.00 -17.88 29.78 o 22 1 2 11.71 -60.00 64.65 o 23 1 2 117.66 86.21 21.23 o 24 1 2 35.34 69.09 28.07 o 0 2 2 26.19 32.80 8.19 o 1 2 2 3899.05 3732.08 91.46 o 2 2 2 119.07 124.86 7.51 o 3 2 2 703.73 712.12 28.78 o 4 2 2 95.46 109.39 8.51 o 5 2 2 8736.24 8671.14 185.78 o 6 2 2 307.40 350.99 14.44 o 7 2 2 1773.79 1785.66 24.04 o 8 2 2 152.73 163.12 10.17 o 9 2 2 869.29 811.08 20.10 o 10 2 2 98.63 94.51 8.00 o 11 2 2 1930.68 1869.84 54.51 o 12 2 2 43.69 52.49 21.12 o 13 2 2 139.78 136.93 9.99 o 14 2 2 136.28 126.11 14.27 o 15 2 2 991.94 916.68 35.02 o 16 2 2 10.23 -16.37 22.71 o 17 2 2 681.00 743.35 52.12 o 18 2 2 15.05 35.63 20.75 o 19 2 2 48.38 -11.18 27.78 o 20 2 2 48.34 -28.82 28.82 o 21 2 2 101.99 120.22 15.46 o 22 2 2 7.41 51.72 30.86 o 23 2 2 73.99 85.35 34.18 o 1 3 2 690.39 651.98 17.42 o 2 3 2 1872.27 1811.95 88.96 o 3 3 2 1056.04 975.70 81.62 o 4 3 2 492.40 472.91 17.67 o 5 3 2 26.86 31.65 9.33 o 6 3 2 219.01 233.25 13.05 o 7 3 2 1265.92 1271.13 72.86 o 8 3 2 903.64 868.26 41.68 o 9 3 2 309.24 331.18 19.56 o 10 3 2 126.70 147.02 10.24 o 11 3 2 185.05 198.46 13.12 o 12 3 2 646.69 629.98 25.72 o 13 3 2 930.48 911.59 75.66 o 14 3 2 111.97 99.99 33.84 o 15 3 2 182.57 198.19 13.37 o 16 3 2 12.96 21.21 42.58 o 17 3 2 97.36 115.48 13.19 o 18 3 2 239.38 201.27 14.77 o 19 3 2 71.69 62.05 29.82 o 20 3 2 58.22 66.08 25.75 o 21 3 2 25.96 56.36 32.38 o 22 3 2 35.27 36.64 44.93 o 0 4 2 2340.18 2338.65 75.60 o 1 4 2 123.25 119.34 9.09 o 2 4 2 366.97 345.70 26.66 o 3 4 2 88.99 94.69 9.03 o 4 4 2 1515.13 1441.03 74.90 o 5 4 2 66.40 72.87 9.48 o 6 4 2 1294.98 1243.66 78.95 o 7 4 2 11.86 19.80 19.21 o 8 4 2 135.96 157.98 23.48 o 9 4 2 12.99 -10.63 20.79 o 10 4 2 687.37 695.72 27.62 o 11 4 2 179.54 150.53 17.12 o 12 4 2 106.65 95.30 24.98 o 13 4 2 44.39 20.87 35.92 o 14 4 2 184.10 184.99 33.60 o 15 4 2 6.70 33.32 26.48 o 16 4 2 125.65 154.48 14.42 o 17 4 2 42.49 24.66 30.15 o 18 4 2 71.76 91.96 15.56 o 19 4 2 5.12 50.23 22.50 o 20 4 2 85.57 49.37 34.32 o 1 5 2 91.08 103.13 37.38 o 2 5 2 345.68 333.69 48.68 o 3 5 2 555.06 540.63 59.43 o 4 5 2 237.79 215.06 14.53 o 5 5 2 3.03 -1.21 35.94 o 6 5 2 75.45 83.04 21.17 o 7 5 2 503.07 470.86 28.20 o 8 5 2 166.14 180.97 12.72 o 9 5 2 100.29 87.43 15.30 o 10 5 2 1.86 -19.58 24.89 o 11 5 2 72.33 40.27 26.08 o 12 5 2 15.97 19.25 26.62 o 13 5 2 138.29 102.58 33.78 o 14 5 2 35.15 52.45 29.27 o 15 5 2 27.72 -16.96 29.77 o 16 5 2 32.72 23.70 30.52 o 17 5 2 69.54 47.47 21.71 o 0 6 2 30.27 55.58 26.41 o 1 6 2 75.50 85.65 37.69 o 2 6 2 4.92 20.73 31.22 o 3 6 2 17.15 1.96 41.36 o 4 6 2 19.24 44.32 26.47 o 5 6 2 245.87 218.02 15.96 o 6 6 2 2.91 -23.57 28.10 o 7 6 2 20.63 28.38 27.11 o 8 6 2 4.66 -6.29 28.97 o 9 6 2 71.10 77.72 29.97 o 10 6 2 36.66 49.36 29.62 o 11 6 2 34.74 39.62 29.77 o 12 6 2 16.87 -31.60 31.60 o 13 6 2 15.57 42.51 26.28 o 1 7 2 12.69 39.06 31.31 o 2 7 2 47.18 2.30 26.66 o 3 7 2 48.13 41.90 33.27 o 4 7 2 10.86 -15.95 54.74 o 5 7 2 5.71 52.50 32.29 o 6 7 2 3.11 -30.03 107.63 o 2 0 3 10160.93 10023.26 73.63 o 4 0 3 2604.63 2413.03 32.84 o 6 0 3 4723.24 4830.85 50.68 o 8 0 3 6091.38 5922.60 61.14 o 10 0 3 262.38 250.94 16.72 o 12 0 3 6192.72 6153.53 73.04 o 14 0 3 1524.25 1418.12 42.59 o 16 0 3 270.59 244.18 19.72 o 18 0 3 844.22 877.93 45.31 o 20 0 3 201.23 180.99 21.31 o 22 0 3 91.74 114.27 21.96 o 0 1 3 4407.86 4257.16 84.71 o 1 1 3 7217.65 7495.27 43.57 o 2 1 3 246.51 326.45 18.45 o 3 1 3 1604.29 1687.74 20.07 o 4 1 3 1759.71 1754.46 22.08 o 5 1 3 7031.47 7264.87 45.47 o 6 1 3 699.74 572.51 15.56 o 7 1 3 1383.25 1344.87 35.29 o 8 1 3 150.62 135.31 8.88 o 9 1 3 1713.16 1630.98 25.05 o 10 1 3 2278.15 2308.14 38.17 o 11 1 3 1637.52 1635.00 41.82 o 12 1 3 280.68 259.82 16.55 o 13 1 3 192.28 195.62 18.68 o 14 1 3 806.47 860.89 48.84 o 15 1 3 1020.78 989.26 46.72 o 16 1 3 331.90 319.03 49.75 o 17 1 3 100.10 98.11 12.32 o 18 1 3 46.49 64.74 34.15 o 19 1 3 102.40 136.82 19.11 o 20 1 3 105.90 103.43 14.69 o 21 1 3 144.02 150.89 15.60 o 22 1 3 85.47 85.47 39.56 o 23 1 3 38.20 58.00 58.68 o 1 2 3 1817.66 1821.97 43.80 o 2 2 3 485.45 532.73 16.20 o 3 2 3 5936.79 5837.08 139.62 o 4 2 3 840.59 905.21 38.45 o 5 2 3 354.05 377.51 15.15 o 6 2 3 250.00 227.11 14.49 o 7 2 3 3237.73 3130.96 32.82 o 8 2 3 272.49 266.03 20.89 o 9 2 3 1432.47 1371.24 43.65 o 10 2 3 82.47 74.46 20.79 o 11 2 3 320.10 349.48 19.87 o 12 2 3 84.34 86.77 23.46 o 13 2 3 1775.39 1693.00 47.77 o 14 2 3 21.66 0.29 21.02 o 15 2 3 247.90 258.60 18.25 o 16 2 3 4.99 28.08 16.83 o 17 2 3 392.40 441.92 27.73 o 18 2 3 76.67 65.09 13.25 o 19 2 3 162.96 187.72 15.78 o 20 2 3 2.27 -10.80 28.77 o 21 2 3 46.77 56.46 31.22 o 22 2 3 1.54 -8.51 32.16 o 0 3 3 3345.09 3289.55 51.87 o 1 3 3 676.59 646.61 35.66 o 2 3 3 347.92 331.24 17.03 o 3 3 3 546.25 529.12 18.58 o 4 3 3 1475.70 1435.07 70.71 o 5 3 3 648.35 627.28 24.62 o 6 3 3 2380.25 2319.73 94.21 o 7 3 3 114.43 132.02 8.92 o 8 3 3 35.92 36.23 14.21 o 9 3 3 395.71 398.95 21.35 o 10 3 3 1050.56 1055.45 27.25 o 11 3 3 656.19 608.91 33.01 o 12 3 3 188.38 178.41 15.62 o 13 3 3 247.33 223.27 21.03 o 14 3 3 148.94 155.69 12.27 o 15 3 3 184.76 197.26 13.16 o 16 3 3 386.28 344.98 20.48 o 17 3 3 62.52 95.69 13.65 o 18 3 3 0.63 11.40 27.57 o 19 3 3 34.81 64.50 32.21 o 20 3 3 94.49 63.59 32.40 o 21 3 3 68.83 83.43 21.07 o 1 4 3 47.06 39.98 24.91 o 2 4 3 2700.03 2679.49 103.85 o 3 4 3 530.70 542.60 33.02 o 4 4 3 1507.37 1498.76 30.33 o 5 4 3 37.36 29.58 16.54 o 6 4 3 415.60 425.43 23.47 o 7 4 3 101.93 112.48 19.33 o 8 4 3 1409.75 1358.52 37.49 o 9 4 3 53.89 54.04 31.68 o 10 4 3 52.26 57.91 14.50 o 11 4 3 9.81 34.08 23.00 o 12 4 3 282.53 266.37 17.40 o 13 4 3 0.39 -2.07 25.45 o 14 4 3 246.72 254.78 17.77 o 15 4 3 0.21 16.23 26.51 o 16 4 3 74.90 44.99 28.93 o 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1613.52 1724.27 31.15 o 4 0 4 255.08 246.51 18.85 o 6 0 4 2611.92 2627.62 41.11 o 8 0 4 372.68 382.27 23.70 o 10 0 4 714.71 665.28 31.23 o 12 0 4 1512.10 1435.25 41.83 o 14 0 4 374.75 377.98 34.78 o 16 0 4 602.35 557.76 41.64 o 18 0 4 209.42 238.09 22.81 o 20 0 4 51.00 9.38 43.51 o 22 0 4 231.40 285.31 25.30 o 1 1 4 1236.26 1203.01 21.75 o 2 1 4 1172.58 1095.49 23.03 o 3 1 4 87.35 83.43 15.05 o 4 1 4 2488.87 2494.12 27.99 o 5 1 4 756.54 727.15 28.87 o 6 1 4 126.20 145.74 10.00 o 7 1 4 476.90 476.14 17.76 o 8 1 4 927.23 872.79 21.27 o 9 1 4 801.13 742.87 30.04 o 10 1 4 464.35 456.00 62.48 o 11 1 4 22.24 11.66 17.90 o 12 1 4 8.03 25.92 18.43 o 13 1 4 172.54 191.46 12.32 o 14 1 4 622.15 668.00 27.27 o 15 1 4 497.75 500.70 39.39 o 16 1 4 21.07 0.98 25.95 o 17 1 4 26.68 17.00 35.98 o 18 1 4 73.22 68.37 17.36 o 19 1 4 238.28 222.46 15.11 o 20 1 4 156.32 127.00 16.03 o 21 1 4 74.58 43.90 32.19 o 22 1 4 10.03 40.58 31.78 o 0 2 4 39.34 42.93 8.56 o 1 2 4 1577.04 1535.25 24.02 o 2 2 4 86.99 79.36 7.11 o 3 2 4 175.00 175.47 10.96 o 4 2 4 30.64 39.42 16.81 o 5 2 4 1447.00 1325.02 69.80 o 6 2 4 107.12 99.52 7.95 o 7 2 4 619.27 616.59 31.24 o 8 2 4 45.04 26.56 16.89 o 9 2 4 191.63 177.03 14.89 o 10 2 4 17.95 29.89 17.81 o 11 2 4 920.58 895.42 43.66 o 12 2 4 0.74 18.80 20.28 o 13 2 4 463.29 463.93 25.60 o 14 2 4 35.00 27.03 22.42 o 15 2 4 136.76 150.75 12.50 o 16 2 4 46.51 48.91 24.86 o 17 2 4 274.00 285.20 25.90 o 18 2 4 16.18 40.37 27.41 o 19 2 4 17.73 -12.17 41.18 o 20 2 4 6.71 -28.77 30.78 o 21 2 4 134.25 145.04 17.05 o 1 3 4 104.72 106.17 8.36 o 2 3 4 352.13 364.45 25.50 o 3 3 4 362.57 306.73 19.80 o 4 3 4 172.04 169.16 14.08 o 5 3 4 159.63 177.59 17.44 o 6 3 4 37.44 40.31 11.34 o 7 3 4 50.52 57.61 16.57 o 8 3 4 357.80 365.73 22.43 o 9 3 4 347.47 342.00 21.88 o 10 3 4 85.46 110.99 19.00 o 11 3 4 91.88 74.68 34.00 o 12 3 4 76.84 51.55 27.90 o 13 3 4 6.78 -19.66 25.19 o 14 3 4 288.82 280.55 19.42 o 15 3 4 138.38 161.33 13.67 o 16 3 4 17.21 32.89 29.33 o 17 3 4 8.91 19.99 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4 13.88 5.26 27.03 o 1 6 4 25.77 6.48 40.13 o 2 6 4 6.19 41.44 27.21 o 3 6 4 2.77 -12.79 32.43 o 4 6 4 9.94 14.75 28.56 o 5 6 4 20.53 29.72 39.68 o 6 6 4 31.09 -19.31 30.26 o 7 6 4 5.08 -30.97 30.97 o 8 6 4 2.87 21.94 30.58 o 9 6 4 9.17 31.34 34.07 o 10 6 4 5.20 62.83 31.78 o 2 0 5 7262.25 7554.02 75.88 o 4 0 5 2347.65 2350.10 43.17 o 6 0 5 787.10 808.28 31.60 o 8 0 5 3371.90 3101.13 53.65 o 10 0 5 222.47 216.31 20.28 o 12 0 5 1627.67 1602.56 48.75 o 14 0 5 116.00 124.18 16.94 o 16 0 5 75.46 120.83 18.36 o 18 0 5 524.90 545.92 46.83 o 20 0 5 3.58 41.68 42.33 o 0 1 5 2478.89 2387.58 30.62 o 1 1 5 1860.77 1846.77 27.56 o 2 1 5 502.95 502.29 18.66 o 3 1 5 217.31 216.68 24.82 o 4 1 5 1105.86 1100.95 38.76 o 5 1 5 2726.99 2756.08 37.20 o 6 1 5 1201.23 1108.67 37.17 o 7 1 5 104.22 103.01 8.86 o 8 1 5 76.92 59.50 9.15 o 9 1 5 1113.71 1115.91 64.90 o 10 1 5 743.22 646.76 60.93 o 11 1 5 888.46 891.77 27.62 o 12 1 5 150.35 140.13 11.32 o 13 1 5 95.53 90.58 16.41 o 14 1 5 194.46 192.94 12.40 o 15 1 5 664.84 668.54 36.00 o 16 1 5 150.94 175.93 13.75 o 17 1 5 44.82 10.80 27.74 o 18 1 5 42.49 20.33 29.11 o 19 1 5 46.60 49.42 30.79 o 20 1 5 117.98 137.68 16.04 o 21 1 5 92.53 74.20 19.89 o 1 2 5 827.79 800.27 22.64 o 2 2 5 422.80 430.07 20.16 o 3 2 5 3508.00 3390.03 55.04 o 4 2 5 74.76 83.01 24.18 o 5 2 5 13.74 26.01 17.41 o 6 2 5 49.14 23.24 15.44 o 7 2 5 1738.40 1613.34 31.12 o 8 2 5 262.71 276.89 15.39 o 9 2 5 911.93 853.58 49.69 o 10 2 5 55.86 86.45 23.05 o 11 2 5 186.20 186.58 12.42 o 12 2 5 94.57 112.66 11.56 o 13 2 5 998.76 990.34 32.29 o 14 2 5 58.04 88.66 15.48 o 15 2 5 6.09 -5.19 25.98 o 16 2 5 10.23 3.56 27.27 o 17 2 5 190.21 191.52 16.68 o 18 2 5 13.50 -28.60 51.80 o 19 2 5 149.14 112.85 35.13 o 20 2 5 26.12 15.68 33.03 o 0 3 5 1867.71 1724.03 68.54 o 1 3 5 984.14 928.44 27.14 o 2 3 5 140.35 137.73 20.60 o 3 3 5 175.59 187.10 11.90 o 4 3 5 683.71 704.11 25.99 o 5 3 5 960.16 904.28 27.15 o 6 3 5 720.38 738.50 26.94 o 7 3 5 216.02 219.12 13.08 o 8 3 5 29.53 29.84 11.59 o 9 3 5 223.10 216.85 13.02 o 10 3 5 803.62 808.70 45.05 o 11 3 5 336.54 410.07 69.17 o 12 3 5 151.23 153.31 27.33 o 13 3 5 33.92 23.50 25.64 o 14 3 5 104.49 69.45 16.07 o 15 3 5 87.35 90.70 18.06 o 16 3 5 129.35 131.42 18.13 o 17 3 5 34.06 50.48 30.47 o 18 3 5 9.62 -2.93 32.06 o 1 4 5 73.50 69.16 11.14 o 2 4 5 1127.75 1095.05 40.53 o 3 4 5 110.01 118.83 11.74 o 4 4 5 233.57 256.29 23.23 o 5 4 5 29.57 39.65 22.47 o 6 4 5 316.10 353.74 34.61 o 7 4 5 81.03 71.98 26.98 o 8 4 5 887.77 868.80 52.18 o 9 4 5 56.39 38.67 26.54 o 10 4 5 35.24 52.84 25.62 o 11 4 5 7.39 -48.85 48.85 o 12 4 5 426.16 455.83 26.51 o 13 4 5 117.88 99.14 20.77 o 14 4 5 136.98 136.85 15.89 o 15 4 5 14.48 -20.31 31.08 o 16 4 5 35.33 83.85 19.58 o 0 5 5 127.16 125.69 19.07 o 1 5 5 265.63 243.02 16.11 o 2 5 5 21.25 -12.43 25.73 o 3 5 5 19.31 21.45 22.54 o 4 5 5 125.23 98.43 17.48 o 5 5 5 434.76 449.82 31.21 o 6 5 5 112.71 132.14 14.28 o 7 5 5 16.91 40.90 33.05 o 8 5 5 29.47 -23.66 57.35 o 9 5 5 118.35 85.59 19.78 o 10 5 5 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3 7 46.80 20.30 27.46 o 9 3 7 73.29 74.24 14.10 o 10 3 7 77.90 101.38 19.95 o 11 3 7 102.43 119.19 17.43 o 12 3 7 65.88 47.87 22.13 o 13 3 7 8.74 26.18 30.59 o 1 4 7 63.93 12.42 28.87 o 2 4 7 217.72 246.54 15.01 o 3 4 7 89.26 113.45 29.39 o 4 4 7 87.94 73.86 18.29 o 5 4 7 9.02 21.37 28.38 o 6 4 7 20.79 30.77 28.95 o 7 4 7 44.00 51.54 28.98 o 8 4 7 104.04 94.57 19.75 o 9 4 7 79.77 57.72 55.66 o 10 4 7 54.57 15.63 32.45 o 0 5 7 113.70 102.00 23.70 o 1 5 7 22.45 48.16 31.04 o 2 5 7 28.79 31.92 21.96 o 0 0 8 1175.05 1123.09 51.22 o 2 0 8 84.50 78.77 18.42 o 4 0 8 454.82 539.87 42.91 o 6 0 8 642.63 689.45 46.11 o 8 0 8 110.08 105.47 20.21 o 10 0 8 567.91 529.70 50.74 o 12 0 8 72.73 61.52 43.25 o 1 1 8 293.55 288.48 18.30 o 2 1 8 343.36 332.37 20.64 o 3 1 8 491.10 489.17 31.32 o 4 1 8 128.31 129.74 24.37 o 5 1 8 9.25 33.34 26.11 o 6 1 8 111.71 145.51 25.19 o 7 1 8 302.07 322.77 19.70 o 8 1 8 232.02 234.26 17.07 o 9 1 8 178.00 187.21 24.43 o 10 1 8 29.75 12.49 29.03 o 11 1 8 52.74 69.52 18.92 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41.00 26.17 30.20 o 2 2 9 44.62 54.20 30.61 o 3 2 9 75.72 53.68 31.60 o 4 2 9 48.50 44.94 31.75 o