#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:52:33 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180925 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/05/2200542.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200542_Fobs loop_ _publ_author_name 'Bond, Andrew D.' 'Linton, David J.' 'Wheatley, Andrew E. H.' _publ_section_title ; Methylzinc tert-butoxide tetrahydrofuran solvate ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m298 _journal_page_last m300 _journal_volume 57 _journal_year 2001 _space_group_IT_number 142 _symmetry_space_group_name_Hall '-I 4bd 2c' _symmetry_space_group_name_H-M 'I 41/a c d :2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.8323 _cell_length_b 14.8323 _cell_length_c 30.0976 _exptl_crystal_F_000 2880.00 _reflns_d_resolution_high 0.7703 _cod_data_source_file wn6021Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' aw0101 in I4(1)/acd' _shelx_refln_list_code 4 _shelx_f_calc_maximum 598.30 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, z+1/2' 'y+1/4, x+1/4, z+1/4' '-y+3/4, x+1/4, z+3/4' 'x, -y+1/2, z+1/2' '-x, -y+1/2, z' 'y+1/4, -x+1/4, z+3/4' '-y+3/4, -x+1/4, z+1/4' 'x+1/2, y+1/2, z+1/2' '-x+1/2, y+1/2, z+1' 'y+3/4, x+3/4, z+3/4' '-y+5/4, x+3/4, z+5/4' 'x+1/2, -y+1, z+1' '-x+1/2, -y+1, z+1/2' 'y+3/4, -x+3/4, z+5/4' '-y+5/4, -x+3/4, z+3/4' '-x, -y, -z' 'x, -y, -z-1/2' '-y-1/4, -x-1/4, -z-1/4' 'y-3/4, -x-1/4, -z-3/4' '-x, y-1/2, -z-1/2' 'x, y-1/2, -z' '-y-1/4, x-1/4, -z-3/4' 'y-3/4, x-1/4, -z-1/4' '-x+1/2, -y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-y+1/4, -x+1/4, -z+1/4' 'y-1/4, -x+1/4, -z-1/4' '-x+1/2, y, -z' 'x+1/2, y, -z+1/2' '-y+1/4, x+1/4, -z-1/4' 'y-1/4, x+1/4, -z+1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 2 0 224359.77 103228.44 9107.74 o 0 4 0 238199.75 267301.31 7971.99 o 2 4 0 2183.60 2577.82 60.56 o 4 4 0 8364.48 7146.44 201.07 o 2 6 0 210410.45 231389.86 3898.16 o 4 6 0 7987.71 7791.84 167.90 o 6 6 0 283621.31 270833.00 9805.86 o 0 8 0 215866.94 219950.78 6426.26 o 2 8 0 119008.77 123867.48 2303.91 o 4 8 0 6854.88 6393.34 278.35 o 6 8 0 154438.50 149614.08 3797.79 o 8 8 0 79632.35 76887.83 4180.76 o 0 10 0 7181.65 7674.46 726.63 o 2 10 0 2865.78 3087.21 112.73 o 4 10 0 3251.44 3134.35 175.51 o 6 10 0 6046.72 5572.23 313.38 o 8 10 0 1428.47 1480.80 152.76 o 10 10 0 1975.13 2200.13 249.57 o 0 12 0 32732.41 34084.31 4328.83 o 2 12 0 19599.00 20877.47 840.42 o 4 12 0 119.59 241.98 91.05 o 6 12 0 19212.23 18705.61 676.78 o 8 12 0 22864.46 22995.00 822.74 o 10 12 0 6030.53 4636.21 330.23 o 12 12 0 1047.83 1160.16 186.41 o 0 14 0 59154.74 62320.55 3205.77 o 2 14 0 19545.95 21940.26 686.39 o 4 14 0 3713.53 3437.31 179.05 o 6 14 0 30451.35 29674.74 956.77 o 8 14 0 18207.76 18494.83 675.36 o 10 14 0 333.44 502.28 206.95 o 12 14 0 5150.82 4793.40 326.22 o 0 16 0 7691.69 8222.91 539.61 o 2 16 0 1853.95 2396.45 187.59 o 4 16 0 1346.00 1119.33 142.87 o 6 16 0 5813.66 6066.80 382.63 o 8 16 0 2001.86 2123.09 175.94 o 10 16 0 515.02 568.01 151.77 o 0 18 0 378.74 641.44 174.76 o 2 18 0 447.79 323.20 146.99 o 4 18 0 320.08 434.35 211.44 o 6 18 0 21.70 140.25 147.47 o 2 3 1 1692.34 2172.71 62.82 o 1 4 1 7588.78 7857.61 109.00 o 3 4 1 9184.65 8855.27 109.15 o 2 5 1 10710.82 11714.54 147.05 o 4 5 1 505.09 710.83 48.92 o 1 6 1 11137.40 12666.13 170.55 o 3 6 1 22134.83 24398.43 295.41 o 5 6 1 4967.86 5170.80 72.71 o 2 7 1 3973.83 3637.52 58.68 o 4 7 1 20639.71 20152.51 297.15 o 6 7 1 7798.61 7516.32 119.42 o 1 8 1 467.43 347.86 37.10 o 3 8 1 8307.61 8281.23 122.14 o 5 8 1 7228.62 7291.57 148.48 o 7 8 1 1291.91 1195.87 52.70 o 2 9 1 2215.39 2225.98 71.74 o 4 9 1 16691.57 16476.25 442.47 o 6 9 1 9691.60 9069.23 215.79 o 8 9 1 846.13 839.97 58.14 o 1 10 1 1514.76 1527.64 58.64 o 3 10 1 2020.17 2219.47 114.32 o 5 10 1 143.82 209.84 47.45 o 7 10 1 5481.92 5116.16 274.87 o 9 10 1 4408.33 4621.72 140.14 o 2 11 1 1220.08 1397.52 80.63 o 4 11 1 347.79 473.82 65.47 o 6 11 1 70.99 19.04 57.59 o 8 11 1 1840.25 1521.73 90.26 o 10 11 1 58.64 161.02 82.39 o 1 12 1 2048.47 2016.92 132.62 o 3 12 1 6526.83 7060.98 345.53 o 5 12 1 1763.63 1664.91 97.09 o 7 12 1 1163.88 1249.55 97.00 o 9 12 1 3976.42 4051.32 146.72 o 11 12 1 977.09 953.65 105.24 o 2 13 1 5284.96 5386.25 141.04 o 4 13 1 6300.77 6853.92 197.56 o 6 13 1 361.45 422.44 85.59 o 8 13 1 671.12 421.61 108.43 o 10 13 1 1585.81 1473.70 134.23 o 12 13 1 372.77 301.79 103.91 o 1 14 1 1698.50 1948.55 127.53 o 3 14 1 8417.04 8620.40 233.71 o 5 14 1 2894.16 3089.67 143.53 o 7 14 1 25.55 -107.69 156.30 o 9 14 1 1943.49 1837.86 137.72 o 11 14 1 1663.52 1634.69 174.18 o 13 14 1 3.59 -112.97 112.97 o 2 15 1 4523.79 4191.17 162.23 o 4 15 1 6679.92 6926.13 261.75 o 6 15 1 1412.02 1570.83 113.35 o 8 15 1 50.86 1.56 85.76 o 10 15 1 2051.46 2118.14 139.87 o 12 15 1 1359.10 1355.45 123.43 o 1 16 1 27.48 81.03 95.31 o 3 16 1 499.54 302.47 95.70 o 5 16 1 352.43 301.14 164.36 o 7 16 1 66.82 133.74 98.53 o 9 16 1 14.45 -2.88 102.09 o 2 17 1 453.39 512.38 111.89 o 4 17 1 763.48 776.61 103.11 o 6 17 1 247.63 276.30 105.80 o 8 17 1 0.04 -35.57 101.57 o 1 18 1 82.54 25.02 102.39 o 3 18 1 411.54 424.67 136.22 o 5 18 1 148.21 506.70 122.10 o 2 19 1 389.85 229.08 127.32 o 1 3 2 14264.34 15700.48 216.52 o 3 3 2 16934.81 17594.69 331.39 o 0 4 2 126.79 207.23 25.90 o 2 4 2 3031.09 3210.42 47.95 o 1 5 2 220127.78 228352.13 3178.11 o 3 5 2 6091.01 6167.62 118.97 o 5 5 2 33027.15 31369.36 731.87 o 0 6 2 1581.15 1774.94 65.32 o 2 6 2 8.05 21.41 24.38 o 4 6 2 474.05 512.52 30.16 o 1 7 2 330445.78 340771.72 4327.73 o 3 7 2 20914.45 20345.19 260.07 o 5 7 2 127563.65 125270.13 1617.77 o 7 7 2 209855.17 203851.69 4862.28 o 0 8 2 2045.65 1790.66 52.72 o 2 8 2 221.33 115.05 33.16 o 4 8 2 81.13 -37.22 37.22 o 6 8 2 291.79 179.95 39.68 o 1 9 2 42220.76 38692.66 724.26 o 3 9 2 2880.33 2774.28 110.87 o 5 9 2 29318.73 27731.18 553.24 o 7 9 2 37517.87 33915.23 1371.64 o 9 9 2 5689.71 5627.31 485.61 o 0 10 2 7530.78 8678.27 376.24 o 2 10 2 1299.86 1321.34 61.82 o 4 10 2 1285.66 1104.37 46.83 o 6 10 2 1871.98 2014.32 77.93 o 8 10 2 299.61 251.26 70.35 o 1 11 2 3129.70 2957.70 131.96 o 3 11 2 3793.97 3700.28 134.37 o 5 11 2 111.97 152.37 66.68 o 7 11 2 3899.20 3882.46 210.84 o 9 11 2 6285.36 6802.20 218.79 o 11 11 2 3016.34 2754.53 170.73 o 0 12 2 4001.33 4259.45 292.62 o 2 12 2 297.13 357.72 58.52 o 4 12 2 42.25 51.56 55.44 o 6 12 2 571.87 526.78 73.70 o 8 12 2 673.69 804.40 89.54 o 10 12 2 97.38 26.33 82.68 o 1 13 2 45590.07 49098.10 1036.57 o 3 13 2 4063.55 4037.61 134.54 o 5 13 2 14116.32 15849.72 378.81 o 7 13 2 31524.12 32615.73 822.48 o 9 13 2 10623.64 11055.70 405.23 o 11 13 2 210.24 364.40 99.15 o 13 13 2 5675.79 6122.16 350.25 o 0 14 2 157.50 96.90 115.51 o 2 14 2 21.62 112.69 69.97 o 4 14 2 288.94 383.87 83.65 o 6 14 2 32.85 44.48 82.20 o 8 14 2 9.88 56.52 107.98 o 10 14 2 75.47 -3.24 100.81 o 12 14 2 77.30 -19.00 167.36 o 1 15 2 17402.95 16514.34 506.00 o 3 15 2 246.83 -37.05 96.29 o 5 15 2 8575.42 8766.16 261.00 o 7 15 2 11438.27 11484.38 354.21 o 9 15 2 1413.52 1132.40 118.17 o 11 15 2 1494.13 1377.50 124.65 o 0 16 2 1789.73 2621.24 579.77 o 2 16 2 293.42 327.42 103.46 o 4 16 2 188.01 207.56 109.70 o 6 16 2 500.80 483.16 109.36 o 8 16 2 236.63 119.73 94.88 o 10 16 2 2.10 234.19 111.83 o 1 17 2 355.35 318.81 97.86 o 3 17 2 95.38 32.10 95.55 o 5 17 2 943.05 1094.13 111.03 o 7 17 2 338.87 210.22 107.89 o 0 18 2 646.56 776.07 140.54 o 2 18 2 263.49 450.03 122.25 o 4 18 2 2.21 -41.57 81.25 o 6 18 2 460.59 589.23 138.44 o 1 19 2 1895.58 1917.46 153.49 o 1 2 3 2905.09 2951.72 171.41 o 2 3 3 29898.64 29690.34 451.56 o 1 4 3 84.91 120.90 20.93 o 3 4 3 65739.90 57766.75 728.09 o 2 5 3 23858.54 22904.76 292.08 o 4 5 3 37346.27 33413.86 629.84 o 1 6 3 54.25 12.48 30.57 o 3 6 3 346.27 229.13 34.51 o 5 6 3 184.96 43.09 28.32 o 2 7 3 25283.29 28079.01 357.52 o 4 7 3 7260.62 7581.43 100.99 o 6 7 3 96.43 38.42 35.11 o 1 8 3 52.19 -19.88 30.17 o 3 8 3 19045.87 19159.66 338.59 o 5 8 3 30241.14 30037.05 428.13 o 7 8 3 4832.40 4432.20 85.23 o 2 9 3 5398.30 5605.11 94.46 o 4 9 3 7397.10 6991.67 131.90 o 6 9 3 67.93 52.88 37.81 o 8 9 3 5665.43 5190.54 162.05 o 1 10 3 6718.38 7368.00 210.44 o 3 10 3 38461.99 39146.64 813.63 o 5 10 3 13077.18 12967.02 430.18 o 7 10 3 300.84 283.02 50.69 o 9 10 3 2956.99 3067.69 214.81 o 2 11 3 22041.51 21350.24 682.28 o 4 11 3 12983.17 12435.71 454.63 o 6 11 3 42.06 16.89 51.63 o 8 11 3 9046.04 8206.26 509.25 o 10 11 3 5144.57 4765.51 165.64 o 1 12 3 376.55 415.33 39.24 o 3 12 3 306.43 271.10 61.01 o 5 12 3 33.80 -18.49 65.85 o 7 12 3 7.52 22.31 70.27 o 9 12 3 6.79 -61.65 72.13 o 11 12 3 215.75 133.38 79.68 o 2 13 3 6438.38 6816.63 178.42 o 4 13 3 6089.04 6598.42 197.28 o 6 13 3 142.33 34.47 74.63 o 8 13 3 2445.19 2342.95 115.41 o 10 13 3 3732.56 3587.60 160.90 o 12 13 3 179.44 190.31 102.76 o 1 14 3 1691.79 1781.68 181.97 o 3 14 3 8654.20 9292.65 288.53 o 5 14 3 3618.24 3284.55 150.84 o 7 14 3 218.35 32.15 90.15 o 9 14 3 447.48 419.60 99.95 o 11 14 3 1622.52 1739.71 131.10 o 13 14 3 1147.27 1050.58 150.73 o 2 15 3 325.84 294.68 85.07 o 4 15 3 597.10 544.04 107.00 o 6 15 3 0.90 134.31 136.93 o 8 15 3 261.72 77.40 140.94 o 10 15 3 126.69 173.79 109.10 o 1 16 3 1051.78 921.73 103.34 o 3 16 3 5848.94 6000.26 258.14 o 5 16 3 3859.05 3958.50 165.38 o 7 16 3 339.79 261.58 108.08 o 9 16 3 1057.10 1164.59 124.99 o 2 17 3 777.38 747.98 107.12 o 4 17 3 916.09 1140.05 153.15 o 6 17 3 41.71 202.76 98.87 o 8 17 3 473.38 591.14 184.36 o 1 18 3 94.39 121.81 116.35 o 3 18 3 354.67 514.69 130.26 o 5 18 3 111.11 -51.90 139.93 o 2 19 3 1077.76 1062.66 159.84 o 0 2 4 234703.13 149880.75 25656.53 o 2 2 4 91960.47 97508.50 2321.69 o 1 3 4 1388.31 1673.52 33.26 o 0 4 4 3022.97 3796.97 78.24 o 2 4 4 97.51 91.60 19.23 o 4 4 4 9086.16 10592.98 193.55 o 1 5 4 770.01 701.60 25.20 o 3 5 4 6570.70 6824.54 97.76 o 0 6 4 210506.44 240944.88 3969.52 o 2 6 4 66454.77 76182.83 955.85 o 4 6 4 2301.48 2167.28 55.72 o 6 6 4 79461.69 79723.31 1893.02 o 1 7 4 844.45 965.52 31.35 o 3 7 4 570.02 721.51 29.88 o 5 7 4 2160.50 1891.01 46.97 o 0 8 4 132522.89 139119.48 3119.03 o 2 8 4 45872.59 48238.39 610.26 o 4 8 4 6703.86 6550.32 114.79 o 6 8 4 53780.85 52427.68 784.25 o 8 8 4 30267.64 29712.30 1585.60 o 1 9 4 5175.66 5684.48 105.43 o 3 9 4 48.60 -33.48 33.48 o 5 9 4 6270.98 5875.11 169.10 o 7 9 4 968.30 1039.57 59.52 o 0 10 4 4681.84 5345.53 271.18 o 2 10 4 1558.01 1612.30 61.77 o 4 10 4 1786.63 1820.28 56.14 o 6 10 4 3912.83 3597.63 152.15 o 8 10 4 300.08 233.36 45.29 o 10 10 4 1759.40 1721.81 222.28 o 1 11 4 15524.12 15719.99 477.04 o 3 11 4 5.26 29.79 42.34 o 5 11 4 3115.64 2622.02 291.02 o 7 11 4 5144.45 4850.68 256.10 o 9 11 4 966.40 945.00 84.44 o 0 12 4 16842.00 18194.39 774.15 o 2 12 4 7957.86 8465.97 292.49 o 4 12 4 10.76 -7.23 58.14 o 6 12 4 7907.38 7831.90 313.69 o 8 12 4 9615.51 9430.89 262.59 o 10 12 4 1694.84 1353.85 101.69 o 12 12 4 702.52 857.13 148.41 o 1 13 4 196.24 327.09 78.22 o 3 13 4 134.59 10.22 77.63 o 5 13 4 268.36 301.85 77.40 o 7 13 4 647.94 505.51 82.68 o 9 13 4 448.82 579.26 88.95 o 11 13 4 401.32 483.55 94.59 o 0 14 4 21962.44 23710.62 772.08 o 2 14 4 7419.43 7817.51 210.43 o 4 14 4 1441.19 1271.09 92.80 o 6 14 4 11815.32 12033.45 593.66 o 8 14 4 6471.28 6743.34 220.40 o 10 14 4 44.29 -68.15 99.54 o 12 14 4 1760.24 1792.04 240.65 o 1 15 4 1910.41 2134.38 108.71 o 3 15 4 47.69 179.23 80.52 o 5 15 4 910.46 1036.38 162.23 o 7 15 4 476.01 475.19 124.09 o 9 15 4 5.34 56.30 88.42 o 11 15 4 250.42 344.45 108.33 o 0 16 4 2819.40 2695.59 268.58 o 2 16 4 694.46 641.19 91.09 o 4 16 4 610.89 279.34 95.16 o 6 16 4 2209.99 2270.30 129.11 o 8 16 4 560.78 397.10 106.49 o 10 16 4 213.68 376.81 108.70 o 1 17 4 3475.73 3907.38 168.39 o 3 17 4 93.43 22.97 100.86 o 5 17 4 1064.57 1015.29 119.74 o 7 17 4 2236.26 2693.60 156.03 o 0 18 4 276.37 375.64 150.90 o 2 18 4 246.18 216.03 130.90 o 4 18 4 84.74 178.65 177.48 o 6 18 4 50.46 58.02 126.07 o 1 19 4 253.82 296.60 131.48 o 1 2 5 602.47 658.71 16.51 o 2 3 5 121619.60 118302.91 2361.71 o 1 4 5 12256.57 11431.04 141.60 o 3 4 5 154309.14 145286.09 2957.90 o 2 5 5 20878.33 19329.04 238.66 o 4 5 5 38763.40 36170.14 540.20 o 1 6 5 9182.85 9246.84 124.87 o 3 6 5 12375.75 12061.52 177.00 o 5 6 5 1700.67 1580.62 49.30 o 2 7 5 1114.62 911.90 40.77 o 4 7 5 9345.31 8714.31 126.47 o 6 7 5 4272.13 3879.01 69.29 o 1 8 5 667.23 808.05 28.94 o 3 8 5 3041.21 2624.37 67.04 o 5 8 5 7934.55 7356.17 134.02 o 7 8 5 713.21 705.27 40.01 o 2 9 5 36949.52 37422.12 620.78 o 4 9 5 60529.68 58773.34 765.28 o 6 9 5 8967.58 8314.31 256.59 o 8 9 5 3135.05 2761.73 104.88 o 1 10 5 14261.59 14024.59 314.77 o 3 10 5 44697.21 43637.84 1001.86 o 5 10 5 8897.67 8597.13 380.03 o 7 10 5 2717.13 2354.59 71.68 o 9 10 5 12973.44 12544.85 470.50 o 2 11 5 20441.22 19680.05 699.27 o 4 11 5 16724.46 16482.66 587.57 o 6 11 5 968.00 951.78 65.93 o 8 11 5 2705.64 2859.23 182.31 o 10 11 5 4930.48 4888.29 165.14 o 1 12 5 4708.84 4574.82 248.36 o 3 12 5 12776.35 12988.02 400.05 o 5 12 5 1898.89 1846.11 76.86 o 7 12 5 1613.13 1598.27 152.10 o 9 12 5 5851.63 5725.50 184.32 o 11 12 5 2331.55 2319.17 117.87 o 2 13 5 475.00 546.92 59.80 o 4 13 5 751.09 640.96 167.79 o 6 13 5 113.01 91.11 81.45 o 8 13 5 170.29 322.86 105.71 o 10 13 5 68.59 188.98 105.41 o 12 13 5 133.52 32.04 89.85 o 1 14 5 40.07 55.48 149.66 o 3 14 5 407.31 477.10 97.51 o 5 14 5 80.63 157.75 80.20 o 7 14 5 805.63 634.15 94.95 o 9 14 5 1218.51 951.44 99.05 o 11 14 5 0.76 -97.21 100.54 o 2 15 5 3732.25 3941.38 125.08 o 4 15 5 6018.83 5929.43 200.64 o 6 15 5 2456.36 2352.86 120.13 o 8 15 5 1.86 36.23 92.86 o 10 15 5 1952.84 2082.14 150.21 o 1 16 5 401.43 537.63 84.13 o 3 16 5 2082.22 2194.58 213.11 o 5 16 5 1466.58 1310.76 122.85 o 7 16 5 46.69 23.80 116.68 o 9 16 5 808.19 1006.40 140.37 o 2 17 5 2695.35 2657.50 146.37 o 4 17 5 3409.42 3435.13 305.52 o 6 17 5 588.19 479.06 151.17 o 8 17 5 409.49 426.35 106.15 o 1 18 5 518.68 487.37 107.55 o 3 18 5 2382.24 2279.62 278.97 o 5 18 5 672.07 879.42 159.67 o 1 1 6 10432.33 12789.90 439.36 o 0 2 6 219.73 279.46 17.69 o 1 3 6 20697.60 25162.24 332.92 o 3 3 6 18532.38 19863.72 518.47 o 0 4 6 8305.75 7354.17 184.03 o 2 4 6 14319.43 14790.79 203.11 o 1 5 6 3654.25 3799.42 57.82 o 3 5 6 5297.03 6134.23 118.68 o 5 5 6 4136.36 3618.62 139.21 o 0 6 6 3107.61 3408.41 159.67 o 2 6 6 329.91 283.71 30.34 o 4 6 6 4376.34 4328.54 73.65 o 1 7 6 22868.65 23291.89 277.99 o 3 7 6 676.83 877.33 45.19 o 5 7 6 9966.25 10269.29 154.82 o 7 7 6 6296.16 7184.30 394.11 o 0 8 6 458.49 460.16 50.33 o 2 8 6 1832.38 1749.90 49.46 o 4 8 6 4104.27 3579.01 65.18 o 6 8 6 3249.37 3466.55 80.26 o 1 9 6 5577.88 5309.61 96.83 o 3 9 6 124.41 181.29 34.19 o 5 9 6 3360.90 3375.55 90.13 o 7 9 6 2516.91 2365.43 175.39 o 9 9 6 0.27 -35.29 119.86 o 0 10 6 28989.44 31298.66 1367.34 o 2 10 6 5800.81 5804.02 193.93 o 4 10 6 3442.14 2767.55 93.95 o 6 10 6 8951.90 9076.51 304.63 o 8 10 6 2745.78 2785.20 133.00 o 1 11 6 1574.49 1942.73 82.30 o 3 11 6 68.07 -11.68 51.92 o 5 11 6 137.97 78.25 46.78 o 7 11 6 626.39 665.93 65.09 o 9 11 6 917.54 1008.24 75.20 o 11 11 6 0.44 -89.15 122.33 o 0 12 6 6101.95 6302.58 573.16 o 2 12 6 1258.93 1222.08 105.86 o 4 12 6 222.41 123.07 51.39 o 6 12 6 2044.58 1949.97 137.96 o 8 12 6 3398.94 3385.72 121.02 o 10 12 6 683.99 789.65 91.12 o 1 13 6 2972.92 3428.39 168.26 o 3 13 6 39.61 -5.31 39.22 o 5 13 6 1274.14 1447.36 131.26 o 7 13 6 1727.87 2218.88 177.99 o 9 13 6 261.50 438.88 99.91 o 11 13 6 87.31 112.06 90.59 o 13 13 6 167.39 159.91 180.28 o 0 14 6 824.71 1015.45 249.57 o 2 14 6 133.77 52.71 86.15 o 4 14 6 857.63 852.40 85.68 o 6 14 6 360.15 303.13 87.57 o 8 14 6 0.67 65.71 83.54 o 10 14 6 463.93 369.68 87.33 o 12 14 6 400.50 375.72 101.72 o 1 15 6 680.44 965.60 137.63 o 3 15 6 23.31 -43.74 81.31 o 5 15 6 467.55 623.34 93.24 o 7 15 6 550.17 603.34 88.35 o 9 15 6 36.89 -86.19 94.27 o 11 15 6 65.43 -33.77 114.87 o 0 16 6 6198.43 7316.40 358.22 o 2 16 6 1533.88 1662.32 156.37 o 4 16 6 413.68 206.86 100.75 o 6 16 6 2731.40 2990.20 156.87 o 8 16 6 1324.90 1142.04 105.60 o 10 16 6 8.36 -1.49 109.05 o 1 17 6 0.92 -50.84 118.58 o 3 17 6 22.28 22.99 101.25 o 5 17 6 24.78 -93.36 132.58 o 7 17 6 5.37 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