#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2200556.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200556_Fobs loop_ _publ_author_name 'Asano, Akiko' 'Taniguchi, Taizo' 'Sasaki, Masahiro' 'Hasegawa, Hiroshi' 'Katsuya, Yoshio' 'Doi, Mitsunobu' _publ_section_title ; A \b-sheet structure formed by C--H···O hydrogen bonds between the thiazole rings and amide bonds of a dimeric desoxazoline ascidiacyclamide analogue ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o834 _journal_page_last o838 _journal_volume 57 _journal_year 2001 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.349 _cell_angle_gamma 90.000 _cell_length_a 11.5563 _cell_length_b 9.9957 _cell_length_c 42.9208 _exptl_crystal_F_000 1956.00 _reflns_d_resolution_high 0.8297 _[local]_cod_data_source_file wn6037Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' O6 Dimer (hexadecapeptide): P21 SP8 100KF' _shelx_refln_list_code 4 _shelx_f_calc_maximum 115.17 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 812.15 972.62 66.82 o 7 0 0 1372.65 1260.77 83.49 o 1 1 0 360.93 614.87 42.13 o 4 1 0 951.38 705.50 70.43 o 6 1 0 214.78 125.44 13.03 o 7 1 0 394.08 403.40 43.84 o 8 1 0 129.09 170.72 19.11 o 9 1 0 626.46 594.57 58.54 o 10 1 0 1363.22 1118.38 78.32 o 3 2 0 3668.51 3361.40 327.27 o 4 2 0 66.70 201.02 19.61 o 5 2 0 857.56 1175.68 86.68 o 6 2 0 352.02 318.64 33.68 o 7 2 0 934.77 935.14 79.87 o 8 2 0 486.24 598.77 63.69 o 9 2 0 1017.84 899.19 80.81 o 10 2 0 304.41 348.91 39.12 o 11 2 0 14.83 3.76 0.80 o 12 2 0 238.53 234.38 34.82 o 1 3 0 1628.27 1242.29 87.83 o 4 3 0 1649.94 2303.50 108.99 o 5 3 0 777.12 1046.62 54.90 o 6 3 0 71.88 201.07 16.52 o 7 3 0 360.69 298.54 31.49 o 8 3 0 219.63 212.67 19.08 o 9 3 0 588.31 688.51 68.23 o 10 3 0 385.41 513.80 42.83 o 11 3 0 76.27 83.13 7.94 o 12 3 0 280.26 231.88 28.34 o 13 3 0 0.65 1.61 0.73 o 0 4 0 1475.32 2904.61 190.24 o 1 4 0 3688.41 3819.39 184.50 o 2 4 0 362.49 273.45 17.62 o 3 4 0 1745.91 1134.56 63.75 o 4 4 0 997.61 548.81 36.66 o 5 4 0 317.83 412.36 27.69 o 6 4 0 411.95 291.47 17.22 o 7 4 0 760.50 715.22 41.35 o 8 4 0 141.66 169.05 21.25 o 9 4 0 11.36 17.23 1.87 o 10 4 0 119.47 150.28 12.89 o 11 4 0 123.28 88.69 12.63 o 12 4 0 346.49 375.38 37.08 o 13 4 0 74.66 36.82 8.19 o 1 5 0 3895.60 4323.29 195.35 o 2 5 0 884.65 427.94 27.17 o 3 5 0 529.83 708.98 48.53 o 4 5 0 773.80 810.77 51.72 o 5 5 0 333.53 280.70 13.85 o 6 5 0 4.48 42.05 3.72 o 7 5 0 65.90 104.66 12.30 o 8 5 0 49.24 59.91 5.75 o 9 5 0 245.01 235.77 20.05 o 10 5 0 52.54 80.02 9.66 o 12 5 0 28.28 21.08 3.93 o 0 6 0 1478.22 1778.83 138.76 o 1 6 0 199.03 143.56 8.76 o 2 6 0 1516.43 1431.75 89.14 o 3 6 0 358.50 530.25 52.46 o 4 6 0 82.55 132.29 8.44 o 5 6 0 734.10 862.24 58.85 o 6 6 0 119.12 141.28 8.53 o 7 6 0 1098.45 1332.17 159.26 o 8 6 0 137.53 155.33 9.29 o 11 6 0 245.62 174.87 18.30 o 1 7 0 323.18 254.00 23.43 o 2 7 0 28.46 43.41 3.48 o 3 7 0 200.88 238.60 19.96 o 4 7 0 595.95 594.77 33.50 o 5 7 0 345.28 551.73 28.14 o 6 7 0 500.75 401.02 21.54 o 7 7 0 38.61 54.25 7.17 o 8 7 0 443.56 445.13 37.20 o 9 7 0 53.91 49.06 4.99 o 10 7 0 92.56 82.76 9.31 o 1 8 0 374.66 391.11 22.47 o 2 8 0 224.45 263.00 15.39 o 3 8 0 196.74 243.24 13.15 o 4 8 0 1247.39 1167.60 73.65 o 5 8 0 305.81 359.18 35.37 o 6 8 0 418.49 377.40 33.19 o 7 8 0 8.88 19.78 2.07 o 8 8 0 49.92 33.73 5.57 o 9 8 0 12.44 16.83 2.08 o 1 9 0 107.88 143.57 9.07 o 2 9 0 195.80 186.13 22.18 o 3 9 0 1.45 2.68 1.29 o 4 9 0 23.89 15.86 1.77 o 5 9 0 164.51 153.43 11.84 o 6 9 0 14.57 2.85 0.78 o 8 9 0 113.25 134.43 16.13 o 9 9 0 33.83 34.45 3.86 o 2 10 0 27.88 39.59 3.29 o 4 10 0 205.08 249.98 30.06 o 5 10 0 10.68 5.99 1.86 o 6 10 0 39.70 39.23 8.59 o 7 10 0 81.19 102.04 14.69 o 1 11 0 76.08 110.94 12.18 o 2 11 0 72.19 99.01 9.18 o 3 11 0 225.55 240.92 27.24 o 5 11 0 21.38 33.94 4.62 o -8 0 1 62.41 27.64 5.03 o -7 0 1 1728.83 1639.65 112.02 o -6 0 1 452.07 310.07 25.77 o -5 0 1 2222.17 1360.63 131.62 o -4 0 1 75.86 35.92 5.33 o -3 0 1 1465.46 860.43 83.14 o 2 0 1 31.76 51.66 4.69 o 4 0 1 380.71 640.19 46.24 o 6 0 1 246.37 184.20 17.89 o 7 0 1 6.01 2.06 0.33 o -10 1 1 411.02 593.41 48.93 o -9 1 1 50.96 58.01 6.47 o -8 1 1 398.20 402.67 43.39 o -7 1 1 1774.31 1678.95 116.87 o -6 1 1 303.96 271.50 30.80 o -5 1 1 1700.24 2188.29 212.73 o -1 1 1 1925.57 1093.31 75.05 o 3 1 1 2493.47 2215.07 218.34 o 4 1 1 3715.27 4391.69 432.54 o 5 1 1 1300.46 1467.26 102.87 o 6 1 1 569.81 573.10 49.25 o 7 1 1 68.70 67.12 7.59 o 8 1 1 93.18 87.71 13.40 o 9 1 1 2065.58 2360.22 161.15 o 10 1 1 748.03 535.12 40.65 o -12 2 1 715.07 672.05 59.56 o -11 2 1 48.23 33.68 5.72 o -10 2 1 503.32 485.46 48.07 o -9 2 1 1647.76 1591.47 124.50 o -8 2 1 1137.55 1213.36 99.41 o -7 2 1 380.48 526.34 53.69 o -6 2 1 656.56 668.45 62.27 o -5 2 1 2128.22 1839.82 180.34 o -4 2 1 22.63 8.74 1.66 o -3 2 1 342.92 805.37 109.66 o 2 2 1 2335.99 2909.45 203.24 o 3 2 1 3352.15 4274.44 422.24 o 4 2 1 5767.65 4719.24 459.23 o 5 2 1 2333.18 2040.41 149.82 o 6 2 1 1072.20 944.82 76.20 o 7 2 1 1855.36 1678.26 123.63 o 8 2 1 477.83 414.82 43.76 o 9 2 1 445.20 443.57 49.84 o 10 2 1 1303.80 1287.94 103.73 o 11 2 1 261.82 296.72 36.00 o 12 2 1 1011.94 778.62 57.09 o -13 3 1 311.80 291.10 25.68 o -12 3 1 604.51 504.05 56.10 o -11 3 1 304.45 287.65 26.43 o -10 3 1 229.13 232.85 22.31 o -9 3 1 305.40 430.94 54.57 o -8 3 1 65.51 52.85 6.16 o -7 3 1 263.85 192.16 14.47 o -6 3 1 654.66 781.94 42.81 o -5 3 1 2136.07 1411.38 75.12 o -4 3 1 1358.21 1596.18 91.05 o -2 3 1 4112.74 3317.94 232.48 o 0 3 1 3244.25 2384.22 133.91 o 1 3 1 7827.58 6743.74 465.53 o 2 3 1 527.77 243.45 15.19 o 3 3 1 2101.10 2086.77 94.10 o 4 3 1 1098.62 1592.58 79.83 o 5 3 1 3081.35 2962.15 169.55 o 6 3 1 298.89 189.98 13.77 o 7 3 1 353.47 336.99 40.86 o 8 3 1 193.13 235.27 20.93 o 9 3 1 71.21 79.69 7.91 o 10 3 1 299.99 299.84 27.46 o 11 3 1 43.69 76.17 8.56 o 12 3 1 187.89 248.79 39.87 o 13 3 1 88.24 54.56 6.62 o -13 4 1 173.70 189.88 21.97 o -12 4 1 1.46 12.91 5.14 o -11 4 1 35.69 17.54 1.83 o -10 4 1 468.51 470.98 45.69 o -9 4 1 586.03 513.75 39.64 o -8 4 1 1064.78 1132.90 171.87 o -7 4 1 48.38 55.13 3.62 o -6 4 1 497.42 691.15 40.42 o -5 4 1 1899.55 1826.68 95.23 o -4 4 1 300.82 300.66 43.51 o -3 4 1 2372.79 2874.10 164.25 o -2 4 1 1280.22 1206.94 72.06 o -1 4 1 3910.18 3334.91 194.77 o 0 4 1 7054.63 6371.54 451.02 o 1 4 1 182.71 146.79 10.49 o 2 4 1 1349.84 1601.18 80.79 o 3 4 1 514.31 805.91 47.67 o 4 4 1 709.20 467.98 32.29 o 5 4 1 1010.37 767.09 47.33 o 6 4 1 902.41 719.33 43.41 o 7 4 1 71.49 63.69 5.17 o 8 4 1 2.92 4.65 0.97 o 9 4 1 475.68 509.53 43.95 o 10 4 1 8.72 15.35 1.45 o 11 4 1 169.54 280.43 56.79 o 12 4 1 99.09 120.87 16.22 o 13 4 1 243.59 300.04 29.22 o -12 5 1 98.86 125.97 10.66 o -11 5 1 178.12 149.04 18.02 o -10 5 1 197.07 222.37 17.25 o -9 5 1 217.64 205.76 15.24 o -8 5 1 251.01 273.44 23.95 o -7 5 1 167.81 146.00 12.71 o -6 5 1 267.19 271.82 18.02 o -5 5 1 570.92 507.51 35.14 o -4 5 1 426.47 246.79 22.35 o -3 5 1 286.83 413.79 28.63 o -2 5 1 703.20 408.86 26.14 o -1 5 1 806.37 1122.10 68.89 o 0 5 1 61.71 70.61 4.81 o 1 5 1 2861.93 3048.76 145.89 o 2 5 1 5018.27 4169.44 201.24 o 3 5 1 622.56 687.39 48.21 o 4 5 1 285.39 431.27 31.81 o 5 5 1 903.34 878.99 55.46 o 6 5 1 445.51 466.75 39.07 o 7 5 1 490.38 460.20 43.35 o 8 5 1 211.00 255.37 31.06 o 9 5 1 179.93 267.24 20.08 o 10 5 1 77.64 69.78 8.62 o 12 5 1 25.40 31.68 4.27 o -12 6 1 11.19 21.83 4.13 o -9 6 1 83.39 83.29 7.30 o -8 6 1 238.10 283.84 21.54 o -7 6 1 91.41 96.18 6.79 o -6 6 1 240.20 174.98 13.60 o -5 6 1 176.33 282.03 18.82 o -4 6 1 2103.56 1927.18 119.70 o -3 6 1 157.15 209.35 13.08 o -2 6 1 1012.24 1059.51 67.23 o -1 6 1 97.31 136.40 9.63 o 0 6 1 257.93 393.65 38.35 o 1 6 1 590.76 661.20 47.15 o 2 6 1 196.26 290.46 15.39 o 3 6 1 632.30 595.11 32.71 o 4 6 1 160.08 259.48 16.01 o 5 6 1 125.76 134.76 8.32 o 6 6 1 13.58 28.70 1.94 o 7 6 1 91.63 69.72 5.29 o 8 6 1 51.41 39.27 10.90 o 10 6 1 4.76 16.49 3.00 o 11 6 1 80.19 85.89 9.90 o -11 7 1 32.89 42.50 5.27 o -10 7 1 191.10 177.29 21.87 o -9 7 1 233.08 231.84 26.89 o -8 7 1 133.35 92.93 5.81 o -7 7 1 252.71 231.25 16.45 o -6 7 1 227.06 256.74 13.49 o -5 7 1 742.41 786.96 68.84 o -4 7 1 52.77 99.92 14.79 o -3 7 1 303.96 317.83 19.27 o -2 7 1 457.90 422.03 62.41 o -1 7 1 3.33 15.10 5.77 o 0 7 1 154.15 165.89 10.12 o 1 7 1 31.79 76.43 4.49 o 2 7 1 1479.20 1434.96 111.06 o 3 7 1 430.13 591.05 42.47 o 4 7 1 92.43 118.93 7.56 o 5 7 1 647.60 653.13 37.57 o 6 7 1 59.54 49.09 6.30 o 7 7 1 82.47 110.12 7.54 o 8 7 1 195.44 240.29 47.78 o 9 7 1 294.57 275.85 43.26 o -9 8 1 211.96 229.99 21.50 o -8 8 1 183.26 226.41 17.37 o -7 8 1 82.11 94.33 8.55 o -6 8 1 83.14 83.57 9.41 o -5 8 1 92.98 141.80 15.11 o -4 8 1 83.03 104.25 9.54 o -3 8 1 225.95 222.95 15.33 o -2 8 1 507.72 498.87 29.39 o -1 8 1 125.24 140.02 15.60 o 0 8 1 132.19 183.50 15.90 o 1 8 1 40.29 71.41 6.10 o 2 8 1 184.19 233.23 18.89 o 3 8 1 642.58 688.91 41.73 o 4 8 1 26.47 20.96 4.25 o 5 8 1 447.84 410.56 25.09 o 6 8 1 27.19 33.71 2.83 o 7 8 1 267.53 305.09 31.38 o 8 8 1 54.43 52.43 5.01 o 9 8 1 137.89 119.13 10.14 o 10 8 1 35.50 44.78 10.06 o -9 9 1 51.40 43.90 4.89 o -8 9 1 7.45 15.29 4.64 o -7 9 1 49.81 52.81 5.94 o -6 9 1 114.66 120.50 14.50 o -5 9 1 236.91 353.73 28.25 o -4 9 1 311.88 475.99 36.26 o -3 9 1 215.22 184.94 15.21 o -1 9 1 129.05 175.97 18.67 o 0 9 1 147.37 118.08 12.58 o 1 9 1 33.42 49.89 3.96 o 2 9 1 259.51 262.64 17.54 o 3 9 1 194.12 183.44 16.12 o 4 9 1 555.70 553.66 33.37 o 5 9 1 146.83 112.22 13.71 o 6 9 1 163.26 155.75 12.98 o 8 9 1 392.74 494.28 51.94 o 9 9 1 73.59 118.53 9.17 o -5 10 1 23.85 21.34 2.93 o -4 10 1 171.03 148.44 22.85 o -3 10 1 276.61 336.66 38.11 o -2 10 1 68.82 89.65 10.42 o -1 10 1 247.47 292.93 32.10 o 0 10 1 87.01 68.91 5.91 o 2 10 1 154.08 145.15 16.54 o 4 10 1 53.49 84.04 9.39 o 6 10 1 43.64 35.25 4.21 o 7 10 1 112.91 96.48 13.48 o -4 11 1 30.15 52.89 6.72 o -3 11 1 5.88 3.87 1.64 o 2 11 1 15.83 15.06 1.90 o 3 11 1 39.33 27.64 5.78 o 1 12 1 127.76 78.84 8.81 o -8 0 2 939.85 1164.49 80.43 o -7 0 2 88.49 172.55 17.78 o -6 0 2 3.19 17.64 2.16 o -5 0 2 1133.46 1079.07 72.93 o -2 0 2 242.12 98.13 8.56 o 7 0 2 556.56 452.43 30.52 o -10 1 2 327.62 370.28 37.94 o -9 1 2 226.98 297.08 31.43 o -8 1 2 780.36 725.51 62.64 o -7 1 2 937.94 1108.09 83.71 o -6 1 2 372.38 321.34 42.44 o -5 1 2 1538.69 2167.91 205.09 o -4 1 2 936.88 496.50 33.28 o 1 1 2 2994.06 2493.42 170.42 o 3 1 2 3883.98 1738.78 173.18 o 4 1 2 936.34 680.19 47.06 o 5 1 2 2050.83 2258.47 224.93 o 6 1 2 236.86 272.67 28.15 o 7 1 2 67.01 98.51 7.06 o 8 1 2 448.06 492.16 47.28 o 9 1 2 954.73 1072.84 76.30 o 10 1 2 496.13 485.07 35.47 o -12 2 2 252.36 217.79 27.23 o -11 2 2 168.82 147.71 19.08 o -10 2 2 179.77 212.07 24.88 o -9 2 2 695.17 903.08 78.83 o -8 2 2 228.05 300.85 21.26 o -7 2 2 52.03 35.09 3.77 o -6 2 2 71.43 108.24 11.36 o -5 2 2 829.17 576.43 34.94 o -4 2 2 525.70 278.71 38.42 o -3 2 2 455.96 1292.95 263.11 o -2 2 2 4087.99 4274.02 420.02 o 1 2 2 3858.39 3633.41 358.94 o 2 2 2 4.70 148.57 8.74 o 3 2 2 10514.22 8299.96 827.36 o 4 2 2 1162.34 781.41 41.38 o 5 2 2 130.01 95.26 7.41 o 6 2 2 1065.54 1160.11 84.76 o 7 2 2 185.36 176.24 13.47 o 8 2 2 529.54 721.82 65.94 o 9 2 2 589.41 887.83 81.12 o 10 2 2 209.60 351.62 31.62 o 11 2 2 447.09 458.29 91.94 o 12 2 2 273.51 157.46 27.61 o -13 3 2 350.10 340.94 33.95 o -12 3 2 312.72 349.85 41.47 o -11 3 2 191.27 151.68 19.45 o -10 3 2 35.90 50.76 4.09 o -9 3 2 179.03 257.95 19.15 o -8 3 2 1494.58 1946.95 148.12 o -7 3 2 770.73 939.19 78.41 o -6 3 2 1307.11 1218.78 68.98 o -5 3 2 1190.17 845.66 52.76 o -4 3 2 126.28 86.78 10.87 o -3 3 2 1618.59 1882.35 175.47 o -2 3 2 4534.29 3887.23 384.71 o 3 3 2 3222.04 2039.97 105.64 o 4 3 2 5279.83 7110.81 711.05 o 5 3 2 2311.68 2771.61 150.71 o 6 3 2 1417.04 2100.94 146.19 o 7 3 2 433.62 449.27 47.71 o 8 3 2 475.07 561.40 64.83 o 9 3 2 9.59 13.83 1.38 o 10 3 2 62.29 48.04 3.80 o 11 3 2 311.83 302.57 23.97 o 12 3 2 283.79 310.47 49.62 o 13 3 2 188.65 212.94 30.07 o -13 4 2 33.44 39.94 3.69 o -12 4 2 181.95 179.99 24.37 o -11 4 2 15.17 8.16 1.15 o -10 4 2 24.69 10.02 1.45 o -9 4 2 356.96 343.72 24.77 o -8 4 2 324.07 258.66 19.90 o -7 4 2 108.03 127.57 8.80 o -6 4 2 899.91 757.59 45.65 o -5 4 2 174.17 217.51 19.41 o -4 4 2 909.75 838.67 55.64 o -3 4 2 486.03 480.01 38.26 o -2 4 2 2803.19 2630.74 145.01 o -1 4 2 1489.37 1319.60 81.35 o 0 4 2 2059.52 1564.89 104.51 o 1 4 2 178.31 281.22 43.47 o 2 4 2 931.35 1585.60 84.17 o 3 4 2 1730.00 1326.45 72.06 o 4 4 2 1818.01 1675.97 91.05 o 5 4 2 161.69 155.68 11.35 o 6 4 2 150.58 176.72 19.65 o 7 4 2 140.71 210.75 26.58 o 8 4 2 45.63 60.27 5.63 o 9 4 2 46.21 50.58 4.88 o 10 4 2 165.51 187.91 15.88 o 11 4 2 442.03 396.03 46.00 o 12 4 2 53.85 72.53 11.61 o 13 4 2 98.97 109.63 11.08 o -12 5 2 34.68 50.06 7.29 o -10 5 2 290.28 222.37 17.06 o -9 5 2 492.95 689.63 72.48 o -8 5 2 383.94 377.16 30.15 o -7 5 2 403.22 438.76 27.80 o -6 5 2 32.88 150.39 9.78 o -5 5 2 2599.80 2330.77 119.37 o -4 5 2 1124.42 1272.28 73.78 o -3 5 2 522.33 474.68 37.30 o -2 5 2 326.99 295.65 24.52 o -1 5 2 3706.22 4010.02 283.29 o 0 5 2 6397.96 6578.92 434.34 o 1 5 2 1296.85 986.08 61.39 o 2 5 2 2720.20 3224.98 154.67 o 3 5 2 2980.82 3087.54 151.13 o 4 5 2 72.57 116.82 6.25 o 5 5 2 364.26 485.09 34.03 o 6 5 2 810.51 766.16 62.81 o 7 5 2 801.35 902.04 63.46 o 8 5 2 69.87 71.08 6.59 o 9 5 2 294.97 426.08 37.37 o 10 5 2 107.12 108.37 13.39 o 12 5 2 3.75 16.75 1.72 o -12 6 2 139.88 179.55 12.34 o -10 6 2 304.41 270.76 29.67 o -9 6 2 33.70 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86.09 111.42 7.96 o -3 3 49 27.25 18.24 3.38 o -2 3 49 73.15 52.09 6.57 o -1 3 49 49.75 43.62 3.14 o 0 3 49 17.38 19.93 1.89 o 1 3 49 120.00 158.31 15.05 o 2 3 49 12.77 12.92 1.30 o -3 0 50 34.84 18.96 3.69 o -2 0 50 57.96 78.56 8.90 o -1 0 50 70.26 66.44 6.20 o 0 0 50 19.46 11.85 1.69 o 1 0 50 351.39 370.10 28.78 o 2 0 50 266.86 315.54 26.98 o 3 0 50 360.49 385.68 32.18 o -3 1 50 26.92 15.45 2.20 o -2 1 50 89.07 84.46 5.64 o -1 1 50 5.61 3.36 0.93 o 0 1 50 242.39 237.73 13.28 o 1 1 50 10.94 6.52 1.06 o 2 1 50 54.98 38.38 2.70 o 3 1 50 46.92 44.77 3.19 o -3 2 50 40.67 28.38 4.03 o -2 2 50 31.91 24.63 3.25 o -1 2 50 52.33 39.61 4.24 o 0 2 50 32.24 59.76 6.55 o 1 2 50 65.58 63.85 5.71 o 2 2 50 66.67 61.70 3.87 o -1 3 50 64.91 35.04 8.52 o 0 3 50 29.75 21.50 5.47 o -2 0 51 338.49 261.56 60.26 o -1 0 51 164.90 163.52 15.57 o 0 0 51 101.63 81.52 11.47 o 1 0 51 8.80 6.16 1.62 o 2 0 51 41.80 30.79 5.41 o -2 1 51 98.16 41.72 6.70 o -1 1 51 27.96 36.50 4.89 o 0 1 51 39.68 38.84 3.88 o 1 1 51 227.02 238.27 15.15 o