#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/05/2200599.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200599_Fobs loop_ _publ_author_name 'Bond, Andrew D.' 'Davies, John E.' _publ_section_title ; 2-Picoline ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1089 _journal_page_last o1090 _journal_volume 57 _journal_year 2001 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.6593 _cell_length_b 7.0878 _cell_length_c 11.7358 _exptl_crystal_F_000 200.00 _reflns_d_resolution_high 0.7704 _[local]_cod_data_source_file bt6088Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' jd0010 in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 41.58 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 193.45 198.22 7.49 o 4 0 0 42.74 54.46 2.47 o 6 0 0 159.26 167.91 7.68 o 8 0 0 0.13 -0.01 0.45 o 2 1 0 20.45 18.15 0.78 o 3 1 0 121.53 129.35 5.36 o 4 1 0 47.03 44.83 1.68 o 5 1 0 0.70 0.66 0.26 o 6 1 0 30.47 34.51 1.56 o 7 1 0 18.52 16.94 1.19 o 8 1 0 0.47 0.53 0.53 o 1 2 0 1729.06 1459.65 48.78 o 2 2 0 32.34 27.62 1.00 o 3 2 0 9.94 7.91 0.38 o 4 2 0 17.57 12.79 0.65 o 5 2 0 30.48 33.06 1.49 o 6 2 0 58.00 54.35 2.75 o 7 2 0 0.41 0.00 0.14 o 8 2 0 5.77 6.60 0.74 o 1 3 0 22.97 20.07 0.82 o 2 3 0 5.40 5.73 0.35 o 3 3 0 13.55 10.58 0.44 o 4 3 0 78.31 71.74 2.64 o 5 3 0 25.60 25.74 1.16 o 6 3 0 50.07 59.57 2.93 o 7 3 0 1.31 1.69 0.60 o 8 3 0 1.81 2.44 0.52 o 0 4 0 369.51 327.45 13.75 o 1 4 0 109.52 98.97 3.25 o 2 4 0 43.12 44.12 1.62 o 3 4 0 3.57 3.57 0.40 o 4 4 0 0.03 0.24 0.22 o 5 4 0 17.75 13.95 0.85 o 6 4 0 3.58 4.18 0.43 o 7 4 0 1.31 1.50 0.42 o 1 5 0 83.68 80.02 2.99 o 2 5 0 7.88 5.43 0.97 o 3 5 0 12.77 15.77 0.94 o 4 5 0 11.02 11.39 0.67 o 5 5 0 13.03 13.59 0.76 o 6 5 0 0.06 -0.11 0.47 o 7 5 0 5.59 7.20 0.84 o 0 6 0 221.10 226.33 8.92 o 1 6 0 0.23 0.03 0.45 o 2 6 0 50.44 50.82 2.87 o 4 6 0 0.00 0.56 0.43 o 5 6 0 0.43 0.56 0.46 o 6 6 0 22.04 20.69 1.45 o 1 7 0 12.63 13.50 0.92 o 2 7 0 0.43 0.42 0.42 o 3 7 0 9.47 9.10 0.76 o 4 7 0 3.08 4.07 0.57 o 5 7 0 0.38 0.80 0.54 o 0 8 0 4.11 5.44 0.85 o 1 8 0 3.12 2.91 0.79 o 2 8 0 1.54 1.08 0.74 o 3 8 0 14.39 16.22 1.25 o 1 9 0 0.00 0.16 0.40 o 1 0 1 318.71 320.75 12.11 o 2 0 1 84.92 67.18 2.18 o 3 0 1 255.23 286.21 11.96 o 4 0 1 98.90 99.73 4.02 o 5 0 1 36.91 42.27 1.78 o 6 0 1 9.53 10.29 0.76 o 7 0 1 22.51 25.20 1.18 o 8 0 1 1.93 2.28 0.75 o -5 1 1 116.83 120.02 4.00 o 1 1 1 848.28 659.88 24.99 o 2 1 1 110.16 100.57 3.73 o 3 1 1 21.24 22.10 0.93 o 4 1 1 71.33 95.90 3.80 o 6 1 1 84.93 92.72 3.44 o 7 1 1 20.39 20.28 1.33 o 8 1 1 0.63 0.84 0.56 o -8 2 1 4.84 5.62 0.83 o -1 2 1 1379.10 1182.95 47.05 o 0 2 1 367.48 286.21 14.14 o 2 2 1 43.11 39.27 1.52 o 3 2 1 41.32 46.47 1.71 o 4 2 1 182.06 206.98 7.22 o 5 2 1 237.35 233.59 8.83 o 6 2 1 42.84 42.97 1.99 o 7 2 1 17.15 16.32 0.89 o -2 3 1 234.11 237.44 10.31 o -1 3 1 29.96 24.93 0.95 o 0 3 1 20.26 19.67 0.98 o 3 3 1 10.30 7.16 0.35 o 4 3 1 46.98 44.17 1.77 o 5 3 1 225.89 244.28 11.52 o 6 3 1 7.21 8.85 0.54 o 7 3 1 1.81 2.21 0.37 o 8 3 1 1.91 2.07 0.47 o -2 4 1 32.51 26.36 1.02 o -1 4 1 271.58 255.09 8.38 o 0 4 1 0.08 0.07 0.23 o 3 4 1 1.15 1.28 0.19 o 4 4 1 117.82 100.80 4.04 o 5 4 1 121.12 124.05 6.26 o 6 4 1 6.53 6.54 0.49 o 7 4 1 5.17 6.44 0.68 o -7 5 1 3.99 3.55 0.66 o -3 5 1 44.61 48.31 2.38 o -2 5 1 45.72 50.60 2.22 o -1 5 1 26.49 25.43 1.00 o 0 5 1 2.59 1.95 0.32 o 4 5 1 39.88 39.65 1.72 o 5 5 1 12.21 12.04 0.66 o 6 5 1 1.00 1.37 0.48 o -6 6 1 5.30 4.96 0.71 o -3 6 1 3.77 3.48 0.54 o -2 6 1 1.27 1.59 0.51 o -1 6 1 6.87 7.16 0.61 o 0 6 1 28.47 29.03 1.31 o 4 6 1 17.82 18.77 0.89 o 5 6 1 1.34 1.56 0.31 o -5 7 1 4.95 3.57 0.65 o -3 7 1 12.01 13.36 0.89 o -2 7 1 2.03 2.11 0.46 o -1 7 1 18.30 17.41 0.89 o 0 7 1 2.34 2.11 0.41 o 4 7 1 15.00 14.12 0.83 o -3 8 1 3.76 3.00 0.68 o -2 8 1 14.76 18.77 1.28 o 0 8 1 4.10 3.48 0.75 o 1 8 1 16.57 16.07 1.07 o -1 9 1 7.50 3.86 0.55 o 0 9 1 3.66 2.94 0.63 o 1 0 2 634.06 639.92 22.69 o 2 0 2 103.56 107.86 3.71 o 3 0 2 314.82 323.75 12.58 o 4 0 2 90.09 110.48 4.31 o 5 0 2 12.21 13.09 0.71 o 6 0 2 146.99 169.99 6.54 o 7 0 2 57.52 62.35 2.82 o 8 0 2 4.84 5.18 0.64 o 1 1 2 1155.59 1032.77 33.95 o 2 1 2 399.94 390.91 14.88 o 3 1 2 0.21 0.32 0.13 o 4 1 2 34.48 50.12 1.78 o 5 1 2 14.72 19.40 0.90 o 6 1 2 101.67 112.32 4.91 o 7 1 2 10.56 10.46 0.98 o 8 1 2 3.49 2.82 0.79 o -1 2 2 302.13 270.24 11.24 o 0 2 2 0.14 0.19 0.12 o 2 2 2 50.12 43.72 1.66 o 3 2 2 33.36 37.48 1.30 o 4 2 2 24.46 28.50 1.26 o 5 2 2 3.80 3.26 0.34 o 6 2 2 39.98 39.50 1.77 o 7 2 2 17.20 13.20 0.99 o 8 2 2 9.82 9.40 0.89 o -8 3 2 11.28 12.87 1.01 o -2 3 2 567.72 570.59 23.42 o -1 3 2 207.85 181.37 6.45 o 0 3 2 11.25 13.11 0.50 o 3 3 2 5.32 6.27 0.32 o 4 3 2 36.93 33.67 1.37 o 5 3 2 29.03 30.99 1.73 o 6 3 2 1.93 2.43 0.32 o 7 3 2 10.10 12.09 0.82 o -7 4 2 6.16 7.91 0.68 o -2 4 2 17.05 13.84 0.59 o -1 4 2 26.31 21.99 0.93 o 0 4 2 0.21 0.59 0.20 o 3 4 2 46.27 36.74 1.43 o 4 4 2 95.62 90.97 4.28 o 5 4 2 2.92 3.04 0.32 o 6 4 2 30.08 32.45 1.86 o -7 5 2 1.92 0.07 0.71 o -6 5 2 37.41 35.87 2.09 o -3 5 2 33.19 33.85 1.77 o -2 5 2 40.89 41.39 1.81 o -1 5 2 26.31 25.58 1.00 o 0 5 2 78.56 73.56 3.59 o 4 5 2 54.39 51.36 2.29 o 5 5 2 26.47 29.57 1.41 o -6 6 2 26.52 26.63 1.57 o -5 6 2 5.46 5.97 0.69 o -3 6 2 54.65 53.18 2.61 o -1 6 2 6.34 6.35 0.61 o 0 6 2 18.51 18.80 1.02 o 2 6 2 3.55 3.98 0.56 o 4 6 2 53.66 46.63 1.97 o -5 7 2 1.35 1.11 0.59 o -4 7 2 1.83 2.67 0.77 o -3 7 2 44.74 45.75 2.21 o -2 7 2 0.53 0.01 0.44 o -1 7 2 0.89 0.13 0.36 o 0 7 2 11.73 11.34 0.69 o -4 8 2 3.45 2.42 0.68 o -3 8 2 6.93 7.61 1.03 o -2 8 2 7.19 6.46 0.85 o -1 8 2 1.46 2.26 0.78 o 0 8 2 20.16 21.81 1.31 o 0 9 2 0.31 0.51 0.48 o 1 0 3 260.77 238.96 9.40 o 2 0 3 15.05 17.22 0.69 o 3 0 3 27.78 19.33 0.87 o 4 0 3 90.70 110.48 4.31 o 5 0 3 0.08 -0.32 0.32 o 6 0 3 25.75 33.80 1.55 o 7 0 3 96.79 112.16 4.91 o 8 0 3 0.73 1.00 0.71 o -4 1 3 20.36 18.50 0.88 o -1 1 3 753.63 688.09 23.92 o 0 1 3 28.40 18.47 0.75 o 2 1 3 185.31 155.54 5.59 o 3 1 3 685.90 748.37 27.03 o 5 1 3 5.07 4.37 0.44 o 6 1 3 24.58 23.66 1.26 o 7 1 3 30.84 30.44 1.89 o 8 1 3 10.35 11.41 0.95 o -8 2 3 11.85 9.85 1.10 o -6 2 3 10.71 11.41 0.72 o -1 2 3 622.44 531.69 20.68 o 0 2 3 648.61 690.09 32.34 o 2 2 3 212.78 277.66 12.03 o 3 2 3 95.00 142.83 6.27 o 4 2 3 8.12 13.20 0.69 o 5 2 3 0.56 0.40 0.17 o 7 2 3 38.83 52.29 2.20 o -7 3 3 12.15 11.85 1.02 o -2 3 3 358.02 346.42 12.31 o -1 3 3 703.85 625.97 20.16 o 0 3 3 19.75 14.85 0.76 o 3 3 3 34.94 39.41 1.57 o 4 3 3 12.11 12.38 0.75 o 5 3 3 33.48 41.05 1.70 o 6 3 3 3.08 3.86 0.40 o -7 4 3 10.42 11.13 0.89 o -5 4 3 6.55 5.91 0.65 o -2 4 3 261.82 277.28 10.12 o -1 4 3 133.50 114.67 3.74 o 0 4 3 1.66 1.73 0.38 o 3 4 3 4.04 4.19 0.26 o 4 4 3 13.44 16.01 0.82 o 6 4 3 1.04 1.40 0.33 o -7 5 3 4.42 3.83 0.86 o -6 5 3 8.77 10.98 0.81 o -2 5 3 69.90 69.51 2.85 o -1 5 3 4.01 4.19 0.36 o 0 5 3 0.73 0.84 0.16 o 3 5 3 99.66 82.55 2.83 o 4 5 3 6.72 6.80 0.42 o 5 5 3 23.94 27.98 1.09 o -6 6 3 1.26 0.87 0.72 o -5 6 3 1.22 1.59 0.49 o -3 6 3 8.47 9.29 0.63 o -2 6 3 30.46 29.28 1.48 o 0 6 3 112.47 158.59 9.57 o 1 6 3 3.49 2.82 0.40 o 4 6 3 4.28 3.83 0.39 o -5 7 3 0.26 0.20 0.46 o -3 7 3 13.08 14.18 1.00 o -2 7 3 9.46 12.41 0.83 o -1 7 3 64.56 68.75 2.96 o 0 7 3 3.50 2.78 0.44 o 4 7 3 3.98 3.51 0.80 o -3 8 3 1.17 1.79 0.76 o -2 8 3 3.34 2.80 0.76 o -1 8 3 33.17 35.23 1.99 o 0 8 3 54.94 60.92 3.14 o 0 0 4 549.54 607.10 26.59 o 1 0 4 50.67 50.17 1.72 o 2 0 4 110.33 121.69 4.53 o 3 0 4 75.76 86.89 3.19 o 4 0 4 27.77 32.15 1.29 o 5 0 4 2.51 2.68 0.40 o 6 0 4 24.23 24.03 1.16 o 7 0 4 7.17 6.41 0.79 o 8 0 4 5.06 4.51 0.65 o -6 1 4 69.01 67.87 3.38 o -2 1 4 250.58 236.62 9.24 o -1 1 4 33.92 33.45 1.36 o 0 1 4 627.59 878.54 38.07 o 3 1 4 4.08 3.74 0.28 o 4 1 4 27.12 27.98 1.17 o 5 1 4 13.52 12.65 0.70 o 7 1 4 47.61 51.85 3.06 o 8 1 4 10.68 11.72 1.22 o -8 2 4 12.67 10.58 0.99 o -7 2 4 15.69 16.26 1.20 o -6 2 4 6.25 4.51 0.53 o -4 2 4 30.18 28.71 1.30 o -3 2 4 10.02 11.75 0.68 o -2 2 4 380.28 391.81 14.29 o -1 2 4 14.86 14.38 0.61 o 0 2 4 65.90 71.81 2.90 o 5 2 4 13.39 18.18 0.84 o -7 3 4 2.23 2.39 0.53 o -4 3 4 48.93 44.88 1.99 o -3 3 4 8.28 8.25 0.46 o 0 3 4 8.15 7.89 0.51 o 1 3 4 53.86 86.32 4.02 o 2 3 4 85.21 75.66 2.97 o 5 3 4 67.89 89.60 4.17 o 6 3 4 0.04 0.26 0.26 o -7 4 4 6.13 7.89 0.83 o -6 4 4 28.59 28.91 1.59 o -2 4 4 127.56 126.69 4.88 o -1 4 4 18.89 17.50 0.76 o 0 4 4 5.91 6.37 0.38 o 3 4 4 40.23 42.47 1.59 o 4 4 4 49.13 53.45 2.50 o 5 4 4 23.18 30.07 1.79 o -6 5 4 29.48 28.50 1.74 o -5 5 4 62.40 58.51 2.38 o -2 5 4 63.38 95.97 4.62 o -1 5 4 7.14 6.46 0.52 o 0 5 4 73.96 72.20 3.62 o 3 5 4 77.27 71.74 2.90 o 4 5 4 29.31 26.67 1.33 o -6 6 4 16.98 15.05 1.09 o -5 6 4 2.60 2.25 0.52 o -4 6 4 31.44 28.18 1.33 o -2 6 4 13.81 13.09 0.74 o -1 6 4 35.23 34.47 1.47 o 0 6 4 4.70 3.47 0.42 o 3 6 4 34.46 25.93 1.08 o -5 7 4 0.37 0.39 0.47 o -4 7 4 21.12 21.39 1.41 o -3 7 4 52.50 59.10 3.04 o -2 7 4 7.51 8.30 0.77 o -1 7 4 1.05 0.20 0.43 o 0 7 4 91.93 86.39 3.60 o -3 8 4 10.91 10.58 0.86 o -2 8 4 18.98 21.32 1.30 o -1 8 4 9.89 12.28 0.96 o 0 8 4 0.83 -0.01 0.50 o 1 0 5 158.57 173.57 5.91 o 2 0 5 21.36 22.49 0.83 o 3 0 5 307.29 352.82 12.28 o 4 0 5 2.45 4.51 0.39 o 5 0 5 36.16 44.32 1.92 o 6 0 5 8.64 9.06 0.69 o 7 0 5 2.33 2.48 0.57 o 8 0 5 0.99 0.33 0.71 o -2 1 5 24.70 27.42 1.15 o -1 1 5 34.69 38.89 1.61 o 0 1 5 97.24 142.01 7.70 o 3 1 5 39.69 38.22 1.36 o 4 1 5 29.13 30.23 1.21 o 5 1 5 26.45 22.96 1.13 o 6 1 5 8.48 7.26 0.59 o 7 1 5 8.77 6.35 0.67 o 8 1 5 9.48 8.99 1.05 o -7 2 5 11.50 13.25 1.02 o -6 2 5 2.78 2.06 0.62 o -5 2 5 8.24 6.16 0.53 o -4 2 5 18.23 15.14 0.83 o -3 2 5 67.28 67.12 2.37 o -2 2 5 116.19 113.37 4.29 o -1 2 5 7.02 6.90 0.34 o 0 2 5 42.40 41.78 1.87 o -7 3 5 12.69 15.44 1.46 o -6 3 5 8.37 7.82 0.66 o -5 3 5 96.86 89.67 4.10 o -4 3 5 32.90 26.16 1.13 o -3 3 5 27.61 29.20 1.36 o -2 3 5 12.40 12.35 0.53 o 0 3 5 2.27 1.52 0.27 o 1 3 5 274.17 284.15 12.43 o -7 4 5 1.14 1.11 0.79 o -6 4 5 10.73 10.24 0.75 o -5 4 5 8.70 8.25 0.66 o -4 4 5 29.17 26.47 1.29 o -3 4 5 50.70 55.02 2.37 o -1 4 5 65.99 53.79 2.40 o 0 4 5 3.55 4.13 0.31 o 2 4 5 88.69 73.43 2.67 o -6 5 5 0.53 1.42 0.61 o -5 5 5 19.11 18.15 1.07 o -4 5 5 5.50 5.77 0.69 o -2 5 5 54.35 57.07 2.35 o -1 5 5 75.32 65.15 2.58 o 0 5 5 170.38 253.63 12.71 o 3 5 5 30.11 27.66 1.36 o -5 6 5 8.01 8.14 0.89 o -4 6 5 9.67 8.90 0.86 o -3 6 5 85.71 98.67 4.15 o -2 6 5 0.89 1.43 0.35 o -1 6 5 49.85 48.62 2.54 o 0 6 5 58.95 88.38 4.14 o -4 7 5 5.79 5.15 0.66 o -2 7 5 13.40 13.87 0.79 o 0 7 5 106.85 109.36 4.21 o 1 7 5 17.94 18.93 1.09 o 3 7 5 8.80 9.06 0.76 o -3 8 5 10.33 10.73 1.00 o -2 8 5 13.98 15.17 1.12 o -1 8 5 2.32 2.11 0.55 o 0 8 5 19.21 18.44 1.14 o 0 0 6 870.72 870.00 34.07 o 1 0 6 2.48 2.37 0.18 o 2 0 6 1.31 1.43 0.15 o 3 0 6 170.10 167.72 6.30 o 4 0 6 12.61 15.65 0.81 o 5 0 6 2.76 4.53 0.37 o 6 0 6 8.68 6.93 0.58 o 7 0 6 11.19 12.38 0.96 o -3 1 6 21.25 20.24 1.26 o -2 1 6 14.27 15.17 1.51 o -1 1 6 320.42 534.15 21.96 o 0 1 6 234.48 335.90 24.24 o 4 1 6 180.05 177.90 6.28 o 5 1 6 13.01 11.62 0.67 o 6 1 6 6.83 6.10 0.60 o 7 1 6 10.54 9.71 0.90 o -7 2 6 7.29 5.73 0.73 o -6 2 6 6.09 3.23 0.57 o -5 2 6 45.33 46.42 2.28 o -4 2 6 208.46 200.58 8.93 o -3 2 6 22.44 23.70 2.22 o -2 2 6 99.13 99.65 4.02 o -1 2 6 35.33 36.00 1.69 o 0 2 6 163.15 173.47 7.71 o -7 3 6 2.27 1.85 0.69 o -6 3 6 11.10 9.90 0.91 o -5 3 6 32.02 32.10 1.42 o -4 3 6 41.71 38.84 1.75 o -3 3 6 14.53 15.29 0.95 o -2 3 6 72.23 68.56 2.64 o -1 3 6 5.62 7.34 0.37 o 0 3 6 1.10 0.84 0.16 o -6 4 6 8.21 6.90 0.90 o -5 4 6 67.63 61.34 2.92 o -4 4 6 28.55 28.99 1.39 o -3 4 6 26.90 26.55 1.21 o -2 4 6 85.84 91.34 3.78 o 0 4 6 2.70 2.18 0.21 o 1 4 6 59.69 64.11 3.53 o 7 4 6 0.28 0.59 0.61 o -6 5 6 2.48 2.60 0.99 o -5 5 6 6.66 7.38 0.70 o -4 5 6 4.77 4.18 0.51 o -3 5 6 18.49 16.47 0.93 o -1 5 6 67.43 60.74 2.55 o 0 5 6 1.46 1.52 0.24 o 2 5 6 16.63 16.91 0.78 o -5 6 6 0.26 1.63 0.89 o -4 6 6 29.45 24.74 1.51 o -3 6 6 14.78 16.32 0.98 o -2 6 6 7.38 7.34 0.66 o -1 6 6 26.45 28.79 1.35 o 0 6 6 25.61 37.71 1.91 o -4 7 6 17.65 15.32 1.19 o -3 7 6 20.92 21.60 1.41 o -2 7 6 8.11 8.10 0.82 o -1 7 6 15.15 16.72 0.90 o 0 7 6 2.23 2.14 0.58 o -2 8 6 21.26 23.51 1.40 o -1 8 6 2.47 2.76 0.57 o 0 8 6 5.68 6.23 0.65 o 1 0 7 22.04 18.86 0.92 o 2 0 7 12.06 12.14 0.82 o 3 0 7 372.44 344.31 11.42 o 4 0 7 4.59 3.93 0.33 o 5 0 7 0.67 0.70 0.35 o 6 0 7 12.83 10.98 0.81 o 7 0 7 16.55 15.95 1.24 o -7 1 7 0.26 0.53 0.72 o -5 1 7 7.07 4.93 0.69 o -4 1 7 24.92 24.10 1.27 o -3 1 7 11.22 9.26 0.79 o -2 1 7 47.33 56.44 4.05 o -1 1 7 30.05 34.60 1.39 o 0 1 7 0.29 -0.07 0.27 o 6 1 7 11.57 8.21 0.63 o -7 2 7 5.60 5.88 0.81 o -6 2 7 17.29 16.26 1.01 o -5 2 7 19.14 15.65 0.96 o -4 2 7 27.94 23.18 1.10 o -3 2 7 131.19 113.53 5.26 o -2 2 7 7.08 10.24 0.70 o -1 2 7 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