#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/06/2200617.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200617_Fobs loop_ _publ_author_name 'Bond, Andrew D.' 'Davies, John E.' _publ_section_title ; (1R)-({-})-Fenchone ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1034 _journal_page_last o1035 _journal_volume 57 _journal_year 2001 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.335 _cell_angle_gamma 90.000 _cell_length_a 6.0520 _cell_length_b 10.2748 _cell_length_c 7.1621 _exptl_crystal_F_000 168.00 _reflns_d_resolution_high 0.8406 _[local]_cod_data_source_file cf6114Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' jd0104 (Fenchone) in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 33.92 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 -12 0 8.58 7.97 1.00 o 1 -12 0 1.88 1.22 1.28 o 1 -11 0 26.67 30.08 2.02 o 2 -11 0 9.42 9.39 1.35 o 3 -11 0 17.98 19.30 1.77 o 0 -10 0 31.58 34.84 1.86 o 1 -10 0 25.01 23.91 1.51 o 2 -10 0 28.26 30.57 1.91 o 3 -10 0 1.57 1.77 0.87 o 1 -9 0 100.02 115.63 5.03 o 0 -8 0 36.14 44.34 2.62 o 1 -8 0 61.19 54.68 2.93 o 0 -6 0 72.07 63.65 3.63 o 0 -4 0 61.38 48.90 2.69 o 0 -2 0 1150.60 535.44 34.43 o 2 0 0 569.69 476.04 19.63 o 3 0 0 172.34 185.50 9.06 o 4 0 0 75.40 67.74 3.89 o 5 0 0 0.70 1.03 1.32 o 6 0 0 31.21 33.13 2.26 o 7 0 0 1.66 0.87 1.14 o 2 1 0 354.28 360.19 15.67 o 3 1 0 97.68 101.10 4.29 o 4 1 0 46.60 50.62 2.90 o 5 1 0 102.04 89.86 4.12 o 6 1 0 43.09 45.00 3.20 o 7 1 0 8.98 8.60 1.17 o 1 2 0 798.65 718.69 34.05 o 2 2 0 472.40 423.42 18.18 o 3 2 0 54.26 45.79 1.73 o 4 2 0 0.51 1.17 0.51 o 5 2 0 37.18 36.49 2.71 o 6 2 0 32.66 34.59 3.14 o 1 3 0 794.85 729.42 35.23 o 2 3 0 39.20 40.58 2.36 o 3 3 0 308.78 349.67 16.27 o 4 3 0 53.24 52.60 2.91 o 5 3 0 2.66 2.49 0.82 o 6 3 0 7.12 6.49 0.94 o 1 4 0 209.05 182.84 8.62 o 2 4 0 291.81 300.24 13.80 o 3 4 0 124.32 116.60 5.61 o 4 4 0 132.50 139.19 9.24 o 5 4 0 18.25 16.22 1.18 o 6 4 0 18.90 17.30 1.49 o 1 5 0 6.75 5.67 0.36 o 2 5 0 99.40 103.46 4.57 o 3 5 0 202.36 199.23 10.44 o 4 5 0 52.13 54.77 2.66 o 5 5 0 77.68 74.38 4.39 o 6 5 0 18.13 17.34 1.87 o 1 6 0 37.00 31.98 1.53 o 2 6 0 18.83 18.92 0.95 o 3 6 0 47.39 45.17 2.74 o 4 6 0 69.89 70.50 4.69 o 5 6 0 25.84 27.27 2.18 o 6 6 0 17.00 21.11 2.10 o 1 7 0 28.80 26.29 1.12 o 2 7 0 21.16 19.97 1.00 o 3 7 0 15.54 15.79 1.11 o 4 7 0 22.09 22.48 1.34 o 5 7 0 4.00 5.07 0.92 o 2 8 0 87.39 82.47 4.98 o 3 8 0 20.81 20.74 1.47 o 4 8 0 0.64 1.38 0.57 o 5 8 0 1.26 2.05 1.15 o 2 9 0 17.06 16.33 0.92 o 3 9 0 3.75 2.75 0.47 o 4 9 0 0.21 0.25 0.50 o -1 -12 1 21.98 13.27 1.07 o 0 -12 1 7.85 8.66 1.30 o 1 -12 1 0.16 0.57 1.12 o -3 -11 1 0.28 0.38 0.76 o -2 -11 1 9.23 10.40 1.19 o -1 -11 1 55.25 58.21 3.37 o 0 -11 1 6.38 8.81 0.89 o 1 -11 1 24.68 28.91 1.92 o 2 -11 1 0.91 2.18 1.10 o -4 -10 1 7.91 9.75 1.25 o -3 -10 1 18.07 17.98 1.40 o -2 -10 1 7.04 6.30 0.88 o -1 -10 1 0.51 4.51 1.17 o 0 -10 1 20.19 22.81 1.56 o 1 -10 1 2.99 2.64 0.91 o 2 -10 1 6.55 6.38 0.78 o 3 -10 1 2.10 3.83 3.02 o 4 -10 1 16.22 17.69 1.68 o -3 -9 1 0.94 0.77 0.32 o -2 -9 1 34.90 35.47 1.83 o -1 -9 1 10.94 14.80 1.39 o 0 -9 1 27.25 26.28 1.99 o 1 -9 1 29.73 27.06 1.24 o 4 -9 1 7.83 7.63 0.94 o -1 -8 1 24.98 26.82 2.37 o 0 -8 1 25.84 23.56 1.18 o 1 -8 1 148.86 156.75 7.90 o -1 -7 1 64.18 59.85 4.22 o 0 -7 1 45.59 44.07 1.94 o 1 -7 1 7.33 8.98 0.58 o -7 -2 1 2.14 2.80 1.12 o -7 0 1 0.67 0.62 0.69 o -6 0 1 37.23 36.07 2.45 o -5 0 1 187.89 163.03 9.01 o -4 0 1 93.39 95.19 4.37 o -3 0 1 27.59 29.42 2.26 o -2 0 1 109.88 156.27 23.01 o -1 0 1 337.83 367.38 19.27 o 2 0 1 166.64 160.83 7.43 o 3 0 1 39.91 44.17 2.24 o 4 0 1 0.74 1.33 0.61 o 5 0 1 0.59 4.09 1.08 o 6 0 1 0.22 -0.38 0.67 o -7 1 1 0.10 0.27 0.60 o -6 1 1 3.25 5.57 1.11 o -5 1 1 35.85 32.57 2.12 o -4 1 1 86.95 94.15 4.68 o -3 1 1 24.87 30.72 1.80 o -2 1 1 234.64 247.60 11.81 o -1 1 1 143.98 136.65 6.16 o 1 1 1 19.72 31.20 1.95 o 2 1 1 11.11 18.08 1.63 o 3 1 1 175.95 155.48 7.12 o 4 1 1 19.50 21.49 1.41 o 5 1 1 9.94 10.27 1.15 o 6 1 1 6.51 7.53 1.36 o -6 2 1 37.67 40.61 3.56 o -5 2 1 59.37 55.85 2.90 o -4 2 1 13.55 14.69 1.20 o -3 2 1 406.49 441.18 24.04 o -2 2 1 168.07 187.40 9.00 o -1 2 1 294.64 264.90 12.52 o 0 2 1 179.43 151.70 6.40 o 1 2 1 216.01 227.36 11.23 o 2 2 1 16.23 18.71 0.99 o 3 2 1 38.26 53.61 3.36 o 4 2 1 24.08 24.49 1.65 o 5 2 1 13.51 14.28 1.13 o 6 2 1 1.63 1.32 0.74 o -6 3 1 2.28 1.93 1.09 o -5 3 1 31.95 32.28 1.78 o -4 3 1 30.92 36.94 1.85 o -3 3 1 42.77 50.64 2.80 o -2 3 1 914.81 896.73 39.27 o -1 3 1 92.63 84.94 4.55 o 0 3 1 5.99 6.94 0.46 o 1 3 1 83.46 64.53 2.77 o 2 3 1 68.68 114.13 7.44 o 3 3 1 14.17 14.49 0.84 o 4 3 1 72.58 68.58 2.92 o 5 3 1 12.05 11.12 0.83 o 6 3 1 10.90 13.86 1.08 o -6 4 1 1.91 3.05 0.85 o -5 4 1 12.90 13.38 1.33 o -4 4 1 32.89 29.94 1.73 o -3 4 1 210.16 209.22 9.73 o -2 4 1 28.78 27.36 1.30 o -1 4 1 190.26 173.31 11.44 o 0 4 1 132.04 149.37 8.19 o 1 4 1 62.60 64.43 3.15 o 2 4 1 42.39 40.40 2.60 o 3 4 1 239.65 242.69 16.63 o 4 4 1 68.56 63.10 3.26 o 5 4 1 102.67 101.87 5.98 o 6 4 1 10.59 10.35 1.46 o -6 5 1 3.68 4.90 1.05 o -5 5 1 5.45 5.12 0.95 o -4 5 1 3.29 7.91 1.03 o -3 5 1 26.11 25.33 1.28 o -2 5 1 125.15 125.69 4.91 o -1 5 1 141.05 134.72 5.78 o 0 5 1 23.84 27.00 1.57 o 1 5 1 147.10 142.40 7.10 o 2 5 1 12.33 16.39 0.93 o 3 5 1 2.24 1.87 0.36 o 4 5 1 180.24 182.58 12.94 o 5 5 1 6.68 7.01 0.90 o 6 5 1 25.30 23.27 2.24 o -6 6 1 5.65 7.00 1.11 o -5 6 1 11.51 13.18 1.23 o -4 6 1 65.96 63.80 3.67 o -3 6 1 5.92 6.55 0.70 o -2 6 1 9.86 7.51 0.78 o -1 6 1 6.50 5.78 0.48 o 0 6 1 3.74 3.78 0.51 o 1 6 1 15.75 17.24 0.99 o 2 6 1 2.97 3.54 0.39 o 3 6 1 9.86 8.95 0.88 o 4 6 1 52.41 54.77 2.71 o 5 6 1 58.77 56.44 4.56 o 6 6 1 4.46 5.74 0.80 o -5 7 1 2.34 3.08 0.83 o -4 7 1 2.67 4.16 0.51 o -3 7 1 0.39 2.22 0.62 o -2 7 1 1.78 8.28 1.01 o 2 7 1 261.29 242.84 15.64 o 3 7 1 69.64 70.79 3.94 o 4 7 1 6.20 6.45 0.72 o 5 7 1 3.98 4.19 0.96 o -5 8 1 0.63 1.04 0.56 o -4 8 1 25.36 23.85 1.45 o -3 8 1 38.13 39.31 2.37 o -2 8 1 53.24 48.30 2.57 o 2 8 1 1.74 2.04 0.32 o 3 8 1 78.41 78.98 3.30 o 4 8 1 2.46 3.46 0.64 o 5 8 1 9.40 9.68 1.05 o -4 9 1 10.29 10.43 0.96 o 2 9 1 146.77 149.88 8.37 o 3 9 1 26.21 25.19 1.52 o -2 -11 2 14.82 16.14 1.30 o -1 -11 2 24.35 22.69 2.37 o 0 -11 2 13.03 12.36 1.09 o 1 -11 2 3.03 3.99 1.13 o 2 -11 2 5.93 7.27 1.02 o -3 -10 2 12.71 12.94 1.42 o -2 -10 2 8.93 8.11 0.96 o -1 -10 2 6.82 8.28 3.00 o 0 -10 2 13.12 11.41 0.96 o 1 -10 2 2.49 2.77 0.44 o 2 -10 2 11.41 13.03 2.39 o 3 -10 2 2.28 2.81 1.04 o -3 -9 2 11.08 15.28 1.56 o -2 -9 2 22.87 22.79 1.97 o -1 -9 2 48.90 50.68 3.26 o 0 -9 2 2.31 2.03 0.61 o 1 -9 2 6.93 7.70 0.64 o 2 -9 2 3.64 2.75 0.62 o 4 -9 2 9.36 9.60 1.17 o -5 -8 2 3.92 4.65 0.82 o -5 -7 2 2.98 1.51 0.80 o 2 -6 2 18.24 16.06 1.19 o -5 -1 2 62.78 66.60 3.99 o -6 0 2 23.43 24.80 1.70 o -5 0 2 35.01 36.66 2.43 o -4 0 2 153.38 160.78 6.71 o -3 0 2 45.83 43.47 1.90 o -2 0 2 457.96 452.95 18.25 o -1 0 2 200.11 171.59 8.34 o 0 0 2 60.19 58.19 2.32 o 1 0 2 413.66 377.18 16.33 o 2 0 2 61.21 91.70 6.17 o 3 0 2 65.64 68.44 3.71 o 4 0 2 50.45 51.05 2.79 o 5 0 2 90.48 87.09 5.45 o 6 0 2 0.00 0.49 0.75 o -6 1 2 10.93 11.44 1.49 o -4 1 2 83.64 77.40 3.95 o -3 1 2 81.47 69.06 2.92 o -2 1 2 281.85 283.39 12.63 o -1 1 2 230.34 186.21 9.59 o 0 1 2 856.26 826.95 33.63 o 1 1 2 293.34 268.16 11.61 o 2 1 2 19.41 25.90 2.32 o 3 1 2 28.37 38.62 2.07 o 4 1 2 23.72 23.79 1.41 o 5 1 2 10.97 12.90 1.15 o 6 1 2 14.52 13.65 1.58 o -6 2 2 0.26 1.22 0.95 o -5 2 2 16.53 16.04 1.17 o -4 2 2 85.76 75.82 4.85 o -3 2 2 234.31 246.00 8.50 o -2 2 2 69.86 74.63 3.73 o -1 2 2 192.57 219.81 14.28 o 0 2 2 455.31 463.77 18.17 o 1 2 2 474.23 453.44 28.17 o 2 2 2 148.42 166.70 11.15 o 3 2 2 105.85 113.97 7.44 o 4 2 2 15.94 17.31 1.44 o 5 2 2 11.80 10.35 0.96 o 6 2 2 43.30 51.00 4.23 o -6 3 2 2.89 5.28 1.07 o -5 3 2 16.60 15.16 1.42 o -4 3 2 5.69 8.86 1.04 o -3 3 2 9.25 8.53 0.74 o -2 3 2 141.92 167.33 9.08 o -1 3 2 519.57 451.18 26.11 o 0 3 2 90.37 81.11 3.28 o 1 3 2 43.47 64.97 3.86 o 2 3 2 503.57 539.52 26.17 o 3 3 2 25.40 29.16 1.91 o 4 3 2 25.76 28.77 1.64 o 5 3 2 52.05 54.64 3.56 o 6 3 2 24.22 26.69 2.01 o -6 4 2 1.03 2.10 1.04 o -5 4 2 41.50 37.22 2.72 o -4 4 2 2.08 1.39 0.68 o -3 4 2 42.26 34.94 1.91 o -2 4 2 274.58 310.02 13.36 o -1 4 2 69.58 77.99 3.08 o 0 4 2 261.11 268.90 12.44 o 1 4 2 284.17 294.99 18.53 o 2 4 2 82.16 81.09 3.54 o 3 4 2 33.71 35.75 1.90 o 4 4 2 6.18 5.79 0.76 o 5 4 2 12.31 13.42 1.03 o 6 4 2 21.85 24.48 2.10 o -6 5 2 7.94 8.67 1.00 o -5 5 2 3.14 4.37 0.94 o -4 5 2 70.57 63.93 3.09 o -3 5 2 19.47 18.86 0.98 o -2 5 2 28.44 24.57 1.12 o -1 5 2 338.13 375.35 17.16 o 0 5 2 118.80 114.74 5.80 o 1 5 2 81.96 103.47 5.69 o 2 5 2 7.24 9.19 0.69 o 3 5 2 28.94 30.12 1.58 o 4 5 2 33.94 32.45 2.95 o 5 5 2 8.79 7.23 0.98 o 6 5 2 6.60 7.45 1.00 o -6 6 2 8.86 10.45 1.45 o -5 6 2 5.78 6.21 1.07 o -4 6 2 2.74 2.18 0.51 o -3 6 2 47.78 48.16 2.78 o -2 6 2 6.93 6.06 0.84 o -1 6 2 12.13 16.54 0.84 o 0 6 2 112.26 126.04 7.32 o 1 6 2 84.37 78.26 4.80 o 3 6 2 66.19 64.24 4.65 o 4 6 2 21.99 22.30 1.28 o 5 6 2 25.27 23.46 1.92 o 6 6 2 1.92 1.12 0.98 o -4 7 2 10.40 11.03 1.02 o -3 7 2 42.29 48.49 2.88 o -2 7 2 54.97 51.36 3.62 o -1 7 2 10.33 13.45 1.05 o 0 7 2 20.17 20.87 1.32 o 1 7 2 101.69 102.01 5.02 o 2 7 2 110.23 102.65 6.49 o 3 7 2 51.98 50.48 3.08 o 4 7 2 10.96 10.52 0.92 o 5 7 2 9.30 8.28 1.16 o -4 8 2 3.69 3.93 0.86 o -3 8 2 26.64 26.65 1.63 o -2 8 2 15.05 18.14 1.12 o -1 8 2 34.58 30.19 2.06 o 0 8 2 4.61 4.72 0.56 o 1 8 2 21.54 20.04 1.39 o 2 8 2 72.31 70.33 3.77 o 3 8 2 6.37 5.73 0.65 o 4 8 2 1.84 1.64 0.50 o 5 8 2 2.38 1.66 0.70 o -4 9 2 30.27 33.77 2.71 o 3 9 2 34.01 29.04 1.70 o -1 -11 3 5.40 6.65 1.35 o 0 -11 3 0.21 0.74 0.81 o 1 -11 3 0.80 1.45 0.74 o -2 -10 3 8.61 6.12 0.89 o -1 -10 3 6.64 5.32 0.97 o 0 -10 3 23.22 27.83 1.61 o 1 -10 3 7.03 6.15 0.70 o 2 -10 3 5.92 5.19 0.75 o 3 -10 3 8.28 8.96 1.16 o -3 -9 3 5.36 7.93 1.18 o -1 -9 3 93.74 82.92 4.78 o 0 -9 3 41.80 39.87 1.85 o 1 -9 3 30.95 26.77 1.66 o 2 -9 3 14.25 11.25 1.22 o 4 -9 3 6.40 6.66 1.02 o -4 -8 3 0.75 -0.04 0.57 o -1 -8 3 34.19 29.99 1.37 o 0 -8 3 27.83 23.82 1.40 o 1 -8 3 8.77 8.35 0.75 o -5 -7 3 6.65 5.81 0.71 o -5 -5 3 41.12 42.49 2.57 o -5 -4 3 0.50 0.39 0.55 o -2 -1 3 159.42 166.05 7.93 o -6 0 3 5.13 4.74 0.85 o -5 0 3 5.34 5.03 0.89 o -4 0 3 17.66 14.02 1.31 o -3 0 3 0.98 4.30 1.25 o -2 0 3 58.66 61.35 3.05 o -1 0 3 83.06 71.90 3.95 o 0 0 3 872.99 858.99 31.80 o 1 0 3 16.23 17.89 0.86 o 2 0 3 9.44 8.69 0.73 o 3 0 3 129.68 122.66 5.39 o 4 0 3 0.00 0.63 0.53 o 5 0 3 24.51 24.10 1.87 o 6 0 3 19.12 18.94 1.58 o -6 1 3 2.98 1.24 1.04 o -5 1 3 3.54 2.97 0.27 o -4 1 3 81.18 82.35 3.76 o -3 1 3 23.04 22.79 1.16 o -1 1 3 84.62 99.49 4.79 o 0 1 3 342.08 344.38 13.34 o 1 1 3 229.85 182.36 7.19 o 2 1 3 42.24 42.28 2.23 o 3 1 3 20.25 23.01 1.62 o 4 1 3 7.50 9.69 0.89 o 5 1 3 0.87 0.68 0.85 o 6 1 3 0.41 -0.98 0.98 o -6 2 3 1.41 0.98 0.96 o -5 2 3 32.17 26.39 1.57 o -4 2 3 6.91 6.71 0.84 o -3 2 3 116.39 97.51 3.85 o -2 2 3 17.96 21.85 1.91 o -1 2 3 108.41 119.22 6.67 o 0 2 3 205.70 235.44 12.41 o 1 2 3 324.98 304.64 11.44 o 2 2 3 176.70 173.35 7.10 o 3 2 3 14.45 17.44 1.60 o 4 2 3 28.41 27.45 2.16 o 5 2 3 11.54 12.48 1.22 o 6 2 3 23.24 26.56 1.86 o -6 3 3 1.48 4.09 1.13 o -5 3 3 94.92 91.69 4.44 o -4 3 3 52.13 51.48 3.12 o -3 3 3 89.92 100.83 3.78 o -2 3 3 38.35 36.58 1.56 o -1 3 3 19.41 24.63 1.52 o 0 3 3 34.01 36.70 1.59 o 1 3 3 99.32 89.55 3.64 o 2 3 3 24.84 26.86 1.55 o 3 3 3 45.17 50.02 3.47 o 4 3 3 52.24 50.42 2.49 o 5 3 3 2.30 5.33 1.03 o 6 3 3 19.66 21.06 1.56 o -6 4 3 12.14 12.89 1.67 o -4 4 3 104.39 94.41 6.11 o -3 4 3 29.00 27.23 1.72 o -2 4 3 58.84 71.77 3.16 o -1 4 3 100.32 135.22 14.98 o 0 4 3 60.11 66.23 3.12 o 1 4 3 308.57 313.83 20.13 o 2 4 3 149.72 162.56 9.69 o 3 4 3 9.65 10.96 0.77 o 4 4 3 39.69 37.32 1.93 o 5 4 3 26.48 28.66 1.80 o 6 4 3 0.78 -0.91 0.91 o -6 5 3 18.27 20.15 2.30 o -4 5 3 28.82 22.76 1.72 o -3 5 3 76.69 71.89 3.65 o -2 5 3 21.50 21.32 1.44 o -1 5 3 81.30 89.25 3.87 o 0 5 3 81.38 85.69 3.73 o 1 5 3 15.11 19.11 1.12 o 2 5 3 4.02 3.44 0.59 o 3 5 3 68.57 63.70 4.21 o 4 5 3 11.73 12.58 1.20 o 5 5 3 6.38 6.64 0.95 o 6 5 3 2.16 1.96 0.79 o -5 6 3 4.65 2.93 0.73 o -4 6 3 7.41 4.83 0.73 o -3 6 3 0.14 1.59 0.77 o -2 6 3 10.74 7.90 0.68 o -1 6 3 11.58 13.01 1.30 o 0 6 3 118.31 116.99 5.59 o 1 6 3 12.23 13.88 0.95 o 2 6 3 13.68 13.50 0.89 o 3 6 3 87.79 81.39 4.85 o 4 6 3 47.59 43.35 3.07 o 5 6 3 11.02 9.09 0.96 o -4 7 3 7.83 8.79 0.79 o -3 7 3 1.98 2.33 0.52 o -2 7 3 45.39 46.27 2.68 o -1 7 3 65.71 60.49 3.81 o 0 7 3 49.76 50.74 2.85 o 1 7 3 2.58 3.79 0.39 o 2 7 3 25.11 25.58 1.32 o 3 7 3 21.35 20.26 1.52 o 4 7 3 3.65 4.11 0.83 o 5 7 3 4.25 4.57 0.69 o -3 8 3 7.99 6.95 0.96 o -2 8 3 5.20 3.02 0.54 o 2 8 3 36.04 34.96 2.09 o 3 8 3 5.02 5.56 0.56 o 4 8 3 2.79 2.86 0.63 o -4 9 3 0.08 1.64 1.01 o -2 9 3 0.39 1.76 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