#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/06/2200619.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200619_Fobs loop_ _publ_author_name 'Groux, Laurent F.' 'Zargarian, Davit' _publ_section_title ; Chloro[1-(dimethylaminoethyl)indenyl](triphenylphosphine)nickel(II) ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m547 _journal_page_last m548 _journal_volume 57 _journal_year 2001 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 83.522 _cell_angle_beta 75.195 _cell_angle_gamma 69.287 _cell_length_a 9.0763 _cell_length_b 12.8096 _cell_length_c 13.0012 _exptl_crystal_F_000 568.00 _reflns_d_resolution_high 0.8076 _[local]_cod_data_source_file cf6116Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' laur11 in P1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 127.60 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1431.07 1738.56 72.53 o 2 0 0 2899.12 3283.24 31.34 o 3 0 0 4290.93 4762.74 164.00 o 4 0 0 272.02 339.07 13.14 o 5 0 0 460.69 348.49 59.49 o 6 0 0 8.05 9.46 1.84 o 7 0 0 62.38 48.21 2.17 o 8 0 0 5.75 6.68 1.80 o 9 0 0 60.28 63.26 7.75 o 10 0 0 8.90 4.83 0.78 o -9 1 0 571.69 554.68 28.24 o -8 1 0 79.52 66.66 5.41 o -7 1 0 233.34 195.31 13.52 o -6 1 0 62.41 71.88 10.84 o -5 1 0 269.70 209.74 31.39 o -4 1 0 624.61 626.51 44.59 o -3 1 0 1837.68 2088.33 40.22 o -2 1 0 633.00 654.87 15.11 o -1 1 0 1689.55 1724.97 12.35 o 0 1 0 1417.87 1438.57 55.84 o 1 1 0 5542.19 5863.18 235.00 o 2 1 0 721.32 811.26 11.77 o 3 1 0 1510.65 1896.10 34.63 o 4 1 0 4944.43 6704.03 436.62 o 5 1 0 254.29 264.91 28.00 o 6 1 0 1432.78 1372.33 88.12 o 7 1 0 68.95 61.23 10.04 o 8 1 0 0.71 0.80 0.91 < 9 1 0 78.72 95.78 21.90 o 10 1 0 120.57 118.67 3.37 o -9 2 0 81.69 107.16 12.32 o -8 2 0 382.63 409.93 42.89 o -7 2 0 62.97 47.71 2.65 o -6 2 0 1578.00 1458.83 47.10 o -5 2 0 772.82 779.35 85.97 o -4 2 0 623.96 610.56 32.80 o -3 2 0 548.19 546.35 40.18 o -2 2 0 1398.70 1648.26 67.30 o -1 2 0 1006.17 1161.23 32.75 o 0 2 0 1897.69 1946.58 86.06 o 1 2 0 773.41 938.54 45.33 o 2 2 0 1442.70 1608.94 36.81 o 3 2 0 775.82 891.51 22.51 o 4 2 0 1214.13 1411.26 23.64 o 5 2 0 604.23 676.13 20.21 o 6 2 0 1454.94 1218.03 98.41 o 7 2 0 11.38 13.55 2.91 o 8 2 0 17.81 15.42 3.53 o 9 2 0 125.84 88.96 20.40 o 10 2 0 7.85 3.47 0.82 o -9 3 0 21.99 24.74 1.77 o -8 3 0 14.49 9.85 0.88 o -7 3 0 197.87 186.81 6.11 o -6 3 0 75.21 85.14 3.46 o -5 3 0 351.71 321.29 19.84 o -4 3 0 880.63 779.62 26.97 o -3 3 0 621.31 629.99 39.18 o -2 3 0 249.07 291.88 15.43 o -1 3 0 8963.23 8580.93 139.75 o 0 3 0 704.58 840.54 22.92 o 1 3 0 1327.87 1363.54 40.43 o 2 3 0 810.24 913.76 35.28 o 3 3 0 1659.15 1782.35 54.17 o 4 3 0 583.49 598.97 46.26 o 5 3 0 693.55 689.05 37.40 o 6 3 0 35.76 34.96 3.64 o 7 3 0 987.55 1071.44 70.20 o 8 3 0 28.17 37.02 2.93 o 9 3 0 34.21 24.38 3.15 o 10 3 0 15.87 16.88 4.34 o -8 4 0 28.13 28.31 1.43 o -7 4 0 64.82 71.06 2.60 o -6 4 0 29.12 33.28 1.41 o -5 4 0 1907.84 1680.90 97.02 o -4 4 0 1636.25 1659.38 51.12 o -3 4 0 92.57 62.36 2.84 o -2 4 0 25.72 54.76 1.12 o -1 4 0 615.57 648.24 15.69 o 0 4 0 4757.76 4846.02 123.44 o 1 4 0 154.16 174.74 4.92 o 2 4 0 840.04 938.06 12.35 o 3 4 0 89.21 94.88 4.76 o 4 4 0 77.56 118.60 4.62 o 5 4 0 174.30 200.24 7.84 o 6 4 0 1406.81 1021.07 89.02 o 7 4 0 488.56 523.66 15.83 o 8 4 0 11.12 9.56 0.96 o 9 4 0 169.28 174.86 7.68 o 10 4 0 59.77 55.64 3.58 o -8 5 0 1.60 2.89 0.64 o -7 5 0 56.88 55.96 5.22 o -6 5 0 73.93 72.79 1.92 o -5 5 0 19.78 16.93 1.02 o -4 5 0 118.57 88.51 18.53 o -3 5 0 3898.65 3202.35 210.49 o -2 5 0 108.11 143.70 25.89 o -1 5 0 1638.02 1708.15 34.96 o 0 5 0 30.49 37.88 2.25 o 1 5 0 185.34 145.05 6.77 o 2 5 0 852.61 859.40 29.63 o 3 5 0 1835.91 1949.27 132.59 o 4 5 0 1069.37 1322.70 10.43 o 5 5 0 202.63 206.21 9.87 o 6 5 0 331.36 291.46 12.22 o 7 5 0 1.01 1.74 0.79 o 8 5 0 911.96 977.80 47.06 o 9 5 0 297.84 262.69 10.92 o 10 5 0 7.80 8.14 1.79 o -7 6 0 28.44 33.15 1.29 o -6 6 0 11.52 14.13 1.21 o -5 6 0 360.20 387.02 32.42 o -4 6 0 1244.79 1095.17 150.76 o -3 6 0 854.78 866.12 90.13 o -2 6 0 2000.81 1577.04 204.03 o -1 6 0 2779.82 2688.73 288.94 o 0 6 0 249.56 304.90 7.85 o 1 6 0 3104.92 3098.10 85.95 o 2 6 0 107.93 102.18 11.67 o 3 6 0 548.08 393.44 32.55 o 4 6 0 162.81 177.83 9.44 o 5 6 0 42.77 44.06 6.80 o 6 6 0 577.51 628.73 63.58 o 7 6 0 818.74 902.60 63.85 o 8 6 0 261.67 286.45 14.24 o 9 6 0 145.06 146.91 4.03 o 10 6 0 228.73 208.17 23.76 o -7 7 0 3.29 2.81 0.55 o -6 7 0 2.53 2.31 0.74 o -5 7 0 51.57 46.08 10.04 o -4 7 0 1.36 2.02 0.76 o -3 7 0 945.81 794.00 15.05 o -2 7 0 1021.51 1096.24 117.16 o -1 7 0 118.37 136.70 15.23 o 0 7 0 1670.87 1403.61 117.42 o 1 7 0 88.99 78.56 9.45 o 2 7 0 5458.45 2654.68 242.90 o 3 7 0 1915.41 1667.26 73.21 o 4 7 0 0.55 3.89 1.26 o 5 7 0 68.50 61.79 10.93 o 6 7 0 18.67 14.26 3.01 o 7 7 0 12.41 15.68 1.53 o 8 7 0 6.14 7.28 0.95 o 9 7 0 444.03 415.92 6.15 o 10 7 0 28.74 34.19 4.27 o -6 8 0 33.84 36.76 1.59 o -5 8 0 19.78 23.25 3.78 o -4 8 0 0.39 0.57 0.49 < -3 8 0 98.65 123.94 3.61 o -2 8 0 0.18 1.15 0.49 o -1 8 0 0.59 0.73 0.47 < 0 8 0 138.85 138.38 18.98 o 1 8 0 4151.96 3192.85 302.90 o 2 8 0 1680.02 1402.25 73.21 o 3 8 0 368.13 485.21 51.96 o 4 8 0 2551.47 2610.93 81.28 o 5 8 0 741.47 848.34 29.31 o 6 8 0 26.51 27.19 2.62 o 7 8 0 159.06 115.04 20.58 o 8 8 0 8.15 7.69 1.26 o 9 8 0 27.96 23.88 2.97 o 10 8 0 21.12 14.60 1.21 o -6 9 0 121.79 124.13 7.01 o -5 9 0 45.93 56.14 4.71 o -4 9 0 158.61 172.01 3.98 o -3 9 0 7.49 8.61 0.88 o -2 9 0 1.66 1.46 0.65 o -1 9 0 86.57 93.07 2.33 o 0 9 0 179.21 187.04 12.93 o 1 9 0 63.04 55.96 10.40 o 2 9 0 795.03 781.76 204.70 o 3 9 0 1301.83 1335.36 63.82 o 4 9 0 618.17 733.63 14.85 o 5 9 0 748.90 717.35 30.11 o 6 9 0 398.29 393.51 15.69 o 7 9 0 29.02 32.96 1.91 o 8 9 0 231.68 239.36 6.12 o 9 9 0 6.65 7.09 1.25 o 10 9 0 0.55 0.24 0.60 < -5 10 0 8.57 10.49 1.41 o -4 10 0 28.68 34.84 2.46 o -3 10 0 30.43 35.16 1.55 o -2 10 0 70.54 74.78 4.11 o -1 10 0 387.78 519.37 49.80 o 0 10 0 111.75 135.86 9.27 o 1 10 0 666.76 663.71 28.80 o 2 10 0 390.05 322.86 20.46 o 3 10 0 44.79 33.02 1.95 o 4 10 0 230.87 246.79 5.19 o 5 10 0 286.95 292.11 6.04 o 6 10 0 0.30 2.06 2.00 < 7 10 0 51.46 52.22 4.37 o 8 10 0 23.66 21.59 5.48 o 9 10 0 36.69 36.02 4.99 o 10 10 0 30.27 28.29 1.33 o -4 11 0 11.31 10.55 0.85 o -3 11 0 360.17 342.69 6.23 o -2 11 0 337.91 290.45 32.19 o -1 11 0 15.36 12.75 1.27 o 0 11 0 21.28 19.41 1.85 o 1 11 0 1.91 2.69 0.61 o 2 11 0 11.48 23.30 3.92 o 3 11 0 132.73 100.68 12.68 o 4 11 0 781.79 741.72 13.16 o 5 11 0 138.24 169.07 4.66 o 6 11 0 195.08 204.42 4.96 o 7 11 0 78.44 80.86 5.19 o 8 11 0 11.71 11.76 0.96 o 9 11 0 28.10 29.23 3.47 o -3 12 0 123.01 134.81 10.07 o -2 12 0 4.07 5.10 0.82 o -1 12 0 207.21 206.35 20.06 o 0 12 0 55.32 70.58 7.69 o 1 12 0 52.54 49.74 6.25 o 2 12 0 44.07 40.30 1.48 o 3 12 0 264.80 197.90 17.21 o 4 12 0 27.33 23.29 1.56 o 5 12 0 9.26 13.20 2.50 o 6 12 0 171.90 177.07 4.25 o 7 12 0 16.92 16.41 1.43 o 8 12 0 194.35 218.76 13.71 o 9 12 0 40.67 51.42 2.95 o -2 13 0 416.42 391.32 24.91 o -1 13 0 156.46 179.64 8.13 o 0 13 0 18.15 22.94 4.36 o 1 13 0 323.40 346.53 36.85 o 2 13 0 242.91 247.63 10.74 o 3 13 0 17.01 14.31 1.84 o 4 13 0 17.31 22.07 1.46 o 5 13 0 3.69 3.27 0.76 o 6 13 0 0.70 1.13 0.56 o 7 13 0 7.56 8.95 1.01 o 8 13 0 10.81 11.92 0.95 o -1 14 0 90.94 80.97 10.88 o 0 14 0 208.14 203.33 12.03 o 1 14 0 276.69 263.14 12.51 o 2 14 0 76.30 75.00 2.00 o 3 14 0 26.93 26.96 2.29 o 4 14 0 10.24 8.28 1.09 o 5 14 0 41.96 37.18 1.41 o 6 14 0 33.65 32.79 3.96 o 7 14 0 16.06 15.27 1.21 o 1 15 0 126.10 110.07 2.72 o 2 15 0 163.48 167.25 9.52 o 3 15 0 99.07 124.24 3.66 o 4 15 0 179.72 298.73 5.54 o 5 15 0 14.16 9.83 1.07 o -4 -15 1 0.13 0.96 0.52 < -3 -15 1 280.41 323.23 8.02 o -2 -15 1 165.49 171.28 3.20 o -1 -15 1 2.91 2.57 0.36 o -7 -14 1 0.02 0.45 0.33 < -6 -14 1 1.95 1.91 0.48 o -5 -14 1 6.43 6.43 0.68 o -4 -14 1 163.99 147.24 24.81 o -3 -14 1 231.77 253.70 12.58 o -2 -14 1 5.33 4.60 1.19 o -1 -14 1 267.87 281.54 5.69 o 0 -14 1 4.27 4.00 0.52 o 1 -14 1 217.39 193.42 21.71 o -8 -13 1 122.54 122.65 2.30 o -7 -13 1 1.47 3.76 0.83 o -6 -13 1 54.25 51.28 1.99 o -5 -13 1 197.37 206.15 30.58 o -4 -13 1 12.50 11.45 2.21 o -3 -13 1 21.40 20.19 2.39 o -2 -13 1 325.64 401.92 5.87 o -1 -13 1 17.04 17.15 1.96 o 0 -13 1 683.35 760.01 16.65 o 1 -13 1 77.74 71.15 7.27 o 2 -13 1 6.03 6.76 0.61 o -9 -12 1 229.08 269.88 5.98 o -8 -12 1 31.85 33.75 4.26 o -7 -12 1 114.46 119.94 3.31 o -6 -12 1 27.72 23.22 1.51 o -5 -12 1 24.60 22.05 3.96 o -4 -12 1 2.30 1.13 0.51 o -3 -12 1 18.40 14.89 1.36 o -2 -12 1 0.30 1.91 0.68 o -1 -12 1 235.98 237.69 4.60 o 0 -12 1 12.04 13.70 1.98 o 1 -12 1 277.84 276.70 9.92 o 2 -12 1 320.87 267.25 21.20 o 3 -12 1 61.75 52.68 6.56 o -9 -11 1 46.39 60.74 9.42 o -8 -11 1 319.20 288.37 36.59 o -7 -11 1 70.53 72.72 6.85 o -6 -11 1 214.53 186.63 7.06 o -5 -11 1 0.50 3.76 1.08 o -4 -11 1 273.85 217.46 34.87 o -3 -11 1 693.91 656.08 43.19 o -2 -11 1 160.37 169.05 6.85 o -1 -11 1 300.49 347.36 9.85 o 0 -11 1 92.92 106.66 8.30 o 1 -11 1 116.93 105.07 2.80 o 2 -11 1 85.06 78.71 6.64 o 3 -11 1 118.72 118.35 11.72 o 4 -11 1 220.67 260.32 19.26 o -9 -10 1 104.71 102.47 2.88 o -8 -10 1 100.87 115.30 15.79 o -7 -10 1 44.63 46.29 6.07 o -6 -10 1 31.78 32.41 1.64 o -5 -10 1 118.32 105.50 5.19 o -4 -10 1 83.41 71.57 2.18 o -3 -10 1 27.32 28.68 1.41 o -2 -10 1 4.07 5.55 0.76 o -1 -10 1 678.77 710.97 10.64 o 0 -10 1 220.93 239.68 17.62 o 1 -10 1 103.73 107.73 11.33 o 2 -10 1 496.38 446.97 37.97 o 3 -10 1 1194.25 1301.12 79.62 o 4 -10 1 0.20 0.84 0.57 < 5 -10 1 94.29 99.68 5.01 o -10 -9 1 95.33 86.13 9.57 o -9 -9 1 55.91 62.46 5.08 o -8 -9 1 29.81 30.04 2.22 o -7 -9 1 266.38 195.10 31.69 o -6 -9 1 501.53 445.88 33.71 o -5 -9 1 117.47 118.91 12.36 o -4 -9 1 852.53 911.64 55.87 o -3 -9 1 0.99 1.59 1.39 < -2 -9 1 1065.53 1098.31 244.85 o -1 -9 1 1126.78 999.91 38.11 o 0 -9 1 172.46 186.66 57.28 o 1 -9 1 2.55 3.51 0.96 o 2 -9 1 37.52 50.51 6.48 o 3 -9 1 151.80 199.65 19.71 o 4 -9 1 220.18 220.28 4.15 o 5 -9 1 35.67 37.06 3.73 o 6 -9 1 0.03 0.98 0.86 < -10 -8 1 73.05 76.57 2.52 o -9 -8 1 112.72 128.26 12.63 o -8 -8 1 129.23 128.10 13.64 o -7 -8 1 56.68 59.05 2.34 o -6 -8 1 99.23 109.33 2.76 o -5 -8 1 307.94 231.77 32.22 o -4 -8 1 397.54 359.30 4.39 o -3 -8 1 2807.79 2258.24 81.56 o -2 -8 1 313.93 297.04 20.98 o -1 -8 1 6.37 3.14 0.85 o 0 -8 1 1567.90 1375.36 92.36 o 1 -8 1 242.80 223.80 18.31 o 2 -8 1 30.99 26.72 1.72 o 3 -8 1 658.49 686.55 6.56 o 4 -8 1 70.30 71.92 4.67 o 5 -8 1 0.21 0.83 0.61 < 6 -8 1 162.12 131.13 28.04 o 7 -8 1 2.36 1.24 0.56 o -10 -7 1 74.95 84.85 2.77 o -9 -7 1 49.68 59.93 6.36 o -8 -7 1 23.90 25.79 3.34 o -7 -7 1 429.24 561.26 25.15 o -6 -7 1 3.19 1.38 0.53 o -5 -7 1 30.26 25.79 6.11 o -4 -7 1 814.30 762.11 25.06 o -3 -7 1 50.73 57.79 4.69 o -2 -7 1 1645.22 1531.89 128.30 o -1 -7 1 2970.43 2089.19 270.44 o 0 -7 1 2336.35 2885.53 177.80 o 1 -7 1 551.75 585.58 24.72 o 2 -7 1 8.70 10.15 1.44 o 3 -7 1 40.28 32.36 3.08 o 4 -7 1 109.83 97.85 21.84 o 5 -7 1 0.74 1.46 0.60 o 6 -7 1 0.28 1.45 1.10 < 7 -7 1 35.46 34.01 2.33 o -10 -6 1 48.19 50.93 2.72 o -9 -6 1 87.06 77.71 3.33 o -8 -6 1 38.53 30.62 3.86 o -7 -6 1 314.11 289.50 13.67 o -6 -6 1 103.35 107.87 15.46 o -5 -6 1 0.84 4.30 0.68 o -4 -6 1 210.20 230.07 23.53 o -3 -6 1 510.35 385.10 45.29 o -2 -6 1 3344.56 3447.69 60.75 o -1 -6 1 882.76 968.01 52.68 o 0 -6 1 4250.08 4707.60 111.89 o 1 -6 1 2586.34 3251.97 147.39 o 2 -6 1 901.68 981.99 18.31 o 3 -6 1 531.86 585.75 91.38 o 4 -6 1 267.62 266.31 16.10 o 5 -6 1 391.41 388.65 13.41 o 6 -6 1 123.01 137.29 3.06 o 7 -6 1 11.83 12.23 1.18 o 8 -6 1 39.82 36.74 2.01 o -10 -5 1 80.02 72.24 4.93 o -9 -5 1 136.02 154.87 12.41 o -8 -5 1 3.00 2.54 0.67 o -7 -5 1 1814.26 1814.08 38.41 o -6 -5 1 434.69 456.22 38.79 o -5 -5 1 20.02 18.50 2.48 o -4 -5 1 39.53 44.42 3.00 o -3 -5 1 23.75 35.77 7.29 o -2 -5 1 246.83 272.97 17.88 o -1 -5 1 2925.96 2939.14 132.54 o 0 -5 1 4931.37 5288.39 245.17 o 1 -5 1 4.79 6.57 1.46 o 2 -5 1 156.99 98.29 16.08 o 3 -5 1 19.49 16.33 2.90 o 4 -5 1 1150.79 1153.56 120.58 o 5 -5 1 467.43 530.77 19.26 o 6 -5 1 62.48 81.40 3.72 o 7 -5 1 41.10 36.36 1.91 o 8 -5 1 8.95 9.98 0.98 o -10 -4 1 12.10 13.27 0.97 o -9 -4 1 0.32 0.65 0.53 < -8 -4 1 358.71 343.70 12.35 o -7 -4 1 112.89 111.74 2.72 o -6 -4 1 1240.88 1310.93 66.47 o -5 -4 1 166.24 122.07 5.35 o -4 -4 1 123.35 121.36 9.03 o -3 -4 1 84.06 102.34 5.05 o -2 -4 1 919.29 919.64 38.03 o -1 -4 1 9142.97 9266.04 147.73 o 0 -4 1 17.43 31.78 4.50 o 1 -4 1 939.10 917.63 55.52 o 2 -4 1 328.31 366.56 28.11 o 3 -4 1 1700.68 1455.45 184.31 o 4 -4 1 995.51 891.26 136.07 o 5 -4 1 80.38 70.95 12.53 o 6 -4 1 247.98 272.48 7.30 o 7 -4 1 266.13 318.96 36.70 o 8 -4 1 1.02 1.41 0.65 o -10 -3 1 0.00 1.03 1.14 < -9 -3 1 77.20 58.04 5.02 o -8 -3 1 36.55 33.94 1.96 o -7 -3 1 600.19 674.65 14.68 o -6 -3 1 1400.21 1410.34 96.54 o -5 -3 1 7.27 4.25 0.50 o -4 -3 1 35.61 71.56 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43.52 51.69 2.27 o 3 5 12 2.54 0.40 0.54 < 4 5 12 1.28 1.32 0.65 o 5 5 12 401.75 461.93 14.89 o 6 5 12 157.03 183.66 17.17 o 7 5 12 89.44 89.72 4.84 o 8 5 12 90.23 99.52 4.29 o 9 5 12 67.69 57.53 2.19 o -2 6 12 2.55 4.24 0.90 o -1 6 12 87.84 65.83 2.79 o 0 6 12 23.69 12.63 1.15 o 1 6 12 142.42 115.43 38.03 o 2 6 12 233.02 185.84 47.52 o 3 6 12 31.40 27.88 7.06 o 4 6 12 2.09 2.07 0.58 o 5 6 12 180.31 144.82 21.84 o 6 6 12 27.07 32.35 2.75 o 7 6 12 117.10 126.04 2.67 o 8 6 12 52.73 56.82 1.52 o 9 6 12 1.02 0.68 0.54 < -1 7 12 0.06 0.54 0.66 < 0 7 12 103.64 114.31 5.48 o 1 7 12 55.02 69.44 8.47 o 2 7 12 0.10 1.03 0.50 o 3 7 12 211.19 233.02 9.94 o 4 7 12 9.67 9.15 0.75 o 5 7 12 1.17 1.30 0.46 o 6 7 12 17.28 18.38 1.01 o 7 7 12 145.80 136.43 5.90 o 8 7 12 2.13 1.72 0.47 o -1 8 12 27.55 32.68 1.72 o 0 8 12 6.05 9.47 0.99 o 1 8 12 93.66 115.50 5.16 o 2 8 12 281.83 287.76 3.63 o 3 8 12 134.57 150.91 4.05 o 4 8 12 21.45 22.18 2.38 o 5 8 12 4.49 3.54 0.55 o 6 8 12 0.20 1.14 0.43 o 7 8 12 54.97 72.28 4.19 o 8 8 12 72.54 73.34 4.22 o 0 9 12 167.44 243.37 26.12 o 1 9 12 123.33 145.32 7.48 o 2 9 12 3.95 6.19 0.66 o 3 9 12 85.82 90.49 1.90 o 4 9 12 18.95 24.65 2.34 o 5 9 12 11.12 10.53 0.69 o 6 9 12 52.12 56.72 3.74 o 7 9 12 19.94 22.36 0.85 o 8 9 12 35.11 31.37 2.91 o 1 10 12 2.25 4.21 0.56 o 2 10 12 362.44 444.19 3.94 o 3 10 12 33.09 32.59 1.11 o 4 10 12 1.29 1.90 0.42 o 5 10 12 12.01 13.78 0.78 o 6 10 12 9.88 8.84 1.02 o 7 10 12 24.00 23.77 0.98 o 3 11 12 37.22 44.92 3.08 o 4 11 12 84.16 105.18 4.14 o 5 11 12 19.80 19.55 0.75 o 6 11 12 56.93 65.42 3.26 o -2 -7 13 1.62 1.47 0.36 o -1 -7 13 41.08 51.87 3.27 o 0 -7 13 21.11 20.23 1.37 o 1 -7 13 0.94 2.07 0.36 o 2 -7 13 2.26 2.07 0.54 o -2 -6 13 155.30 182.63 3.81 o -1 -6 13 55.84 72.75 1.90 o 0 -6 13 0.32 0.99 0.35 o 1 -6 13 17.04 15.68 0.85 o 2 -6 13 2.11 2.70 0.37 o 3 -6 13 131.34 147.62 9.69 o 4 -6 13 4.70 5.55 0.74 o -3 -5 13 114.19 138.08 7.41 o -2 -5 13 10.97 15.71 0.94 o -1 -5 13 62.01 64.12 5.22 o 0 -5 13 57.21 72.51 1.72 o 1 -5 13 2.79 3.79 0.52 o 2 -5 13 73.74 98.93 5.61 o 3 -5 13 14.56 15.65 1.17 o 4 -5 13 21.85 23.84 0.81 o 5 -5 13 5.25 9.63 1.19 o -3 -4 13 0.91 2.16 0.49 o -2 -4 13 27.61 29.10 1.34 o -1 -4 13 100.37 120.03 2.23 o 0 -4 13 1.79 2.67 0.53 o 1 -4 13 154.29 192.26 3.00 o 2 -4 13 16.58 16.37 0.80 o 3 -4 13 155.19 210.36 6.57 o 4 -4 13 76.30 88.07 5.29 o 5 -4 13 149.26 175.01 10.03 o -3 -3 13 10.71 12.50 1.30 o -2 -3 13 9.98 16.33 1.11 o -1 -3 13 16.54 15.60 3.32 o 0 -3 13 10.35 11.95 2.08 o 1 -3 13 4.23 5.75 1.21 o 2 -3 13 144.91 157.32 14.96 o 3 -3 13 135.17 146.78 7.79 o 4 -3 13 3.32 3.70 0.58 o 5 -3 13 136.91 146.43 5.88 o 6 -3 13 86.81 98.86 5.01 o -2 -2 13 24.99 13.30 1.49 o -1 -2 13 25.88 11.95 3.54 o 0 -2 13 14.17 14.50 1.22 o 1 -2 13 8.76 7.11 1.02 o 2 -2 13 19.30 23.22 2.64 o 3 -2 13 33.52 37.99 1.54 o 4 -2 13 122.82 153.53 11.40 o 5 -2 13 180.66 196.66 5.62 o 6 -2 13 3.00 2.51 0.56 o 0 -1 13 191.80 98.65 5.17 o 1 -1 13 10.78 12.68 1.33 o 2 -1 13 7.34 6.41 0.80 o 3 -1 13 8.32 8.37 1.18 o 4 -1 13 45.35 56.85 4.26 o 5 -1 13 21.50 25.06 1.85 o 6 -1 13 193.79 241.85 3.02 o 7 -1 13 5.40 8.05 0.73 o 1 0 13 7.39 5.42 0.98 o 2 0 13 51.42 52.56 3.00 o 3 0 13 8.42 8.71 1.38 o 4 0 13 1.09 1.76 0.58 o 5 0 13 171.14 169.77 18.04 o 6 0 13 66.02 84.87 3.23 o 7 0 13 0.06 0.51 0.37 < 1 1 13 227.37 105.54 4.63 o 2 1 13 28.31 23.69 5.36 o 3 1 13 1.63 2.59 0.69 o 4 1 13 3.43 2.45 0.60 o 5 1 13 31.11 31.58 1.26 o 6 1 13 8.94 10.70 0.79 o 7 1 13 30.57 33.90 1.06 o 8 1 13 5.17 3.22 0.50 o 2 2 13 64.67 39.04 3.96 o 3 2 13 71.03 55.16 10.54 o 4 2 13 30.24 21.20 2.99 o 5 2 13 11.88 11.92 0.93 o 6 2 13 0.59 0.88 0.42 o 7 2 13 1.06 2.21 0.85 o 8 2 13 39.89 40.40 1.40 o 2 3 13 210.53 135.84 43.59 o 3 3 13 40.48 32.86 4.71 o 4 3 13 192.16 209.53 11.14 o 5 3 13 15.62 9.93 0.86 o 6 3 13 64.34 65.40 3.73 o 7 3 13 30.93 31.49 2.50 o 8 3 13 0.11 0.67 0.35 < 2 4 13 17.78 11.75 2.71 o 3 4 13 195.08 203.39 4.79 o 4 4 13 59.43 56.13 1.85 o 5 4 13 118.49 116.04 4.74 o 6 4 13 103.15 94.07 13.84 o 7 4 13 72.25 78.63 3.99 o 8 4 13 17.84 17.44 0.84 o 2 5 13 57.87 40.76 4.19 o 3 5 13 22.01 24.59 7.41 o 4 5 13 45.23 44.22 3.22 o 5 5 13 30.91 30.39 2.38 o 6 5 13 36.41 35.52 3.77 o 7 5 13 237.68 238.10 5.39 o 8 5 13 44.45 48.94 2.16 o 1 6 13 9.85 3.85 0.94 o 2 6 13 26.34 28.25 2.94 o 3 6 13 32.96 39.34 1.96 o 4 6 13 20.19 22.02 1.78 o 5 6 13 52.18 66.35 6.97 o 6 6 13 185.14 185.98 3.11 o 7 6 13 42.82 41.06 2.76 o 8 6 13 13.25 13.95 0.97 o 0 7 13 26.85 35.31 1.85 o 1 7 13 7.83 6.14 1.44 o 2 7 13 19.82 16.01 4.43 o 3 7 13 2.59 1.16 0.47 o 4 7 13 4.16 3.35 0.73 o 5 7 13 11.88 11.56 0.91 o 6 7 13 37.42 41.72 1.44 o 7 7 13 224.57 263.35 4.63 o 8 7 13 31.74 37.90 1.37 o 1 8 13 29.90 32.20 6.19 o 2 8 13 15.07 19.81 0.95 o 3 8 13 62.37 77.26 3.01 o 4 8 13 57.51 57.83 3.68 o 5 8 13 11.37 12.09 0.78 o 6 8 13 27.14 27.76 2.75 o 7 8 13 41.77 41.78 1.64 o 8 8 13 0.10 -0.22 0.45 < 2 9 13 117.96 133.05 8.63 o 3 9 13 31.40 26.54 1.36 o 4 9 13 3.54 5.97 0.56 o 5 9 13 38.40 43.50 2.65 o 6 9 13 0.38 0.75 0.30 o 7 9 13 34.59 30.74 1.60 o 3 10 13 44.25 59.69 1.56 o 4 10 13 50.05 56.77 2.10 o 5 10 13 26.55 28.50 0.92 o 6 10 13 6.26 5.81 0.85 o 0 -6 14 81.29 114.39 2.79 o 1 -6 14 10.83 10.21 0.96 o -1 -5 14 106.48 142.33 3.32 o 0 -5 14 3.56 3.31 0.43 o 1 -5 14 54.80 67.57 1.42 o 2 -5 14 12.83 11.26 0.99 o 3 -5 14 35.71 42.03 1.19 o -1 -4 14 38.58 55.24 2.31 o 0 -4 14 118.16 158.87 2.28 o 1 -4 14 39.30 47.80 1.28 o 2 -4 14 3.95 7.67 0.56 o 3 -4 14 24.82 31.75 1.83 o 4 -4 14 2.58 3.47 0.42 o -1 -3 14 115.65 169.40 4.27 o 0 -3 14 27.16 37.46 1.54 o 1 -3 14 27.58 29.41 1.52 o 2 -3 14 73.97 104.83 4.08 o 3 -3 14 21.79 23.81 1.02 o 4 -3 14 54.04 54.51 2.11 o 5 -3 14 101.43 123.61 3.57 o -1 -2 14 0.13 0.58 0.75 < 0 -2 14 19.59 18.90 5.32 o 1 -2 14 37.40 38.98 1.67 o 2 -2 14 0.52 0.53 0.45 < 3 -2 14 69.79 89.73 5.12 o 4 -2 14 2.30 1.83 0.62 o 5 -2 14 115.35 163.59 3.14 o 6 -2 14 54.93 85.38 2.70 o 0 -1 14 1.09 1.14 0.81 < 1 -1 14 3.75 4.83 1.00 o 2 -1 14 24.50 23.19 2.91 o 3 -1 14 0.23 0.77 0.50 < 4 -1 14 114.85 157.68 13.50 o 5 -1 14 203.20 276.14 12.84 o 6 -1 14 12.45 16.60 0.93 o 1 0 14 6.10 3.23 1.10 o 2 0 14 5.22 5.50 0.90 o 3 0 14 0.16 -0.03 0.44 < 4 0 14 41.57 55.22 1.83 o 5 0 14 6.26 6.89 0.78 o 6 0 14 141.08 170.88 3.34 o 7 0 14 65.84 66.23 2.16 o 2 1 14 31.77 31.46 13.46 o 3 1 14 2.04 2.97 0.69 o 4 1 14 2.68 2.82 0.94 o 5 1 14 113.37 107.88 16.33 o 6 1 14 80.58 91.60 2.67 o 7 1 14 1.42 2.23 0.43 o 2 2 14 46.13 22.98 1.49 o 3 2 14 6.42 9.48 1.06 o 4 2 14 2.13 3.49 0.92 o 5 2 14 31.78 33.41 1.28 o 6 2 14 41.78 51.57 3.84 o 7 2 14 77.05 90.37 5.59 o 2 3 14 146.90 86.85 4.00 o 3 3 14 184.64 193.47 4.47 o 4 3 14 1.02 1.30 0.52 o 5 3 14 3.20 2.68 0.49 o 6 3 14 3.99 7.54 0.84 o 7 3 14 0.04 0.57 0.29 < 2 4 14 194.02 101.79 3.91 o 3 4 14 3.19 4.35 1.46 o 4 4 14 55.19 66.18 4.04 o 5 4 14 30.02 34.62 1.76 o 6 4 14 46.84 40.36 2.81 o 7 4 14 2.19 2.36 0.44 o 2 5 14 5.51 5.15 1.41 o 3 5 14 127.76 150.21 6.14 o 4 5 14 35.19 36.56 2.01 o 5 5 14 1.42 1.87 0.55 o 6 5 14 71.05 78.30 2.05 o 7 5 14 1.21 0.89 0.38 o 2 6 14 85.69 97.09 26.74 o 3 6 14 36.55 41.21 1.79 o 4 6 14 1.36 1.90 0.52 o 5 6 14 92.74 103.26 2.15 o 6 6 14 1.62 2.49 0.70 o 7 6 14 54.51 63.35 2.07 o 2 7 14 0.63 1.32 0.73 < 3 7 14 17.24 25.38 10.23 o 4 7 14 13.70 12.99 1.62 o 5 7 14 0.10 0.51 0.44 < 6 7 14 87.80 99.46 1.87 o 7 7 14 31.17 29.60 0.93 o 2 8 14 10.95 11.66 1.03 o 3 8 14 0.24 1.12 0.44 o 4 8 14 29.14 29.90 2.48 o 5 8 14 0.00 0.08 0.36 < 6 8 14 0.75 0.38 0.35 < 4 9 14 0.67 0.82 0.34 o 5 9 14 34.20 44.43 2.80 o 1 -3 15 74.49 112.17 2.13 o 2 -3 15 5.49 7.52 1.49 o 3 -3 15 9.17 10.53 0.93 o 1 -2 15 60.72 78.11 2.08 o 2 -2 15 90.91 121.03 6.65 o 3 -2 15 0.08 0.28 0.36 < 4 -2 15 41.34 64.43 1.46 o 1 -1 15 77.19 101.36 3.12 o 2 -1 15 2.52 2.67 0.70 o 3 -1 15 36.59 49.52 1.33 o 4 -1 15 4.08 5.72 0.60 o 5 -1 15 42.98 51.43 1.44 o 2 0 15 1.36 2.65 0.88 o 3 0 15 37.54 51.53 1.38 o 4 0 15 4.33 4.81 1.19 o 5 0 15 35.73 42.73 4.38 o 2 1 15 15.13 17.69 1.49 o 3 1 15 23.55 41.07 7.28 o 4 1 15 0.40 1.28 0.47 o 5 1 15 12.26 9.93 1.20 o 6 1 15 56.74 91.85 3.30 o 3 2 15 8.16 10.00 0.91 o 4 2 15 9.98 9.44 1.06 o 5 2 15 6.48 7.81 0.85 o 6 2 15 63.40 74.70 2.58 o 3 3 15 17.58 18.77 1.57 o 4 3 15 59.85 49.00 1.60 o 5 3 15 1.47 0.41 0.37 < 6 3 15 6.58 7.94 2.29 o 3 4 15 101.72 135.74 4.09 o 4 4 15 0.15 0.94 0.40 o 5 4 15 30.20 39.37 2.01 o 6 4 15 12.39 14.07 0.74 o 3 5 15 1.13 0.39 0.74 < 4 5 15 101.37 132.54 3.00 o 5 5 15 54.29 79.23 3.92 o 6 5 15 0.09 0.92 0.33 o 4 6 15 57.28 64.62 7.57 o 5 6 15 0.83 1.67 0.39 o 6 6 15 23.22 27.68 1.58 o