#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/07/2200711.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200711_Fobs loop_ _publ_author_name 'Rickard, Clifton E. F.' _publ_section_title ; Dinitratodioxobis(4-picoline N-oxide)uranium(VI) ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m446 _journal_page_last m447 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.583 _cell_angle_gamma 90.000 _cell_length_a 7.9772 _cell_length_b 13.5738 _cell_length_c 8.2288 _exptl_crystal_F_000 572.00 _reflns_d_resolution_high 0.7709 _[local]_cod_data_source_file ob6071Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' cer3 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 219.26 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 23167.56 21220.67 304.14 o 2 0 0 35700.95 33086.78 580.55 o 3 0 0 19653.02 18951.95 239.57 o 4 0 0 12801.17 13177.71 172.59 o 5 0 0 3273.61 3196.54 48.67 o 6 0 0 5828.22 5987.11 88.44 o 7 0 0 3913.77 4197.21 145.37 o 8 0 0 3328.58 3285.09 50.45 o 9 0 0 1762.51 1806.02 29.83 o 10 0 0 1684.38 1765.00 36.21 o 1 1 0 1101.57 1280.31 12.87 o 2 1 0 1154.40 1336.20 13.50 o 3 1 0 3511.05 3872.65 36.00 o 4 1 0 332.44 439.26 5.76 o 5 1 0 412.20 487.20 7.22 o 6 1 0 101.00 103.51 3.98 o 7 1 0 9.50 17.16 3.45 o 8 1 0 76.35 76.09 4.19 o 9 1 0 91.25 83.83 5.23 o 10 1 0 10.54 16.01 7.43 o 0 2 0 27837.58 23381.71 338.37 o 1 2 0 48076.59 39747.17 451.40 o 2 2 0 19858.89 19849.20 177.30 o 3 2 0 13928.58 14025.99 125.80 o 4 2 0 10269.44 10264.49 98.38 o 5 2 0 9770.66 9865.10 94.72 o 6 2 0 6618.29 6533.02 75.46 o 7 2 0 6172.27 6120.55 64.05 o 8 2 0 3098.53 3073.05 36.84 o 9 2 0 2121.73 2161.97 27.00 o 10 2 0 1786.17 1811.05 37.47 o 1 3 0 340.53 393.94 7.54 o 2 3 0 1369.90 1513.29 15.07 o 3 3 0 849.06 965.91 10.36 o 4 3 0 13.61 30.77 2.41 o 5 3 0 125.85 147.36 3.87 o 6 3 0 326.90 327.80 5.97 o 7 3 0 134.77 142.13 4.92 o 8 3 0 30.41 32.55 4.40 o 9 3 0 23.62 30.67 4.61 o 10 3 0 0.22 10.47 8.37 o 0 4 0 4693.75 5058.04 158.14 o 1 4 0 11326.76 11827.49 179.81 o 2 4 0 5510.76 5579.77 71.69 o 3 4 0 9387.69 9384.40 84.88 o 4 4 0 12575.24 12473.04 156.15 o 5 4 0 13951.81 13706.77 130.93 o 6 4 0 6713.67 6477.97 74.10 o 7 4 0 9282.63 8811.59 125.17 o 8 4 0 3710.00 3652.87 43.33 o 9 4 0 2351.72 2322.52 58.30 o 10 4 0 1345.49 1413.34 43.96 o 1 5 0 79.92 116.91 3.56 o 2 5 0 969.20 1119.45 17.69 o 3 5 0 668.15 799.61 10.57 o 4 5 0 494.62 554.18 7.33 o 5 5 0 502.38 510.53 7.74 o 6 5 0 162.51 160.34 5.02 o 7 5 0 435.81 417.91 12.04 o 8 5 0 0.39 5.76 3.98 o 9 5 0 11.81 13.61 4.92 o 0 6 0 5229.28 5337.80 87.81 o 1 6 0 5774.90 5848.54 62.06 o 2 6 0 11814.65 12197.57 138.68 o 3 6 0 8497.72 8523.46 82.47 o 4 6 0 8277.29 8019.83 84.36 o 5 6 0 5951.31 5976.65 69.08 o 6 6 0 12381.00 11931.10 134.38 o 7 6 0 2182.64 2128.90 26.48 o 8 6 0 3775.91 3621.89 47.83 o 9 6 0 2256.41 2238.17 31.19 o 1 7 0 82.55 114.81 3.77 o 2 7 0 482.94 588.72 9.31 o 3 7 0 526.65 613.00 8.69 o 4 7 0 306.04 324.76 7.95 o 5 7 0 67.64 81.74 4.50 o 6 7 0 3.43 13.40 3.98 o 7 7 0 9.89 18.94 4.61 o 8 7 0 51.58 45.11 5.34 o 9 7 0 53.90 61.12 6.70 o 0 8 0 8830.26 8814.10 114.29 o 1 8 0 12825.98 13156.89 137.21 o 2 8 0 11358.29 11146.78 147.26 o 3 8 0 7588.07 7778.06 81.95 o 4 8 0 5277.56 5487.67 63.63 o 5 8 0 5323.11 5394.00 62.69 o 6 8 0 2657.91 2684.86 32.76 o 7 8 0 2380.81 2286.83 31.50 o 8 8 0 2114.91 2136.96 29.93 o 9 8 0 1648.91 1592.83 32.65 o 1 9 0 45.17 43.85 3.56 o 2 9 0 321.62 336.80 6.80 o 3 9 0 12.78 17.16 3.87 o 4 9 0 4.29 7.33 3.66 o 5 9 0 6.00 13.29 3.98 o 6 9 0 31.72 27.21 4.29 o 7 9 0 0.39 0.84 4.50 o 8 9 0 3.46 10.05 5.76 o 0 10 0 5122.69 5056.05 97.13 o 1 10 0 10762.87 10777.74 134.59 o 2 10 0 8908.36 8803.53 102.25 o 3 10 0 5863.30 5936.35 69.91 o 4 10 0 3624.37 3627.96 45.21 o 5 10 0 3701.65 3689.39 43.96 o 6 10 0 1788.15 1839.72 23.55 o 7 10 0 1836.19 1864.01 54.95 o 8 10 0 1263.59 1292.77 19.78 o 1 11 0 399.14 392.16 8.69 o 2 11 0 48.11 40.50 4.08 o 3 11 0 0.20 3.45 6.07 o 4 11 0 295.18 267.51 6.49 o 5 11 0 1.42 2.62 3.87 o 6 11 0 1.81 5.65 4.40 o 7 11 0 0.59 3.45 4.61 o 8 11 0 0.61 5.86 14.13 o 0 12 0 6462.92 6078.48 166.62 o 1 12 0 3032.36 2969.33 41.86 o 2 12 0 4758.59 4717.58 47.52 o 3 12 0 4136.36 4073.60 58.51 o 4 12 0 3471.36 3438.62 55.78 o 5 12 0 2290.02 2308.60 28.78 o 6 12 0 1894.97 1959.14 25.12 o 7 12 0 1512.08 1529.20 32.86 o 1 13 0 9.35 8.16 4.81 o 2 13 0 0.36 -3.04 4.29 o 3 13 0 2.94 3.45 7.54 o 4 13 0 6.24 4.29 5.44 o 5 13 0 31.56 24.07 5.97 o 6 13 0 3.45 5.76 6.38 o 0 14 0 2557.31 2613.27 53.06 o 1 14 0 2091.14 2074.06 33.28 o 2 14 0 2343.87 2322.73 40.19 o 3 14 0 2571.31 2641.32 43.64 o 4 14 0 2317.10 2262.13 32.44 o 5 14 0 1822.27 1742.70 30.14 o 6 14 0 1291.54 1337.14 30.14 o 1 15 0 0.12 1.47 4.92 o 2 15 0 25.02 16.43 5.23 o 3 15 0 1.32 -9.11 10.36 o 4 15 0 0.31 -6.59 6.59 o 5 15 0 27.11 11.93 12.87 o 0 16 0 1574.43 1626.64 104.97 o 1 16 0 1583.80 1612.09 24.91 o 2 16 0 1222.73 1241.90 20.20 o 3 16 0 1542.44 1521.45 34.01 o 1 17 0 3.55 11.62 9.84 o 2 17 0 2.15 7.95 7.85 o -10 1 1 1990.40 1996.09 56.62 o -9 1 1 3260.09 3353.12 91.47 o -8 1 1 6078.67 5930.39 62.27 o -7 1 1 7888.75 7565.81 99.74 o -6 1 1 7574.29 7656.34 128.00 o -5 1 1 5710.53 5605.83 54.74 o -4 1 1 11515.19 11583.31 104.24 o -3 1 1 11864.92 12102.96 131.45 o -2 1 1 15381.59 15513.32 152.60 o -1 1 1 20520.81 19423.96 201.05 o 0 1 1 29034.31 25080.56 505.82 o 1 1 1 15578.94 15913.33 134.38 o 2 1 1 8605.44 9040.69 81.64 o 3 1 1 21559.97 21425.29 203.15 o 4 1 1 15407.46 15210.43 155.00 o 5 1 1 7429.00 7683.24 79.54 o 6 1 1 5362.73 5425.92 56.94 o 7 1 1 3228.10 3225.85 34.96 o 8 1 1 2719.35 2737.50 30.25 o 9 1 1 1606.51 1631.66 21.25 o 10 1 1 1791.29 1878.45 53.17 o -10 2 1 3.37 7.74 8.37 o -9 2 1 4.47 18.94 5.23 o -8 2 1 32.89 43.43 3.98 o -7 2 1 7.44 12.98 3.45 o -6 2 1 18.18 19.26 3.14 o -5 2 1 3.98 9.21 2.62 o -4 2 1 44.55 45.74 2.51 o -3 2 1 127.66 199.06 3.56 o -2 2 1 4.68 88.02 11.20 o -1 2 1 6494.95 7043.45 74.10 o 0 2 1 816.06 873.60 12.14 o 1 2 1 460.24 512.73 6.17 o 2 2 1 588.57 683.75 8.27 o 3 2 1 0.07 33.18 3.87 o 4 2 1 334.55 371.34 5.55 o 5 2 1 99.90 108.95 3.77 o 6 2 1 11.47 19.26 3.24 o 7 2 1 35.97 40.50 3.77 o 8 2 1 56.91 66.15 4.71 o 9 2 1 36.75 42.49 4.61 o 10 2 1 0.28 5.44 11.72 o -10 3 1 1693.85 1758.40 36.63 o -9 3 1 2468.07 2571.51 40.29 o -8 3 1 3674.33 3638.74 47.93 o -7 3 1 5775.27 5649.58 62.17 o -6 3 1 6714.27 6592.05 78.60 o -5 3 1 7222.57 7282.29 70.44 o -4 3 1 12681.40 12699.42 114.18 o -3 3 1 16224.46 16493.78 147.68 o -2 3 1 22633.46 22433.90 232.03 o -1 3 1 26527.99 25957.09 268.04 o 0 3 1 18780.49 18853.15 199.27 o 1 3 1 18509.60 18284.73 163.27 o 2 3 1 10554.31 10463.03 88.96 o 3 3 1 14435.57 14232.80 127.69 o 4 3 1 13482.29 13385.88 127.79 o 5 3 1 8873.10 8964.18 86.35 o 6 3 1 5870.76 5926.72 61.96 o 7 3 1 4863.78 4716.53 54.84 o 8 3 1 2612.96 2568.69 31.40 o 9 3 1 1999.00 1952.65 24.70 o 10 3 1 1796.21 1838.05 31.08 o -10 4 1 1.87 -8.16 8.16 o -9 4 1 28.44 33.70 5.34 o -8 4 1 45.28 43.85 4.92 o -7 4 1 8.66 15.07 3.87 o -6 4 1 7.87 13.50 3.14 o -5 4 1 1.21 11.72 2.83 o -4 4 1 0.09 12.77 2.62 o -3 4 1 316.44 387.24 5.65 o -2 4 1 177.89 272.22 6.59 o -1 4 1 4437.08 4824.12 64.89 o 0 4 1 986.25 1125.00 15.18 o 1 4 1 312.33 361.18 5.34 o 2 4 1 504.38 616.03 10.05 o 3 4 1 31.66 40.92 2.51 o 4 4 1 77.43 101.94 3.66 o 5 4 1 251.34 278.40 5.02 o 6 4 1 246.56 258.41 5.97 o 7 4 1 74.24 77.76 4.50 o 8 4 1 35.21 46.78 4.61 o 9 4 1 1.06 6.07 4.40 o 10 4 1 1.46 9.84 9.94 o -9 5 1 1695.81 1678.97 24.39 o -8 5 1 2445.31 2385.63 36.84 o -7 5 1 4501.86 4327.61 56.20 o -6 5 1 3935.04 3965.80 42.81 o -5 5 1 10091.50 10197.50 97.96 o -4 5 1 9957.16 10184.63 98.17 o -3 5 1 19182.18 19185.13 183.05 o -2 5 1 17015.99 17020.22 194.67 o -1 5 1 25048.35 25017.45 258.62 o 0 5 1 14012.47 14365.40 150.50 o 1 5 1 11899.84 11760.71 113.66 o 2 5 1 13650.64 13302.99 138.26 o 3 5 1 7647.27 7336.81 66.67 o 4 5 1 10102.09 9835.06 111.67 o 5 5 1 10454.05 10267.42 106.86 o 6 5 1 5542.15 5504.42 63.53 o 7 5 1 5503.91 5164.90 59.87 o 8 5 1 2985.34 2866.34 35.79 o 9 5 1 2380.62 2324.83 28.89 o -9 6 1 14.38 21.77 6.07 o -8 6 1 0.43 -4.71 4.71 o -7 6 1 4.60 6.17 6.38 o -6 6 1 125.62 136.58 5.02 o -5 6 1 297.63 312.52 7.12 o -4 6 1 103.46 113.56 3.98 o -3 6 1 644.60 709.18 10.88 o -2 6 1 0.13 50.03 22.08 o -1 6 1 537.17 626.18 7.95 o 0 6 1 86.14 120.88 3.77 o 1 6 1 16.15 31.08 2.93 o 2 6 1 457.29 545.07 7.85 o 3 6 1 44.82 84.67 6.07 o 4 6 1 120.54 138.68 4.61 o 5 6 1 0.77 16.75 5.86 o 6 6 1 129.55 124.34 4.81 o 7 6 1 277.73 252.65 6.17 o 8 6 1 27.81 30.98 4.50 o 9 6 1 5.79 0.73 4.29 o -9 7 1 2099.54 2055.85 29.10 o -8 7 1 2218.75 2116.24 34.96 o -7 7 1 1673.88 1655.84 25.33 o -6 7 1 5979.64 5843.83 67.72 o -5 7 1 6231.23 6293.87 79.33 o -4 7 1 5685.39 5819.86 61.96 o -3 7 1 10396.46 10771.15 144.95 o -2 7 1 16429.60 16543.18 171.85 o -1 7 1 9665.51 9677.03 94.09 o 0 7 1 11530.85 11393.04 111.15 o 1 7 1 9497.39 9402.61 85.40 o 2 7 1 14039.84 13787.99 158.46 o 3 7 1 7413.60 7663.04 80.69 o 4 7 1 5772.90 5691.65 66.67 o 5 7 1 6175.38 6073.35 70.12 o 6 7 1 7315.35 6939.31 88.12 o 7 7 1 2474.10 2388.36 32.65 o 8 7 1 2648.20 2536.97 34.64 o 9 7 1 2026.45 1995.46 28.26 o -9 8 1 75.74 68.66 6.91 o -8 8 1 47.71 46.26 5.55 o -7 8 1 2.09 -1.99 4.71 o -6 8 1 29.39 31.82 4.40 o -5 8 1 51.09 51.81 4.29 o -4 8 1 12.94 12.35 3.35 o -3 8 1 5.97 17.37 8.27 o -2 8 1 209.57 236.32 5.55 o -1 8 1 29.47 33.81 2.93 o 0 8 1 3.16 9.94 3.24 o 1 8 1 92.00 100.06 4.40 o 2 8 1 40.43 47.20 4.71 o 3 8 1 288.13 337.74 6.07 o 4 8 1 12.30 21.04 3.66 o 5 8 1 280.17 263.54 6.28 o 6 8 1 98.57 89.59 5.13 o 7 8 1 42.19 39.04 5.13 o 8 8 1 89.47 78.29 5.97 o 9 8 1 12.85 35.38 11.20 o -8 9 1 2120.03 2158.21 30.25 o -7 9 1 2281.37 2314.67 35.90 o -6 9 1 2890.05 2894.39 50.24 o -5 9 1 4601.67 4699.68 55.16 o -4 9 1 4159.27 4339.86 46.99 o -3 9 1 5341.19 5584.38 65.83 o -2 9 1 6947.25 6943.08 81.11 o -1 9 1 6705.92 6940.78 68.24 o 0 9 1 9289.36 9455.14 110.84 o 1 9 1 9168.59 9188.26 97.23 o 2 9 1 10435.46 10076.31 106.34 o 3 9 1 5226.35 5250.41 56.20 o 4 9 1 5030.42 5001.73 60.60 o 5 9 1 3905.80 3893.48 46.16 o 6 9 1 2796.15 2776.23 33.81 o 7 9 1 2295.08 2273.65 31.40 o 8 9 1 1553.12 1585.29 37.68 o -8 10 1 58.30 74.31 7.85 o -7 10 1 18.43 22.61 5.23 o -6 10 1 6.76 5.76 4.81 o -5 10 1 56.42 57.77 4.81 o -4 10 1 0.71 3.98 3.77 o -3 10 1 196.20 169.76 5.44 o -2 10 1 19.72 16.54 3.45 o -1 10 1 425.15 420.84 9.63 o 0 10 1 91.40 96.60 4.50 o 1 10 1 256.40 251.29 5.97 o 2 10 1 2.51 1.26 3.24 o 3 10 1 0.68 5.13 3.04 o 4 10 1 2.00 7.74 4.29 o 5 10 1 153.24 158.98 5.65 o 6 10 1 23.78 20.09 4.29 o 7 10 1 21.81 21.46 5.23 o 8 10 1 47.39 52.23 7.12 o -8 11 1 1186.37 1173.14 36.53 o -7 11 1 2371.77 2414.10 48.98 o -6 11 1 2391.82 2382.49 29.72 o -5 11 1 3723.28 3706.24 44.27 o -4 11 1 4040.71 4116.72 48.67 o -3 11 1 2850.57 2960.74 36.42 o -2 11 1 4335.46 4359.53 78.81 o -1 11 1 6334.57 6500.58 87.50 o 0 11 1 2209.71 2233.46 70.02 o 1 11 1 8646.98 8439.21 90.53 o 2 11 1 5312.61 5167.20 55.89 o 3 11 1 4471.95 4384.23 47.93 o 4 11 1 2217.10 2267.05 28.47 o 5 11 1 3387.99 3315.65 45.00 o 6 11 1 1615.40 1707.64 29.51 o 7 11 1 1587.19 1676.04 28.36 o -7 12 1 0.84 4.08 7.22 o -6 12 1 5.03 8.58 5.13 o -5 12 1 2.90 5.65 4.92 o -4 12 1 322.52 299.75 9.31 o -3 12 1 22.35 23.97 4.71 o -2 12 1 0.88 2.83 4.19 o -1 12 1 142.79 140.04 5.97 o 0 12 1 65.71 62.06 5.34 o 1 12 1 703.32 685.11 12.56 o 2 12 1 66.51 67.72 4.29 o 3 12 1 6.47 6.07 4.08 o 4 12 1 169.21 161.81 5.65 o 5 12 1 11.43 21.46 6.28 o 6 12 1 8.60 6.80 5.34 o 7 12 1 17.79 21.35 6.38 o -6 13 1 2278.85 2255.96 58.92 o -5 13 1 2299.77 2334.04 32.97 o -4 13 1 3450.98 3490.96 87.50 o -3 13 1 3309.94 3389.43 96.81 o -2 13 1 2333.88 2356.64 34.75 o -1 13 1 1826.84 1846.74 27.53 o 0 13 1 4898.96 4649.34 73.05 o 1 13 1 2334.69 2304.00 33.49 o 2 13 1 2348.66 2224.77 32.34 o 3 13 1 2868.36 2834.00 34.96 o 4 13 1 2441.86 2400.71 32.97 o 5 13 1 1240.25 1347.71 18.63 o 6 13 1 1701.82 1733.28 33.70 o -6 14 1 10.15 24.60 8.58 o -5 14 1 44.80 37.05 7.12 o -4 14 1 0.32 1.99 7.12 o -3 14 1 0.68 4.71 7.95 o -2 14 1 10.00 6.28 5.55 o -1 14 1 29.14 17.16 5.13 o 0 14 1 31.26 41.55 7.95 o 1 14 1 1.39 -0.73 4.61 o 2 14 1 8.21 3.56 4.71 o 3 14 1 8.12 -0.52 5.34 o 4 14 1 3.84 2.93 6.17 o 5 14 1 0.81 3.87 9.11 o 6 14 1 6.32 13.50 8.90 o -4 15 1 2079.62 2087.14 51.07 o -3 15 1 1704.88 1737.37 96.81 o -2 15 1 1989.90 2015.45 34.85 o -1 15 1 1711.46 1688.07 29.93 o 0 15 1 2117.11 2108.81 31.19 o 1 15 1 1922.35 1879.60 28.15 o 2 15 1 1611.96 1669.65 25.54 o 3 15 1 1884.69 1915.39 33.07 o 4 15 1 1261.56 1310.35 37.26 o 5 15 1 957.24 954.82 19.15 o -3 16 1 44.46 45.00 9.52 o -2 16 1 1.65 8.48 7.22 o -1 16 1 32.09 29.72 7.01 o 0 16 1 3.64 2.62 5.02 o 1 16 1 1.43 -4.40 5.34 o 2 16 1 40.59 30.25 5.76 o 3 16 1 31.09 34.12 7.22 o -2 17 1 702.54 745.92 29.41 o -1 17 1 1799.27 1856.57 40.19 o 0 17 1 1268.31 1290.05 24.39 o 1 17 1 1483.47 1468.81 47.62 o 2 17 1 1180.12 1162.47 22.29 o -10 0 2 1998.22 2000.69 56.94 o -9 0 2 2050.22 2106.50 47.83 o -8 0 2 6020.37 5774.13 103.61 o -7 0 2 3296.59 3449.40 82.89 o -6 0 2 5033.67 4997.02 74.41 o -5 0 2 5626.66 5837.45 75.67 o -4 0 2 8656.48 8842.99 134.38 o -3 0 2 25087.26 24734.13 311.99 o -2 0 2 3359.11 3465.21 45.74 o -1 0 2 8622.61 9117.20 261.76 o 0 0 2 38166.86 35835.48 1114.74 o 1 0 2 15026.81 15041.30 252.34 o 2 0 2 19571.55 19461.85 220.31 o 3 0 2 30012.31 28944.21 326.75 o 4 0 2 27057.22 26744.97 302.16 o 5 0 2 4384.40 4431.75 66.25 o 6 0 2 7069.45 6931.78 101.94 o 7 0 2 4122.05 4048.38 115.65 o 8 0 2 2520.75 2536.03 39.98 o 9 0 2 2155.75 2127.86 108.11 o -10 1 2 11.64 -0.63 9.21 o -9 1 2 75.14 65.31 7.95 o -8 1 2 73.68 75.77 4.61 o -7 1 2 26.31 31.19 3.56 o -6 1 2 64.13 56.31 3.45 o -5 1 2 116.80 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