#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2200712.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200712_Fobs loop_ _publ_author_name 'Fujimoto, Kazuya' 'Nagata, Kiyonori' 'Suzuki, Honoh' 'Kanamori, Kan' _publ_section_title ; trans-Bis(1,4-butanediamine)dichlorocobalt(III) chloride monohydrate ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m467 _journal_page_last m469 _journal_volume 57 _journal_year 2001 _space_group_IT_number 9 _symmetry_space_group_name_Hall 'C -2yc' _symmetry_space_group_name_H-M 'C 1 c 1' _cell_angle_alpha 90.000 _cell_angle_beta 122.745 _cell_angle_gamma 90.000 _cell_length_a 14.9139 _cell_length_b 13.5602 _cell_length_c 8.9938 _exptl_crystal_F_000 752.00 _reflns_d_resolution_high 0.7112 _[local]_cod_data_source_file ob6072Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' [Co(tmd)2Cl2]Cl.H2O, tmd = H2N(CH2)4NH2 (2nd sample) no disorder' _shelx_refln_list_code 4 _shelx_f_calc_maximum 238.91 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 -12 45.45 95.37 8.37 o 8 0 -12 428.00 379.50 19.22 o 10 0 -12 676.46 710.72 24.56 o 12 0 -12 307.59 332.36 17.63 o 14 0 -12 408.40 400.05 19.20 o 16 0 -12 227.57 236.80 16.50 o 7 1 -12 0.21 9.27 9.30 o 9 1 -12 27.47 10.38 10.39 o 11 1 -12 24.55 1.14 10.79 o 13 1 -12 185.72 190.19 15.12 o 15 1 -12 39.71 34.45 5.06 o 6 2 -12 209.79 214.24 16.51 o 8 2 -12 251.11 235.01 17.03 o 10 2 -12 315.30 291.22 17.36 o 12 2 -12 266.62 282.57 18.07 o 14 2 -12 177.13 168.79 15.14 o 16 2 -12 256.49 214.63 16.44 o 7 3 -12 127.28 94.69 7.67 o 9 3 -12 79.65 87.61 7.08 o 11 3 -12 221.51 195.50 16.00 o 13 3 -12 113.41 124.62 9.40 o 15 3 -12 31.08 45.29 5.16 o 8 4 -12 249.25 239.36 15.95 o 10 4 -12 107.23 132.04 9.25 o 12 4 -12 101.07 89.81 8.75 o 14 4 -12 368.97 374.75 20.54 o 9 5 -12 187.34 205.56 16.31 o 11 5 -12 94.87 49.23 5.01 o 13 5 -12 111.33 100.11 9.28 o 3 1 -11 0.88 -5.37 8.77 o 5 1 -11 96.36 91.80 7.61 o 7 1 -11 1756.22 1689.41 34.82 o 9 1 -11 1647.92 1679.27 33.84 o 11 1 -11 70.84 104.53 8.04 o 13 1 -11 99.44 86.60 8.05 o 15 1 -11 1311.02 1233.40 30.67 o 17 1 -11 798.76 838.05 26.33 o 2 2 -11 138.70 124.84 9.41 o 4 2 -11 24.68 29.19 4.28 o 6 2 -11 89.20 104.04 8.49 o 8 2 -11 12.95 2.12 9.97 o 10 2 -11 142.13 125.55 12.24 o 12 2 -11 8.45 0.05 8.29 o 14 2 -11 28.41 12.73 10.19 o 16 2 -11 19.94 17.30 4.36 o 18 2 -11 20.81 26.24 4.51 o 3 3 -11 42.06 39.91 4.70 o 5 3 -11 71.08 62.04 6.09 o 7 3 -11 811.11 825.32 24.73 o 9 3 -11 954.88 998.84 27.17 o 11 3 -11 26.10 31.98 4.10 o 13 3 -11 45.95 31.65 4.17 o 15 3 -11 472.92 454.59 19.69 o 17 3 -11 447.50 438.54 20.32 o 2 4 -11 166.93 140.20 10.31 o 4 4 -11 3.36 11.76 9.33 o 6 4 -11 241.70 239.32 15.98 o 8 4 -11 61.60 88.20 6.73 o 10 4 -11 177.93 151.56 12.61 o 12 4 -11 197.59 229.00 14.90 o 14 4 -11 65.27 65.84 5.56 o 16 4 -11 194.26 221.14 16.26 o 3 5 -11 264.11 273.41 17.00 o 5 5 -11 422.67 485.44 21.13 o 7 5 -11 196.88 207.92 15.38 o 9 5 -11 98.12 116.51 10.96 o 11 5 -11 467.22 474.29 20.18 o 13 5 -11 489.23 457.19 20.33 o 15 5 -11 154.60 138.32 13.70 o 17 5 -11 142.83 162.46 14.57 o 4 6 -11 31.45 12.36 11.79 o 6 6 -11 176.77 157.23 14.27 o 8 6 -11 208.41 193.53 15.73 o 10 6 -11 85.63 97.64 8.69 o 12 6 -11 74.01 100.37 8.35 o 14 6 -11 37.63 52.84 5.00 o 16 6 -11 14.37 -7.17 11.10 o 5 7 -11 645.60 597.04 25.23 o 7 7 -11 146.61 166.03 14.82 o 9 7 -11 118.50 107.08 9.85 o 11 7 -11 514.30 452.23 20.99 o 13 7 -11 991.62 1035.83 29.68 o 15 7 -11 356.61 346.37 19.46 o 6 8 -11 8.95 11.55 10.03 o 8 8 -11 51.49 36.95 5.13 o 10 8 -11 61.29 60.67 6.05 o 12 8 -11 62.25 55.62 5.51 o 14 8 -11 68.94 53.85 5.63 o 9 9 -11 15.68 6.03 10.01 o 11 9 -11 701.93 692.24 25.88 o 0 0 -10 344.77 413.00 19.54 o 2 0 -10 59.24 63.23 5.50 o 4 0 -10 763.42 784.04 22.86 o 6 0 -10 2369.27 2394.45 37.58 o 8 0 -10 1403.20 1394.43 28.89 o 10 0 -10 121.16 101.73 9.57 o 12 0 -10 439.98 378.56 17.06 o 14 0 -10 3358.67 3485.48 46.87 o 16 0 -10 1352.07 1353.41 30.69 o 18 0 -10 23.37 28.55 4.25 o 1 1 -10 34.94 37.72 4.35 o 3 1 -10 93.14 102.92 7.78 o 5 1 -10 45.14 41.42 4.29 o 7 1 -10 224.38 232.19 13.56 o 9 1 -10 28.42 45.98 4.23 o 11 1 -10 275.86 355.96 15.68 o 13 1 -10 2.11 0.63 8.31 o 15 1 -10 37.58 40.16 4.73 o 17 1 -10 25.93 43.69 4.43 o 19 1 -10 8.41 8.98 4.26 o 0 2 -10 324.51 312.70 18.15 o 2 2 -10 1.57 15.91 3.71 o 4 2 -10 535.94 509.23 19.13 o 6 2 -10 2050.94 2028.80 35.79 o 8 2 -10 447.38 479.52 18.12 o 10 2 -10 159.92 192.12 12.27 o 12 2 -10 699.66 771.53 22.53 o 14 2 -10 685.71 664.83 21.48 o 16 2 -10 545.06 604.34 22.36 o 18 2 -10 212.71 168.76 15.69 o 1 3 -10 19.74 24.13 4.31 o 3 3 -10 214.40 227.55 13.96 o 5 3 -10 44.32 37.66 3.95 o 7 3 -10 204.53 188.15 12.94 o 9 3 -10 99.39 92.89 7.10 o 11 3 -10 333.56 268.04 15.06 o 13 3 -10 304.50 267.23 15.84 o 15 3 -10 194.22 171.13 13.16 o 17 3 -10 109.04 110.14 8.82 o 19 3 -10 123.03 106.18 8.98 o 0 4 -10 241.47 245.95 16.58 o 2 4 -10 238.65 208.31 14.96 o 4 4 -10 159.53 163.61 12.81 o 6 4 -10 273.66 305.85 15.66 o 8 4 -10 737.35 739.90 22.01 o 10 4 -10 385.45 441.03 17.52 o 12 4 -10 135.97 128.10 11.62 o 14 4 -10 477.57 501.20 19.58 o 16 4 -10 260.29 281.24 16.14 o 18 4 -10 86.09 84.41 6.76 o 1 5 -10 39.72 54.02 4.99 o 3 5 -10 325.40 294.75 16.71 o 5 5 -10 45.34 65.25 6.39 o 7 5 -10 506.41 479.71 18.64 o 9 5 -10 9.04 12.18 8.27 o 11 5 -10 334.39 404.91 18.03 o 13 5 -10 14.89 14.83 3.96 o 15 5 -10 170.33 145.47 13.55 o 17 5 -10 33.38 55.93 5.54 o 0 6 -10 489.59 431.16 21.93 o 2 6 -10 748.11 752.17 26.46 o 4 6 -10 211.99 229.74 15.40 o 6 6 -10 179.13 163.85 13.30 o 8 6 -10 763.69 744.15 23.04 o 10 6 -10 1063.77 996.74 25.98 o 12 6 -10 415.40 430.08 18.32 o 14 6 -10 130.41 127.27 9.06 o 16 6 -10 539.49 463.05 21.03 o 18 6 -10 488.89 391.23 21.76 o 1 7 -10 0.17 -10.90 10.90 o 3 7 -10 39.20 56.56 5.59 o 5 7 -10 5.91 11.13 7.47 o 7 7 -10 36.09 38.50 4.34 o 9 7 -10 2.51 4.65 9.43 o 11 7 -10 82.85 82.81 7.53 o 13 7 -10 26.16 34.03 4.39 o 15 7 -10 87.41 77.11 6.96 o 17 7 -10 52.86 77.90 7.10 o 2 8 -10 1026.70 887.90 29.82 o 4 8 -10 304.86 308.68 18.93 o 6 8 -10 67.38 97.35 8.14 o 8 8 -10 995.21 885.45 26.86 o 10 8 -10 1451.85 1421.35 32.77 o 12 8 -10 262.70 290.14 16.36 o 14 8 -10 58.02 62.54 5.58 o 16 8 -10 301.60 226.76 16.62 o 3 9 -10 11.17 17.06 4.76 o 5 9 -10 0.71 4.00 8.22 o 7 9 -10 30.01 24.60 4.70 o 9 9 -10 12.53 9.53 9.13 o 11 9 -10 5.71 9.24 4.53 o 13 9 -10 0.78 -10.39 10.39 o 15 9 -10 32.79 31.99 4.75 o 4 10 -10 180.22 172.90 16.24 o 6 10 -10 14.55 16.00 4.66 o 8 10 -10 208.05 170.53 15.25 o 10 10 -10 580.20 556.16 22.82 o 12 10 -10 352.96 337.62 19.78 o 14 10 -10 49.55 41.72 4.87 o 7 11 -10 65.52 33.92 4.85 o 9 11 -10 84.16 86.78 7.79 o 11 11 -10 34.57 31.09 5.07 o 1 1 -9 341.75 344.17 15.85 o 3 1 -9 3007.87 2969.06 40.24 o 5 1 -9 2679.29 2840.56 37.61 o 7 1 -9 185.42 236.10 11.95 o 9 1 -9 240.64 234.88 12.75 o 11 1 -9 2513.81 2345.92 34.46 o 13 1 -9 1857.60 2004.88 33.28 o 15 1 -9 196.94 155.81 12.45 o 17 1 -9 219.91 191.90 14.11 o 19 1 -9 601.32 625.64 23.54 o 0 2 -9 172.88 204.68 13.34 o 2 2 -9 415.97 438.87 17.80 o 4 2 -9 36.12 49.74 4.87 o 6 2 -9 194.05 188.81 11.49 o 8 2 -9 86.56 61.41 4.71 o 10 2 -9 418.86 387.27 15.32 o 12 2 -9 44.34 54.19 4.56 o 14 2 -9 26.00 21.15 3.57 o 16 2 -9 38.27 64.29 6.28 o 18 2 -9 131.44 172.42 13.22 o 20 2 -9 9.42 -10.89 10.89 o 1 3 -9 248.76 267.26 14.62 o 3 3 -9 981.64 969.19 24.38 o 5 3 -9 996.18 1007.29 23.91 o 7 3 -9 588.78 672.00 19.10 o 9 3 -9 378.62 382.50 15.71 o 11 3 -9 649.93 671.73 20.05 o 13 3 -9 1183.75 1173.13 26.37 o 15 3 -9 357.67 347.25 15.26 o 17 3 -9 53.56 48.16 4.35 o 19 3 -9 339.21 365.02 18.75 o 0 4 -9 51.62 45.89 4.46 o 2 4 -9 622.89 631.27 20.40 o 4 4 -9 23.04 14.90 3.40 o 6 4 -9 1089.47 1122.48 24.80 o 8 4 -9 36.86 47.80 4.27 o 10 4 -9 844.97 860.86 22.00 o 12 4 -9 60.32 56.14 4.65 o 14 4 -9 504.64 504.58 18.94 o 16 4 -9 40.18 41.04 4.34 o 18 4 -9 173.06 181.13 13.60 o 1 5 -9 383.80 342.16 17.12 o 3 5 -9 184.24 190.34 13.70 o 5 5 -9 723.96 832.42 22.60 o 7 5 -9 749.18 740.71 21.37 o 9 5 -9 537.46 516.14 18.05 o 11 5 -9 598.22 602.35 19.50 o 13 5 -9 469.31 437.25 17.90 o 15 5 -9 598.32 565.54 20.96 o 17 5 -9 575.41 547.32 21.92 o 19 5 -9 93.68 97.96 8.53 o 0 6 -9 77.67 142.66 11.93 o 2 6 -9 285.07 259.75 16.05 o 4 6 -9 140.03 158.72 12.09 o 6 6 -9 511.85 508.74 18.55 o 8 6 -9 95.25 108.43 10.04 o 10 6 -9 80.36 102.10 7.56 o 12 6 -9 78.69 61.59 5.54 o 14 6 -9 245.67 284.40 16.04 o 16 6 -9 167.94 186.39 13.12 o 18 6 -9 30.79 58.32 5.52 o 1 7 -9 1013.31 1044.40 29.59 o 3 7 -9 94.18 86.10 7.83 o 5 7 -9 88.49 48.86 4.71 o 7 7 -9 2404.91 2433.94 38.52 o 9 7 -9 2660.69 2748.43 40.25 o 11 7 -9 46.33 64.99 5.43 o 13 7 -9 175.80 186.46 13.06 o 15 7 -9 1066.70 1048.66 28.45 o 17 7 -9 492.60 437.77 20.93 o 0 8 -9 0.85 8.39 10.09 o 2 8 -9 63.32 104.75 8.36 o 4 8 -9 52.19 64.48 5.88 o 6 8 -9 53.51 73.64 6.05 o 8 8 -9 17.58 42.95 4.56 o 10 8 -9 101.27 114.68 8.85 o 12 8 -9 27.93 32.79 4.06 o 14 8 -9 38.98 40.43 4.58 o 16 8 -9 59.63 55.67 5.23 o 18 8 -9 5.43 -3.28 10.45 o 1 9 -9 563.15 543.48 22.23 o 3 9 -9 26.60 25.20 4.35 o 5 9 -9 258.89 244.94 15.55 o 7 9 -9 1215.26 1168.16 28.49 o 9 9 -9 1151.54 1161.23 28.81 o 11 9 -9 317.31 325.03 16.43 o 13 9 -9 56.83 59.47 5.12 o 15 9 -9 444.70 466.57 20.84 o 17 9 -9 640.00 601.56 25.80 o 0 10 -9 2.45 10.16 10.94 o 2 10 -9 17.38 21.21 4.85 o 4 10 -9 34.58 23.14 4.33 o 6 10 -9 307.33 280.96 16.19 o 8 10 -9 25.94 27.01 4.52 o 10 10 -9 207.56 178.31 14.88 o 12 10 -9 84.03 83.06 8.04 o 14 10 -9 128.95 138.85 9.87 o 16 10 -9 0.21 -10.31 10.31 o 1 11 -9 361.91 405.23 21.24 o 3 11 -9 148.31 125.16 9.91 o 5 11 -9 6.55 1.16 10.27 o 7 11 -9 368.61 373.52 19.49 o 9 11 -9 538.05 574.28 22.37 o 11 11 -9 51.35 53.48 4.98 o 13 11 -9 188.84 190.15 15.42 o 15 11 -9 395.38 368.53 21.36 o 4 12 -9 18.31 9.70 11.14 o 6 12 -9 16.62 9.30 4.63 o 8 12 -9 30.65 20.58 5.03 o 10 12 -9 27.65 34.69 5.23 o 12 12 -9 2.02 8.54 10.36 o 7 13 -9 93.26 94.22 7.98 o 9 13 -9 286.26 290.68 20.19 o 11 13 -9 473.25 426.72 22.27 o 0 0 -8 1832.17 1856.69 31.64 o 2 0 -8 4927.35 5035.08 47.93 o 4 0 -8 396.91 420.44 14.08 o 6 0 -8 217.36 263.44 11.13 o 8 0 -8 4417.03 4770.40 43.67 o 10 0 -8 2588.23 2852.04 34.71 o 12 0 -8 536.53 632.81 17.81 o 14 0 -8 696.44 698.48 20.35 o 16 0 -8 459.55 400.13 16.43 o 18 0 -8 562.70 506.35 19.94 o 20 0 -8 367.11 352.46 19.46 o 1 1 -8 50.87 52.31 4.95 o 3 1 -8 6.77 14.76 2.95 o 5 1 -8 60.03 43.58 4.28 o 7 1 -8 148.29 114.73 8.79 o 9 1 -8 809.85 799.82 18.83 o 11 1 -8 194.85 158.41 10.47 o 13 1 -8 200.40 205.28 11.67 o 15 1 -8 437.80 439.25 16.40 o 17 1 -8 125.78 129.19 11.50 o 19 1 -8 71.13 55.78 5.01 o 0 2 -8 1596.15 1657.74 30.47 o 2 2 -8 1371.81 1447.35 26.54 o 4 2 -8 782.99 683.93 18.17 o 6 2 -8 1017.54 932.43 20.46 o 8 2 -8 1652.79 1716.93 26.83 o 10 2 -8 3681.59 3878.36 40.59 o 12 2 -8 1255.08 1160.95 23.83 o 14 2 -8 29.92 64.42 6.14 o 16 2 -8 750.06 669.46 21.26 o 18 2 -8 814.91 740.09 24.54 o 20 2 -8 148.38 185.96 15.49 o 1 3 -8 275.95 306.32 13.77 o 3 3 -8 1333.74 1319.68 25.47 o 5 3 -8 103.66 123.86 9.62 o 7 3 -8 3133.09 3439.53 38.10 o 9 3 -8 96.15 76.05 5.83 o 11 3 -8 834.49 989.42 21.84 o 13 3 -8 48.91 103.64 8.48 o 15 3 -8 225.02 187.10 12.57 o 17 3 -8 358.69 370.26 17.74 o 19 3 -8 10.17 -7.23 9.24 o 0 4 -8 474.44 513.43 18.50 o 2 4 -8 997.26 1009.01 23.01 o 4 4 -8 803.63 833.40 20.76 o 6 4 -8 1288.20 1296.88 24.58 o 8 4 -8 2178.70 2306.90 31.97 o 10 4 -8 461.86 504.20 16.06 o 12 4 -8 591.91 682.83 18.96 o 14 4 -8 1693.94 1657.65 30.50 o 16 4 -8 504.74 434.74 17.90 o 18 4 -8 211.36 276.80 17.06 o 20 4 -8 353.48 366.75 19.14 o 1 5 -8 20.90 -5.81 7.18 o 3 5 -8 962.58 1048.11 23.49 o 5 5 -8 128.96 96.26 9.50 o 7 5 -8 634.70 542.69 16.58 o 9 5 -8 69.22 70.20 5.93 o 11 5 -8 1630.80 1569.38 27.73 o 13 5 -8 772.08 740.81 21.09 o 15 5 -8 494.60 456.06 17.65 o 17 5 -8 79.53 132.06 12.02 o 19 5 -8 262.15 174.89 15.16 o 0 6 -8 245.10 247.98 14.71 o 2 6 -8 159.71 185.75 12.46 o 4 6 -8 2289.15 2264.65 34.37 o 6 6 -8 2381.60 2420.40 34.79 o 8 6 -8 75.92 67.98 6.45 o 10 6 -8 280.85 303.16 13.99 o 12 6 -8 1695.31 1832.77 31.56 o 14 6 -8 1124.61 1024.40 25.80 o 16 6 -8 379.18 446.12 18.45 o 18 6 -8 113.39 126.06 11.68 o 1 7 -8 121.42 117.76 8.45 o 3 7 -8 353.46 280.85 14.51 o 5 7 -8 251.65 232.90 13.20 o 7 7 -8 220.40 215.79 12.10 o 9 7 -8 10.68 3.03 7.47 o 11 7 -8 217.23 259.28 13.75 o 13 7 -8 68.10 90.85 7.12 o 15 7 -8 22.21 15.17 3.84 o 17 7 -8 41.99 63.51 6.26 o 19 7 -8 44.26 9.94 12.02 o 0 8 -8 165.45 202.76 14.80 o 2 8 -8 107.90 84.85 7.48 o 4 8 -8 1382.02 1432.39 29.42 o 6 8 -8 1812.67 1727.86 31.45 o 8 8 -8 494.77 509.52 18.16 o 10 8 -8 205.16 209.27 12.81 o 12 8 -8 929.97 883.10 23.95 o 14 8 -8 1033.00 1025.63 27.38 o 16 8 -8 96.74 105.25 8.36 o 18 8 -8 31.02 35.20 4.66 o 1 9 -8 38.61 46.28 4.64 o 3 9 -8 72.23 44.52 4.22 o 5 9 -8 27.35 30.98 4.12 o 7 9 -8 39.81 42.16 4.34 o 9 9 -8 188.77 176.92 12.83 o 11 9 -8 30.10 24.62 3.70 o 13 9 -8 30.52 43.06 4.54 o 15 9 -8 10.17 8.48 9.65 o 17 9 -8 68.28 58.70 5.40 o 0 10 -8 204.80 251.37 16.44 o 2 10 -8 111.50 131.44 9.98 o 4 10 -8 722.79 678.08 22.99 o 6 10 -8 1340.71 1306.03 29.97 o 8 10 -8 357.66 362.67 16.85 o 10 10 -8 64.27 48.44 4.32 o 12 10 -8 368.23 364.05 17.55 o 14 10 -8 802.41 826.48 26.67 o 16 10 -8 402.56 462.94 21.70 o 1 11 -8 11.07 12.71 10.39 o 3 11 -8 361.12 352.79 18.76 o 5 11 -8 13.44 31.57 4.46 o 7 11 -8 181.96 178.35 13.93 o 9 11 -8 12.43 18.61 4.20 o 11 11 -8 115.68 108.55 8.82 o 13 11 -8 35.58 35.63 4.96 o 15 11 -8 26.16 20.01 4.86 o 0 12 -8 185.64 181.62 17.06 o 2 12 -8 260.70 242.42 16.34 o 4 12 -8 350.42 358.78 19.73 o 6 12 -8 196.88 217.38 15.57 o 8 12 -8 223.27 227.70 15.95 o 10 12 -8 437.62 408.02 20.59 o 12 12 -8 313.72 307.45 17.61 o 14 12 -8 179.83 178.61 15.95 o 1 13 -8 11.86 -3.68 11.27 o 3 13 -8 66.50 42.24 5.23 o 5 13 -8 11.35 6.99 10.64 o 7 13 -8 336.59 336.28 18.91 o 9 13 -8 131.24 147.90 10.70 o 11 13 -8 107.91 85.07 7.61 o 13 13 -8 34.83 48.33 5.44 o 4 14 -8 24.11 7.37 11.96 o 6 14 -8 34.08 44.74 5.17 o 8 14 -8 552.02 546.68 23.39 o 10 14 -8 593.06 593.16 23.95 o 1 1 -7 1250.22 1315.42 23.04 o 3 1 -7 70.84 71.19 6.52 o 5 1 -7 1710.00 1749.83 24.39 o 7 1 -7 7915.04 7568.48 49.63 o 9 1 -7 1687.81 1744.88 25.20 o 11 1 -7 84.75 99.32 8.11 o 13 1 -7 769.74 711.58 18.14 o 15 1 -7 3554.91 3650.79 43.15 o 17 1 -7 673.33 623.30 20.72 o 19 1 -7 35.80 57.62 5.43 o 0 2 -7 32.07 14.92 3.14 o 2 2 -7 94.35 128.48 8.13 o 4 2 -7 217.28 148.50 8.95 o 6 2 -7 892.10 849.34 17.39 o 8 2 -7 4.32 28.23 2.83 o 10 2 -7 48.39 55.89 4.19 o 12 2 -7 509.94 456.65 15.10 o 14 2 -7 291.24 363.25 14.19 o 16 2 -7 12.93 13.53 3.56 o 18 2 -7 21.97 28.91 3.92 o 20 2 -7 2.36 2.95 8.84 o 1 3 -7 2338.07 2444.22 32.29 o 3 3 -7 137.58 146.47 8.69 o 5 3 -7 703.15 668.90 16.25 o 7 3 -7 7096.18 7172.97 50.08 o 9 3 -7 4141.95 4143.05 39.13 o 11 3 -7 297.58 284.46 12.16 o 13 3 -7 1193.35 1273.79 24.77 o 15 3 -7 2116.39 2189.92 34.39 o 17 3 -7 597.81 544.88 19.57 o 19 3 -7 138.93 102.73 8.20 o 0 4 -7 424.21 489.16 16.06 o 2 4 -7 1254.92 1218.28 22.62 o 4 4 -7 25.39 82.62 7.84 o 6 4 -7 893.00 832.68 18.13 o 8 4 -7 408.57 414.70 13.25 o 10 4 -7 380.15 414.17 14.27 o 12 4 -7 468.72 435.27 14.74 o 14 4 -7 151.51 212.16 12.12 o 16 4 -7 43.16 37.30 4.18 o 18 4 -7 138.31 161.47 13.38 o 20 4 -7 6.17 8.98 4.15 o 1 5 -7 558.86 560.76 16.93 o 3 5 -7 2475.22 2491.22 32.44 o 5 5 -7 3933.39 3925.85 39.23 o 7 5 -7 904.74 1035.46 20.38 o 9 5 -7 974.16 1043.29 21.13 o 11 5 -7 2131.62 2081.48 30.68 o 13 5 -7 997.91 983.16 22.67 o 15 5 -7 747.40 740.92 21.83 o 17 5 -7 787.16 770.19 23.63 o 19 5 -7 312.74 296.22 17.27 o 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765.52 24.75 o 4 16 0 351.50 384.99 18.98 o 6 16 0 169.14 136.38 10.78 o 8 16 0 434.59 469.26 23.15 o 1 17 0 87.98 97.61 9.47 o 3 17 0 95.83 95.76 8.31 o 5 17 0 45.19 63.70 5.83 o 7 17 0 10.07 -0.73 13.52 o 0 18 0 497.25 482.18 23.03 o 2 18 0 111.29 128.43 10.87 o 4 18 0 28.10 16.18 12.45 o 1 19 0 40.13 32.94 5.78 o 1 1 1 27896.64 26990.21 117.85 o 3 1 1 4783.26 4165.41 22.13 o 9 1 1 1123.46 1336.64 22.26 o 11 1 1 69.89 40.13 3.76 o 13 1 1 931.79 1018.68 24.35 o 15 1 1 1195.07 1255.11 31.23 o 0 2 1 217.34 246.80 4.92 o 2 2 1 2261.11 1977.20 15.45 o 4 2 1 5702.73 5228.27 29.02 o 6 2 1 153.76 61.87 5.19 o 8 2 1 957.85 837.35 16.42 o 10 2 1 262.49 220.84 11.48 o 12 2 1 861.10 896.97 22.07 o 14 2 1 19.08 11.67 3.50 o 16 2 1 71.07 73.56 6.08 o 1 3 1 1398.31 1682.18 14.09 o 3 3 1 67.63 104.50 5.27 o 5 3 1 6254.94 5432.41 33.64 o 7 3 1 7012.60 7043.35 43.30 o 9 3 1 904.45 927.13 18.76 o 11 3 1 245.17 181.55 10.99 o 13 3 1 513.58 644.36 19.80 o 15 3 1 519.91 542.13 21.02 o 0 4 1 19732.97 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29.72 o 8 10 2 1839.01 1667.43 33.04 o 10 10 2 211.07 172.87 14.10 o 12 10 2 36.43 53.88 5.69 o 1 11 2 712.48 795.88 19.53 o 3 11 2 129.54 103.94 10.08 o 5 11 2 297.26 261.93 14.94 o 7 11 2 157.34 148.09 13.00 o 9 11 2 87.60 123.02 9.43 o 11 11 2 96.21 95.12 7.84 o 0 12 2 1000.86 988.18 22.27 o 2 12 2 937.79 981.63 23.03 o 4 12 2 1182.68 1260.83 27.58 o 6 12 2 669.79 629.48 21.58 o 8 12 2 365.23 401.77 20.08 o 10 12 2 247.82 245.64 18.58 o 1 13 2 945.78 894.59 23.18 o 3 13 2 646.73 710.58 21.52 o 5 13 2 66.26 93.45 8.35 o 7 13 2 5.17 4.17 11.02 o 9 13 2 198.99 183.28 17.00 o 0 14 2 137.36 139.09 11.50 o 2 14 2 240.33 243.31 15.09 o 4 14 2 1133.01 1112.38 28.54 o 6 14 2 786.77 863.00 26.74 o 8 14 2 74.38 76.09 7.57 o 1 15 2 30.43 21.57 4.45 o 3 15 2 36.53 50.57 5.18 o 5 15 2 32.11 17.54 5.44 o 7 15 2 34.12 48.96 5.82 o 0 16 2 17.28 17.11 4.73 o 2 16 2 597.57 526.73 22.58 o 4 16 2 1068.31 1095.28 30.89 o 6 16 2 110.56 95.85 8.86 o 1 17 2 10.97 13.10 11.09 o 3 17 2 37.20 31.65 5.81 o 5 17 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864.98 26.28 o 9 11 3 44.70 56.09 5.65 o 11 11 3 206.89 180.86 12.41 o 0 12 3 196.05 122.22 11.95 o 2 12 3 137.00 161.76 13.38 o 4 12 3 15.47 34.21 4.81 o 6 12 3 81.83 78.18 7.17 o 8 12 3 278.56 351.02 19.76 o 10 12 3 9.22 2.88 13.05 o 1 13 3 677.76 655.75 21.28 o 3 13 3 1056.56 1081.27 27.36 o 5 13 3 286.86 317.04 17.36 o 7 13 3 279.10 261.38 19.30 o 9 13 3 306.71 301.41 21.12 o 0 14 3 562.04 514.09 19.56 o 2 14 3 16.28 20.47 4.73 o 4 14 3 171.93 191.95 16.38 o 6 14 3 97.66 87.16 7.88 o 8 14 3 160.64 164.12 12.40 o 1 15 3 664.09 680.23 24.27 o 3 15 3 401.53 407.91 20.26 o 5 15 3 93.00 89.76 7.87 o 7 15 3 22.20 31.45 5.79 o 0 16 3 3.43 10.44 4.69 o 2 16 3 12.86 22.82 5.41 o 4 16 3 17.95 25.15 5.48 o 1 17 3 654.94 653.99 25.31 o 3 17 3 459.66 388.20 22.34 o 0 18 3 97.52 112.30 10.75 o 2 0 4 77.12 137.41 7.10 o 4 0 4 113.52 221.32 9.23 o 6 0 4 2891.09 3397.84 38.02 o 8 0 4 2588.88 2556.47 38.36 o 10 0 4 149.48 88.49 8.01 o 12 0 4 44.65 22.32 4.41 o 1 1 4 525.78 488.41 10.94 o 3 1 4 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7 4 234.60 226.72 10.76 o 3 7 4 104.93 74.78 6.77 o 5 7 4 16.76 21.07 3.79 o 7 7 4 48.36 54.16 4.78 o 9 7 4 41.03 27.24 5.18 o 11 7 4 1.94 3.94 11.21 o 0 8 4 20.20 26.77 3.25 o 2 8 4 1346.85 1432.13 24.97 o 4 8 4 3265.44 3086.27 39.25 o 6 8 4 146.62 130.38 11.84 o 8 8 4 18.25 11.66 9.97 o 10 8 4 407.12 486.30 21.72 o 1 9 4 165.20 127.40 10.77 o 3 9 4 32.75 50.85 4.20 o 5 9 4 27.95 32.12 4.55 o 7 9 4 43.19 66.95 6.67 o 9 9 4 18.25 -1.75 11.72 o 0 10 4 96.76 115.16 10.67 o 2 10 4 2263.02 2170.48 33.62 o 4 10 4 2687.51 2561.61 39.15 o 6 10 4 444.16 414.72 18.80 o 8 10 4 26.72 37.23 5.55 o 10 10 4 310.31 432.06 21.68 o 1 11 4 976.21 953.49 23.40 o 3 11 4 125.55 106.43 8.76 o 5 11 4 599.22 617.54 23.03 o 7 11 4 90.07 63.38 5.85 o 9 11 4 110.97 78.23 7.54 o 0 12 4 460.17 418.70 17.21 o 2 12 4 1229.08 1227.74 28.60 o 4 12 4 1265.71 1134.60 29.07 o 6 12 4 351.78 268.37 18.46 o 8 12 4 198.37 283.73 18.81 o 1 13 4 265.95 206.37 15.46 o 3 13 4 44.76 77.73 6.74 o 5 13 4 255.48 228.35 17.66 o 7 13 4 105.22 92.61 9.01 o 0 14 4 1029.86 1024.26 27.48 o 2 14 4 99.92 85.03 7.24 o 4 14 4 67.56 79.96 6.70 o 6 14 4 275.32 307.55 21.25 o 1 15 4 53.05 56.33 5.48 o 3 15 4 12.90 14.92 13.20 o 5 15 4 70.64 57.17 6.42 o 0 16 4 255.74 212.19 18.35 o 2 16 4 150.44 192.35 16.19 o 4 16 4 54.98 57.23 6.34 o 1 17 4 11.35 7.46 12.11 o 1 1 5 167.04 215.27 8.83 o 3 1 5 559.68 536.76 14.48 o 5 1 5 2950.76 2802.77 34.85 o 7 1 5 1424.03 1745.99 31.46 o 9 1 5 33.18 44.04 4.40 o 11 1 5 35.24 19.44 4.96 o 0 2 5 1039.90 1064.66 17.27 o 2 2 5 806.96 761.99 16.28 o 4 2 5 867.39 942.66 19.74 o 6 2 5 372.59 347.03 14.28 o 8 2 5 523.69 697.09 21.95 o 10 2 5 14.99 16.45 4.29 o 1 3 5 2189.87 2286.64 26.52 o 3 3 5 1431.57 1214.42 21.86 o 5 3 5 2510.72 2436.78 33.41 o 7 3 5 1242.98 1310.62 27.75 o 9 3 5 338.63 359.31 17.15 o 11 3 5 222.22 264.38 18.41 o 0 4 5 1422.96 1368.50 20.44 o 2 4 5 1315.97 1240.11 21.29 o 4 4 5 856.87 851.68 19.91 o 6 4 5 319.25 273.61 13.75 o 8 4 5 648.58 683.21 21.57 o 10 4 5 52.37 15.93 5.13 o 1 5 5 5365.07 5173.02 41.93 o 3 5 5 2683.15 2820.20 34.13 o 5 5 5 252.52 253.69 13.65 o 7 5 5 628.45 592.85 20.75 o 9 5 5 875.39 911.69 27.66 o 11 5 5 261.01 235.66 19.92 o 0 6 5 1724.49 1590.70 24.06 o 2 6 5 1433.27 1315.62 24.08 o 4 6 5 1305.94 1364.32 26.14 o 6 6 5 472.08 447.52 18.35 o 8 6 5 359.36 446.01 19.70 o 10 6 5 111.10 124.47 10.99 o 1 7 5 3610.55 3375.84 37.06 o 3 7 5 795.57 786.47 21.11 o 5 7 5 10.39 22.24 4.30 o 9 7 5 709.20 696.94 26.09 o 0 8 5 152.24 116.22 10.27 o 2 8 5 313.95 325.29 13.99 o 4 8 5 18.24 26.74 4.28 o 6 8 5 53.57 53.47 5.16 o 8 8 5 30.28 23.02 5.59 o 1 9 5 3514.66 3467.89 41.12 o 3 9 5 1286.32 1378.18 28.66 o 5 9 5 9.47 22.09 4.38 o 7 9 5 192.39 114.05 8.82 o 9 9 5 682.96 793.43 29.64 o 0 10 5 13.40 -0.37 8.46 o 2 10 5 36.22 54.66 5.36 o 4 10 5 76.68 84.12 7.25 o 6 10 5 41.89 52.21 5.47 o 8 10 5 24.56 23.73 5.99 o 1 11 5 942.17 980.86 24.93 o 3 11 5 790.81 852.24 25.74 o 5 11 5 642.09 594.09 23.38 o 7 11 5 247.95 177.60 12.74 o 0 12 5 424.17 458.93 18.41 o 2 12 5 48.45 47.36 4.95 o 4 12 5 337.52 371.07 19.85 o 6 12 5 31.72 22.38 5.56 o 1 13 5 339.09 274.65 17.45 o 3 13 5 383.46 349.83 18.90 o 5 13 5 355.12 323.42 21.17 o 0 14 5 25.81 25.62 4.91 o 2 14 5 77.40 101.38 7.58 o 4 14 5 56.33 59.65 6.51 o 1 15 5 24.55 22.19 5.55 o 3 15 5 92.74 92.66 7.49 o 0 16 5 10.41 12.51 11.41 o 2 16 5 55.14 59.07 6.13 o 0 0 6 300.56 202.71 9.67 o 2 0 6 3049.33 3383.99 36.50 o 4 0 6 2710.35 2747.38 36.33 o 6 0 6 1.05 19.47 3.41 o 8 0 6 5.08 11.04 8.49 o 10 0 6 781.17 877.75 29.87 o 1 1 6 533.65 530.57 14.47 o 3 1 6 42.25 43.97 3.95 o 5 1 6 186.86 203.49 12.03 o 7 1 6 18.84 6.85 7.83 o 9 1 6 8.13 15.16 4.27 o 0 2 6 1481.33 1507.60 22.94 o 2 2 6 5862.89 6196.75 49.45 o 4 2 6 1326.84 1315.56 25.91 o 6 2 6 41.39 10.63 7.92 o 8 2 6 156.81 229.32 15.17 o 10 2 6 587.86 704.28 26.41 o 1 3 6 627.42 644.21 16.58 o 3 3 6 193.52 147.22 11.27 o 5 3 6 900.98 885.32 22.99 o 7 3 6 140.73 113.31 8.25 o 9 3 6 214.08 232.32 15.90 o 0 4 6 3391.15 3299.18 34.55 o 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458.26 378.55 23.56 o 1 13 6 212.67 201.12 15.99 o 3 13 6 15.84 42.44 5.86 o 0 14 6 42.82 56.21 5.87 o 2 14 6 129.59 108.45 10.72 o 1 15 6 7.97 5.94 6.90 o 1 1 7 5648.05 5535.05 49.92 o 3 1 7 1020.86 1187.93 25.87 o 5 1 7 34.82 41.84 4.06 o 7 1 7 184.35 142.18 12.97 o 0 2 7 27.55 16.18 3.23 o 2 2 7 408.52 363.26 14.50 o 4 2 7 213.30 230.57 13.60 o 6 2 7 18.13 -2.06 8.92 o 8 2 7 22.19 29.81 4.90 o 1 3 7 3088.94 2964.86 37.39 o 3 3 7 858.39 947.58 23.41 o 5 3 7 70.20 116.43 11.13 o 7 3 7 184.01 194.60 14.74 o 0 4 7 420.75 449.18 16.14 o 2 4 7 643.65 568.52 18.45 o 4 4 7 285.71 324.60 16.39 o 6 4 7 199.38 185.01 13.79 o 1 5 7 585.47 606.67 18.90 o 3 5 7 582.03 629.94 19.88 o 5 5 7 519.41 458.19 19.99 o 7 5 7 309.73 353.19 19.26 o 0 6 7 2.59 8.86 7.38 o 2 6 7 80.28 95.56 8.12 o 4 6 7 0.94 9.10 4.29 o 6 6 7 88.87 41.01 5.58 o 1 7 7 37.88 50.46 4.79 o 3 7 7 440.37 305.15 17.32 o 5 7 7 1397.48 1374.18 33.78 o 0 8 7 34.61 24.41 4.16 o 2 8 7 39.39 41.14 4.64 o 4 8 7 7.66 7.39 11.76 o 6 8 7 1.65 14.66 12.51 o 1 9 7 47.30 34.31 4.83 o 3 9 7 371.23 342.22 18.96 o 5 9 7 904.40 871.63 30.34 o 0 10 7 599.12 586.57 21.10 o 2 10 7 31.93 19.47 5.09 o 4 10 7 48.37 78.66 7.75 o 1 11 7 1.35 -5.37 10.96 o 3 11 7 244.20 195.90 17.40 o 0 12 7 38.23 38.78 5.29 o 2 12 7 97.84 122.80 10.63 o 1 13 7 257.53 242.66 17.49 o 0 14 7 16.38 9.93 5.66 o 0 0 8 1798.26 1827.15 30.99 o 2 0 8 30.31 10.75 3.50 o 4 0 8 175.21 210.14 15.23 o 6 0 8 875.32 974.83 29.78 o 1 1 8 244.10 203.44 13.04 o 3 1 8 11.00 0.77 7.85 o 5 1 8 60.75 60.24 5.50 o 0 2 8 1630.30 1495.57 28.91 o 2 2 8 257.84 263.37 14.75 o 4 2 8 97.57 99.42 8.43 o 6 2 8 558.83 539.45 22.51 o 1 3 8 878.65 939.50 23.50 o 3 3 8 29.87 49.06 4.90 o 5 3 8 227.63 222.07 16.49 o 0 4 8 442.83 445.14 17.55 o 2 4 8 375.50 311.37 16.00 o 4 4 8 345.74 295.16 17.37 o 1 5 8 412.72 471.20 17.91 o 3 5 8 37.86 48.09 4.94 o 5 5 8 361.92 369.44 20.56 o 0 6 8 263.20 215.64 14.30 o 2 6 8 924.55 933.28 26.03 o 4 6 8 515.96 525.31 22.57 o 1 7 8 125.39 136.53 12.67 o 3 7 8 47.16 52.25 5.56 o 0 8 8 166.69 180.10 14.59 o 2 8 8 1189.55 1219.82 31.43 o 4 8 8 661.82 535.96 24.57 o 1 9 8 1.84 6.17 7.73 o 3 9 8 0.34 5.44 11.73 o 0 10 8 198.72 201.05 15.85 o 2 10 8 490.17 423.16 22.28 o 1 11 8 138.96 122.41 10.72 o 0 12 8 183.92 197.47 17.76 o 1 1 9 28.99 28.68 3.89 o 3 1 9 550.43 466.50 21.24 o 0 2 9 174.32 192.74 12.98 o 2 2 9 119.18 115.22 8.51 o 4 2 9 43.41 66.29 6.25 o 1 3 9 80.72 97.73 8.06 o 3 3 9 335.12 274.55 17.81 o 0 4 9 51.62 38.05 4.48 o 2 4 9 276.69 182.78 15.15 o 1 5 9 676.99 662.61 23.21 o 3 5 9 170.69 188.66 16.24 o 0 6 9 79.69 98.86 8.92 o 2 6 9 195.77 125.57 11.31 o 1 7 9 1036.87 934.57 29.31 o 0 8 9 0.76 5.13 10.33 o 1 9 9 910.47 916.32 29.66 o 0 10 9 2.11 12.29 11.99 o 0 0 10 343.02 354.24 18.66 o 1 1 10 33.28 27.16 4.93 o 0 2 10 335.16 337.25 18.46 o 1 3 10 186.42 157.96 15.31 o 0 4 10 232.98 267.78 16.06 o 0 6 10 488.46 408.66 21.56 o