#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/07/2200716.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200716_Fobs loop_ _publ_author_name 'Sridhar, B.' 'Srinivasan, N.' 'Rajaram, R. K.' _publ_section_title ; Bis(\b-alanine) hydrogen nitrate ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1004 _journal_page_last o1006 _journal_volume 57 _journal_year 2001 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 113.923 _cell_angle_gamma 90.000 _cell_length_a 19.7910 _cell_length_b 5.3220 _cell_length_c 10.9740 _exptl_crystal_F_000 512.00 _reflns_d_resolution_high 0.8418 _[local]_cod_data_source_file ob6076Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' BETA ALANINE NITRATE' _shelx_refln_list_code 4 _shelx_f_calc_maximum 131.08 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 700.26 670.29 3.37 o 6 0 0 5713.35 5272.81 17.92 o 8 0 0 1107.53 1101.00 8.44 o 10 0 0 783.66 719.60 6.70 o 12 0 0 449.20 442.30 4.41 o 14 0 0 347.26 343.33 3.81 o 16 0 0 45.29 42.86 1.73 o 18 0 0 33.31 34.62 1.75 o 20 0 0 173.90 188.22 4.00 o 1 1 0 533.70 584.47 4.26 o 3 1 0 3409.73 3680.43 12.80 o 5 1 0 3108.70 3113.96 13.09 o 7 1 0 375.43 350.26 3.62 o 9 1 0 470.47 493.04 4.86 o 11 1 0 747.98 715.42 7.20 o 13 1 0 46.28 42.06 1.44 o 15 1 0 60.33 58.61 1.87 o 17 1 0 107.27 102.16 2.54 o 19 1 0 12.64 16.02 1.54 o 21 1 0 65.58 70.03 2.74 o 2 2 0 1226.04 1370.12 9.17 o 4 2 0 181.63 177.26 1.98 o 6 2 0 8.29 6.24 0.73 o 8 2 0 204.97 181.75 2.25 o 10 2 0 643.35 628.16 6.26 o 12 2 0 124.31 116.74 2.33 o 14 2 0 155.62 155.53 2.82 o 16 2 0 87.95 87.45 2.33 o 18 2 0 0.24 -1.94 2.06 o 20 2 0 28.52 31.26 2.04 o 1 3 0 906.79 834.42 7.36 o 3 3 0 850.35 935.12 9.31 o 5 3 0 103.15 107.42 1.96 o 7 3 0 1026.67 1024.48 9.41 o 9 3 0 159.81 157.06 2.65 o 11 3 0 1129.85 1105.80 10.68 o 13 3 0 30.79 37.45 1.67 o 15 3 0 102.95 110.04 2.79 o 17 3 0 2.67 0.86 2.21 o 0 4 0 65.34 83.30 2.03 o 2 4 0 1.54 3.13 1.71 o 4 4 0 523.56 513.85 5.14 o 6 4 0 50.36 49.36 1.91 o 8 4 0 0.11 2.79 2.08 o 10 4 0 205.05 193.78 3.54 o 12 4 0 16.11 20.42 1.71 o 14 4 0 78.79 75.90 2.67 o 16 4 0 18.94 23.67 1.93 o 1 5 0 8.50 6.31 1.22 o 3 5 0 7.48 3.15 2.25 o 5 5 0 2.52 0.63 2.36 o 7 5 0 0.46 3.03 2.11 o 9 5 0 1.95 0.36 2.81 o 11 5 0 547.12 572.08 7.16 o 13 5 0 19.25 22.52 2.18 o 0 6 0 39.59 36.22 2.23 o 2 6 0 162.19 160.63 3.85 o 4 6 0 13.21 13.10 1.78 o 6 6 0 34.91 33.70 2.34 o -21 1 1 56.67 50.14 2.39 o -19 1 1 84.53 93.34 2.56 o -17 1 1 1.04 -0.14 1.77 o -15 1 1 174.92 175.92 2.87 o -13 1 1 1226.67 1169.65 11.46 o -11 1 1 297.07 286.55 2.81 o -9 1 1 1359.15 1374.15 10.11 o -7 1 1 148.15 137.35 1.61 o -5 1 1 10804.52 9731.93 93.95 o -3 1 1 14375.74 13383.40 106.10 o 3 1 1 117.78 93.79 1.22 o 5 1 1 615.00 632.60 5.96 o 7 1 1 5388.63 5858.31 22.23 o 9 1 1 58.64 55.38 1.32 o 11 1 1 358.60 322.51 3.25 o 13 1 1 87.05 89.30 2.12 o 15 1 1 267.51 241.78 3.59 o 17 1 1 48.17 42.02 1.84 o 19 1 1 126.08 125.08 3.29 o -20 2 1 3.09 5.69 1.29 o -18 2 1 9.92 9.86 1.34 o -16 2 1 1.21 1.22 1.89 o -14 2 1 65.57 57.74 1.86 o -12 2 1 127.20 137.58 2.26 o -10 2 1 576.02 542.99 5.61 o -8 2 1 490.47 518.41 5.08 o -6 2 1 50.44 79.42 1.47 o -4 2 1 4290.77 3907.80 16.98 o -2 2 1 104.60 97.10 1.36 o 0 2 1 3.02 0.39 0.77 o 4 2 1 1689.38 1856.39 11.88 o 6 2 1 171.49 168.79 2.08 o 8 2 1 1128.75 1157.84 10.56 o 10 2 1 31.31 30.94 1.29 o 12 2 1 128.99 129.68 2.48 o 14 2 1 43.82 39.96 1.67 o 16 2 1 183.63 186.05 3.41 o 18 2 1 0.62 2.92 2.19 o -19 3 1 0.13 -0.55 1.92 o -17 3 1 76.57 74.62 2.62 o -15 3 1 1133.47 1166.95 12.20 o -13 3 1 28.72 24.33 1.52 o -11 3 1 6.95 10.05 1.22 o -9 3 1 312.34 317.52 3.42 o -7 3 1 35.09 32.67 1.31 o -5 3 1 413.41 408.30 4.16 o -3 3 1 1399.20 1426.09 11.23 o -1 3 1 1481.58 1406.16 11.01 o 1 3 1 311.74 311.31 3.12 o 3 3 1 66.30 97.30 1.81 o 5 3 1 784.46 737.28 6.97 o 7 3 1 1.11 0.83 1.58 o 9 3 1 771.86 748.49 7.63 o 11 3 1 42.36 38.30 1.68 o 13 3 1 80.91 91.44 2.43 o 15 3 1 1.70 1.59 2.05 o 17 3 1 0.40 3.95 2.27 o -16 4 1 183.71 198.79 4.15 o -14 4 1 113.91 96.78 2.98 o -12 4 1 138.67 151.51 3.16 o -10 4 1 884.79 957.05 9.98 o -8 4 1 42.03 43.48 1.86 o -6 4 1 43.67 53.61 1.89 o -4 4 1 22.79 30.12 1.52 o -2 4 1 66.54 78.97 1.97 o 0 4 1 240.61 229.25 6.44 o 2 4 1 142.81 153.43 2.70 o 4 4 1 668.40 666.07 6.39 o 6 4 1 1184.14 1214.23 11.88 o 8 4 1 598.88 604.18 6.22 o 10 4 1 656.02 668.42 6.77 o 12 4 1 484.53 492.99 5.71 o 14 4 1 1.35 1.08 2.25 o -13 5 1 8.72 9.70 1.94 o -11 5 1 56.01 69.89 2.90 o -9 5 1 4.66 0.70 2.39 o -7 5 1 74.90 75.33 2.46 o -5 5 1 277.10 269.94 4.07 o -3 5 1 126.55 139.47 2.99 o -1 5 1 147.35 134.13 2.94 o 1 5 1 197.13 192.16 3.52 o 3 5 1 63.39 64.50 2.27 o 5 5 1 148.87 132.60 3.18 o 7 5 1 73.04 79.41 2.61 o 9 5 1 117.61 127.30 3.49 o 11 5 1 17.39 23.55 1.98 o -6 6 1 13.39 9.15 1.95 o -4 6 1 145.83 153.92 3.88 o -2 6 1 18.38 13.10 1.83 o 0 6 1 0.50 -1.39 1.89 o 2 6 1 0.19 0.58 2.60 o 4 6 1 47.27 48.81 2.60 o -22 0 2 32.41 30.93 1.99 o -20 0 2 9.84 11.51 1.35 o -18 0 2 20.72 15.32 1.39 o -16 0 2 1072.62 1048.10 10.38 o -14 0 2 1678.08 1548.06 13.41 o -12 0 2 12.57 13.41 0.92 o -10 0 2 2833.63 2487.89 14.20 o -8 0 2 722.83 751.90 6.67 o -4 0 2 1518.60 1413.67 7.39 o 2 0 2 26.40 14.96 0.71 o 4 0 2 9064.50 9729.41 84.36 o 6 0 2 1096.36 1213.60 9.02 o 8 0 2 178.25 183.28 2.18 o 10 0 2 529.69 491.10 4.99 o 12 0 2 4.34 5.29 0.93 o 14 0 2 12.06 14.72 1.25 o 16 0 2 1575.25 1530.77 14.24 o 18 0 2 43.37 41.43 2.27 o -21 1 2 1.39 2.95 1.98 o -19 1 2 9.12 8.41 1.27 o -17 1 2 93.37 94.55 2.31 o -15 1 2 29.57 30.75 1.40 o -13 1 2 0.55 1.40 1.51 o -11 1 2 602.36 609.00 6.31 o -9 1 2 1615.17 1556.11 10.78 o -7 1 2 1618.82 1646.24 10.12 o -5 1 2 3503.56 3550.98 14.59 o -3 1 2 7652.50 7268.15 64.55 o -1 1 2 2065.87 2168.05 9.51 o 1 1 2 1017.16 1146.78 7.34 o 7 1 2 859.55 934.47 8.73 o 9 1 2 12.87 9.65 0.86 o 11 1 2 867.82 863.03 8.75 o 13 1 2 13.39 13.48 1.18 o 15 1 2 185.32 186.63 3.33 o 17 1 2 26.37 29.08 1.85 o 19 1 2 166.18 187.61 4.13 o -20 2 2 192.06 191.45 3.91 o -18 2 2 249.64 262.21 3.99 o -16 2 2 8.08 8.77 1.11 o -14 2 2 900.74 817.41 7.96 o -12 2 2 91.03 72.62 1.72 o -10 2 2 8.82 11.43 0.92 o -8 2 2 109.19 120.90 1.78 o -6 2 2 112.28 110.89 1.62 o -4 2 2 3190.99 3168.56 14.73 o -2 2 2 1173.70 1159.24 8.34 o 0 2 2 2692.40 2772.86 29.80 o 2 2 2 18.16 18.41 0.89 o 4 2 2 704.77 673.33 6.37 o 6 2 2 114.68 114.34 1.83 o 8 2 2 1900.75 1943.36 14.49 o 10 2 2 15.27 12.49 1.09 o 12 2 2 13.03 15.17 1.19 o 14 2 2 7.84 7.11 1.17 o 16 2 2 65.97 67.15 2.27 o 18 2 2 15.99 18.09 1.79 o -19 3 2 0.40 1.76 1.92 o -17 3 2 137.81 124.11 2.96 o -15 3 2 57.91 58.90 2.05 o -13 3 2 42.94 42.99 1.76 o -11 3 2 50.71 49.13 1.81 o -9 3 2 467.06 541.10 5.40 o -7 3 2 25.25 31.89 1.27 o -5 3 2 149.34 138.49 2.06 o -3 3 2 3298.57 3365.44 17.94 o -1 3 2 14.72 13.44 0.94 o 1 3 2 821.07 843.73 7.88 o 3 3 2 10.06 9.14 0.89 o 5 3 2 1009.11 1015.26 9.51 o 7 3 2 30.07 36.37 1.52 o 9 3 2 158.43 157.67 2.83 o 11 3 2 20.36 16.18 1.36 o 13 3 2 0.09 -0.30 1.67 o 15 3 2 0.00 0.00 2.02 o 17 3 2 26.40 37.13 2.09 o -16 4 2 16.90 16.20 1.88 o -14 4 2 22.58 19.95 1.68 o -12 4 2 5.01 2.96 2.50 o -10 4 2 46.51 42.10 1.94 o -8 4 2 0.11 -0.13 2.15 o -6 4 2 120.10 139.23 2.68 o -4 4 2 15.54 15.53 1.23 o -2 4 2 328.55 333.16 3.76 o 0 4 2 9.47 4.51 1.95 o 2 4 2 40.51 40.91 1.66 o 4 4 2 74.74 68.85 2.11 o 6 4 2 0.38 -1.97 2.28 o 8 4 2 352.77 323.87 4.40 o 10 4 2 116.79 128.19 3.07 o 12 4 2 108.41 112.32 3.11 o 14 4 2 42.30 40.89 2.34 o -13 5 2 53.20 62.99 2.87 o -11 5 2 17.95 22.18 2.02 o -9 5 2 0.30 1.87 2.24 o -7 5 2 24.93 27.75 1.68 o -5 5 2 21.00 21.36 1.65 o -3 5 2 405.23 387.68 4.74 o -1 5 2 6.18 5.25 1.24 o 1 5 2 152.87 160.03 3.21 o 3 5 2 175.58 163.30 3.39 o 5 5 2 665.85 656.42 6.76 o 7 5 2 2.72 0.00 2.81 o 9 5 2 0.10 3.64 2.21 o 11 5 2 7.33 -1.01 2.83 o -6 6 2 27.19 25.69 1.94 o -4 6 2 77.21 88.20 3.04 o -2 6 2 0.11 -2.34 2.34 o 0 6 2 33.65 35.63 1.52 o 2 6 2 27.66 22.44 1.96 o 4 6 2 8.33 11.22 1.77 o -21 1 3 2.45 2.19 2.23 o -19 1 3 565.37 542.80 5.56 o -17 1 3 64.70 52.50 1.77 o -15 1 3 8.79 7.34 1.09 o -13 1 3 374.62 338.39 3.47 o -11 1 3 0.43 -0.24 1.35 o -9 1 3 733.25 754.05 6.56 o -7 1 3 6294.05 5953.67 22.12 o -5 1 3 206.74 243.66 2.47 o -3 1 3 382.64 369.28 3.68 o -1 1 3 2593.01 2456.46 11.49 o 3 1 3 3695.38 4001.59 17.22 o 5 1 3 86.46 95.25 1.58 o 7 1 3 314.77 322.64 3.18 o 9 1 3 392.60 434.42 4.29 o 11 1 3 160.42 149.52 2.68 o 13 1 3 54.77 56.61 1.89 o 15 1 3 71.95 72.39 2.32 o 17 1 3 164.24 167.09 3.72 o -20 2 3 13.00 17.77 1.60 o -18 2 3 0.68 0.74 1.64 o -16 2 3 43.87 35.80 1.62 o -14 2 3 14.94 13.15 1.20 o -12 2 3 827.33 861.68 8.44 o -10 2 3 2720.66 2664.04 16.65 o -8 2 3 191.30 202.66 2.45 o -6 2 3 103.32 119.59 1.76 o -4 2 3 259.22 258.49 2.63 o -2 2 3 339.07 405.89 4.00 o 0 2 3 2046.75 2097.98 38.83 o 2 2 3 4133.31 4549.76 20.41 o 4 2 3 23.59 23.85 1.06 o 6 2 3 211.10 195.92 2.51 o 8 2 3 744.88 698.63 7.05 o 10 2 3 232.54 222.08 3.24 o 12 2 3 9.02 6.57 1.04 o 14 2 3 384.53 372.36 4.77 o 16 2 3 125.73 120.06 3.20 o -19 3 3 10.92 11.05 1.63 o -17 3 3 0.28 0.00 1.81 o -15 3 3 52.97 67.28 2.12 o -13 3 3 7.80 12.31 1.30 o -11 3 3 400.27 420.44 4.22 o -9 3 3 590.51 547.75 5.54 o -7 3 3 220.85 222.64 2.66 o -5 3 3 82.21 92.26 1.75 o -3 3 3 185.69 212.56 2.48 o -1 3 3 1.42 3.96 0.77 o 1 3 3 602.39 578.26 5.57 o 3 3 3 815.59 768.16 7.41 o 5 3 3 365.28 392.28 3.87 o 7 3 3 203.24 198.40 3.07 o 9 3 3 182.63 165.82 2.98 o 11 3 3 21.93 23.47 1.47 o 13 3 3 29.04 23.10 1.68 o 15 3 3 11.06 11.42 1.55 o -18 4 3 139.02 153.74 3.82 o -16 4 3 183.68 198.14 4.09 o -14 4 3 1.44 2.44 2.37 o -12 4 3 174.57 206.76 3.72 o -10 4 3 73.36 83.45 2.39 o -8 4 3 689.66 664.70 6.39 o -6 4 3 291.31 312.10 3.81 o -4 4 3 26.19 24.92 1.51 o -2 4 3 31.84 25.32 1.36 o 0 4 3 897.34 848.91 12.43 o 2 4 3 215.64 243.55 3.59 o 4 4 3 1307.79 1251.95 12.25 o 6 4 3 602.06 579.96 5.71 o 8 4 3 1.93 -0.94 2.17 o 10 4 3 195.42 196.99 3.77 o 12 4 3 222.69 241.91 4.61 o -13 5 3 9.03 10.33 1.87 o -11 5 3 84.14 94.85 2.98 o -9 5 3 15.72 17.15 1.63 o -7 5 3 58.17 61.19 2.23 o -5 5 3 146.93 141.63 3.06 o -3 5 3 177.67 201.64 3.53 o -1 5 3 237.08 218.58 3.64 o 1 5 3 173.70 176.24 3.51 o 3 5 3 14.82 15.58 1.55 o 5 5 3 130.23 134.69 3.50 o 7 5 3 37.84 40.22 2.26 o 9 5 3 89.53 96.65 3.27 o -6 6 3 23.78 29.05 2.11 o -4 6 3 0.34 -1.70 2.52 o -2 6 3 171.84 177.94 4.12 o 0 6 3 4.76 6.70 1.06 o 2 6 3 4.59 4.33 2.93 o -22 0 4 327.78 315.70 5.08 o -20 0 4 29.44 76.60 2.35 o -18 0 4 183.52 186.21 3.23 o -16 0 4 0.23 1.43 1.72 o -14 0 4 31.81 35.61 1.37 o -12 0 4 6784.16 6501.03 27.76 o -10 0 4 944.72 1044.67 9.45 o -8 0 4 1015.45 1007.11 8.60 o -6 0 4 17181.91 18171.81 160.58 o -4 0 4 66.79 79.36 1.28 o -2 0 4 699.61 651.90 6.06 o 0 0 4 4677.26 4883.75 40.12 o 2 0 4 481.86 442.37 4.24 o 6 0 4 469.20 458.72 4.69 o 8 0 4 103.54 89.49 1.87 o 10 0 4 2584.99 2569.09 18.75 o 12 0 4 0.08 1.88 1.84 o 14 0 4 18.56 17.00 1.51 o 16 0 4 417.78 436.28 5.90 o -23 1 4 0.02 -2.10 2.52 o -21 1 4 1.36 1.95 1.24 o -19 1 4 11.26 13.52 1.30 o -17 1 4 4.21 3.77 1.12 o -15 1 4 396.48 401.55 4.15 o -13 1 4 559.40 610.00 5.79 o -11 1 4 889.91 805.43 7.62 o -9 1 4 1031.18 1028.96 9.29 o -7 1 4 804.02 802.96 7.72 o -5 1 4 3498.97 3519.85 15.82 o -3 1 4 1588.79 1744.59 10.36 o 3 1 4 105.27 116.12 1.74 o 5 1 4 2299.70 2431.68 15.54 o 7 1 4 67.10 62.22 1.57 o 9 1 4 316.34 344.96 3.84 o 11 1 4 9.30 6.38 1.19 o 13 1 4 498.50 491.94 5.31 o 15 1 4 86.47 96.27 2.90 o 17 1 4 27.09 27.47 2.04 o -22 2 4 0.42 2.45 2.13 o -20 2 4 114.05 96.61 2.94 o -18 2 4 37.28 31.16 1.75 o -16 2 4 157.31 154.20 2.87 o -14 2 4 67.67 73.51 2.02 o -12 2 4 25.21 32.87 1.41 o -10 2 4 66.66 66.98 1.67 o -8 2 4 521.81 562.79 5.59 o -6 2 4 83.16 99.80 1.68 o -4 2 4 176.26 153.63 1.96 o -2 2 4 663.20 685.46 6.29 o 0 2 4 40.71 38.31 1.01 o 4 2 4 934.60 914.24 8.45 o 6 2 4 52.96 49.01 1.49 o 8 2 4 138.20 122.07 2.44 o 10 2 4 57.69 58.41 1.96 o 12 2 4 19.82 14.21 1.35 o 14 2 4 72.35 71.59 2.51 o 16 2 4 9.01 11.21 1.60 o -19 3 4 47.63 50.85 2.42 o -17 3 4 251.81 246.49 4.01 o -15 3 4 22.28 19.67 1.54 o -13 3 4 0.82 2.50 2.15 o -11 3 4 87.03 87.18 2.30 o -9 3 4 596.83 636.09 6.13 o -7 3 4 971.02 899.19 8.59 o -5 3 4 673.66 667.64 6.39 o -3 3 4 116.04 113.29 1.96 o -1 3 4 205.99 200.20 2.51 o 1 3 4 110.09 96.83 1.98 o 3 3 4 28.81 29.17 1.44 o 5 3 4 217.05 233.07 3.30 o 7 3 4 34.09 25.87 1.48 o 9 3 4 16.19 17.41 1.37 o 11 3 4 0.23 2.21 1.82 o 13 3 4 360.11 343.96 5.23 o -18 4 4 1.78 2.27 2.49 o -16 4 4 26.55 25.64 1.98 o -14 4 4 7.13 5.24 1.42 o -12 4 4 2.58 2.46 2.13 o -10 4 4 11.95 7.52 1.28 o -8 4 4 122.72 114.87 2.59 o -6 4 4 169.55 158.84 2.93 o -4 4 4 293.33 286.26 3.68 o -2 4 4 112.48 116.03 2.46 o 0 4 4 78.75 78.27 1.54 o 2 4 4 310.57 295.80 4.08 o 4 4 4 11.43 11.35 1.33 o 6 4 4 161.51 158.47 3.30 o 8 4 4 1.00 1.34 2.06 o 10 4 4 5.22 2.94 2.36 o 12 4 4 36.19 44.14 2.38 o -13 5 4 6.17 9.88 1.74 o -11 5 4 138.00 120.60 3.30 o -9 5 4 103.05 110.09 3.06 o -7 5 4 177.18 190.52 3.61 o -5 5 4 83.21 74.90 2.36 o -3 5 4 51.36 43.24 1.97 o -1 5 4 442.59 458.11 5.23 o 1 5 4 80.81 70.30 2.53 o 3 5 4 55.13 63.06 2.64 o 5 5 4 163.39 154.73 3.85 o 7 5 4 133.67 141.99 3.72 o -4 6 4 16.58 15.91 1.90 o -2 6 4 7.60 8.86 1.61 o -23 1 5 14.86 10.99 1.68 o -21 1 5 9.72 6.93 1.48 o -19 1 5 4.45 1.95 2.11 o -17 1 5 3.21 3.32 2.13 o -15 1 5 1050.87 1050.46 10.30 o -13 1 5 1368.77 1383.63 12.85 o -11 1 5 1536.30 1557.92 12.88 o -9 1 5 123.62 145.80 2.09 o -7 1 5 41.88 39.57 1.18 o -5 1 5 112.66 113.85 1.69 o -3 1 5 1597.04 1639.83 11.11 o -1 1 5 489.72 449.50 4.53 o 1 1 5 2.48 1.10 1.17 o 3 1 5 788.79 858.11 7.91 o 5 1 5 203.92 197.65 2.62 o 7 1 5 642.10 637.73 6.37 o 9 1 5 983.06 998.61 10.47 o 11 1 5 252.77 247.74 3.72 o 13 1 5 130.09 133.12 3.04 o 15 1 5 160.89 156.02 3.70 o -22 2 5 56.36 60.96 2.59 o -20 2 5 11.10 13.02 1.58 o -18 2 5 61.85 57.63 2.09 o -16 2 5 446.19 448.88 4.87 o -14 2 5 57.82 48.90 1.88 o -12 2 5 5.88 3.74 1.18 o -10 2 5 522.29 516.80 5.09 o -8 2 5 570.15 544.56 5.71 o -6 2 5 2943.79 2904.44 16.90 o -4 2 5 604.95 625.89 6.44 o -2 2 5 31.84 25.19 1.03 o 0 2 5 312.47 321.46 2.66 o 2 2 5 907.56 877.44 8.51 o 4 2 5 105.46 99.94 2.03 o 6 2 5 65.78 78.21 2.04 o 8 2 5 358.49 330.02 4.08 o 10 2 5 93.71 73.00 2.19 o 12 2 5 3.23 3.26 1.17 o 14 2 5 63.43 63.51 2.56 o -19 3 5 1.80 3.17 2.02 o -17 3 5 21.42 26.22 1.71 o -15 3 5 48.68 58.66 2.18 o -13 3 5 8.74 12.74 1.53 o -11 3 5 24.08 12.85 1.40 o -9 3 5 25.48 28.22 1.49 o -7 3 5 30.36 24.55 1.39 o -5 3 5 282.91 279.60 3.15 o -3 3 5 56.72 59.77 1.64 o -1 3 5 0.65 3.09 0.85 o 1 3 5 305.10 287.80 3.58 o 3 3 5 20.64 27.71 1.45 o 5 3 5 820.55 829.10 8.71 o 7 3 5 52.75 54.03 1.92 o 9 3 5 3.69 9.49 1.29 o 11 3 5 51.46 56.08 2.37 o 13 3 5 37.12 30.56 2.03 o -18 4 5 0.11 1.37 2.49 o -16 4 5 179.83 216.91 4.53 o -14 4 5 90.27 74.89 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