#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/07/2200719.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200719_Fobs loop_ _publ_author_name 'Rosair, Georgina M.' 'Schmidt, Falk H.' 'Welch, Alan J.' _publ_section_title ; Tetraphenylphosphonium 7-phenylethynyl-8-phenyl-7,8-nido-dicarbadecahydroundecaborate(1--) ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1168 _journal_page_last o1170 _journal_volume 57 _journal_year 2001 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 71.469 _cell_angle_beta 83.522 _cell_angle_gamma 84.235 _cell_length_a 10.0629 _cell_length_b 19.0067 _cell_length_c 20.3441 _exptl_crystal_F_000 1360.00 _reflns_d_resolution_high 0.8428 _[local]_cod_data_source_file ob6079Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' fhs010 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 214.25 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 6.79 7.20 9.37 o 2 0 0 344.97 325.35 45.33 o 3 0 0 385.28 271.44 58.40 o 4 0 0 15.32 40.57 54.32 o 5 0 0 5038.34 5086.66 151.65 o 6 0 0 2886.23 3007.13 139.81 o 7 0 0 0.02 25.18 77.46 o 8 0 0 406.69 434.26 119.66 o 9 0 0 54.92 -118.30 118.30 o 10 0 0 177.26 92.57 124.83 o 11 0 0 53.03 244.22 137.90 o -11 1 0 6.92 27.77 137.08 o -10 1 0 10.68 -43.29 123.61 o -9 1 0 164.60 118.57 119.11 o -8 1 0 702.10 298.40 128.92 o -6 1 0 173.57 120.34 68.20 o -5 1 0 677.00 759.88 64.66 o -4 1 0 84.62 84.40 54.59 o -3 1 0 1115.84 1213.74 72.29 o -2 1 0 0.03 -22.46 47.10 o -1 1 0 19380.67 17897.22 876.27 o 1 1 0 804.69 783.93 33.25 o 2 1 0 13.69 41.25 44.51 o 3 1 0 1649.05 1744.65 125.24 o 4 1 0 1.12 63.30 52.82 o 5 1 0 587.92 673.85 65.07 o 6 1 0 421.08 498.10 70.79 o 7 1 0 443.03 516.62 82.22 o 8 1 0 102.62 177.11 119.80 o 9 1 0 333.26 390.42 128.64 o 10 1 0 60.72 46.15 125.24 o 11 1 0 162.75 94.34 144.71 o -11 2 0 0.75 -48.05 141.44 o -10 2 0 15.48 -129.32 129.32 o -9 2 0 463.35 414.11 122.52 o -8 2 0 512.09 648.39 125.24 o -7 2 0 64.52 31.17 77.73 o -6 2 0 279.23 284.92 71.33 o -5 2 0 367.10 422.01 62.35 o -4 2 0 3656.48 3868.02 144.84 o -3 2 0 3867.62 3742.23 140.35 o -2 2 0 25771.75 24743.12 246.94 o -1 2 0 1841.65 1658.81 106.05 o 0 2 0 10440.00 8455.57 218.83 o 1 2 0 6584.76 7006.33 84.36 o 2 2 0 1185.64 1273.78 65.75 o 3 2 0 11409.77 11031.76 196.16 o 4 2 0 3735.04 3591.81 138.58 o 5 2 0 1328.87 1265.88 79.09 o 6 2 0 46.42 29.68 70.38 o 7 2 0 56.89 66.02 80.45 o 8 2 0 45.67 -29.27 117.21 o 9 2 0 139.97 20.15 121.97 o 10 2 0 95.56 142.12 125.10 o 11 2 0 376.47 373.68 149.74 o -11 3 0 623.41 645.53 153.28 o -10 3 0 13.87 -95.70 124.02 o -9 3 0 353.60 378.44 123.47 o -8 3 0 609.08 640.50 123.06 o -7 3 0 276.96 263.69 78.55 o -6 3 0 6047.43 5602.19 168.80 o -5 3 0 288.88 236.60 64.80 o -4 3 0 996.00 931.00 60.85 o -3 3 0 3019.35 2412.24 132.46 o -2 3 0 652.88 593.12 62.21 o -1 3 0 2411.70 2283.92 183.30 o 0 3 0 24.36 56.36 34.71 o 1 3 0 182.60 166.17 28.95 o 2 3 0 17390.79 16772.26 220.26 o 3 3 0 2701.92 2938.65 137.08 o 4 3 0 1249.17 1146.77 70.65 o 5 3 0 92.20 243.13 60.99 o 6 3 0 1802.34 1778.41 127.01 o 7 3 0 54.08 135.45 79.50 o 8 3 0 78.22 41.79 117.89 o 9 3 0 28.55 86.85 114.35 o 10 3 0 190.02 209.51 129.32 o 11 3 0 173.21 154.10 142.39 o -11 4 0 89.41 127.96 144.84 o -10 4 0 201.94 202.02 127.69 o -9 4 0 228.02 134.09 122.93 o -8 4 0 293.70 477.27 121.70 o -7 4 0 171.01 83.58 115.98 o -6 4 0 5165.98 5099.46 160.09 o -5 4 0 90.96 173.43 63.16 o -4 4 0 0.90 -30.90 55.68 o -3 4 0 180.00 289.82 54.18 o -2 4 0 103.61 142.94 52.82 o -1 4 0 90.70 25.29 41.42 o 0 4 0 9142.39 9289.87 136.20 o 1 4 0 4268.95 4204.51 101.70 o 2 4 0 0.12 -66.43 66.43 o 3 4 0 338.86 406.35 60.44 o 4 4 0 449.15 534.72 60.71 o 5 4 0 156.22 142.39 64.53 o 7 4 0 24.44 70.79 78.14 o 8 4 0 4.74 155.05 120.20 o 9 4 0 664.97 718.50 126.47 o 10 4 0 0.19 104.14 126.74 o 11 4 0 1.50 39.89 141.71 o -10 5 0 408.24 341.96 141.17 o -9 5 0 12.57 230.33 115.98 o -8 5 0 781.14 790.38 123.33 o -7 5 0 244.81 620.21 117.07 o -6 5 0 977.74 1043.31 79.64 o -5 5 0 683.68 756.34 68.20 o -4 5 0 324.63 347.81 60.85 o -3 5 0 6490.23 7191.79 179.42 o -2 5 0 563.36 609.32 55.68 o -1 5 0 145.43 273.85 85.08 o 0 5 0 23.98 6.97 43.39 o 1 5 0 28.28 9.33 42.86 o 2 5 0 104.84 174.79 58.94 o 3 5 0 110.20 122.25 57.72 o 4 5 0 3225.16 3568.53 144.30 o 5 5 0 390.07 506.95 69.43 o 6 5 0 530.89 436.57 77.73 o 7 5 0 123.29 147.29 81.13 o 8 5 0 790.54 710.33 132.18 o 9 5 0 243.47 289.41 121.02 o 10 5 0 10.06 102.23 123.47 o 11 5 0 3.66 64.53 133.82 o -10 6 0 578.39 253.88 144.71 o -9 6 0 5.45 -19.74 124.83 o -8 6 0 2802.06 2281.82 144.03 o -7 6 0 168.61 145.12 119.66 o -6 6 0 23.54 67.66 73.37 o -5 6 0 1794.09 1818.71 128.37 o -4 6 0 294.57 255.52 62.08 o -3 6 0 352.13 282.34 60.17 o -2 6 0 2.21 -25.73 52.00 o -1 6 0 381.95 416.26 40.86 o 0 6 0 16931.42 16614.03 526.96 o 1 6 0 43.71 8.39 38.41 o 2 6 0 755.27 754.98 62.21 o 3 6 0 2.22 85.35 58.67 o 4 6 0 7725.60 8155.73 185.82 o 5 6 0 170.06 190.04 68.07 o 6 6 0 0.89 45.88 74.46 o 7 6 0 103.62 170.57 119.25 o 8 6 0 41.01 149.47 120.20 o 9 6 0 109.90 198.21 119.11 o 10 6 0 17.62 -107.54 130.41 o 11 6 0 27.06 65.48 142.80 o -10 7 0 8.98 11.57 133.54 o -9 7 0 262.94 251.57 124.97 o -8 7 0 28.75 318.00 107.68 o -7 7 0 49.63 -15.11 114.21 o -6 7 0 434.57 462.44 109.86 o -5 7 0 107.41 106.32 70.38 o -4 7 0 731.47 771.45 68.75 o -3 7 0 20.29 9.39 61.53 o -2 7 0 70.31 135.31 53.36 o -1 7 0 2737.90 2799.97 93.22 o 0 7 0 0.00 49.45 53.77 o 1 7 0 150.88 161.37 40.75 o 2 7 0 74.78 85.49 61.80 o 3 7 0 2014.78 1940.00 134.63 o 4 7 0 15.77 71.47 66.57 o 5 7 0 971.64 992.94 79.09 o 6 7 0 1231.31 1006.96 89.30 o 7 7 0 427.14 369.32 125.65 o 8 7 0 309.89 389.61 126.33 o 9 7 0 699.04 785.61 134.09 o 10 7 0 43.78 -39.48 135.04 o 11 7 0 4.65 200.25 140.49 o -10 8 0 294.17 523.42 131.77 o -9 8 0 91.48 -128.10 128.10 o -8 8 0 7.86 137.22 106.32 o -7 8 0 33.39 66.16 113.53 o -6 8 0 187.98 222.03 114.08 o -5 8 0 878.31 855.45 80.73 o -4 8 0 161.05 143.75 66.84 o -3 8 0 1734.59 1802.64 90.25 o -2 8 0 8.52 -50.37 55.81 o -1 8 0 1520.90 1585.97 59.03 o 0 8 0 122.10 80.76 40.94 o 1 8 0 394.36 374.30 43.47 o 2 8 0 48.98 40.84 63.71 o 3 8 0 5673.99 5735.19 177.24 o 4 8 0 629.05 548.47 76.23 o 5 8 0 200.55 231.83 75.28 o 6 8 0 347.52 222.57 83.58 o 7 8 0 58.62 -115.57 127.28 o 8 8 0 657.12 664.32 131.91 o 9 8 0 38.64 177.24 125.38 o 10 8 0 2.91 -121.56 137.08 o -9 9 0 374.16 584.55 130.14 o -8 9 0 34.40 71.60 114.62 o -7 9 0 54.25 158.59 109.99 o -6 9 0 876.08 969.93 123.88 o -5 9 0 125.91 137.08 73.24 o -4 9 0 628.90 506.00 74.19 o -3 9 0 1611.35 1649.22 84.81 o -2 9 0 1559.83 1427.60 79.77 o -1 9 0 1364.90 1401.21 55.99 o 0 9 0 52.89 66.40 43.38 o 1 9 0 9.65 24.67 44.97 o 2 9 0 658.35 501.78 73.92 o 3 9 0 88.75 -20.83 71.60 o 4 9 0 83.02 159.95 73.37 o 5 9 0 3.25 181.87 78.00 o 6 9 0 1174.94 1202.44 130.00 o 7 9 0 22.20 80.73 132.05 o 8 9 0 16.57 -17.56 121.84 o 9 9 0 211.07 229.92 131.91 o 10 9 0 50.84 -145.39 145.39 o -9 10 0 5.55 -63.03 128.24 o -8 10 0 30.51 -6.53 118.98 o -7 10 0 410.81 284.24 114.62 o -6 10 0 7.68 -118.16 118.16 o -5 10 0 2032.15 1852.47 131.91 o -4 10 0 740.27 709.65 77.32 o -3 10 0 41.26 -40.70 72.56 o -2 10 0 916.64 1113.28 70.92 o -1 10 0 4.64 -30.07 45.93 o 0 10 0 8.96 -15.46 44.46 o 1 10 0 384.78 373.58 49.55 o 2 10 0 567.95 633.28 77.19 o 3 10 0 825.34 850.54 81.54 o 4 10 0 9.61 -78.96 78.96 o 5 10 0 70.65 221.08 79.23 o 6 10 0 118.73 199.84 123.61 o 7 10 0 83.39 -62.21 130.69 o 8 10 0 879.29 648.94 137.49 o 9 10 0 465.97 649.21 136.13 o 10 10 0 47.47 113.40 143.62 o -9 11 0 11.25 77.46 127.01 o -8 11 0 534.04 618.85 133.54 o -7 11 0 396.45 310.92 121.56 o -6 11 0 330.61 267.77 117.75 o -5 11 0 831.83 867.29 124.02 o -4 11 0 5.13 75.28 105.37 o -3 11 0 1500.24 1568.23 90.80 o -2 11 0 1057.72 1028.74 79.23 o -1 11 0 2.49 36.41 49.21 o 0 11 0 65.04 84.97 48.68 o 1 11 0 0.12 -16.46 48.02 o 2 11 0 156.31 196.71 78.55 o 3 11 0 0.03 22.19 80.32 o 4 11 0 102.73 63.16 85.76 o 5 11 0 491.06 509.27 121.56 o 6 11 0 941.02 986.68 140.76 o 7 11 0 400.40 419.28 135.59 o 8 11 0 34.49 153.56 121.02 o 9 11 0 252.58 448.55 140.08 o 10 11 0 40.94 68.75 144.43 o -8 12 0 125.04 17.97 124.97 o -7 12 0 21.14 -41.93 119.52 o -6 12 0 666.23 646.62 119.52 o -5 12 0 9.83 -10.89 114.21 o -4 12 0 610.23 618.31 121.70 o -3 12 0 0.02 -78.96 112.44 o -2 12 0 335.95 245.44 75.01 o -1 12 0 4.87 4.76 52.33 o 0 12 0 87.00 115.61 53.65 o 1 12 0 0.85 17.15 53.30 o 2 12 0 218.41 284.79 86.99 o 3 12 0 251.98 255.52 86.58 o 4 12 0 526.82 348.49 130.00 o 5 12 0 3.85 344.55 125.65 o 6 12 0 80.09 124.97 126.06 o 7 12 0 96.17 59.63 129.05 o 8 12 0 258.61 254.70 136.68 o 9 12 0 98.37 132.18 141.85 o -8 13 0 4.39 -98.15 128.37 o -7 13 0 3.10 108.90 115.30 o -6 13 0 92.43 63.16 114.76 o -5 13 0 284.82 499.19 111.76 o -4 13 0 11.24 -120.07 120.07 o -3 13 0 27.09 -2.59 118.43 o -2 13 0 240.50 238.64 108.22 o -1 13 0 24.98 54.74 53.01 o 0 13 0 19.86 110.43 54.33 o 1 13 0 205.62 228.28 101.08 o 2 13 0 6.49 80.59 85.22 o 3 13 0 38.96 4.90 127.01 o 4 13 0 570.26 585.63 136.40 o 5 13 0 34.04 183.37 128.64 o 6 13 0 172.13 257.15 121.29 o 7 13 0 49.93 172.21 132.73 o 8 13 0 0.87 175.88 136.68 o 9 13 0 477.73 520.97 145.52 o -7 14 0 45.97 108.09 121.56 o -6 14 0 161.31 209.51 125.65 o -5 14 0 0.11 -50.37 114.08 o -4 14 0 591.93 607.14 117.62 o -3 14 0 492.79 549.83 127.83 o -2 14 0 44.54 -71.88 114.49 o -1 14 0 286.10 276.83 87.63 o 0 14 0 1347.61 1358.98 98.12 o 1 14 0 655.75 741.04 101.89 o 2 14 0 81.38 33.90 136.40 o 3 14 0 876.84 709.79 149.34 o 4 14 0 389.11 527.51 145.12 o 5 14 0 1.57 -52.00 124.02 o 6 14 0 97.86 187.59 127.96 o 7 14 0 29.79 -6.94 135.99 o 8 14 0 56.63 110.81 136.13 o -7 15 0 161.16 232.51 127.01 o -6 15 0 0.20 -91.34 124.97 o -5 15 0 44.52 -50.50 121.97 o -4 15 0 350.85 527.10 122.79 o -3 15 0 1.81 207.60 107.95 o -2 15 0 30.80 -32.26 110.54 o -1 15 0 1.19 -12.23 87.65 o 0 15 0 52.68 142.16 95.36 o 1 15 0 115.55 165.68 90.96 o 2 15 0 713.93 619.39 149.06 o 3 15 0 1136.13 846.60 149.06 o 4 15 0 515.17 631.65 137.49 o 5 15 0 19.57 -127.83 127.83 o 6 15 0 389.78 579.10 137.08 o 7 15 0 20.72 122.25 130.69 o 8 15 0 76.06 132.18 147.16 o -6 16 0 31.27 -54.45 128.24 o -5 16 0 198.84 420.78 124.70 o -4 16 0 17.23 206.92 118.71 o -3 16 0 610.55 669.08 125.38 o -2 16 0 151.32 83.18 115.57 o -1 16 0 261.26 188.87 84.91 o 0 16 0 1080.87 1014.32 98.27 o 1 16 0 0.57 -2.56 146.68 o 2 16 0 68.04 64.39 132.05 o 3 16 0 133.15 257.56 131.37 o 4 16 0 123.60 -101.28 134.22 o 5 16 0 188.69 115.85 135.72 o 6 16 0 8.58 66.16 130.14 o 7 16 0 3.13 172.48 140.21 o -5 17 0 105.82 -65.34 132.18 o -4 17 0 3.66 -14.57 125.92 o -3 17 0 26.89 -120.75 120.75 o -2 17 0 173.22 115.57 121.56 o -1 17 0 62.29 48.01 86.35 o 0 17 0 8.13 2.48 86.86 o 1 17 0 361.70 376.72 226.11 o 2 17 0 137.67 119.11 134.50 o 3 17 0 213.16 57.58 135.31 o 4 17 0 29.68 77.05 140.76 o 5 17 0 62.37 183.91 141.17 o 6 17 0 122.94 -25.86 141.30 o 7 17 0 241.95 360.88 151.11 o -4 18 0 192.53 -120.07 139.13 o -3 18 0 166.14 226.11 128.10 o -2 18 0 906.01 909.90 135.31 o -1 18 0 2.58 61.65 88.79 o 0 18 0 279.37 150.88 105.37 o 1 18 0 22.30 -67.75 89.84 o 2 18 0 14.14 -144.98 144.98 o 3 18 0 353.11 418.06 151.51 o 4 18 0 43.59 82.63 144.03 o 5 18 0 5.30 -120.88 143.75 o 6 18 0 24.60 23.69 148.25 o -3 19 0 138.06 390.01 134.50 o -2 19 0 20.12 241.90 122.25 o -1 19 0 0.83 33.81 122.72 o 0 19 0 2.71 89.50 94.80 o 1 19 0 285.17 330.99 119.86 o 2 19 0 199.37 72.97 143.48 o 3 19 0 0.40 7.90 149.74 o 4 19 0 490.83 736.06 161.31 o 5 19 0 9.17 197.39 146.48 o -1 20 0 14.85 -78.27 97.78 o 0 20 0 0.17 151.82 97.61 o 1 20 0 0.04 22.27 150.97 o 2 20 0 86.11 304.80 144.98 o 3 20 0 544.78 612.59 161.18 o -1 -21 1 0.14 86.44 112.58 o -2 -20 1 6.05 -75.82 156.14 o -1 -20 1 0.00 70.31 72.29 o 0 -20 1 10.89 -108.16 108.16 o 1 -20 1 102.60 -43.67 102.56 o -4 -19 1 62.16 -41.11 155.19 o -3 -19 1 26.22 -32.54 153.01 o -2 -19 1 59.31 90.25 151.65 o -1 -19 1 64.33 65.01 75.23 o 0 -19 1 160.41 326.34 97.39 o 1 -19 1 118.01 50.70 125.92 o 2 -19 1 131.26 -7.62 129.60 o 3 -19 1 49.61 226.52 132.46 o -5 -18 1 245.71 228.02 148.11 o -4 -18 1 64.38 -153.96 153.96 o -3 -18 1 53.10 -136.40 146.61 o -2 -18 1 8.59 14.57 144.43 o -1 -18 1 20.13 12.34 67.76 o 0 -18 1 3.40 -0.96 92.30 o 1 -18 1 127.25 279.76 95.45 o 2 -18 1 197.38 290.09 126.06 o 3 -18 1 30.76 -11.57 135.45 o 4 -18 1 18.58 -63.30 133.27 o -6 -17 1 29.29 -144.71 144.71 o -5 -17 1 6.14 -65.21 140.35 o -4 -17 1 42.25 -32.40 141.30 o -3 -17 1 156.63 326.17 133.82 o -2 -17 1 507.71 773.36 139.40 o -1 -17 1 117.78 171.36 65.76 o 0 -17 1 185.78 188.77 88.48 o 1 -17 1 33.61 -43.59 90.68 o 2 -17 1 4.49 246.40 113.94 o 3 -17 1 135.10 85.76 134.22 o 4 -17 1 40.48 287.78 126.87 o 5 -17 1 36.53 23.69 132.32 o -7 -16 1 27.27 -64.12 150.56 o -6 -16 1 3.84 174.79 134.22 o -5 -16 1 70.32 57.72 129.46 o -4 -16 1 79.14 -80.45 137.76 o -3 -16 1 99.25 125.65 128.92 o -2 -16 1 379.93 414.93 140.08 o -1 -16 1 42.17 -31.83 76.53 o 0 -16 1 11.19 -8.93 85.10 o 1 -16 1 550.88 554.53 99.72 o 2 -16 1 285.67 197.80 116.80 o 3 -16 1 205.38 371.77 121.56 o 4 -16 1 13.82 34.44 125.24 o 5 -16 1 8.17 -29.54 129.73 o 6 -16 1 102.54 209.23 133.27 o -8 -15 1 148.63 51.73 151.79 o -7 -15 1 421.66 386.75 152.87 o -6 -15 1 37.12 40.29 128.64 o -5 -15 1 23.28 -82.50 129.32 o -4 -15 1 0.23 -52.95 128.10 o -3 -15 1 46.12 119.52 133.95 o -2 -15 1 370.62 368.91 144.84 o -1 -15 1 684.21 643.90 60.64 o 0 -15 1 255.05 335.67 90.32 o 1 -15 1 408.33 344.27 92.71 o 2 -15 1 27.51 -64.66 109.18 o 3 -15 1 6.42 120.07 110.95 o 4 -15 1 35.31 128.10 115.44 o 5 -15 1 39.74 273.49 121.43 o 6 -15 1 131.77 111.35 133.00 o 7 -15 1 18.33 -7.76 129.73 o -8 -14 1 205.93 340.19 142.26 o -7 -14 1 0.01 -118.30 135.99 o -6 -14 1 365.75 271.17 130.69 o -5 -14 1 113.96 -41.52 129.73 o -4 -14 1 192.34 127.55 136.27 o -3 -14 1 242.96 304.12 140.08 o -2 -14 1 573.36 578.42 142.80 o -1 -14 1 491.69 557.32 57.02 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