#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:53:10 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180927 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/07/2200742.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200742_Fobs loop_ _publ_author_name 'Grossie, David A.' 'Turnbull, Kenneth' 'Krein, Douglas M.' _publ_section_title ; 3-(2-Bromophenyl)-4-(triisopropylsilyl)sydnone ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o985 _journal_page_last o987 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.820 _cell_angle_gamma 90.000 _cell_length_a 11.7560 _cell_length_b 12.7719 _cell_length_c 12.8527 _exptl_crystal_F_000 824.00 _reflns_d_resolution_high 0.7114 _cod_data_source_file om6056Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' t03' _shelx_refln_list_code 4 _shelx_f_calc_maximum 247.89 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, z+1/2' '-x, -y, -z' '-x-1/2, y-1/2, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 529.68 517.81 17.30 o 4 0 0 1080.67 1062.28 55.61 o 6 0 0 5077.55 5180.99 81.29 o 8 0 0 52.05 61.07 9.50 o 10 0 0 144.04 157.35 16.81 o 12 0 0 205.40 233.10 14.75 o 14 0 0 1.23 12.72 20.31 o 16 0 0 24.21 24.75 69.91 o 1 1 0 2789.41 2995.89 119.40 o 2 1 0 3513.80 3651.43 113.80 o 3 1 0 1464.63 1424.12 31.45 o 4 1 0 793.77 767.73 27.39 o 5 1 0 1838.63 1774.61 85.58 o 6 1 0 64.91 62.56 6.62 o 7 1 0 2781.34 2807.54 106.54 o 8 1 0 384.07 390.62 22.74 o 9 1 0 132.31 144.37 10.92 o 10 1 0 650.83 644.82 67.26 o 11 1 0 30.90 43.19 12.33 o 12 1 0 71.68 46.87 18.58 o 13 1 0 52.73 44.79 19.76 o 14 1 0 64.93 54.23 22.13 o 15 1 0 13.04 27.26 23.41 o 16 1 0 4.08 10.23 25.56 o 0 2 0 17805.23 19649.12 220.87 o 1 2 0 3464.57 3776.60 43.49 o 2 2 0 2813.48 2930.68 41.24 o 3 2 0 12188.74 12402.12 719.34 o 4 2 0 708.48 807.80 65.94 o 5 2 0 1369.70 1342.24 57.36 o 6 2 0 389.66 391.68 24.81 o 7 2 0 78.52 64.30 7.97 o 8 2 0 2567.58 2664.47 89.58 o 9 2 0 847.53 848.46 44.73 o 10 2 0 44.60 23.98 37.82 o 11 2 0 49.18 29.35 41.60 o 12 2 0 35.45 55.14 18.17 o 13 2 0 5.69 16.69 47.00 o 14 2 0 24.67 19.03 53.51 o 15 2 0 56.79 55.09 23.44 o 16 2 0 5.50 41.63 25.08 o 1 3 0 963.54 1055.90 25.47 o 2 3 0 42157.51 44539.29 419.23 o 3 3 0 189.07 191.96 11.33 o 4 3 0 1098.60 1028.53 32.53 o 5 3 0 395.27 430.46 23.46 o 6 3 0 389.77 409.03 20.53 o 7 3 0 11.99 22.85 10.80 o 8 3 0 468.17 544.65 60.04 o 9 3 0 0.18 11.94 34.03 o 10 3 0 408.61 416.21 46.45 o 11 3 0 5.99 6.39 15.91 o 12 3 0 11.64 29.43 45.85 o 13 3 0 16.16 17.72 50.32 o 14 3 0 15.30 19.28 54.60 o 15 3 0 20.13 44.47 57.79 o 16 3 0 17.75 40.02 24.71 o 0 4 0 248.79 283.64 22.71 o 1 4 0 10938.63 10409.05 393.11 o 2 4 0 3149.86 3509.92 111.70 o 3 4 0 318.63 503.54 54.68 o 4 4 0 259.48 220.57 16.96 o 5 4 0 6544.22 6597.95 180.96 o 6 4 0 152.93 145.04 8.76 o 7 4 0 960.54 1027.25 44.25 o 8 4 0 1018.60 1058.26 48.56 o 9 4 0 141.36 157.56 15.79 o 10 4 0 70.70 74.69 11.13 o 11 4 0 343.11 388.03 24.90 o 12 4 0 4.85 15.30 43.48 o 13 4 0 0.10 26.26 49.45 o 14 4 0 4.77 39.57 22.43 o 15 4 0 0.72 9.98 25.13 o 16 4 0 10.11 47.24 69.20 o 1 5 0 327.91 323.78 30.95 o 2 5 0 440.83 492.72 24.32 o 3 5 0 642.87 775.13 31.22 o 4 5 0 1824.08 1845.06 46.93 o 5 5 0 715.91 726.60 34.82 o 6 5 0 2146.93 2392.82 59.17 o 7 5 0 1795.29 1684.91 55.07 o 8 5 0 38.81 24.56 31.65 o 9 5 0 251.70 265.76 12.96 o 10 5 0 552.11 577.35 30.00 o 11 5 0 121.35 129.17 13.16 o 12 5 0 36.29 36.67 19.21 o 13 5 0 146.78 152.43 16.40 o 14 5 0 19.36 25.25 16.81 o 15 5 0 13.26 22.12 62.60 o 0 6 0 15706.09 17329.38 238.32 o 1 6 0 909.27 932.77 33.25 o 2 6 0 3801.58 3793.46 64.92 o 3 6 0 2267.15 2551.58 55.12 o 4 6 0 4735.33 5201.27 82.56 o 5 6 0 287.38 247.15 13.69 o 6 6 0 578.84 630.05 39.91 o 7 6 0 739.66 815.41 43.03 o 8 6 0 502.92 549.93 45.03 o 9 6 0 40.51 34.98 14.58 o 10 6 0 9.21 18.98 16.06 o 11 6 0 36.12 16.84 47.49 o 12 6 0 168.44 193.07 15.16 o 13 6 0 8.79 32.08 53.61 o 14 6 0 18.95 47.56 57.55 o 15 6 0 4.00 21.44 60.69 o 1 7 0 3298.55 3408.74 74.37 o 2 7 0 232.78 224.95 20.42 o 3 7 0 21.39 8.86 24.99 o 4 7 0 407.96 414.96 22.30 o 5 7 0 1739.74 1691.80 55.24 o 6 7 0 142.01 147.11 9.68 o 7 7 0 604.25 696.76 37.86 o 8 7 0 201.90 198.58 12.93 o 9 7 0 2.72 13.87 39.23 o 10 7 0 395.67 416.01 25.39 o 11 7 0 22.11 55.35 24.12 o 12 7 0 0.01 43.65 41.48 o 13 7 0 5.31 34.72 55.22 o 14 7 0 18.53 9.76 24.28 o 15 7 0 49.70 58.04 26.26 o 0 8 0 1964.24 2055.01 76.71 o 1 8 0 6.07 14.91 22.77 o 2 8 0 65.34 52.50 8.03 o 3 8 0 5205.94 5298.73 220.48 o 4 8 0 614.74 648.39 51.81 o 5 8 0 522.27 540.13 39.91 o 6 8 0 772.77 889.06 43.66 o 7 8 0 409.32 478.08 38.16 o 8 8 0 230.57 254.88 18.00 o 9 8 0 617.69 605.51 31.56 o 10 8 0 21.35 16.32 46.13 o 11 8 0 1.06 16.95 48.09 o 12 8 0 26.21 32.48 20.29 o 13 8 0 0.15 20.08 56.61 o 14 8 0 1.48 33.62 63.37 o 1 9 0 1.67 16.21 28.97 o 2 9 0 3161.28 3352.11 75.63 o 3 9 0 113.13 120.61 13.79 o 4 9 0 1592.76 1640.99 58.41 o 5 9 0 332.90 297.64 19.32 o 6 9 0 14.69 13.25 37.55 o 7 9 0 33.38 48.35 14.96 o 8 9 0 90.09 114.90 13.41 o 9 9 0 47.21 42.26 17.20 o 10 9 0 96.70 79.70 20.96 o 11 9 0 11.96 5.17 14.65 o 12 9 0 33.03 38.94 49.89 o 13 9 0 1.57 21.63 61.13 o 14 9 0 0.41 10.26 25.86 o 0 10 0 1623.71 1528.27 82.95 o 1 10 0 464.47 507.44 36.02 o 2 10 0 51.36 40.88 17.59 o 3 10 0 1186.60 1172.70 112.53 o 4 10 0 358.80 355.87 39.18 o 5 10 0 20.48 32.16 14.03 o 6 10 0 556.10 625.17 33.97 o 7 10 0 118.35 112.75 13.47 o 8 10 0 41.96 42.16 17.62 o 9 10 0 11.05 25.86 20.62 o 10 10 0 1.43 15.68 23.73 o 11 10 0 66.27 20.66 58.65 o 12 10 0 83.94 116.04 17.57 o 13 10 0 8.77 22.40 63.46 o 1 11 0 656.82 708.03 105.66 o 2 11 0 94.25 93.94 10.65 o 3 11 0 25.62 23.57 36.01 o 4 11 0 103.26 109.87 15.45 o 5 11 0 83.82 15.44 43.60 o 6 11 0 327.62 297.47 19.58 o 7 11 0 192.20 197.84 14.58 o 8 11 0 3.83 42.97 44.94 o 9 11 0 18.73 7.78 19.69 o 10 11 0 116.25 134.81 16.61 o 11 11 0 24.30 19.43 54.91 o 12 11 0 3.97 21.38 60.55 o 13 11 0 18.78 52.01 62.57 o 0 12 0 329.55 329.07 38.50 o 1 12 0 87.14 69.49 17.89 o 2 12 0 456.55 448.78 26.90 o 3 12 0 114.16 89.03 41.72 o 4 12 0 570.11 594.45 30.84 o 5 12 0 56.92 64.21 28.27 o 6 12 0 88.70 114.71 13.74 o 7 12 0 28.42 49.23 18.62 o 8 12 0 298.05 340.02 23.65 o 9 12 0 8.01 20.03 56.48 o 10 12 0 17.74 21.03 59.46 o 11 12 0 15.89 23.33 17.85 o 12 12 0 0.76 17.53 25.42 o 1 13 0 551.83 561.80 29.96 o 2 13 0 11.53 56.08 24.37 o 3 13 0 37.51 16.61 47.17 o 4 13 0 37.63 28.78 18.28 o 5 13 0 209.48 215.95 18.28 o 6 13 0 3.91 17.07 48.33 o 7 13 0 46.72 35.14 21.07 o 8 13 0 23.37 16.94 23.34 o 9 13 0 16.87 32.10 22.66 o 10 13 0 22.88 48.97 60.77 o 11 13 0 0.83 43.57 65.21 o 0 14 0 359.58 241.73 36.16 o 1 14 0 224.96 211.89 20.27 o 2 14 0 0.60 16.99 47.99 o 3 14 0 30.15 22.60 14.03 o 4 14 0 54.69 33.98 49.86 o 5 14 0 212.13 217.34 17.79 o 6 14 0 79.85 69.16 16.51 o 7 14 0 33.47 25.69 19.88 o 8 14 0 32.87 49.76 23.38 o 9 14 0 33.62 55.48 24.23 o 10 14 0 6.49 22.38 63.19 o 1 15 0 20.27 17.55 49.58 o 2 15 0 169.79 154.52 44.40 o 3 15 0 14.18 9.23 15.29 o 4 15 0 76.43 71.03 32.21 o 5 15 0 55.92 73.55 22.69 o 6 15 0 9.97 29.77 55.20 o 7 15 0 1.39 49.21 61.63 o 8 15 0 36.14 23.67 18.77 o 9 15 0 5.76 38.21 65.82 o 0 16 0 44.05 16.96 24.17 o 1 16 0 6.04 20.39 57.36 o 2 16 0 4.40 5.94 16.75 o 3 16 0 166.39 170.91 18.67 o 4 16 0 10.70 41.40 23.74 o 5 16 0 1.57 31.94 59.96 o 6 16 0 29.26 10.28 25.62 o 7 16 0 1.74 21.27 60.01 o 1 17 0 35.93 78.37 36.50 o 2 17 0 15.98 44.09 62.47 o 3 17 0 0.20 9.79 24.39 o 4 17 0 12.29 10.44 25.83 o 5 17 0 5.62 22.98 65.11 o -15 0 1 0.81 53.71 67.45 o -13 0 1 2.65 4.58 18.23 o -11 0 1 1649.15 1782.18 100.49 o -9 0 1 1777.63 1669.60 84.61 o -7 0 1 453.00 562.12 42.40 o -5 0 1 1690.72 1507.89 55.66 o -3 0 1 12469.37 10921.95 148.84 o -1 0 1 4163.27 4230.88 58.48 o 1 0 1 428.63 500.32 18.71 o 3 0 1 30439.66 28629.91 329.16 o 5 0 1 370.29 409.38 31.00 o 7 0 1 163.41 165.41 20.27 o 9 0 1 6185.28 5894.34 147.28 o 11 0 1 884.62 871.89 60.14 o 13 0 1 9.83 16.86 67.55 o 15 0 1 41.29 83.73 84.22 o -16 1 1 2.35 48.15 76.81 o -15 1 1 41.12 21.64 86.26 o -14 1 1 21.35 5.26 21.25 o -13 1 1 0.47 14.91 59.95 o -12 1 1 35.02 15.11 60.34 o -11 1 1 199.75 199.92 17.84 o -10 1 1 95.91 91.23 15.30 o -9 1 1 918.50 929.01 71.35 o -8 1 1 593.06 584.54 45.32 o -7 1 1 549.13 578.11 43.08 o -6 1 1 718.29 665.05 45.81 o -5 1 1 2528.38 2426.96 67.45 o -4 1 1 5847.04 5669.86 100.59 o -3 1 1 9.37 6.04 23.78 o -2 1 1 7146.42 7504.87 101.86 o -1 1 1 2577.91 2779.32 45.42 o 0 1 1 199.68 187.63 13.06 o 1 1 1 25531.79 24635.79 267.17 o 2 1 1 2747.16 2478.33 49.32 o 3 1 1 0.94 5.17 20.66 o 4 1 1 11411.14 10708.00 157.13 o 5 1 1 478.81 518.55 35.67 o 6 1 1 4.53 10.43 8.29 o 7 1 1 1152.98 1080.67 61.02 o 8 1 1 340.64 337.84 31.78 o 9 1 1 567.53 561.93 33.04 o 10 1 1 404.84 411.82 32.85 o 11 1 1 8.31 46.79 53.90 o 12 1 1 2.36 14.91 59.46 o 13 1 1 80.52 121.35 18.62 o 14 1 1 0.16 17.25 69.21 o 15 1 1 2.45 17.93 71.54 o 16 1 1 15.63 21.05 84.51 o -16 2 1 0.22 37.43 24.56 o -15 2 1 21.83 20.47 81.97 o -14 2 1 101.75 88.89 21.93 o -13 2 1 49.71 58.68 19.69 o -12 2 1 34.07 53.02 63.94 o -11 2 1 96.42 47.66 61.99 o -10 2 1 28.53 82.17 14.33 o -9 2 1 244.26 261.52 23.10 o -8 2 1 903.35 885.63 61.12 o -7 2 1 211.17 214.83 15.60 o -6 2 1 5502.53 5784.29 119.31 o -5 2 1 2786.38 2953.41 76.32 o -4 2 1 1873.40 1845.64 55.85 o -3 2 1 243.34 211.71 17.64 o -2 2 1 868.35 1029.31 35.38 o -1 2 1 5278.70 5630.58 82.17 o 0 2 1 12446.03 12968.48 154.01 o 1 2 1 2700.66 2808.37 51.17 o 2 2 1 101.02 103.03 7.02 o 3 2 1 8586.08 8448.89 125.64 o 4 2 1 660.76 701.31 37.14 o 5 2 1 1597.10 1638.31 57.70 o 6 2 1 7060.34 7090.32 137.24 o 7 2 1 1665.43 1584.12 69.01 o 8 2 1 18.09 10.72 42.69 o 9 2 1 544.55 472.06 43.08 o 10 2 1 7.70 11.60 46.49 o 11 2 1 20.61 13.35 53.02 o 12 2 1 57.95 16.18 64.72 o 13 2 1 3.24 15.50 62.38 o 14 2 1 5.33 18.52 73.69 o 15 2 1 0.46 5.75 22.91 o 16 2 1 5.49 20.37 81.68 o -16 3 1 1.11 21.35 85.09 o -15 3 1 0.39 20.57 82.36 o -14 3 1 31.17 51.37 70.47 o -13 3 1 187.18 203.91 22.32 o -12 3 1 21.92 53.41 63.65 o -11 3 1 21.13 14.13 56.73 o -10 3 1 202.04 184.22 16.08 o -9 3 1 19.19 21.64 13.26 o -8 3 1 17.02 10.53 42.21 o -7 3 1 5422.08 5232.89 123.59 o -6 3 1 515.24 628.89 44.45 o -5 3 1 194.42 216.19 17.64 o -4 3 1 5.43 6.04 23.78 o -3 3 1 1677.86 1749.82 52.44 o -2 3 1 515.59 535.22 30.61 o -1 3 1 7622.38 8371.01 118.53 o 0 3 1 2865.36 3240.95 62.19 o 1 3 1 3974.54 3994.90 70.96 o 2 3 1 907.60 1023.17 36.65 o 3 3 1 4856.12 5061.14 92.70 o 4 3 1 2408.24 2700.95 69.69 o 5 3 1 3598.21 3548.47 86.85 o 6 3 1 553.43 561.24 45.23 o 7 3 1 695.66 701.41 53.71 o 8 3 1 23.79 27.97 11.99 o 9 3 1 1021.91 943.14 71.15 o 10 3 1 38.71 12.77 51.27 o 11 3 1 254.24 286.96 23.49 o 12 3 1 23.79 15.21 60.73 o 13 3 1 119.59 112.39 20.57 o 14 3 1 1.30 37.33 67.06 o 15 3 1 0.61 31.39 22.42 o 16 3 1 2.73 21.44 85.78 o -16 4 1 8.67 50.78 82.36 o -15 4 1 9.22 21.15 84.70 o -14 4 1 4.90 47.27 71.06 o -13 4 1 2.31 55.75 69.01 o -12 4 1 163.41 164.63 20.96 o -11 4 1 0.82 13.74 55.07 o -10 4 1 5.26 12.87 51.56 o -9 4 1 188.46 213.37 15.50 o -8 4 1 222.62 233.64 22.91 o -7 4 1 352.73 354.60 32.17 o -6 4 1 769.21 651.89 48.05 o -5 4 1 1069.53 1118.98 52.44 o -4 4 1 698.03 936.32 46.10 o -3 4 1 126.86 96.50 7.41 o -2 4 1 15264.19 17070.69 220.97 o -1 4 1 68.87 66.09 6.53 o 0 4 1 109.59 96.59 6.43 o 1 4 1 2311.17 2382.51 57.90 o 2 4 1 8166.43 8636.42 132.37 o 3 4 1 2926.97 3023.39 72.42 o 4 4 1 1611.82 1537.43 54.88 o 5 4 1 595.97 564.36 37.82 o 6 4 1 26.82 7.60 30.80 o 7 4 1 590.78 434.53 47.66 o 8 4 1 1794.00 1850.12 85.00 o 9 4 1 4.94 27.78 13.06 o 10 4 1 9.80 13.06 52.05 o 11 4 1 43.55 32.36 53.90 o 12 4 1 3.02 4.58 18.32 o 13 4 1 2.70 23.98 18.91 o 14 4 1 68.83 87.43 22.03 o 15 4 1 2.07 21.64 86.56 o 16 4 1 3.35 22.42 89.67 o -15 5 1 14.41 58.29 75.54 o -14 5 1 12.23 29.63 22.71 o -13 5 1 2.26 48.35 66.18 o -12 5 1 41.67 21.64 19.01 o -11 5 1 4.07 4.19 16.96 o -10 5 1 577.02 581.81 55.95 o -9 5 1 20.56 26.03 48.44 o -8 5 1 39.06 59.85 13.16 o -7 5 1 500.24 577.52 48.93 o -6 5 1 289.43 287.54 24.47 o -5 5 1 531.34 588.05 42.60 o -4 5 1 6270.96 6862.33 129.83 o -3 5 1 254.01 260.84 29.53 o -2 5 1 3155.46 3393.49 79.24 o -1 5 1 2313.25 2449.77 64.23 o 0 5 1 26.45 32.17 6.53 o 1 5 1 12503.78 13950.12 193.77 o 2 5 1 14307.50 15763.30 215.80 o 3 5 1 664.51 683.96 40.45 o 4 5 1 162.20 133.54 8.97 o 5 5 1 4310.66 4268.11 104.88 o 6 5 1 566.45 539.31 44.64 o 7 5 1 391.35 405.97 32.46 o 8 5 1 1020.29 968.68 70.37 o 9 5 1 11.53 12.67 50.69 o 10 5 1 23.22 12.87 51.37 o 11 5 1 3.03 14.72 59.17 o 12 5 1 73.19 71.35 19.20 o 13 5 1 11.14 16.67 20.08 o 14 5 1 8.74 19.30 77.20 o 15 5 1 12.29 37.92 23.59 o -15 6 1 6.92 75.74 79.93 o -14 6 1 11.20 17.84 70.96 o -13 6 1 21.38 17.35 69.30 o -12 6 1 10.92 15.99 63.75 o -11 6 1 211.51 242.41 20.08 o -10 6 1 15.58 13.06 52.44 o -9 6 1 1022.79 1079.60 77.59 o -8 6 1 83.06 80.90 13.94 o -7 6 1 98.07 96.69 13.26 o -6 6 1 26.85 29.14 40.84 o -5 6 1 3817.50 4076.58 106.83 o -4 6 1 18.02 8.29 33.43 o -3 6 1 2274.48 2533.98 77.00 o -2 6 1 110.71 143.67 16.96 o -1 6 1 2649.57 2763.04 75.05 o 0 6 1 359.02 380.82 27.10 o 1 6 1 2793.27 3080.90 80.12 o 2 6 1 2209.90 2104.81 67.26 o 3 6 1 2548.93 2521.99 75.64 o 4 6 1 1161.82 1145.40 57.02 o 5 6 1 1451.00 1472.90 69.60 o 6 6 1 384.86 334.52 32.46 o 7 6 1 103.11 116.48 13.55 o 8 6 1 5.30 11.89 47.76 o 9 6 1 646.50 614.95 56.73 o 10 6 1 86.05 15.21 61.21 o 11 6 1 351.84 328.68 21.05 o 12 6 1 47.90 53.51 19.30 o 13 6 1 2.62 5.36 21.25 o 14 6 1 9.77 19.01 75.54 o 15 6 1 41.30 22.71 90.84 o -15 7 1 4.36 23.88 95.52 o -14 7 1 34.63 59.65 24.56 o -13 7 1 19.51 29.24 22.71 o -12 7 1 110.57 136.46 21.93 o -11 7 1 17.55 52.63 59.56 o -10 7 1 151.46 144.65 19.40 o -9 7 1 25.62 14.04 56.44 o -8 7 1 447.96 507.93 38.50 o -7 7 1 335.52 386.48 26.41 o -6 7 1 1205.92 1166.55 71.45 o -5 7 1 677.18 730.46 57.31 o -4 7 1 1956.75 2067.68 78.47 o -3 7 1 177.86 182.86 21.05 o -2 7 1 2287.17 2441.29 78.37 o -1 7 1 2741.09 3163.65 86.65 o 0 7 1 41.47 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o -2 4 17 16.40 6.53 26.03 o -1 4 17 2.08 67.06 87.82 o 0 4 17 9.16 24.86 99.71 o 1 4 17 10.72 20.18 81.00 o 2 4 17 0.12 21.44 85.48 o 3 4 17 8.25 22.91 91.92 o -3 5 17 0.85 22.03 88.02 o -2 5 17 0.01 24.37 97.37 o -1 5 17 0.11 62.28 79.34 o 0 5 17 21.66 22.91 91.33 o 1 5 17 0.50 69.69 80.51 o 2 5 17 0.13 6.63 26.90 o -1 6 17 0.11 22.42 89.77 o 0 6 17 18.13 39.18 26.32 o 0 0 18 6.95 22.81 91.23 o -1 1 18 0.47 22.61 90.75 o 0 1 18 0.52 24.56 98.74 o