#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/08/2200811.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200811_Fobs loop_ _publ_author_name 'Light, Mark E.' 'Camiolo, Salvatore' 'Gale, Philip A.' 'Hursthouse, Michael B.' _publ_section_title ; Methyl 5-methyl-3,4-diphenyl-1H-pyrrole-2-carboxylate ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1245 _journal_page_last o1246 _journal_volume 57 _journal_year 2001 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 118.186 _cell_angle_gamma 90.000 _cell_length_a 34.1913 _cell_length_b 10.7042 _cell_length_c 19.1129 _exptl_crystal_F_000 2464.00 _reflns_d_resolution_high 0.8400 _[local]_cod_data_source_file ya6076Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 01SOT144 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 491.11 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 14417.90 7417.04 272.09 o 8 0 0 16808.79 179950.88 5673.99 o 10 0 0 9702.45 30098.50 897.17 o 12 0 0 4689.63 3975.55 169.04 o 14 0 0 3471.11 3404.12 203.49 o 16 0 0 4564.31 2175.38 213.01 o 18 0 0 2183.87 3610.27 200.82 o 20 0 0 506.48 2819.66 174.33 o 22 0 0 4124.05 71.23 123.37 o 24 0 0 1581.32 3209.24 245.94 o 26 0 0 179.36 0.00 150.61 o 28 0 0 73.02 1771.72 232.72 o 30 0 0 212.40 -107.11 226.09 o 32 0 0 1.72 2149.73 369.71 o 34 0 0 839.70 10250.09 1171.09 o 5 1 0 243.43 3867.26 167.40 o 7 1 0 4135.03 1327.82 95.75 o 9 1 0 4785.26 11679.98 249.69 o 11 1 0 6828.25 7358.42 175.58 o 13 1 0 34.74 213.69 213.69 o 15 1 0 374.59 1425.64 88.69 o 17 1 0 211.53 1625.34 87.24 o 19 1 0 443.24 515.46 87.24 o 21 1 0 756.79 1102.10 93.24 o 23 1 0 2.06 4042.52 183.11 o 25 1 0 491.71 3045.57 194.72 o 27 1 0 22.96 1808.94 174.33 o 29 1 0 0.84 190.18 111.33 o 31 1 0 145.53 166.32 110.35 o 33 1 0 66.94 183.03 128.80 o 35 1 0 1470.22 723.94 250.34 o 0 2 0 22472.71 11043.54 278.32 o 4 2 0 9735.30 58741.36 1298.19 o 6 2 0 14838.50 44422.71 1140.66 o 8 2 0 9202.14 37164.36 745.73 o 10 2 0 908.09 1064.35 106.84 o 12 2 0 50.11 53.42 106.84 o 14 2 0 862.44 2981.52 129.14 o 16 2 0 880.05 8278.90 205.09 o 18 2 0 857.35 1505.24 87.24 o 20 2 0 335.55 71.23 87.24 o 22 2 0 5.79 141.76 105.97 o 24 2 0 216.40 -58.28 93.26 o 26 2 0 242.55 332.27 110.27 o 28 2 0 1535.50 379.24 110.27 o 30 2 0 145.46 -158.96 158.96 o 32 2 0 27.64 42.36 190.38 o 34 2 0 0.31 213.26 213.02 o 1 3 0 47.01 1162.99 80.42 o 3 3 0 87.06 3194.90 75.18 o 5 3 0 1202.73 5619.46 97.74 o 7 3 0 195.43 15460.70 297.52 o 9 3 0 2392.49 160.26 106.84 o 11 3 0 105.44 5591.14 173.90 o 13 3 0 1396.57 2070.14 155.42 o 15 3 0 344.69 883.35 153.61 o 17 3 0 564.45 266.58 106.84 o 19 3 0 485.50 142.46 87.24 o 21 3 0 999.13 852.28 161.19 o 23 3 0 296.91 5751.04 195.34 o 25 3 0 198.73 -38.72 98.00 o 27 3 0 1694.70 3280.31 184.96 o 29 3 0 14.18 380.41 92.10 o 31 3 0 179.99 473.78 108.68 o 33 3 0 126.81 84.97 146.81 o 0 4 0 8718.16 8662.22 229.10 o 2 4 0 3281.53 5185.45 95.26 o 4 4 0 3530.29 2331.61 75.18 o 6 4 0 560.68 15354.40 283.75 o 8 4 0 322.29 142.22 133.76 o 10 4 0 1318.81 479.22 106.84 o 12 4 0 16.35 1024.92 214.69 o 14 4 0 23.68 5113.28 229.20 o 16 4 0 18.45 929.77 142.38 o 18 4 0 114.25 0.00 190.94 o 20 4 0 138.27 0.00 142.38 o 22 4 0 76.62 70.53 245.53 o 24 4 0 314.71 229.39 85.46 o 26 4 0 103.86 -58.23 98.00 o 28 4 0 943.66 659.67 132.12 o 30 4 0 2016.79 1846.86 129.36 o 32 4 0 0.11 213.45 139.80 o 34 4 0 176.69 -212.64 212.64 o 1 5 0 6341.34 20753.82 370.39 o 3 5 0 2434.52 4572.83 103.44 o 5 5 0 3870.82 2703.99 75.18 o 7 5 0 2359.99 18106.90 464.40 o 9 5 0 1116.49 159.48 106.32 o 11 5 0 838.80 713.70 106.84 o 13 5 0 181.12 573.18 153.31 o 15 5 0 516.15 1091.53 130.95 o 17 5 0 475.19 354.75 167.23 o 19 5 0 880.51 2416.83 245.53 o 21 5 0 956.83 1551.77 245.53 o 23 5 0 2077.30 1355.43 383.18 o 25 5 0 1749.95 5763.33 491.47 o 27 5 0 150.02 1095.80 458.27 o 29 5 0 293.41 211.59 272.09 o 31 5 0 3.47 0.42 283.67 o 33 5 0 646.52 -60.58 509.35 o 0 6 0 4487.42 11946.09 319.48 o 2 6 0 1969.66 106.32 86.81 o 4 6 0 694.98 1311.78 75.18 o 6 6 0 14.64 1234.07 110.55 o 8 6 0 728.17 212.11 106.32 o 10 6 0 2312.54 1199.88 133.95 o 12 6 0 43.08 3248.15 212.64 o 14 6 0 180.22 5541.87 250.34 o 16 6 0 97.81 4359.97 309.67 o 18 6 0 16.92 1667.97 309.02 o 20 6 0 1897.07 5025.58 399.23 o 22 6 0 1599.79 1299.38 245.53 o 24 6 0 126.93 1124.66 309.67 o 26 6 0 105.95 212.99 245.53 o 28 6 0 219.98 71.23 368.91 o 30 6 0 26.80 319.48 531.07 o 1 7 0 493.97 2072.13 96.48 o 3 7 0 56.87 -53.16 75.18 o 5 7 0 3375.30 904.53 75.18 o 7 7 0 123.66 4998.67 128.17 o 9 7 0 256.59 390.67 86.81 o 11 7 0 47.64 2316.34 131.27 o 13 7 0 2.69 -71.11 135.01 o 15 7 0 124.19 320.27 174.19 o 17 7 0 3067.19 10360.97 564.21 o 19 7 0 161.28 265.73 313.48 o 21 7 0 1727.59 6958.84 492.28 o 23 7 0 487.88 345.90 272.09 o 25 7 0 4.70 106.84 451.82 o 27 7 0 29.18 -106.84 300.72 o 29 7 0 981.00 850.56 601.43 o 0 8 0 409.44 2504.74 173.33 o 2 8 0 325.11 2752.19 150.73 o 4 8 0 198.02 266.06 80.77 o 6 8 0 84.80 3539.92 161.08 o 8 8 0 601.61 260.08 109.98 o 10 8 0 20.87 5995.76 319.48 o 12 8 0 267.29 922.59 245.94 o 14 8 0 3.30 354.98 245.94 o 16 8 0 89.08 106.58 226.09 o 18 8 0 1359.59 -272.09 272.09 o 20 8 0 61.23 -71.23 245.53 o 22 8 0 430.02 745.81 300.72 o 24 8 0 150.54 1521.03 533.17 o 26 8 0 95.78 -451.82 451.82 o 1 9 0 292.98 309.36 112.84 o 3 9 0 116.31 115.72 92.56 o 5 9 0 2176.99 774.66 141.78 o 7 9 0 6695.17 2871.10 182.50 o 9 9 0 554.58 12486.59 500.26 o 11 9 0 252.11 1318.54 110.27 o 13 9 0 2461.97 3550.92 368.50 o 15 9 0 1995.16 2053.81 370.66 o 17 9 0 53.77 212.64 426.33 o 19 9 0 610.23 2276.88 354.03 o 21 9 0 0.04 213.69 300.72 o 23 9 0 167.42 425.28 300.72 o 25 9 0 412.51 1034.83 958.45 o 0 10 0 257.23 512.17 141.75 o 2 10 0 216.65 1882.76 173.90 o 4 10 0 136.57 94.66 109.98 o 6 10 0 1901.17 6551.43 366.10 o 8 10 0 137.71 1037.81 207.21 o 10 10 0 241.66 60.97 128.74 o 12 10 0 244.05 -212.64 300.47 o 14 10 0 290.95 0.00 300.72 o 16 10 0 41.30 213.69 300.72 o 18 10 0 380.68 -106.84 300.72 o 20 10 0 1.67 85.39 354.03 o 22 10 0 735.94 319.48 451.82 o 1 11 0 636.32 1023.43 141.68 o 3 11 0 5.87 160.03 123.32 o 5 11 0 225.96 224.06 132.20 o 7 11 0 62.95 343.26 136.20 o 9 11 0 656.35 54.60 264.21 o 11 11 0 47.33 -35.38 135.01 o 13 11 0 253.75 318.44 300.72 o 15 11 0 5.95 106.84 450.34 o 17 11 0 59.40 -334.51 510.87 o 0 12 0 1489.07 3876.03 451.82 o 2 12 0 52.76 213.16 213.16 o 4 12 0 66.59 482.14 153.05 o 6 12 0 304.89 917.61 251.36 o 8 12 0 872.97 26.84 143.25 o 10 12 0 155.31 266.44 175.32 o 12 12 0 36.84 318.44 530.03 o -35 1 1 99.53 58.83 231.98 o -33 1 1 83.30 940.05 174.18 o -31 1 1 135.00 213.56 123.32 o -29 1 1 678.78 640.00 174.04 o -27 1 1 6.77 148.91 133.53 o -25 1 1 1315.02 96.75 93.26 o -23 1 1 231.24 1649.99 110.27 o -21 1 1 834.49 3099.17 188.05 o -19 1 1 890.30 1561.07 88.74 o -17 1 1 5656.15 12326.92 302.51 o -15 1 1 4171.11 16069.62 359.75 o -13 1 1 138.22 8265.16 183.49 o -11 1 1 1168.93 1085.99 95.75 o -9 1 1 3219.21 20435.32 478.93 o -7 1 1 209.80 14856.67 375.39 o -5 1 1 9936.26 32478.87 726.41 o 3 1 1 7433.05 2869.61 80.30 o 7 1 1 214.16 12999.07 292.31 o 9 1 1 5706.56 478.44 106.32 o 11 1 1 1266.24 902.62 94.78 o 13 1 1 5724.82 5638.32 160.85 o 15 1 1 2520.00 1090.19 88.26 o 17 1 1 378.16 887.90 87.24 o 19 1 1 149.96 70.88 87.24 o 21 1 1 62.12 284.57 87.24 o 23 1 1 925.44 598.24 95.72 o 25 1 1 590.57 675.01 147.94 o 27 1 1 340.91 3659.22 219.80 o 29 1 1 4.08 -142.30 142.30 o 31 1 1 446.91 -150.82 150.82 o 33 1 1 42.89 478.70 215.30 o -36 2 1 3.12 -141.76 245.53 o -34 2 1 71.53 133.32 123.00 o -32 2 1 908.02 497.61 174.19 o -30 2 1 1085.95 2622.31 182.90 o -28 2 1 389.57 166.10 103.38 o -26 2 1 788.00 6040.93 237.87 o -24 2 1 49.99 -0.11 100.71 o -22 2 1 857.94 390.71 87.24 o -20 2 1 230.22 85.06 95.56 o -18 2 1 37.69 178.07 87.24 o -16 2 1 3705.57 27957.00 624.13 o -14 2 1 631.13 613.30 95.56 o -12 2 1 762.58 4885.07 101.14 o -10 2 1 1729.54 7270.84 174.47 o -8 2 1 2237.11 7323.21 174.19 o -6 2 1 74.26 39432.33 866.06 o -4 2 1 7406.16 20761.07 445.68 o 0 2 1 22419.09 636.87 211.59 o 2 2 1 2952.53 49030.59 1037.47 o 4 2 1 4537.88 20193.81 514.93 o 6 2 1 25717.48 6324.37 212.64 o 8 2 1 2390.48 17523.18 422.56 o 10 2 1 1590.39 1292.69 106.32 o 12 2 1 758.41 158.95 107.42 o 14 2 1 35.31 4662.08 127.46 o 16 2 1 0.25 692.87 80.77 o 18 2 1 1242.19 4057.12 123.27 o 20 2 1 1504.54 2561.30 110.24 o 22 2 1 647.37 -87.24 87.24 o 24 2 1 205.35 1297.54 110.27 o 26 2 1 534.36 738.07 93.26 o 28 2 1 47.05 -46.74 134.07 o 30 2 1 3204.87 2852.94 219.22 o 32 2 1 53.19 53.06 272.64 o 34 2 1 464.60 0.00 193.11 o -35 3 1 141.36 588.42 156.46 o -33 3 1 34.91 1064.79 182.50 o -31 3 1 100.03 463.12 138.92 o -29 3 1 970.16 611.83 91.74 o -27 3 1 95.09 1571.63 101.00 o -25 3 1 70.42 4692.36 184.96 o -23 3 1 3736.92 11695.59 340.28 o -21 3 1 502.25 1611.75 103.62 o -19 3 1 22.53 30.23 88.88 o -17 3 1 820.88 0.00 123.37 o -15 3 1 1043.57 2911.27 120.60 o -13 3 1 4866.58 4758.27 128.68 o -11 3 1 143.29 9914.49 265.39 o -9 3 1 351.02 8923.66 216.28 o -7 3 1 4116.52 3039.41 148.64 o -5 3 1 1448.68 213.69 213.69 o -3 3 1 85.19 1572.50 75.18 o 1 3 1 237.44 0.00 211.59 o 3 3 1 32.98 1695.73 80.09 o 5 3 1 23555.35 81044.45 1976.35 o 7 3 1 1447.45 2246.29 105.80 o 9 3 1 3886.70 6829.56 245.23 o 11 3 1 6315.60 45017.59 1132.04 o 13 3 1 952.43 0.00 106.32 o 15 3 1 9.64 715.24 106.32 o 17 3 1 155.57 0.00 103.62 o 19 3 1 370.57 42.91 142.38 o 21 3 1 1471.07 2879.20 142.15 o 23 3 1 160.76 1814.58 110.24 o 25 3 1 1141.40 0.00 87.24 o 27 3 1 375.66 682.87 161.30 o 29 3 1 20.02 1952.51 250.34 o 31 3 1 590.98 3252.04 398.42 o 33 3 1 35.01 9.02 188.37 o -34 4 1 0.37 359.71 215.60 o -32 4 1 621.73 142.19 110.27 o -30 4 1 2695.82 1187.96 367.40 o -28 4 1 179.80 96.51 117.55 o -26 4 1 2215.46 -94.98 110.27 o -24 4 1 91.01 3899.38 192.78 o -22 4 1 111.96 248.60 87.24 o -20 4 1 7379.00 6175.81 233.78 o -18 4 1 796.61 3264.90 97.97 o -16 4 1 626.27 -71.23 234.06 o -14 4 1 896.74 8700.63 237.55 o -12 4 1 7275.95 54452.68 1143.72 o -10 4 1 503.49 1635.04 95.37 o -8 4 1 2.73 585.54 106.84 o -6 4 1 2884.73 1850.09 85.40 o -4 4 1 1060.08 43274.86 801.12 o -2 4 1 5470.90 45256.08 780.36 o 0 4 1 1836.22 4735.76 88.88 o 2 4 1 362.32 11839.97 228.23 o 4 4 1 7534.26 11712.20 240.81 o 6 4 1 11483.57 1964.61 94.63 o 8 4 1 1457.74 793.62 122.77 o 10 4 1 905.77 477.91 105.80 o 12 4 1 1420.36 212.12 105.80 o 14 4 1 806.87 3675.62 212.64 o 16 4 1 1059.13 6683.21 276.38 o 18 4 1 6029.39 14014.90 515.54 o 20 4 1 298.19 2078.98 91.08 o 22 4 1 2246.05 981.21 131.76 o 24 4 1 527.55 10798.08 403.95 o 26 4 1 307.70 47.64 110.24 o 28 4 1 1388.74 12239.33 447.70 o 30 4 1 3816.37 9328.99 377.09 o 32 4 1 1.68 792.97 192.04 o -33 5 1 31.63 -161.30 161.30 o -31 5 1 188.68 1684.52 137.15 o -29 5 1 1264.19 15111.38 714.06 o -27 5 1 2072.42 7982.34 326.12 o -25 5 1 118.66 255.59 142.46 o -23 5 1 981.21 7242.48 288.07 o -21 5 1 140.13 3150.17 123.17 o -19 5 1 6080.14 12797.79 384.81 o -17 5 1 2746.16 170.78 142.38 o -15 5 1 38.99 9303.19 248.83 o -13 5 1 804.99 0.00 123.37 o -11 5 1 56.41 354.75 123.37 o -9 5 1 7293.38 142.46 123.37 o -7 5 1 7156.48 372.90 106.84 o -5 5 1 2167.11 1817.85 80.91 o -3 5 1 194.22 8486.22 150.54 o -1 5 1 805.65 79.74 75.18 o 1 5 1 700.61 9374.42 186.30 o 3 5 1 1917.18 4165.83 106.19 o 5 5 1 7091.01 35936.16 651.37 o 7 5 1 1644.91 30365.72 622.16 o 9 5 1 728.14 2762.60 183.36 o 11 5 1 3446.84 11353.50 348.14 o 13 5 1 2159.53 4636.22 212.64 o 15 5 1 528.66 26286.64 880.38 o 17 5 1 1220.13 170.45 161.19 o 19 5 1 0.20 212.99 245.53 o 21 5 1 3828.12 8849.50 491.07 o 23 5 1 1893.39 5112.24 399.01 o 25 5 1 576.27 912.17 309.67 o 27 5 1 737.81 53.36 338.01 o 29 5 1 4.41 291.76 282.32 o 31 5 1 679.13 -398.21 398.21 o -32 6 1 18.53 211.59 353.67 o -30 6 1 233.55 425.28 451.82 o -28 6 1 251.83 -266.62 272.64 o -26 6 1 880.92 923.65 245.94 o -24 6 1 73.29 142.34 267.66 o -22 6 1 8.71 348.99 182.95 o -20 6 1 669.94 5156.69 368.91 o -18 6 1 169.51 1194.22 281.48 o -16 6 1 947.47 553.57 142.38 o -14 6 1 825.43 497.21 133.65 o -12 6 1 175.65 71.23 123.37 o -10 6 1 123.93 213.69 106.84 o -8 6 1 1828.21 1064.61 96.09 o -6 6 1 1122.09 4278.22 106.25 o -4 6 1 103.07 2507.34 94.36 o -2 6 1 628.06 837.09 75.18 o 0 6 1 1163.41 5037.37 106.22 o 2 6 1 3232.08 8137.08 175.48 o 4 6 1 109.10 1640.67 80.31 o 6 6 1 139.57 0.00 106.32 o 8 6 1 112.60 2143.43 109.80 o 10 6 1 203.28 1640.32 160.29 o 12 6 1 1731.30 1636.84 171.86 o 14 6 1 248.37 2299.20 212.64 o 16 6 1 470.42 1030.35 161.19 o 18 6 1 743.13 183.03 118.49 o 20 6 1 876.95 425.28 245.53 o 22 6 1 41.73 53.55 174.19 o 24 6 1 0.02 212.29 245.53 o 26 6 1 1086.98 709.50 368.91 o 28 6 1 105.32 0.00 245.53 o 30 6 1 380.65 212.64 450.34 o -29 7 1 547.53 -319.48 319.48 o -27 7 1 428.88 212.64 451.82 o -25 7 1 397.63 937.34 283.60 o -23 7 1 355.22 71.23 246.74 o -21 7 1 2220.31 1122.66 415.22 o -19 7 1 2445.05 0.00 174.33 o -17 7 1 1635.37 7192.12 438.52 o -15 7 1 873.89 709.96 245.94 o -13 7 1 574.74 2415.73 128.74 o -11 7 1 787.51 160.33 174.33 o -9 7 1 823.21 106.32 106.32 o -7 7 1 2689.55 5357.85 167.58 o -5 7 1 21.67 106.14 86.66 o -3 7 1 736.44 486.72 80.31 o -1 7 1 1.99 70.53 86.81 o 1 7 1 109.20 243.33 80.31 o 3 7 1 159.48 924.50 103.40 o 5 7 1 3217.08 4692.15 161.08 o 7 7 1 3555.05 12455.13 327.28 o 9 7 1 206.72 106.32 106.32 o 11 7 1 291.36 1308.82 135.01 o 13 7 1 57.10 318.78 133.95 o 15 7 1 281.05 6467.31 338.44 o 17 7 1 1343.81 3746.22 319.48 o 19 7 1 201.69 142.46 267.63 o 21 7 1 1128.31 6842.60 523.61 o 23 7 1 108.34 -106.97 272.09 o 25 7 1 537.26 0.00 300.72 o 27 7 1 477.89 850.56 510.87 o 29 7 1 17.71 213.69 354.03 o -28 8 1 670.02 -212.64 640.01 o -26 8 1 459.94 1385.82 451.82 o -24 8 1 842.23 213.69 302.20 o -22 8 1 64.30 426.33 451.82 o -20 8 1 18.61 213.69 273.19 o -18 8 1 1.07 1934.74 245.94 o -16 8 1 4.60 852.88 245.94 o -14 8 1 265.77 923.64 245.94 o -12 8 1 1133.80 794.12 121.73 o -10 8 1 138.56 426.15 90.75 o -8 8 1 304.97 703.45 80.31 o -6 8 1 488.55 30.35 80.31 o -4 8 1 3985.81 2130.34 113.89 o -2 8 1 57.58 242.84 80.31 o 0 8 1 413.86 1115.08 90.46 o 2 8 1 101.83 859.78 80.31 o 4 8 1 54.17 657.12 80.31 o 6 8 1 1798.86 3905.85 166.09 o 8 8 1 3085.24 1925.91 213.16 o 10 8 1 1008.23 2140.82 192.71 o 12 8 1 33.41 531.60 212.64 o 14 8 1 216.30 128.38 160.29 o 16 8 1 0.05 -151.56 215.12 o 18 8 1 164.49 1709.78 272.09 o 20 8 1 63.87 1064.24 850.56 o 22 8 1 187.66 -354.03 354.03 o 24 8 1 110.58 469.02 354.03 o 26 8 1 0.37 105.80 319.48 o -25 9 1 45.05 0.00 355.24 o -23 9 1 679.87 0.00 427.37 o -21 9 1 153.50 0.00 852.65 o -19 9 1 4.08 212.64 451.82 o -17 9 1 95.41 1533.01 354.03 o -15 9 1 79.47 80.23 272.25 o -13 9 1 10.53 471.50 168.09 o -11 9 1 276.28 270.61 92.91 o -9 9 1 104.52 6253.29 244.92 o -7 9 1 301.67 493.51 84.94 o -5 9 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