#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:53:26 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180928 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/08/2200815.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200815_Fobs loop_ _publ_author_name 'Lee, Uk' 'Joo, Hea-Chung' 'Kwon, Jae-Sam' _publ_section_title ; Tetraammonium hexahydrogen hexamolybdonickelate(II) tetrahydrate, (NH~4~)~4~[H~6~NiMo~6~O~24~]·4H~2~O ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first i6 _journal_page_last i8 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yab' _symmetry_space_group_name_H-M 'P 1 21/a 1' _cell_angle_alpha 90.000 _cell_angle_beta 109.310 _cell_angle_gamma 90.000 _cell_length_a 11.9940 _cell_length_b 11.1310 _cell_length_c 11.3840 _exptl_crystal_F_000 1124.00 _reflns_d_resolution_high 0.7678 _cod_data_source_file br6038Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' NiMo6' _shelx_refln_list_code 4 _shelx_f_calc_maximum 481.73 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z' '-x, -y, -z' 'x-1/2, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 69375.85 66588.49 267.36 o 4 0 0 6751.13 6689.17 125.93 o 6 0 0 1642.01 1813.90 90.28 o 8 0 0 584.42 1022.46 89.12 o 10 0 0 2409.49 2544.00 136.81 o 12 0 0 96.73 96.30 80.32 o 14 0 0 1204.87 1654.64 162.04 o 1 1 0 56016.26 49993.22 200.93 o 2 1 0 80356.37 74491.80 302.09 o 3 1 0 793.87 690.75 67.13 o 4 1 0 7105.30 7008.39 129.40 o 5 1 0 11.99 60.42 53.24 o 6 1 0 657.79 517.83 64.58 o 7 1 0 1640.17 1711.82 94.45 o 8 1 0 16837.60 18136.49 281.95 o 9 1 0 3389.01 3486.14 145.37 o 10 1 0 1368.67 1387.51 119.21 o 11 1 0 3276.14 3277.57 164.82 o 12 1 0 3386.70 3388.22 174.08 o 13 1 0 1046.91 1434.27 127.08 o 14 1 0 1837.66 2185.67 169.68 o 0 2 0 6936.88 5381.99 83.33 o 1 2 0 601.05 1076.86 55.79 o 2 2 0 100.54 60.65 53.70 o 3 2 0 1225.10 1145.61 67.59 o 4 2 0 600.44 465.98 61.11 o 5 2 0 39.54 1.39 54.86 o 6 2 0 7858.19 7725.29 163.89 o 7 2 0 811.42 1040.52 88.66 o 8 2 0 598.27 695.14 83.10 o 9 2 0 1006.68 1028.02 96.76 o 10 2 0 28645.55 26941.88 399.54 o 11 2 0 288.33 255.33 82.64 o 12 2 0 12291.63 12465.14 311.35 o 13 2 0 1085.08 1190.06 127.78 o 14 2 0 35.75 -2.55 89.12 o 1 3 0 18025.33 17020.97 170.37 o 2 3 0 40875.93 40464.44 273.61 o 3 3 0 3474.65 3470.63 99.54 o 4 3 0 2317.97 2366.45 90.51 o 5 3 0 3496.48 3101.18 109.95 o 6 3 0 25.30 -1.62 49.31 o 7 3 0 3009.62 3082.43 124.08 o 8 3 0 11058.63 12121.39 240.97 o 9 3 0 1952.91 2519.00 130.33 o 10 3 0 489.77 371.76 81.48 o 11 3 0 7298.21 8266.73 244.21 o 12 3 0 1858.08 1948.16 152.78 o 13 3 0 773.98 672.23 113.89 o 14 3 0 643.50 776.86 122.22 o 0 4 0 94519.34 89218.06 429.86 o 1 4 0 2683.14 3238.68 97.45 o 3 4 0 14.85 93.52 52.32 o 5 4 0 424.52 269.22 62.27 o 6 4 0 746.53 742.83 76.85 o 7 4 0 301.61 373.61 68.98 o 8 4 0 36.05 -15.05 66.44 o 9 4 0 228.72 230.79 76.62 o 10 4 0 2455.95 1893.30 135.42 o 11 4 0 65.51 -77.78 77.78 o 12 4 0 27.93 -80.09 80.09 o 13 4 0 205.80 104.86 93.06 o 14 4 0 753.95 608.11 122.45 o 1 5 0 2253.19 1635.66 80.09 o 3 5 0 189.14 114.58 56.71 o 5 5 0 3542.76 3252.57 122.22 o 6 5 0 700.46 532.18 74.07 o 7 5 0 61.58 73.38 60.65 o 8 5 0 6312.07 5500.97 181.95 o 9 5 0 608.62 484.26 86.81 o 10 5 0 808.34 837.97 102.08 o 11 5 0 394.17 156.48 96.76 o 12 5 0 2810.43 2061.36 160.19 o 13 5 0 1752.66 1171.31 130.79 o 0 6 0 3671.55 3819.24 119.21 o 1 6 0 1009.19 1178.02 79.63 o 2 6 0 1395.72 1248.16 81.95 o 3 6 0 5735.81 5910.23 153.24 o 4 6 0 341.64 132.87 60.42 o 5 6 0 19.94 -25.00 62.96 o 6 6 0 7698.22 8338.49 202.08 o 7 6 0 6.32 -11.34 65.28 o 8 6 0 115.24 180.79 78.47 o 9 6 0 386.02 200.46 84.95 o 10 6 0 15424.68 16650.13 348.15 o 11 6 0 628.90 820.15 107.87 o 12 6 0 9118.80 10141.75 301.85 o 13 6 0 147.37 272.46 98.15 o 1 7 0 702.82 830.33 77.32 o 2 7 0 14971.59 15111.93 244.45 o 3 7 0 1047.01 1025.01 91.44 o 4 7 0 628.07 648.15 78.47 o 5 7 0 853.24 727.55 83.57 o 6 7 0 140.14 286.81 72.92 o 7 7 0 105.44 71.07 72.22 o 8 7 0 8274.83 9145.44 248.15 o 9 7 0 3746.48 3989.61 182.18 o 10 7 0 1358.10 1447.00 137.50 o 11 7 0 8405.61 9172.76 278.94 o 12 7 0 3646.85 4050.73 210.65 o 0 8 0 51507.22 49645.99 461.81 o 1 8 0 533.20 604.40 77.55 o 2 8 0 11134.72 10842.91 225.93 o 3 8 0 3060.39 3035.90 134.03 o 5 8 0 0.09 120.83 64.58 o 6 8 0 124.28 205.09 71.07 o 7 8 0 1482.09 1456.49 123.84 o 8 8 0 377.02 373.15 88.20 o 10 8 0 126.52 111.57 90.97 o 11 8 0 84.45 139.35 88.43 o 12 8 0 10.67 -85.65 85.65 o 1 9 0 46766.36 44086.00 472.92 o 2 9 0 6447.50 6391.02 189.12 o 3 9 0 92.61 -64.12 68.29 o 4 9 0 363.01 206.02 74.77 o 6 9 0 10.27 -66.67 66.67 o 7 9 0 41.94 154.40 76.16 o 8 9 0 734.85 544.68 97.45 o 9 9 0 12.69 51.62 76.85 o 10 9 0 386.33 281.72 97.22 o 11 9 0 24.59 222.46 89.35 o 0 10 0 1047.44 880.56 103.47 o 1 10 0 4779.06 4442.40 173.38 o 2 10 0 742.79 773.39 94.21 o 3 10 0 4414.44 4441.01 177.55 o 4 10 0 1001.65 1060.89 109.72 o 5 10 0 13.90 -74.54 74.54 o 6 10 0 1020.83 1091.44 117.36 o 7 10 0 516.57 587.04 98.15 o 8 10 0 9.04 209.03 83.10 o 9 10 0 1021.91 1072.69 123.84 o 10 10 0 7741.38 8038.49 289.59 o 1 11 0 2.06 -13.89 71.53 o 2 11 0 1984.19 2116.68 140.74 o 3 11 0 234.97 -8.56 80.79 o 4 11 0 468.34 693.29 95.83 o 5 11 0 182.03 66.67 86.57 o 6 11 0 80.60 -34.26 76.16 o 7 11 0 554.37 578.71 102.08 o 8 11 0 922.73 1101.63 123.61 o 9 11 0 3166.79 3373.17 196.53 o 0 12 0 13773.41 14518.63 331.02 o 1 12 0 927.00 787.04 111.34 o 2 12 0 4079.47 3336.37 178.24 o 3 12 0 1591.32 1243.30 128.01 o 4 12 0 640.52 618.75 102.32 o 5 12 0 0.16 -22.22 81.95 o 6 12 0 387.39 329.63 96.76 o 7 12 0 1045.49 777.32 121.76 o 8 12 0 1.63 0.00 90.97 o 1 13 0 10717.08 10649.62 307.87 o 2 13 0 2733.86 2947.01 174.77 o 3 13 0 13.66 29.63 79.86 o 4 13 0 378.72 422.69 103.01 o 5 13 0 328.49 31.48 105.09 o 6 13 0 4.36 218.75 96.76 o 0 14 0 500.99 442.13 107.87 o 1 14 0 1972.17 1872.70 165.05 o 2 14 0 12.52 143.75 96.07 o 3 14 0 2768.52 2065.29 181.95 o -14 0 1 5268.81 5369.02 232.64 o -12 0 1 548.36 600.24 100.70 o -10 0 1 8487.18 8445.90 221.76 o -8 0 1 255.59 68.75 65.97 o -6 0 1 3372.20 3557.44 112.96 o -4 0 1 805.98 1529.18 73.84 o -2 0 1 82623.69 77355.94 291.21 o 0 0 1 53396.33 49328.86 209.49 o 2 0 1 12708.95 11242.45 131.48 o 4 0 1 640.99 449.54 62.96 o 6 0 1 78527.73 77684.41 510.19 o 8 0 1 17820.36 18110.79 291.67 o 10 0 1 1054.06 934.50 100.93 o 12 0 1 1132.31 1021.54 124.08 o 14 0 1 358.28 472.92 106.48 o -15 1 1 2264.22 2571.55 194.21 o -14 1 1 6333.74 7154.22 264.12 o -13 1 1 1838.61 2143.54 163.89 o -12 1 1 3396.54 3171.78 164.58 o -11 1 1 0.89 36.81 73.15 o -10 1 1 6.40 123.15 70.37 o -9 1 1 3034.68 3112.52 134.72 o -8 1 1 1402.44 1330.80 99.07 o -7 1 1 74.25 96.53 60.65 o -6 1 1 3418.06 2887.52 103.94 o -5 1 1 1546.68 1773.16 81.25 o -4 1 1 14821.43 12841.07 164.58 o -3 1 1 42217.77 44978.60 262.73 o -2 1 1 74014.92 68407.72 288.20 o -1 1 1 13667.57 13225.57 117.83 o 0 1 1 6.99 32.41 37.96 o 1 1 1 5614.14 4693.09 80.32 o 2 1 1 143.42 0.69 53.70 o 3 1 1 2369.75 2993.77 90.51 o 4 1 1 9066.33 9567.67 156.02 o 5 1 1 1818.76 1771.08 89.12 o 6 1 1 4317.71 4696.33 134.95 o 7 1 1 11744.68 11224.86 214.82 o 8 1 1 32158.97 36364.41 411.35 o 9 1 1 9759.51 10543.37 244.21 o 10 1 1 1555.13 1964.83 127.78 o 11 1 1 67.09 102.78 84.95 o 12 1 1 126.71 -9.49 89.58 o 13 1 1 238.32 195.14 99.54 o 14 1 1 364.71 381.02 103.70 o -14 2 1 205.87 244.91 92.13 o -13 2 1 774.56 826.40 111.81 o -12 2 1 6283.30 6510.70 227.32 o -11 2 1 88.25 72.69 81.71 o -10 2 1 198.79 221.53 76.85 o -9 2 1 19.26 -50.23 61.81 o -8 2 1 189.49 303.24 67.59 o -7 2 1 704.52 804.17 79.40 o -6 2 1 36953.33 36651.21 337.27 o -5 2 1 12349.66 13526.50 192.59 o -4 2 1 50065.26 45160.77 310.88 o -3 2 1 437.48 259.96 57.41 o -2 2 1 2887.16 2351.64 80.32 o -1 2 1 928.25 846.07 75.23 o 0 2 1 40803.11 39198.00 221.30 o 1 2 1 559.53 250.46 55.32 o 2 2 1 3565.26 2606.27 86.34 o 3 2 1 87.05 10.88 54.17 o 4 2 1 8659.43 8499.14 151.85 o 5 2 1 6.33 -51.62 51.62 o 6 2 1 4984.96 4895.18 141.20 o 7 2 1 294.95 155.33 62.73 o 8 2 1 12943.95 12460.51 248.38 o 9 2 1 193.32 159.26 70.60 o 10 2 1 12328.14 11066.75 268.75 o 11 2 1 27.68 134.72 81.02 o 12 2 1 3.39 205.79 82.87 o 13 2 1 46.68 111.81 83.33 o 14 2 1 0.79 231.95 100.23 o -14 3 1 2464.10 2416.92 183.33 o -13 3 1 325.01 178.01 95.37 o -12 3 1 2201.04 2486.83 155.09 o -11 3 1 112.74 -33.10 78.47 o -10 3 1 543.66 503.24 83.80 o -9 3 1 2154.81 2448.40 126.16 o -8 3 1 414.23 477.78 75.93 o -7 3 1 3.55 6.48 57.87 o -6 3 1 243.49 157.87 58.57 o -5 3 1 37749.86 37441.27 328.71 o -4 3 1 36831.14 37813.03 302.78 o -3 3 1 66676.04 73488.54 396.07 o -2 3 1 63123.67 60565.75 415.28 o -1 3 1 346.77 105.09 59.49 o 0 3 1 130.82 -42.36 56.71 o 1 3 1 8826.66 9156.32 134.49 o 2 3 1 2.62 -52.08 52.08 o 3 3 1 8744.85 8638.49 149.77 o 5 3 1 235.30 414.36 62.73 o 6 3 1 2831.38 2659.05 113.43 o 7 3 1 6228.02 6055.37 172.92 o 8 3 1 21290.07 20752.94 322.22 o 9 3 1 4703.83 5114.86 177.78 o 10 3 1 267.50 258.80 81.71 o 11 3 1 588.79 467.60 99.77 o 12 3 1 137.51 192.36 85.88 o 13 3 1 423.10 498.15 111.11 o 14 3 1 434.45 631.02 115.97 o -14 4 1 3890.82 4083.83 210.88 o -13 4 1 404.22 227.09 102.32 o -12 4 1 1423.89 1149.78 128.01 o -11 4 1 9.65 60.88 77.08 o -10 4 1 4318.44 4691.47 178.71 o -9 4 1 26.54 -63.19 63.19 o -8 4 1 356.43 434.73 75.70 o -7 4 1 209.79 336.58 67.13 o -6 4 1 4981.02 4900.96 143.29 o -5 4 1 430.07 235.19 59.26 o -4 4 1 451.16 438.43 62.96 o -3 4 1 10458.76 10763.74 179.17 o -2 4 1 18079.54 16586.94 208.33 o -1 4 1 641.89 1364.59 78.47 o 0 4 1 16861.07 15699.43 187.73 o 1 4 1 4.33 -15.51 54.17 o 2 4 1 811.72 532.64 65.28 o 3 4 1 69.07 -26.16 54.63 o 4 4 1 3479.99 3417.16 113.43 o 5 4 1 1464.14 1435.43 86.34 o 6 4 1 48719.43 50021.23 449.77 o 7 4 1 68.27 -62.96 62.96 o 8 4 1 1384.51 1369.46 113.43 o 9 4 1 3.67 -6.71 69.68 o 10 4 1 1657.90 1788.44 139.12 o 11 4 1 225.26 418.52 90.74 o 12 4 1 671.12 508.80 106.71 o 13 4 1 53.78 -79.40 79.40 o -14 5 1 3663.32 3528.73 204.17 o -13 5 1 1214.43 1378.95 135.42 o -12 5 1 1910.38 1960.20 159.72 o -11 5 1 1282.10 1234.04 119.21 o -10 5 1 119.18 53.47 74.77 o -9 5 1 1109.32 1399.55 117.13 o -8 5 1 350.51 332.18 75.00 o -7 5 1 412.38 525.00 75.23 o -6 5 1 269.85 367.13 69.68 o -5 5 1 795.21 654.40 74.07 o -4 5 1 20809.46 21132.57 265.74 o -3 5 1 18665.93 20537.89 277.55 o -2 5 1 18198.77 17616.34 225.93 o -1 5 1 2190.37 2038.67 92.82 o 0 5 1 62.24 78.01 53.47 o 1 5 1 25.75 -53.24 53.24 o 2 5 1 323.95 353.94 61.57 o 3 5 1 2660.53 2607.43 104.63 o 4 5 1 4133.63 4027.35 130.09 o 5 5 1 9873.44 9732.72 201.62 o 6 5 1 2631.41 2740.76 121.76 o 7 5 1 4511.71 4687.77 162.96 o 8 5 1 9031.94 9560.49 234.96 o 9 5 1 524.84 598.85 90.05 o 10 5 1 125.32 151.39 90.05 o 11 5 1 1.26 141.20 80.79 o 12 5 1 13.79 207.18 88.20 o 13 5 1 543.76 610.19 109.95 o -13 6 1 837.43 751.86 121.53 o -12 6 1 2220.95 2463.68 164.82 o -11 6 1 244.85 333.10 93.75 o -10 6 1 65.58 80.79 72.45 o -9 6 1 102.35 230.09 75.23 o -8 6 1 655.32 695.38 90.05 o -7 6 1 97.72 121.30 67.59 o -6 6 1 18833.68 18961.72 293.98 o -5 6 1 357.54 304.86 69.44 o -4 6 1 77138.69 76294.59 646.53 o -3 6 1 10581.91 10382.49 200.23 o -2 6 1 1088.58 1202.56 82.41 o -1 6 1 175.70 67.82 54.40 o 0 6 1 10399.23 10798.70 189.82 o 1 6 1 9.29 108.10 50.69 o 2 6 1 4049.62 3804.89 122.69 o 3 6 1 727.32 674.08 75.46 o 4 6 1 7077.94 6603.99 168.52 o 5 6 1 735.84 754.64 81.71 o 6 6 1 1187.24 1000.24 94.45 o 7 6 1 1337.53 1436.59 113.20 o 8 6 1 3451.92 3314.84 152.32 o 9 6 1 450.22 245.84 86.57 o 10 6 1 7647.58 6592.88 233.10 o 11 6 1 0.00 -71.30 71.30 o 12 6 1 0.80 121.99 82.64 o 13 6 1 77.47 28.01 93.06 o -13 7 1 323.87 229.63 112.04 o -12 7 1 2065.18 2326.64 174.77 o -11 7 1 515.86 651.16 102.78 o -10 7 1 296.64 -52.78 83.80 o -9 7 1 556.22 812.51 100.93 o -8 7 1 780.09 774.31 96.99 o -7 7 1 200.75 238.20 75.00 o -6 7 1 7821.32 7690.57 205.79 o -5 7 1 23670.04 23614.77 336.81 o -4 7 1 1652.85 1563.44 106.25 o -3 7 1 14231.67 13917.24 242.59 o -2 7 1 26995.97 25722.89 317.60 o -1 7 1 32.93 77.32 58.10 o 0 7 1 18.33 30.09 54.40 o 1 7 1 483.51 572.00 73.38 o 2 7 1 15.74 77.55 58.57 o 4 7 1 1645.89 1588.67 103.01 o 5 7 1 837.10 669.22 89.58 o 6 7 1 2660.09 2450.25 130.33 o 7 7 1 3017.36 2754.65 143.29 o 8 7 1 8857.37 7599.60 231.95 o 9 7 1 4945.84 3823.64 181.02 o 10 7 1 407.75 120.83 90.05 o 11 7 1 663.95 341.21 106.25 o 12 7 1 713.21 465.51 108.57 o -12 8 1 294.96 388.43 97.69 o -11 8 1 201.91 128.70 95.83 o -10 8 1 1597.96 1669.23 139.35 o -9 8 1 213.85 153.70 78.47 o -8 8 1 363.27 415.05 88.89 o -7 8 1 1395.94 1431.96 120.14 o -6 8 1 1733.20 1583.58 121.99 o -5 8 1 406.99 403.94 83.10 o -4 8 1 342.88 509.73 78.70 o -3 8 1 7830.44 7844.51 200.46 o -2 8 1 17506.01 17965.19 287.04 o -1 8 1 1759.05 1946.31 107.87 o 0 8 1 7015.53 7353.76 186.34 o 1 8 1 9.14 -12.96 61.81 o 2 8 1 1719.24 1886.13 110.19 o 3 8 1 2170.36 2189.60 116.90 o 4 8 1 1649.04 1697.47 112.73 o 5 8 1 187.95 134.49 73.84 o 6 8 1 18394.27 18447.83 334.26 o 7 8 1 2951.41 2987.99 155.79 o 8 8 1 5278.59 5407.91 211.11 o 9 8 1 1798.93 1950.48 154.86 o 10 8 1 123.11 54.17 91.67 o 11 8 1 61.02 131.25 84.26 o -11 9 1 1207.72 1309.27 139.58 o -10 9 1 40.81 29.86 88.43 o -9 9 1 1327.93 1538.44 140.51 o -8 9 1 37.79 160.19 81.02 o -7 9 1 33.12 -11.34 72.69 o -6 9 1 539.01 613.20 99.31 o -5 9 1 169.26 153.24 79.63 o -4 9 1 9313.95 9651.00 240.97 o -3 9 1 4089.92 4263.69 164.12 o -2 9 1 4172.22 4232.67 159.49 o -1 9 1 14996.54 15228.13 282.41 o 0 9 1 511.15 471.30 84.95 o 1 9 1 33.98 141.67 68.98 o 2 9 1 107.91 94.68 72.45 o 3 9 1 1574.00 1291.45 113.89 o 4 9 1 2299.62 2472.94 136.81 o 5 9 1 6185.98 6227.13 207.18 o 6 9 1 339.72 196.30 82.41 o 7 9 1 10784.49 10969.99 284.03 o 8 9 1 2808.43 3211.83 171.53 o 9 9 1 1122.57 1128.94 128.70 o 10 9 1 381.58 249.77 100.93 o 11 9 1 196.09 125.00 100.00 o -10 10 1 23.91 -91.44 91.44 o -9 10 1 104.04 225.93 89.82 o -8 10 1 394.49 407.87 96.07 o -7 10 1 588.26 545.14 98.84 o -6 10 1 5414.80 5353.28 204.40 o -5 10 1 2.49 85.42 77.08 o -4 10 1 17283.42 16894.58 330.10 o -3 10 1 7904.51 7553.99 230.56 o -2 10 1 918.67 1046.54 105.79 o -1 10 1 853.64 864.36 97.22 o 0 10 1 1424.11 1742.61 114.58 o 1 10 1 111.07 102.32 74.31 o 2 10 1 625.88 491.21 89.82 o 3 10 1 835.68 977.09 100.70 o 4 10 1 796.27 672.46 97.92 o 5 10 1 177.55 -5.09 79.40 o 6 10 1 348.28 177.55 93.29 o 7 10 1 3370.83 2859.98 169.21 o 8 10 1 3785.37 3556.28 187.73 o 9 10 1 2678.72 2281.27 180.33 o 10 10 1 3759.18 2712.75 188.43 o -9 11 1 95.92 16.90 76.16 o -8 11 1 717.48 508.80 110.65 o -7 11 1 577.22 712.27 107.41 o -6 11 1 268.47 166.21 100.46 o -5 11 1 10194.14 10452.63 286.58 o -4 11 1 3693.00 3733.83 176.62 o -3 11 1 4623.84 4546.33 191.44 o -2 11 1 4985.49 5123.42 193.52 o -1 11 1 464.77 471.30 91.67 o 0 11 1 106.87 119.45 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