#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/08/2200830.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200830_Fobs loop_ _publ_author_name 'Wieczorek, Wanda' 'Kruszynski, Rafal' 'Skoweranda, J. Jolanta' 'Pietrusiewicz, K. Micha\/l' _publ_section_title ; (2-Methoxyphenyl)phenylphosphine oxide ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o229 _journal_page_last o231 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.690 _cell_angle_gamma 90.000 _cell_length_a 8.5760 _cell_length_b 8.8040 _cell_length_c 15.9210 _exptl_crystal_F_000 488.00 _reflns_d_resolution_high 0.7976 _[local]_cod_data_source_file bt6101Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' LL in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 109.87 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 8.72 4.48 0.14 o 2 0 0 2606.53 2344.09 19.55 o 3 0 0 1159.91 1101.20 5.11 o 4 0 0 8.09 6.41 0.31 o 5 0 0 46.75 45.45 1.30 o 6 0 0 8.52 11.19 0.51 o 7 0 0 610.98 581.30 6.89 o 8 0 0 30.02 38.82 1.20 o 9 0 0 35.01 37.36 1.10 o 10 0 0 37.45 37.73 1.15 o 1 1 0 3651.08 3692.12 75.20 o 2 1 0 12070.55 13271.96 353.00 o 3 1 0 360.58 412.78 6.94 o 4 1 0 1218.90 1128.93 92.64 o 5 1 0 312.47 310.12 10.67 o 6 1 0 584.63 592.47 23.48 o 7 1 0 8.83 12.39 0.41 o 8 1 0 58.13 63.43 1.33 o 9 1 0 111.22 104.35 3.88 o 10 1 0 18.04 16.98 0.41 o 0 2 0 2227.15 1923.62 14.62 o 1 2 0 392.31 365.63 1.71 o 2 2 0 251.26 283.01 9.54 o 3 2 0 268.37 259.98 11.32 o 4 2 0 369.77 372.62 8.31 o 5 2 0 595.43 584.17 17.40 o 6 2 0 16.30 16.26 0.97 o 7 2 0 169.03 170.42 5.36 o 8 2 0 88.50 98.17 4.47 o 9 2 0 0.19 0.75 0.22 o 10 2 0 7.57 10.10 0.35 o 1 3 0 351.69 306.47 1.93 o 2 3 0 3.59 3.76 0.15 o 3 3 0 404.54 385.08 17.36 o 4 3 0 128.00 120.68 4.47 o 5 3 0 76.96 79.86 1.62 o 6 3 0 676.22 694.09 34.93 o 7 3 0 24.74 27.74 0.62 o 8 3 0 9.73 10.11 0.44 o 9 3 0 41.78 40.22 3.25 o 10 3 0 0.87 0.24 0.40 o 0 4 0 2672.47 2655.31 21.41 o 1 4 0 0.06 1.06 0.51 o 2 4 0 528.95 563.80 6.78 o 3 4 0 0.33 0.61 0.38 o 4 4 0 113.47 103.76 6.43 o 5 4 0 157.01 161.71 4.54 o 6 4 0 152.97 165.87 2.69 o 7 4 0 134.77 139.07 3.94 o 8 4 0 95.49 98.91 2.01 o 9 4 0 11.74 12.07 0.50 o 1 5 0 636.39 647.14 3.89 o 2 5 0 493.02 508.63 10.01 o 3 5 0 19.06 20.74 0.56 o 4 5 0 200.71 204.03 9.55 o 5 5 0 65.62 67.48 1.41 o 6 5 0 77.76 72.10 1.48 o 7 5 0 6.53 5.14 0.35 o 8 5 0 10.44 12.30 0.41 o 9 5 0 0.76 1.08 0.18 o 0 6 0 99.27 107.35 1.98 o 1 6 0 233.86 224.83 9.33 o 2 6 0 12.74 10.85 0.63 o 3 6 0 206.93 201.64 2.77 o 4 6 0 55.57 55.36 1.19 o 5 6 0 21.38 20.69 1.23 o 6 6 0 0.60 0.44 0.60 o 7 6 0 26.44 27.08 0.90 o 8 6 0 5.15 4.05 0.25 o 1 7 0 6.42 5.64 0.42 o 2 7 0 3.05 3.57 0.66 o 3 7 0 0.77 0.83 0.24 o 4 7 0 46.61 39.73 2.56 o 5 7 0 1.39 1.51 0.25 o 6 7 0 6.12 7.78 0.42 o 7 7 0 2.12 1.35 0.21 o 8 7 0 7.04 5.94 0.55 o 0 8 0 14.16 15.79 1.13 o 1 8 0 1.86 2.35 0.27 o 2 8 0 5.52 5.41 0.82 o 3 8 0 53.37 56.43 1.20 o 4 8 0 0.24 0.37 0.40 o 5 8 0 1.70 -0.16 0.43 o 6 8 0 1.29 1.67 0.28 o 7 8 0 0.00 -0.02 0.25 o 1 9 0 63.67 61.92 1.26 o 2 9 0 0.12 0.23 0.29 o 3 9 0 7.82 7.42 0.64 o 4 9 0 3.33 3.63 0.27 o 5 9 0 0.15 -0.13 0.32 o 6 9 0 0.01 0.06 0.15 o 0 10 0 20.39 20.44 0.70 o 1 10 0 4.74 3.39 0.40 o 2 10 0 2.55 2.78 0.22 o 3 10 0 4.86 4.86 0.24 o 4 10 0 0.81 0.20 0.14 o -10 1 1 2.98 2.75 0.22 o -9 1 1 7.18 7.42 0.42 o -8 1 1 0.27 -0.07 0.30 o -7 1 1 0.38 0.45 0.30 o -6 1 1 56.92 55.87 3.79 o -5 1 1 4.08 3.17 0.23 o -4 1 1 377.47 381.26 30.19 o -3 1 1 473.02 480.96 25.18 o -2 1 1 9360.35 9847.54 203.36 o -1 1 1 179.52 136.40 0.88 o 0 1 1 952.51 803.73 12.11 o 1 1 1 185.92 161.36 3.24 o 2 1 1 31.83 35.22 0.98 o 3 1 1 767.81 760.38 15.69 o 4 1 1 192.88 179.04 1.89 o 5 1 1 94.31 99.61 1.64 o 6 1 1 0.73 0.51 0.51 o 7 1 1 13.64 15.15 0.52 o 8 1 1 77.19 77.16 3.37 o 9 1 1 0.01 1.35 0.24 o 10 1 1 6.22 5.86 0.37 o -10 2 1 1.03 0.96 0.18 o -9 2 1 18.17 20.61 1.72 o -8 2 1 20.48 17.56 1.37 o -7 2 1 0.62 1.11 0.27 o -6 2 1 107.37 100.42 3.05 o -5 2 1 35.70 38.22 1.10 o -4 2 1 41.03 48.59 0.96 o -3 2 1 815.80 908.20 34.47 o -2 2 1 108.83 119.52 2.39 o -1 2 1 33.62 50.06 17.78 o 0 2 1 6184.74 6047.14 43.87 o 1 2 1 85.40 69.00 0.80 o 2 2 1 897.84 855.19 37.52 o 3 2 1 247.96 268.20 2.08 o 4 2 1 156.96 158.56 4.71 o 5 2 1 0.43 1.82 0.71 o 6 2 1 63.96 66.61 1.38 o 7 2 1 3.57 1.91 0.29 o 8 2 1 0.32 1.68 0.25 o 9 2 1 0.18 0.78 0.23 o 10 2 1 7.27 7.33 1.05 o -10 3 1 42.79 37.51 2.01 o -9 3 1 3.28 2.81 0.25 o -8 3 1 139.03 150.49 2.59 o -7 3 1 7.89 7.29 0.37 o -6 3 1 9.60 9.40 0.36 o -5 3 1 13.18 11.54 0.60 o -4 3 1 253.86 259.23 8.74 o -3 3 1 32.26 50.63 2.38 o -2 3 1 1559.12 1603.99 23.17 o -1 3 1 952.11 871.60 25.60 o 0 3 1 540.88 491.77 5.13 o 1 3 1 2.94 7.63 2.17 o 2 3 1 304.44 261.81 9.65 o 3 3 1 7.18 8.01 0.30 o 4 3 1 287.41 284.23 4.35 o 5 3 1 2.18 7.56 1.80 o 6 3 1 151.20 160.16 2.85 o 7 3 1 24.10 23.37 0.54 o 8 3 1 1.02 3.27 0.99 o 9 3 1 87.38 90.34 5.15 o 10 3 1 0.00 -0.24 0.24 o -10 4 1 1.26 0.13 2.12 o -9 4 1 29.55 35.07 1.25 o -8 4 1 3.57 2.00 0.29 o -7 4 1 4.21 5.53 0.35 o -6 4 1 645.75 656.86 22.27 o -5 4 1 193.93 168.98 10.92 o -4 4 1 243.26 235.59 19.21 o -3 4 1 73.17 81.33 4.80 o -2 4 1 110.12 82.32 1.68 o -1 4 1 595.36 642.22 4.29 o 0 4 1 84.01 80.88 1.02 o 1 4 1 400.00 391.60 3.61 o 2 4 1 576.82 603.40 17.52 o 3 4 1 4.55 10.48 0.43 o 4 4 1 7.88 6.03 0.27 o 5 4 1 778.46 799.18 26.46 o 6 4 1 38.54 38.17 1.86 o 7 4 1 75.87 78.52 3.04 o 8 4 1 167.90 169.80 12.22 o 9 4 1 0.49 0.80 0.18 o -9 5 1 1.29 1.32 0.18 o -8 5 1 5.75 5.83 0.38 o -7 5 1 21.91 26.58 0.73 o -6 5 1 3.86 4.61 0.38 o -5 5 1 430.47 444.75 23.46 o -4 5 1 160.28 154.46 9.54 o -3 5 1 240.00 237.07 6.83 o -2 5 1 0.02 0.52 0.17 o -1 5 1 193.57 176.88 3.96 o 0 5 1 19.85 26.53 0.65 o 1 5 1 8.08 7.60 0.32 o 2 5 1 22.49 29.31 1.49 o 3 5 1 84.22 86.89 1.79 o 4 5 1 403.43 381.21 27.30 o 5 5 1 1.99 3.51 1.47 o 6 5 1 585.82 598.48 24.40 o 7 5 1 73.72 80.80 3.92 o 8 5 1 2.95 3.21 0.48 o 9 5 1 39.17 36.18 4.84 o -9 6 1 43.30 32.90 8.01 o -8 6 1 2.23 3.28 0.55 o -7 6 1 14.70 15.60 0.46 o -6 6 1 0.37 1.98 0.43 o -5 6 1 5.17 5.57 0.57 o -4 6 1 1.86 1.05 0.61 o -3 6 1 6.56 4.63 0.28 o -2 6 1 143.52 140.10 4.93 o -1 6 1 34.25 32.35 0.67 o 0 6 1 205.19 199.88 2.79 o 1 6 1 24.76 23.32 1.05 o 2 6 1 57.83 61.66 1.61 o 3 6 1 43.03 43.24 1.59 o 4 6 1 6.60 9.92 1.81 o 5 6 1 334.21 344.13 21.12 o 6 6 1 0.08 0.80 0.23 o 7 6 1 17.09 16.16 1.18 o 8 6 1 53.71 53.96 5.70 o -8 7 1 29.67 29.36 1.85 o -7 7 1 29.33 31.08 0.94 o -6 7 1 7.89 7.86 0.40 o -5 7 1 12.05 13.19 0.68 o -4 7 1 39.94 35.24 0.74 o -3 7 1 0.35 0.82 0.44 o -2 7 1 0.14 -0.15 0.51 o -1 7 1 143.49 136.91 2.34 o 0 7 1 304.67 295.71 2.41 o 1 7 1 316.49 316.30 11.35 o 2 7 1 27.44 23.71 0.53 o 3 7 1 5.89 7.34 0.35 o 4 7 1 28.81 30.29 1.18 o 5 7 1 6.04 6.02 0.36 o 6 7 1 6.19 8.00 0.89 o 7 7 1 22.22 20.16 1.31 o 8 7 1 0.60 1.21 0.24 o -7 8 1 4.92 4.54 0.32 o -6 8 1 29.69 33.00 1.01 o -5 8 1 0.09 -0.18 0.36 o -4 8 1 30.42 30.40 0.64 o -3 8 1 6.96 4.98 0.33 o -2 8 1 107.22 106.05 2.23 o -1 8 1 5.76 4.86 1.26 o 0 8 1 38.47 38.21 0.74 o 1 8 1 76.95 79.12 2.00 o 2 8 1 0.11 -0.07 0.28 o 3 8 1 62.63 64.04 3.31 o 4 8 1 0.48 -0.41 0.42 o 5 8 1 37.26 39.53 0.98 o 6 8 1 2.36 2.64 0.21 o 7 8 1 9.85 10.26 0.46 o -6 9 1 0.98 1.17 0.29 o -5 9 1 28.43 29.30 0.64 o -4 9 1 0.64 0.74 0.42 o -3 9 1 21.83 24.39 0.54 o -2 9 1 0.12 0.65 0.29 o -1 9 1 54.42 54.15 1.12 o 0 9 1 4.39 4.24 0.22 o 1 9 1 5.31 7.41 1.02 o 2 9 1 43.48 39.25 1.51 o 3 9 1 1.99 3.88 0.29 o 4 9 1 24.61 24.85 1.62 o 5 9 1 6.42 5.95 0.77 o 6 9 1 57.36 55.56 3.52 o -4 10 1 5.57 6.37 0.24 o -3 10 1 10.12 10.16 0.31 o -2 10 1 37.51 32.17 0.67 o -1 10 1 1.09 2.09 1.08 o 0 10 1 3.74 3.29 0.22 o 1 10 1 26.42 25.70 0.56 o 2 10 1 8.18 7.70 0.31 o 3 10 1 15.03 16.62 0.66 o 4 10 1 1.38 1.82 0.22 o 0 11 1 5.16 3.25 0.70 o -10 0 2 33.51 23.58 0.74 o -9 0 2 137.61 146.94 3.47 o -8 0 2 230.85 221.41 4.46 o -7 0 2 3.09 3.85 0.44 o -6 0 2 48.42 38.13 1.15 o -5 0 2 147.16 146.91 2.74 o -4 0 2 3337.01 2920.29 33.34 o -3 0 2 12.52 8.40 0.30 o -2 0 2 405.00 379.37 2.46 o -1 0 2 7582.67 7873.64 31.58 o 0 0 2 1408.74 1326.90 12.31 o 1 0 2 50.12 49.98 0.80 o 2 0 2 44.43 58.20 1.06 o 3 0 2 284.98 269.40 2.72 o 4 0 2 1411.15 1491.65 7.74 o 5 0 2 235.40 251.96 3.69 o 6 0 2 45.92 46.33 1.45 o 7 0 2 34.61 49.62 1.50 o 8 0 2 13.56 18.41 0.69 o 9 0 2 17.95 22.91 0.76 o 10 0 2 60.24 58.28 1.67 o -10 1 2 89.72 78.92 2.00 o -9 1 2 34.83 35.77 0.79 o -8 1 2 13.71 18.30 0.86 o -7 1 2 338.77 329.46 3.71 o -6 1 2 34.12 34.62 1.10 o -5 1 2 283.61 299.11 2.76 o -4 1 2 2.66 8.95 4.64 o -3 1 2 2370.60 2315.91 30.00 o -2 1 2 5999.11 5962.37 79.14 o -1 1 2 4313.64 4191.49 17.05 o 0 1 2 6477.06 6534.29 275.99 o 1 1 2 38.91 31.04 4.13 o 2 1 2 1067.83 957.82 3.08 o 3 1 2 2609.78 2739.56 8.44 o 4 1 2 1012.27 1019.18 11.47 o 5 1 2 447.44 465.54 3.55 o 6 1 2 1.19 0.55 0.35 o 7 1 2 2.59 2.62 0.33 o 8 1 2 5.46 7.65 0.40 o 9 1 2 60.81 63.23 1.52 o 10 1 2 3.64 5.03 0.25 o -10 2 2 0.68 0.72 0.19 o -9 2 2 180.93 183.02 3.49 o -8 2 2 34.08 35.53 2.46 o -7 2 2 6.61 8.21 0.96 o -6 2 2 492.90 475.85 19.22 o -5 2 2 13.82 17.74 0.79 o -4 2 2 4594.64 4644.23 209.40 o -3 2 2 600.85 585.63 3.01 o -2 2 2 1809.94 1608.20 6.33 o -1 2 2 7784.90 7844.51 28.61 o 0 2 2 1879.78 1698.97 16.87 o 1 2 2 17.72 27.52 0.54 o 2 2 2 303.11 302.88 3.81 o 3 2 2 495.13 469.98 7.05 o 4 2 2 727.76 757.98 8.77 o 5 2 2 0.60 1.86 0.28 o 6 2 2 924.87 965.50 36.10 o 7 2 2 87.60 86.67 2.13 o 8 2 2 35.02 39.29 0.88 o 9 2 2 0.20 0.98 0.73 o 10 2 2 17.16 14.85 1.50 o -10 3 2 62.47 52.61 6.36 o -9 3 2 19.13 21.10 1.18 o -8 3 2 105.52 105.78 2.20 o -7 3 2 163.51 181.68 7.49 o -6 3 2 53.51 57.96 3.59 o -5 3 2 962.89 973.85 33.91 o -4 3 2 80.24 78.38 5.09 o -3 3 2 1748.93 1755.88 43.45 o -2 3 2 1387.00 1411.12 54.86 o -1 3 2 40.17 45.12 0.79 o 0 3 2 18.46 20.38 6.12 o 1 3 2 1.01 0.64 0.23 o 2 3 2 762.83 721.04 12.85 o 3 3 2 55.71 70.17 1.47 o 4 3 2 338.20 312.15 7.32 o 5 3 2 156.37 151.47 2.26 o 6 3 2 50.23 46.75 1.15 o 7 3 2 6.36 10.64 0.40 o 8 3 2 27.03 28.17 1.53 o 9 3 2 20.57 18.67 1.27 o 10 3 2 6.44 6.36 1.01 o -10 4 2 1.87 1.62 0.29 o -9 4 2 38.76 38.48 2.46 o -8 4 2 46.08 48.08 2.94 o -7 4 2 31.21 36.97 1.16 o -6 4 2 0.68 0.62 0.29 o -5 4 2 2.61 5.20 0.98 o -4 4 2 66.10 62.69 2.17 o -3 4 2 641.78 674.53 18.71 o -2 4 2 20.40 39.83 0.96 o -1 4 2 1465.30 1529.28 41.49 o 0 4 2 163.40 153.21 2.28 o 1 4 2 22.49 17.65 0.37 o 2 4 2 119.27 125.13 6.21 o 3 4 2 604.85 656.39 32.11 o 4 4 2 13.03 10.88 1.03 o 5 4 2 64.62 68.39 1.53 o 6 4 2 8.81 8.79 0.88 o 7 4 2 5.29 6.15 0.50 o 8 4 2 6.64 7.50 0.37 o 9 4 2 4.39 4.53 0.54 o -9 5 2 7.33 7.91 0.62 o -8 5 2 13.38 12.00 0.39 o -7 5 2 108.86 111.70 2.41 o -6 5 2 0.07 -0.22 0.55 o -5 5 2 34.26 37.87 2.46 o -4 5 2 0.24 1.27 0.25 o -3 5 2 336.91 375.42 5.84 o -2 5 2 4.32 3.23 0.21 o -1 5 2 348.71 406.70 4.41 o 0 5 2 436.60 444.89 4.92 o 1 5 2 2.75 3.30 0.20 o 2 5 2 120.05 112.94 1.77 o 3 5 2 23.41 23.18 0.61 o 4 5 2 3.50 4.22 0.41 o 5 5 2 27.24 26.70 0.59 o 6 5 2 43.09 45.21 2.78 o 7 5 2 70.23 68.36 2.16 o 8 5 2 0.20 0.29 0.21 o 9 5 2 14.98 13.06 1.67 o -9 6 2 0.01 0.48 0.16 o -8 6 2 7.19 7.87 0.31 o -7 6 2 0.40 0.67 0.45 o -6 6 2 5.80 4.19 0.32 o -5 6 2 14.98 12.38 0.42 o -4 6 2 34.62 36.85 1.85 o -3 6 2 106.88 112.90 2.10 o -2 6 2 340.88 330.37 3.37 o -1 6 2 24.29 28.95 0.62 o 0 6 2 114.27 111.97 2.56 o 1 6 2 13.69 18.11 0.54 o 2 6 2 112.20 113.28 4.01 o 3 6 2 21.41 23.86 1.74 o 4 6 2 290.11 291.95 10.80 o 5 6 2 0.46 0.32 0.28 o 6 6 2 59.78 61.44 2.46 o 7 6 2 4.85 4.49 0.31 o 8 6 2 20.45 21.72 1.23 o -8 7 2 0.89 1.41 0.16 o -7 7 2 2.63 2.61 0.25 o -6 7 2 7.73 6.82 0.36 o -5 7 2 1.83 2.05 0.29 o -4 7 2 0.51 0.03 0.50 o -3 7 2 18.37 19.98 0.49 o -2 7 2 1.05 1.19 0.25 o -1 7 2 4.80 4.14 0.30 o 0 7 2 0.04 0.03 0.44 o 1 7 2 0.54 0.55 0.35 o 2 7 2 194.99 179.36 2.77 o 3 7 2 0.18 2.44 1.50 o 4 7 2 38.97 37.27 1.67 o 5 7 2 4.25 4.65 0.59 o 6 7 2 0.46 0.40 0.29 o 7 7 2 0.74 0.62 0.18 o 8 7 2 0.02 -0.16 0.16 o -7 8 2 4.31 3.41 0.20 o -6 8 2 0.05 0.62 0.17 o -5 8 2 14.02 14.61 0.43 o -4 8 2 7.67 7.51 0.34 o -3 8 2 0.02 0.52 0.96 o -2 8 2 0.10 -0.31 0.46 o -1 8 2 17.09 17.28 0.64 o 0 8 2 2.00 1.49 0.21 o 1 8 2 0.07 0.54 0.45 o 2 8 2 24.23 26.23 1.29 o 3 8 2 39.90 38.51 1.84 o 4 8 2 47.54 45.94 2.35 o 5 8 2 5.20 5.44 0.37 o 6 8 2 0.22 0.63 0.18 o 7 8 2 1.66 1.23 0.21 o -6 9 2 0.44 0.22 0.14 o -5 9 2 1.82 1.26 0.20 o -4 9 2 0.70 0.86 0.26 o -3 9 2 2.20 2.31 0.25 o -2 9 2 0.70 0.88 0.24 o -1 9 2 12.68 12.56 0.62 o 0 9 2 52.84 54.20 1.33 o 1 9 2 1.94 1.24 0.25 o 2 9 2 0.85 0.93 0.25 o 3 9 2 6.69 5.85 0.31 o 4 9 2 0.02 -0.22 0.38 o 5 9 2 0.53 0.26 0.24 o 6 9 2 2.34 -0.57 0.57 o -4 10 2 0.59 0.94 0.22 o -3 10 2 1.78 1.95 0.19 o -2 10 2 1.64 1.53 0.22 o -1 10 2 18.39 19.81 0.91 o 0 10 2 0.73 0.52 0.14 o 1 10 2 0.37 0.24 0.18 o 2 10 2 0.17 -0.21 0.21 o 3 10 2 0.12 0.38 0.45 o 4 10 2 0.36 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