#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2200833.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200833_Fobs loop_ _publ_author_name 'Yang, Yang-Yi' 'Chen, Xiao-Ming' 'Ng, Seik Weng' _publ_section_title ; Tetrakis(trimethylammonioacetato-O)copper(II) bis(hexafluorophosphate) ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m61 _journal_page_last m62 _journal_volume 58 _journal_year 2002 _space_group_IT_number 121 _symmetry_space_group_name_Hall 'I -4 2' _symmetry_space_group_name_H-M 'I -4 2 m' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.8310 _cell_length_b 11.8310 _cell_length_c 11.7600 _exptl_crystal_F_000 846.00 _reflns_d_resolution_high 0.8111 _[local]_cod_data_source_file bt6104Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' CU in I-42m' _shelx_refln_list_code 4 _shelx_f_calc_maximum 249.12 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'y, -x, -z' '-y, x, -z' '-x, y, -z' 'x, -y, -z' '-y, -x, z' 'y, x, z' 'x+1/2, y+1/2, z+1/2' '-x+1/2, -y+1/2, z+1/2' 'y+1/2, -x+1/2, -z+1/2' '-y+1/2, x+1/2, -z+1/2' '-x+1/2, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z+1/2' '-y+1/2, -x+1/2, z+1/2' 'y+1/2, x+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 4264.13 4298.82 25.23 o 0 2 0 5670.35 6208.81 44.29 o 2 2 0 62059.45 55089.12 128.51 o 1 3 0 8961.92 9698.04 329.97 o 3 3 0 4275.09 4308.95 45.19 o 0 4 0 456.77 425.28 10.77 o 2 4 0 1733.40 1419.11 62.72 o 4 4 0 20821.91 20988.48 117.29 o 1 5 0 12788.05 13106.93 330.77 o 3 5 0 6825.88 7208.48 253.95 o 5 5 0 5465.85 5893.21 70.91 o 0 6 0 21033.02 20819.26 84.08 o 2 6 0 11608.61 11700.34 248.19 o 4 6 0 3777.94 3320.25 77.86 o 6 6 0 12072.80 10587.40 104.78 o 1 7 0 1360.15 1306.39 49.26 o 3 7 0 1213.87 1210.27 65.55 o 5 7 0 3961.91 3801.28 45.65 o 7 7 0 23.97 3.67 16.88 o 0 8 0 29783.23 28133.87 156.52 o 2 8 0 8461.45 8323.23 96.68 o 4 8 0 1391.06 1336.22 74.34 o 6 8 0 2621.07 2601.84 66.54 o 8 8 0 9236.30 9342.29 119.87 o 1 9 0 8.42 13.97 13.61 o 3 9 0 571.62 587.71 21.56 o 5 9 0 65.59 64.07 13.52 o 7 9 0 637.91 688.30 28.42 o 9 9 0 402.22 346.71 40.02 o 0 10 0 3980.05 3771.06 168.49 o 2 10 0 2042.99 2123.69 111.18 o 4 10 0 162.87 167.62 17.93 o 6 10 0 1507.27 1656.74 80.69 o 8 10 0 1420.28 1449.68 42.59 o 10 10 0 673.40 602.14 51.64 o 1 11 0 34.89 57.50 14.89 o 3 11 0 1189.62 1222.00 36.07 o 5 11 0 210.46 231.42 25.87 o 7 11 0 1.97 15.64 17.04 o 9 11 0 9.35 6.25 25.72 o 0 12 0 322.20 377.15 45.59 o 2 12 0 671.36 691.80 30.37 o 4 12 0 1207.52 1408.39 81.88 o 6 12 0 779.83 721.18 55.96 o 8 12 0 297.50 321.86 36.45 o 1 13 0 129.26 109.77 20.12 o 3 13 0 42.45 55.66 19.64 o 5 13 0 185.78 184.20 23.88 o 0 14 0 1762.62 1852.40 63.86 o 2 14 0 736.77 768.70 80.74 o 4 14 0 848.03 897.83 40.07 o 0 1 1 13593.06 14174.63 163.20 o -1 2 1 3258.27 3335.46 68.28 o 1 2 1 3420.55 3439.00 43.65 o -2 3 1 5603.40 5775.72 53.38 o 0 3 1 8.29 12.24 3.04 o 2 3 1 5118.02 5334.12 35.06 o -3 4 1 6134.13 6082.43 126.73 o -1 4 1 211.21 242.27 21.90 o 1 4 1 99.86 103.57 10.97 o 3 4 1 6345.66 6442.75 169.33 o -4 5 1 5239.28 5185.74 106.17 o -2 5 1 2305.05 2482.62 28.40 o 0 5 1 16.29 19.72 6.18 o 2 5 1 2525.88 2690.18 136.51 o 4 5 1 5052.60 4961.21 334.14 o -5 6 1 1514.72 1453.38 33.92 o -3 6 1 1011.69 975.38 25.67 o -1 6 1 860.29 820.20 32.28 o 1 6 1 909.23 885.34 21.25 o 3 6 1 1001.36 921.92 29.25 o 5 6 1 1596.98 1647.88 165.51 o -6 7 1 1222.93 1165.77 27.60 o -4 7 1 235.41 255.39 23.89 o -2 7 1 1303.83 1256.78 24.72 o 0 7 1 3790.61 3808.03 39.87 o 2 7 1 1434.99 1397.39 67.14 o 4 7 1 256.97 271.48 14.46 o 6 7 1 1176.19 1128.95 27.53 o -7 8 1 619.50 618.39 41.81 o -5 8 1 266.61 275.43 16.42 o -3 8 1 197.77 203.90 17.48 o -1 8 1 2490.65 2342.24 34.89 o 1 8 1 2490.49 2562.59 36.37 o 3 8 1 264.52 256.83 14.92 o 5 8 1 241.27 242.37 15.94 o 7 8 1 585.51 610.88 24.44 o -8 9 1 884.95 899.92 47.07 o -6 9 1 205.52 195.51 17.55 o -4 9 1 446.00 445.97 44.49 o -2 9 1 1084.67 1035.76 30.04 o 0 9 1 1803.86 1874.18 28.04 o 2 9 1 976.71 1021.53 44.59 o 4 9 1 566.62 521.52 21.42 o 6 9 1 129.69 146.39 21.15 o 8 9 1 891.61 878.43 48.12 o -9 10 1 377.71 377.27 38.29 o -7 10 1 393.75 364.57 24.89 o -5 10 1 120.75 139.51 25.18 o -3 10 1 773.12 780.80 50.75 o -1 10 1 697.09 761.39 37.54 o 1 10 1 721.23 765.39 26.79 o 3 10 1 727.67 784.17 28.24 o 5 10 1 118.87 139.50 35.80 o 7 10 1 419.30 403.62 24.77 o 9 10 1 376.52 352.37 29.42 o -8 11 1 115.49 108.17 20.74 o -6 11 1 383.81 379.47 25.17 o -4 11 1 846.17 883.79 40.27 o -2 11 1 777.52 769.22 49.91 o 0 11 1 163.38 174.84 12.38 o 2 11 1 856.82 765.05 29.68 o 4 11 1 714.88 733.58 29.95 o 6 11 1 440.88 446.49 37.64 o 8 11 1 130.09 91.44 21.81 o -7 12 1 117.78 90.44 44.15 o -5 12 1 583.86 550.76 29.91 o -3 12 1 235.70 235.80 21.70 o -1 12 1 201.24 186.25 20.28 o 1 12 1 167.19 207.12 20.66 o 3 12 1 229.78 241.52 25.33 o 5 12 1 589.98 599.79 30.99 o 7 12 1 113.96 100.01 21.62 o -6 13 1 334.93 304.95 27.34 o -4 13 1 565.63 523.06 31.18 o -2 13 1 171.95 145.60 21.60 o 0 13 1 345.64 328.89 27.87 o 2 13 1 128.85 134.46 23.49 o 4 13 1 604.19 608.43 32.48 o 6 13 1 321.92 310.00 27.73 o -3 14 1 169.69 163.77 25.36 o -1 14 1 117.88 95.13 27.91 o 1 14 1 113.68 94.28 34.11 o 3 14 1 177.21 164.07 25.62 o 0 0 2 13177.77 13759.99 57.11 o 1 1 2 14469.22 14417.15 63.46 o 0 2 2 41039.41 41330.59 151.21 o 2 2 2 13822.37 14303.04 74.29 o 1 3 2 119.75 130.75 21.15 o 3 3 2 21558.23 22052.73 108.05 o 0 4 2 7821.39 8336.23 246.70 o 2 4 2 665.67 607.25 23.79 o 4 4 2 556.00 587.44 22.35 o 1 5 2 132.78 130.06 8.92 o 3 5 2 5421.38 5864.18 46.24 o 5 5 2 1668.07 1992.94 43.40 o 0 6 2 8732.69 9148.28 275.70 o 2 6 2 8923.92 8659.56 58.35 o 4 6 2 1393.96 1342.13 73.64 o 6 6 2 5280.25 4844.45 72.80 o 1 7 2 1739.37 1669.45 27.95 o 3 7 2 179.00 168.84 12.53 o 5 7 2 182.71 202.90 24.43 o 7 7 2 2028.81 1918.35 51.84 o 0 8 2 13922.38 14294.30 231.85 o 2 8 2 4096.12 4048.37 101.90 o 4 8 2 1915.02 1869.88 109.89 o 6 8 2 4333.45 4375.35 164.32 o 8 8 2 3874.33 3937.41 79.75 o 1 9 2 296.36 274.85 29.25 o 3 9 2 452.96 459.80 19.97 o 5 9 2 155.74 136.54 15.69 o 7 9 2 72.83 80.82 29.55 o 9 9 2 97.78 89.58 30.89 o 0 10 2 1316.55 1222.82 38.43 o 2 10 2 1527.54 1471.61 37.59 o 4 10 2 454.96 458.62 24.01 o 6 10 2 822.65 892.19 32.26 o 8 10 2 844.40 868.84 59.54 o 10 10 2 776.89 825.40 57.21 o 1 11 2 117.98 117.71 45.88 o 3 11 2 525.02 523.63 26.29 o 5 11 2 450.04 442.07 26.36 o 7 11 2 17.56 31.48 23.69 o 9 11 2 98.58 128.21 24.61 o 0 12 2 1405.24 1387.13 92.96 o 2 12 2 294.26 292.12 22.88 o 4 12 2 457.55 491.69 36.15 o 6 12 2 496.10 491.66 29.27 o 8 12 2 612.46 626.93 34.36 o 1 13 2 41.55 50.93 18.03 o 3 13 2 62.91 66.75 21.15 o 5 13 2 114.45 101.30 22.69 o 0 14 2 697.03 799.30 148.57 o 2 14 2 1274.23 1260.16 55.91 o 0 1 3 6298.04 6865.60 198.43 o 1 2 3 3042.25 2922.94 108.05 o 0 3 3 43.84 40.72 5.93 o 2 3 3 4077.45 4013.08 33.25 o 1 4 3 1494.33 1799.96 168.93 o 3 4 3 3014.13 3048.05 72.65 o 0 5 3 2070.61 2024.35 83.97 o 2 5 3 506.05 499.13 15.23 o 4 5 3 3376.60 3561.00 112.72 o 1 6 3 1550.15 1477.37 25.42 o 3 6 3 1225.75 1157.22 23.77 o 5 6 3 1090.44 1058.44 24.86 o 0 7 3 387.98 361.61 15.55 o 2 7 3 2392.59 2361.19 35.65 o 4 7 3 207.08 215.17 14.85 o 6 7 3 708.26 658.26 22.86 o 1 8 3 1782.77 1726.09 31.67 o 3 8 3 522.14 574.10 36.50 o 5 8 3 953.77 913.21 26.64 o 7 8 3 1170.39 1170.93 58.15 o 0 9 3 1879.28 1947.27 35.87 o 2 9 3 179.63 185.17 18.17 o 4 9 3 203.34 238.90 22.69 o 6 9 3 484.94 450.04 25.52 o 8 9 3 422.88 464.72 26.40 o 1 10 3 828.36 828.27 57.80 o 3 10 3 554.02 541.08 25.86 o 5 10 3 726.60 672.12 28.46 o 7 10 3 304.01 271.14 23.29 o 9 10 3 293.72 295.38 28.79 o 0 11 3 80.23 100.00 16.18 o 2 11 3 382.43 415.18 30.54 o 4 11 3 485.70 524.55 27.42 o 6 11 3 346.89 373.03 25.80 o 8 11 3 107.82 81.14 24.53 o 1 12 3 559.08 578.87 28.72 o 3 12 3 678.28 667.42 31.19 o 5 12 3 287.14 294.81 25.72 o 7 12 3 189.91 180.17 24.46 o 0 13 3 24.44 5.66 17.44 o 2 13 3 352.51 378.39 84.52 o 4 13 3 452.22 505.37 78.91 o 1 14 3 305.87 297.58 27.97 o 0 0 4 36257.08 36825.22 132.88 o 1 1 4 55.51 32.18 8.64 o 0 2 4 3990.18 3838.48 101.00 o 2 2 4 5093.96 5329.50 55.81 o 1 3 4 6621.44 6818.26 184.03 o 3 3 4 4909.91 4787.94 58.20 o 0 4 4 56.62 34.06 14.20 o 2 4 4 188.65 168.02 10.61 o 4 4 4 1054.95 1203.79 33.77 o 1 5 4 31.62 19.16 7.65 o 3 5 4 7875.18 7827.94 58.46 o 5 5 4 3146.23 3081.72 57.21 o 0 6 4 6607.15 6546.58 54.12 o 2 6 4 873.82 797.89 20.88 o 4 6 4 2548.66 2479.72 79.95 o 6 6 4 2885.29 2659.93 58.10 o 1 7 4 336.96 323.70 20.56 o 3 7 4 954.45 837.37 23.21 o 5 7 4 607.11 632.44 22.10 o 7 7 4 70.59 71.21 19.96 o 0 8 4 4649.64 4627.95 51.97 o 2 8 4 4281.18 4114.60 56.56 o 4 8 4 1014.35 1057.39 46.13 o 6 8 4 1763.61 1907.82 49.11 o 8 8 4 2347.21 2121.05 63.56 o 1 9 4 266.26 270.83 17.22 o 3 9 4 302.75 306.27 18.36 o 5 9 4 93.16 94.30 15.37 o 7 9 4 17.15 29.18 15.53 o 9 9 4 48.97 44.79 29.50 o 0 10 4 3044.27 2886.12 96.24 o 2 10 4 648.24 585.68 99.12 o 4 10 4 12.97 -7.44 14.70 o 6 10 4 864.14 868.56 104.13 o 8 10 4 1496.88 1554.69 106.02 o 1 11 4 777.31 680.80 29.26 o 3 11 4 447.03 476.91 26.57 o 5 11 4 317.57 279.22 24.47 o 7 11 4 81.15 104.14 20.43 o 0 12 4 257.83 228.34 28.11 o 2 12 4 556.85 542.83 29.57 o 4 12 4 329.49 314.78 26.06 o 6 12 4 560.35 583.90 32.99 o 1 13 4 100.37 117.54 20.41 o 3 13 4 312.10 294.71 27.45 o 5 13 4 92.39 79.81 30.34 o 0 14 4 744.44 793.24 54.03 o 0 1 5 5118.17 5142.94 367.81 o 1 2 5 3585.77 3630.93 200.91 o 0 3 5 1594.09 1639.22 26.02 o 2 3 5 78.85 46.26 8.67 o 1 4 5 272.98 277.79 16.64 o 3 4 5 2781.37 3058.80 69.97 o 0 5 5 1210.04 1446.69 26.18 o 2 5 5 2833.58 2894.80 217.95 o 4 5 5 2552.29 2385.29 65.80 o 1 6 5 344.60 363.86 15.96 o 3 6 5 2057.58 1996.19 33.46 o 5 6 5 1501.86 1440.47 31.14 o 0 7 5 2646.03 2556.36 139.54 o 2 7 5 236.71 201.60 14.57 o 4 7 5 1773.89 1765.47 34.41 o 6 7 5 46.03 52.20 13.36 o 1 8 5 1746.27 1785.85 35.65 o 3 8 5 439.50 452.35 43.20 o 5 8 5 31.65 31.68 13.32 o 7 8 5 381.98 413.46 25.37 o 0 9 5 723.21 794.44 26.46 o 2 9 5 1485.77 1463.44 37.89 o 4 9 5 160.50 147.83 16.42 o 6 9 5 307.24 296.76 22.89 o 8 9 5 752.86 752.63 56.46 o 1 10 5 1508.45 1546.72 39.26 o 3 10 5 17.56 -0.33 14.89 o 5 10 5 125.51 136.93 19.37 o 7 10 5 1018.75 1030.32 79.50 o 9 10 5 210.60 242.76 30.74 o 0 11 5 845.83 868.34 74.78 o 2 11 5 103.15 102.94 18.94 o 4 11 5 316.25 312.96 34.81 o 6 11 5 203.33 208.35 43.05 o 8 11 5 297.93 342.99 29.49 o 1 12 5 96.21 119.79 34.16 o 3 12 5 361.38 438.41 55.47 o 5 12 5 592.75 582.38 31.59 o 0 13 5 29.24 5.71 18.78 o 2 13 5 288.36 315.29 27.59 o 4 13 5 500.39 497.76 31.90 o 0 0 6 22478.84 23659.33 132.39 o 1 1 6 59.13 29.00 12.22 o 0 2 6 19067.80 19251.64 359.77 o 2 2 6 2938.45 2824.79 49.16 o 1 3 6 874.75 846.79 60.23 o 3 3 6 4299.67 4333.38 64.06 o 0 4 6 709.77 702.72 19.83 o 2 4 6 1959.08 1927.11 42.11 o 4 4 6 2747.79 2809.50 56.61 o 1 5 6 768.10 859.41 22.75 o 3 5 6 920.38 953.70 58.99 o 5 5 6 1885.03 1762.23 48.66 o 0 6 6 3949.43 4002.30 47.58 o 2 6 6 3597.64 3779.97 136.46 o 4 6 6 5001.19 5348.02 176.18 o 6 6 6 1366.80 1406.69 46.38 o 1 7 6 581.07 599.50 32.03 o 3 7 6 75.88 85.41 12.57 o 5 7 6 261.49 306.86 18.81 o 7 7 6 623.41 661.73 37.64 o 0 8 6 7953.00 8003.08 73.44 o 2 8 6 4903.47 4946.67 59.04 o 4 8 6 122.36 165.79 16.60 o 6 8 6 2581.99 2620.21 47.68 o 8 8 6 2590.39 2553.57 72.20 o 1 9 6 181.25 168.41 17.19 o 3 9 6 118.87 144.55 26.77 o 5 9 6 215.71 215.64 19.37 o 7 9 6 34.38 43.53 17.57 o 9 9 6 51.44 146.19 33.27 o 0 10 6 4114.76 4165.55 65.35 o 2 10 6 297.00 313.27 23.26 o 4 10 6 466.01 474.54 26.70 o 6 10 6 642.44 688.93 49.81 o 8 10 6 1155.73 1182.66 42.90 o 1 11 6 126.15 124.29 19.59 o 3 11 6 134.23 142.59 25.37 o 5 11 6 168.65 184.07 22.84 o 7 11 6 54.85 48.63 21.60 o 0 12 6 74.85 92.84 27.51 o 2 12 6 830.06 930.21 72.10 o 4 12 6 433.55 534.66 30.77 o 1 13 6 187.55 185.56 24.72 o 0 1 7 1485.62 1427.22 115.95 o 1 2 7 1398.86 1407.56 26.79 o 0 3 7 534.13 610.56 60.48 o 2 3 7 999.46 992.93 23.70 o 1 4 7 1525.38 1633.11 51.74 o 3 4 7 749.51 729.65 22.71 o 0 5 7 791.31 805.62 23.16 o 2 5 7 499.78 490.25 19.55 o 4 5 7 1270.64 1287.20 113.17 o 1 6 7 767.97 888.28 25.97 o 3 6 7 547.44 563.95 28.80 o 5 6 7 793.32 822.21 27.07 o 0 7 7 116.01 107.69 16.59 o 2 7 7 1407.24 1323.97 31.81 o 4 7 7 760.65 797.60 37.69 o 6 7 7 201.78 176.94 26.91 o 1 8 7 562.98 592.92 54.13 o 3 8 7 650.83 744.83 44.15 o 5 8 7 205.63 222.47 18.98 o 7 8 7 433.23 460.47 25.35 o 0 9 7 1084.16 1140.92 41.81 o 2 9 7 589.45 612.54 25.68 o 4 9 7 268.67 267.33 20.71 o 6 9 7 362.34 442.22 61.33 o 8 9 7 190.02 211.01 24.14 o 1 10 7 525.77 522.00 28.44 o 3 10 7 223.54 240.98 44.34 o 5 10 7 183.57 174.24 22.08 o 7 10 7 167.04 159.32 35.41 o 0 11 7 301.29 295.36 25.67 o 2 11 7 262.90 253.53 24.15 o 4 11 7 177.18 202.57 23.78 o 6 11 7 172.02 239.53 36.60 o 1 12 7 195.58 240.20 55.22 o 3 12 7 189.94 200.49 24.39 o 0 0 8 11760.03 12425.21 113.42 o 1 1 8 2030.43 2071.70 48.27 o 0 2 8 10292.87 10005.97 136.61 o 2 2 8 3758.43 3570.35 63.86 o 1 3 8 177.60 193.99 14.08 o 3 3 8 274.39 253.15 22.84 o 0 4 8 2684.20 2862.26 105.02 o 2 4 8 4615.68 4699.67 132.78 o 4 4 8 1396.98 1369.44 46.48 o 1 5 8 643.04 620.00 30.94 o 3 5 8 438.49 412.23 30.79 o 5 5 8 295.58 332.21 28.60 o 0 6 8 6522.29 6883.58 368.21 o 2 6 8 2465.72 2479.41 69.67 o 4 6 8 2210.47 2278.86 43.22 o 6 6 8 2382.88 2235.27 63.76 o 1 7 8 435.15 438.77 21.84 o 3 7 8 422.37 376.11 21.19 o 5 7 8 55.87 81.82 18.03 o 7 7 8 151.01 122.06 27.21 o 0 8 8 3599.78 3510.99 101.15 o 2 8 8 2427.68 2369.02 83.87 o 4 8 8 1614.58 1618.92 40.18 o 6 8 8 1573.46 1676.13 88.44 o 8 8 8 1286.65 1217.99 56.21 o 1 9 8 256.77 264.32 20.59 o 3 9 8 2.77 29.58 15.55 o 5 9 8 43.52 64.17 17.31 o 7 9 8 8.70 23.42 23.14 o 0 10 8 1016.44 914.63 35.57 o 2 10 8 1200.90 1163.80 39.47 o 4 10 8 343.46 324.22 53.38 o 6 10 8 632.81 641.65 77.32 o 1 11 8 21.90 40.77 20.32 o 3 11 8 28.86 47.72 20.57 o 5 11 8 101.23 119.18 42.61 o 0 12 8 711.73 749.91 45.19 o 2 12 8 341.33 353.35 28.97 o 0 1 9 1864.08 1827.28 78.01 o 1 2 9 941.08 868.70 25.38 o 0 3 9 4.46 22.84 11.59 o 2 3 9 921.12 907.78 30.49 o 1 4 9 269.84 244.90 27.36 o 3 4 9 1234.47 1294.63 32.65 o 0 5 9 44.65 69.39 13.90 o 2 5 9 494.43 532.39 22.93 o 4 5 9 1226.89 1220.87 39.33 o 1 6 9 986.68 915.42 29.19 o 3 6 9 275.81 255.63 19.18 o 5 6 9 275.46 306.33 21.38 o 0 7 9 1550.78 1555.54 70.17 o 2 7 9 322.39 296.74 20.72 o 4 7 9 50.86 79.00 16.61 o 6 7 9 467.69 477.60 26.12 o 1 8 9 740.04 672.66 28.48 o 3 8 9 62.31 50.02 17.19 o 5 8 9 30.37 59.46 17.10 o 7 8 9 432.18 476.19 28.20 o 0 9 9 287.49 349.93 24.04 o 2 9 9 379.46 367.10 24.07 o 4 9 9 98.09 70.47 19.10 o 6 9 9 91.23 92.82 22.10 o 1 10 9 290.83 293.07 53.28 o 3 10 9 140.39 156.70 23.02 o 5 10 9 259.84 227.65 32.97 o 0 11 9 5.11 -4.89 36.90 o 2 11 9 192.51 173.17 27.61 o 0 0 10 7528.01 7708.18 102.99 o 1 1 10 1021.28 1000.79 40.52 o 0 2 10 807.79 874.20 27.70 o 2 2 10 2167.90 2170.61 58.40 o 1 3 10 38.74 41.43 13.25 o 3 3 10 1883.40 1926.50 56.61 o 0 4 10 590.85 648.01 25.48 o 2 4 10 193.52 199.23 19.42 o 4 4 10 2412.06 2207.36 64.06 o 1 5 10 12.98 30.63 16.09 o 3 5 10 181.50 179.12 18.31 o 5 5 10 757.14 772.57 43.20 o 0 6 10 760.25 832.61 29.69 o 2 6 10 1545.74 1541.20 39.01 o 4 6 10 389.67 347.38 23.03 o 6 6 10 1368.86 1242.42 53.83 o 1 7 10 4.77 5.11 15.15 o 3 7 10 5.60 11.14 15.84 o 5 7 10 44.86 13.16 17.17 o 7 7 10 155.28 164.17 29.89 o 0 8 10 2381.56 2333.37 81.64 o 2 8 10 789.97 735.23 51.89 o 4 8 10 263.95 237.05 22.30 o 6 8 10 551.73 533.05 28.90 o 1 9 10 79.07 106.94 19.99 o 3 9 10 1.91 16.53 20.26 o 5 9 10 25.25 20.09 18.95 o 0 10 10 554.95 514.53 31.48 o 2 10 10 446.45 393.26 29.26 o 0 1 11 1275.32 1278.26 59.44 o 1 2 11 594.00 547.54 31.38 o 0 3 11 9.90 17.66 13.24 o 2 3 11 196.66 223.47 18.79 o 1 4 11 45.37 19.30 15.38 o 3 4 11 1040.39 1083.10 71.46 o 0 5 11 2.70 37.32 15.13 o 2 5 11 252.51 269.92 21.10 o 4 5 11 712.58 640.87 29.05 o 1 6 11 486.71 463.39 38.34 o 3 6 11 189.60 181.01 20.72 o 5 6 11 341.19 325.63 26.91 o 0 7 11 260.60 217.82 22.44 o 2 7 11 356.70 385.64 24.88 o 4 7 11 98.92 81.12 19.73 o 6 7 11 165.63 169.30 28.45 o 1 8 11 684.22 706.05 31.53 o 3 8 11 33.67 34.09 18.00 o 5 8 11 48.81 59.34 30.14 o 0 9 11 540.45 581.32 38.19 o 2 9 11 100.34 98.98 21.24 o 0 0 12 2619.16 2706.02 70.91 o 1 1 12 607.37 511.47 36.25 o 0 2 12 473.59 487.75 24.65 o 2 2 12 609.81 606.41 38.34 o 1 3 12 56.91 74.82 16.69 o 3 3 12 334.51 311.15 34.36 o 0 4 12 106.35 123.57 19.06 o 2 4 12 270.59 288.55 22.20 o 4 4 12 817.27 755.78 46.78 o 1 5 12 40.59 61.90 22.99 o 3 5 12 349.63 353.96 33.97 o 5 5 12 213.89 246.50 33.67 o 0 6 12 407.47 464.96 27.76 o 2 6 12 607.25 627.51 30.79 o 4 6 12 268.56 242.88 24.08 o 1 7 12 49.41 46.36 28.60 o 3 7 12 16.10 13.57 18.71 o 0 8 12 1337.80 1402.19 67.93 o 0 1 13 246.69 283.55 31.23 o 1 2 13 153.03 137.69 20.32 o 0 3 13 45.01 35.19 17.66 o 2 3 13 339.43 355.56 24.68 o 1 4 13 354.20 354.49 25.86 o 3 4 13 49.29 45.29 35.60 o 0 5 13 226.03 196.14 23.45 o 2 5 13 65.97 61.27 19.06 o 4 5 13 305.77 311.58 26.09 o 1 6 13 147.74 197.68 50.45 o 0 0 14 952.82 942.00 51.64 o 1 1 14 80.65 62.97 28.30 o 0 2 14 954.96 893.36 50.80 o 2 2 14 775.78 791.73 48.07 o 1 3 14 14.45 6.41 17.98 o