#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/08/2200838.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200838_Fobs loop_ _publ_author_name 'Kooijman, Huub' 'Spek, Anthony L.' 'Bouwman, Elisabeth' 'Miccich\`e, Fabrizio' 'Warzeska, Sabine T.' 'Reedijk, Jan' _publ_section_title ; cyclo-Decakis(\m-2,2-diphenylacetato-O,O')dodecakis(\m-methoxo)decairon(III)) mixed solvate ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m93 _journal_page_last m95 _journal_volume 58 _journal_year 2002 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 82.980 _cell_angle_beta 77.686 _cell_angle_gamma 82.656 _cell_length_a 12.4268 _cell_length_b 18.8782 _cell_length_c 19.5576 _exptl_crystal_F_000 1710.00 _reflns_d_resolution_high 0.8276 _[local]_cod_data_source_file bt6110Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' S2298A 040700 K-CCD 150K' _shelx_refln_list_code 4 _shelx_f_calc_maximum 548.32 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 53319.70 61121.33 2566.33 o 2 0 0 1109.44 2220.53 57.80 o 3 0 0 9598.99 9775.96 196.57 o 4 0 0 9779.12 8892.73 184.45 o 5 0 0 132.79 144.33 17.95 o 6 0 0 1545.75 1529.07 53.98 o 7 0 0 422.51 450.30 41.23 o 8 0 0 1390.95 1485.81 61.02 o 9 0 0 252.36 249.30 34.82 o 10 0 0 408.23 319.95 42.20 o 11 0 0 88.86 150.80 46.26 o 12 0 0 13.78 74.79 50.67 o 13 0 0 27.55 131.22 115.25 o 14 0 0 75.71 25.66 192.44 o -14 1 0 18.16 41.28 186.57 o -13 1 0 17.57 149.53 119.90 o -12 1 0 32.26 29.25 62.99 o -11 1 0 57.45 91.27 49.99 o -10 1 0 635.35 654.66 57.78 o -9 1 0 1345.25 1327.26 47.37 o -8 1 0 2274.84 1986.71 56.61 o -7 1 0 5566.98 5658.13 85.77 o -6 1 0 5217.63 4854.51 80.65 o -5 1 0 688.56 629.00 21.75 o -4 1 0 1786.40 1817.37 38.08 o -3 1 0 4285.26 4588.02 107.93 o -2 1 0 22398.84 22971.58 713.57 o -1 1 0 21524.28 25999.08 1122.94 o 0 1 0 27169.01 3214.61 91.64 o 1 1 0 88410.36 116707.49 2451.51 o 2 1 0 9297.23 11143.10 297.76 o 3 1 0 12671.82 13098.83 529.21 o 4 1 0 625.05 654.57 26.56 o 5 1 0 2420.82 2441.25 56.96 o 6 1 0 546.90 601.18 28.96 o 7 1 0 5192.19 5971.17 87.77 o 8 1 0 1126.28 1214.85 79.51 o 9 1 0 176.69 137.44 31.75 o 10 1 0 102.58 172.97 40.06 o 11 1 0 201.01 134.96 47.12 o 12 1 0 0.84 64.98 60.84 o 13 1 0 0.21 69.22 83.47 o 14 1 0 10.84 72.39 174.11 o -14 2 0 4.52 122.36 199.86 o -13 2 0 6.49 132.37 138.43 o -12 2 0 181.90 84.75 83.96 o -11 2 0 131.29 135.95 51.71 o -10 2 0 44.93 67.29 41.73 o -9 2 0 2280.60 2374.24 106.12 o -8 2 0 486.46 559.40 41.48 o -7 2 0 5566.10 5551.68 115.76 o -6 2 0 7707.30 7143.17 119.65 o -5 2 0 5916.60 6497.45 107.48 o -4 2 0 1114.90 1111.52 38.70 o -3 2 0 17449.19 16272.62 309.17 o -2 2 0 895.86 983.98 40.13 o -1 2 0 6935.31 6416.07 262.09 o 0 2 0 16289.03 15310.07 821.67 o 1 2 0 661.72 811.52 105.31 o 2 2 0 2761.05 5046.16 214.58 o 3 2 0 3951.12 4647.92 125.53 o 4 2 0 7811.13 9151.65 252.01 o 5 2 0 124.08 76.45 17.46 o 6 2 0 731.53 684.65 32.66 o 7 2 0 1439.30 1304.24 42.93 o 8 2 0 2665.52 2834.58 61.60 o 9 2 0 1005.77 1029.86 53.32 o 10 2 0 102.94 142.54 43.17 o 11 2 0 3.09 13.45 58.33 o 12 2 0 0.09 39.32 85.75 o 13 2 0 9.12 60.70 82.95 o 14 2 0 2.20 6.41 274.91 o -14 3 0 0.45 273.99 293.24 o -13 3 0 4.96 108.79 108.71 o -12 3 0 89.51 80.17 75.07 o -11 3 0 497.24 343.24 54.12 o -10 3 0 556.42 602.82 55.65 o -9 3 0 2.96 60.36 38.94 o -8 3 0 3862.15 3946.75 111.60 o -7 3 0 186.23 105.68 24.75 o -6 3 0 495.04 460.75 33.42 o -5 3 0 363.03 493.78 59.26 o -4 3 0 2144.14 2048.68 37.82 o -3 3 0 1137.27 1204.74 70.71 o -2 3 0 1074.01 682.41 45.32 o -1 3 0 1008.16 930.08 38.48 o 0 3 0 18882.88 17315.79 701.94 o 1 3 0 32430.92 36803.31 1661.93 o 2 3 0 6206.50 7783.25 198.92 o 3 3 0 98.68 295.54 36.00 o 4 3 0 1724.98 1741.71 70.06 o 5 3 0 44.43 91.37 23.39 o 6 3 0 58.78 103.92 25.48 o 7 3 0 5.22 22.59 24.46 o 8 3 0 82.85 111.01 27.13 o 9 3 0 77.31 86.17 35.79 o 10 3 0 218.03 275.58 38.11 o 11 3 0 5.59 36.19 52.64 o 12 3 0 23.56 140.79 89.67 o 13 3 0 10.80 102.00 98.75 o 14 3 0 0.00 35.50 119.35 o -13 4 0 1.17 43.98 117.01 o -12 4 0 33.37 162.19 88.43 o -11 4 0 0.40 80.29 65.90 o -10 4 0 558.81 531.67 48.55 o -9 4 0 120.52 176.09 40.84 o -8 4 0 162.52 219.13 38.02 o -7 4 0 1099.93 1079.97 45.13 o -6 4 0 29.25 44.37 17.82 o -5 4 0 8779.75 9090.87 193.18 o -4 4 0 5677.92 6067.60 162.56 o -3 4 0 9857.95 10385.63 318.47 o -2 4 0 1092.70 1475.81 47.31 o -1 4 0 63.96 185.41 47.74 o 0 4 0 195.17 17.17 45.24 o 1 4 0 3140.53 3444.51 126.66 o 2 4 0 3628.81 3222.47 100.43 o 3 4 0 5228.37 6949.70 146.92 o 4 4 0 1598.77 2106.65 67.61 o 5 4 0 217.59 287.26 20.51 o 6 4 0 1523.33 1537.19 60.65 o 7 4 0 217.08 242.26 25.74 o 8 4 0 210.04 71.90 26.67 o 9 4 0 1042.56 1032.33 57.59 o 10 4 0 157.90 370.24 38.45 o 11 4 0 100.35 181.69 45.87 o 12 4 0 3.61 60.07 74.04 o 13 4 0 29.30 134.37 83.09 o 14 4 0 3.47 37.30 146.70 o -13 5 0 14.90 23.83 109.43 o -12 5 0 51.30 116.09 79.40 o -11 5 0 257.73 284.44 71.84 o -10 5 0 84.30 113.98 39.06 o -9 5 0 570.31 570.21 42.88 o -8 5 0 95.23 118.50 31.38 o -7 5 0 646.05 836.08 41.78 o -6 5 0 190.05 206.64 29.92 o -5 5 0 513.18 473.13 31.13 o -4 5 0 7117.22 6885.76 172.90 o -3 5 0 4342.04 4001.92 79.56 o -2 5 0 7286.15 7351.74 130.53 o -1 5 0 207.66 499.98 31.65 o 0 5 0 1144.88 1029.39 93.04 o 1 5 0 2906.56 3013.01 102.22 o 2 5 0 23.04 74.49 16.37 o 3 5 0 2335.59 2852.15 81.18 o 4 5 0 30.81 57.43 16.94 o 5 5 0 10.50 30.87 22.54 o 6 5 0 2209.21 2337.90 81.90 o 7 5 0 355.55 497.06 27.86 o 8 5 0 138.75 309.00 36.33 o 9 5 0 305.33 230.43 32.77 o 10 5 0 741.48 640.66 41.62 o 11 5 0 89.81 136.47 60.69 o 12 5 0 40.50 87.56 71.96 o 13 5 0 0.96 163.69 92.01 o 14 5 0 32.27 87.76 164.38 o -13 6 0 33.27 3.67 115.82 o -12 6 0 37.52 132.27 99.50 o -11 6 0 60.67 50.22 82.13 o -10 6 0 1061.48 923.81 79.60 o -9 6 0 28.39 150.37 47.71 o -8 6 0 70.92 143.20 38.78 o -7 6 0 3.59 57.79 35.46 o -6 6 0 1982.34 1658.47 70.55 o -5 6 0 4.06 26.16 27.12 o -4 6 0 4086.14 4162.12 121.60 o -3 6 0 271.10 278.86 19.71 o -2 6 0 97.96 79.48 23.90 o -1 6 0 9321.62 8412.62 230.61 o 0 6 0 15408.14 16729.57 400.05 o 1 6 0 249.60 445.08 28.62 o 2 6 0 2720.47 2726.47 88.38 o 3 6 0 10481.23 10660.10 340.86 o 4 6 0 2158.29 2519.58 79.62 o 5 6 0 1706.26 1911.37 85.16 o 6 6 0 7143.37 9116.71 191.06 o 7 6 0 788.94 1043.23 39.26 o 8 6 0 2194.45 2727.89 74.98 o 9 6 0 429.11 725.56 46.37 o 10 6 0 23.50 114.55 37.28 o 11 6 0 262.18 174.94 63.87 o 12 6 0 9.05 54.11 84.76 o 13 6 0 153.12 132.85 96.48 o 14 6 0 0.00 71.48 201.60 o -13 7 0 3.17 160.36 171.82 o -12 7 0 208.07 319.97 134.99 o -11 7 0 116.14 221.88 96.01 o -10 7 0 81.28 42.97 67.90 o -9 7 0 137.68 273.95 53.66 o -8 7 0 327.93 422.94 53.52 o -7 7 0 514.13 447.42 43.74 o -6 7 0 515.51 554.38 46.67 o -5 7 0 528.85 592.72 37.47 o -4 7 0 3189.66 3486.75 106.24 o -3 7 0 4796.21 5335.03 130.33 o -2 7 0 867.84 830.33 62.03 o -1 7 0 5826.15 4960.44 152.75 o 0 7 0 6179.68 5854.15 139.49 o 1 7 0 9.88 23.86 15.65 o 2 7 0 14961.59 13606.13 266.46 o 3 7 0 5553.78 6487.85 229.83 o 4 7 0 882.07 1013.56 43.29 o 5 7 0 216.04 279.43 25.03 o 6 7 0 766.20 1001.13 59.63 o 7 7 0 944.99 1035.47 36.33 o 8 7 0 307.39 341.29 38.21 o 9 7 0 560.73 436.04 43.03 o 10 7 0 311.97 410.04 37.00 o 11 7 0 1.35 41.39 66.60 o 12 7 0 11.37 90.05 89.82 o 13 7 0 80.49 72.47 107.60 o 14 7 0 48.40 131.96 172.91 o -13 8 0 0.57 3.67 238.25 o -12 8 0 16.70 56.12 140.57 o -11 8 0 192.27 172.40 89.18 o -10 8 0 74.26 166.25 71.68 o -9 8 0 45.64 64.97 69.46 o -8 8 0 310.33 287.04 50.35 o -7 8 0 12.66 62.21 37.72 o -6 8 0 116.01 260.03 42.49 o -5 8 0 55.75 114.40 29.96 o -4 8 0 0.50 9.14 18.27 o -3 8 0 189.76 148.14 31.39 o -2 8 0 26.14 29.75 30.91 o -1 8 0 7836.20 7405.34 162.27 o 0 8 0 2614.26 2593.43 85.99 o 1 8 0 595.44 470.03 47.49 o 2 8 0 10187.26 9988.67 268.94 o 3 8 0 2577.33 2456.44 116.79 o 4 8 0 29.03 30.92 12.66 o 5 8 0 1683.40 1767.81 53.16 o 6 8 0 2802.60 3147.16 136.13 o 7 8 0 1085.70 958.05 68.54 o 8 8 0 14.79 45.12 32.56 o 9 8 0 61.56 106.99 35.22 o 10 8 0 60.15 159.62 39.01 o 11 8 0 40.10 59.28 63.42 o 12 8 0 21.39 80.70 91.49 o 13 8 0 5.01 89.88 148.01 o 14 8 0 24.50 54.52 233.27 o -12 9 0 25.97 78.25 186.57 o -11 9 0 7.67 175.83 154.00 o -10 9 0 61.47 307.79 165.14 o -9 9 0 9.03 90.32 66.92 o -8 9 0 320.58 476.06 67.84 o -7 9 0 1931.73 2172.30 135.85 o -6 9 0 13.47 62.35 52.49 o -5 9 0 132.09 159.07 57.02 o -4 9 0 196.21 156.59 27.90 o -3 9 0 683.91 523.06 44.29 o -2 9 0 2938.61 3112.09 126.89 o -1 9 0 848.44 1186.02 60.29 o 0 9 0 2216.15 2468.32 146.03 o 1 9 0 584.69 742.84 41.05 o 2 9 0 10992.49 10398.33 322.55 o 3 9 0 3454.62 2871.90 56.44 o 4 9 0 16.73 106.68 27.26 o 5 9 0 803.98 847.26 47.72 o 6 9 0 2784.97 3037.07 69.81 o 7 9 0 4815.46 5430.52 144.09 o 8 9 0 194.57 109.33 33.65 o 9 9 0 95.09 217.34 39.70 o 10 9 0 29.27 34.53 48.67 o 11 9 0 0.17 95.64 81.95 o 12 9 0 0.75 56.04 88.23 o 13 9 0 25.13 78.07 152.55 o -12 10 0 145.64 6.41 135.62 o -11 10 0 48.56 63.01 173.52 o -10 10 0 272.04 260.50 262.54 o -9 10 0 856.48 724.40 117.03 o -8 10 0 7.52 50.89 88.56 o -7 10 0 642.59 1483.49 152.17 o -6 10 0 239.83 1031.91 246.39 o -5 10 0 6198.26 6062.34 201.76 o -4 10 0 3505.46 3529.28 113.44 o -3 10 0 116.38 179.51 41.26 o -2 10 0 2176.87 2108.36 151.77 o -1 10 0 4525.40 4816.12 135.78 o 0 10 0 984.95 1190.54 52.55 o 1 10 0 52.35 62.96 20.96 o 2 10 0 2347.61 2247.12 95.27 o 3 10 0 2164.04 2187.82 63.22 o 4 10 0 91.07 155.07 28.58 o 5 10 0 7285.13 8301.62 248.19 o 6 10 0 669.00 777.83 32.43 o 7 10 0 2487.77 2489.62 85.45 o 8 10 0 406.20 492.81 76.34 o 9 10 0 229.93 292.45 44.60 o 10 10 0 111.36 136.88 70.06 o 11 10 0 13.02 44.51 85.20 o 12 10 0 14.57 46.01 91.12 o 13 10 0 10.14 38.18 159.61 o -11 11 0 164.48 136.54 158.52 o -10 11 0 2.43 98.51 181.43 o -9 11 0 1196.70 1686.49 328.98 o -8 11 0 2002.71 2297.82 342.97 o -7 11 0 621.83 424.48 157.16 o -6 11 0 182.94 555.80 274.91 o -5 11 0 3648.42 3848.71 224.32 o -4 11 0 12607.68 12714.40 357.79 o -3 11 0 41.57 159.51 79.91 o -2 11 0 5145.41 5315.61 158.63 o -1 11 0 1904.56 2152.09 87.36 o 0 11 0 2915.70 2974.58 100.31 o 1 11 0 2200.06 2417.93 73.02 o 2 11 0 213.38 199.55 30.22 o 3 11 0 583.84 470.42 53.57 o 4 11 0 87.01 35.90 38.23 o 5 11 0 1971.18 2155.63 106.51 o 6 11 0 2954.44 3491.44 101.02 o 7 11 0 30.52 45.29 26.80 o 8 11 0 356.33 386.76 44.56 o 9 11 0 36.37 44.09 46.71 o 10 11 0 114.43 120.39 77.04 o 11 11 0 32.85 20.59 75.30 o 12 11 0 2.37 29.99 87.45 o 13 11 0 0.47 137.83 219.17 o -11 12 0 39.70 4.58 182.55 o -10 12 0 49.53 19.89 160.61 o -9 12 0 7.52 90.26 155.51 o -8 12 0 1291.96 1897.23 564.48 o -7 12 0 241.22 1646.12 580.98 o -6 12 0 988.89 732.66 251.08 o -5 12 0 121.90 100.75 33.39 o -4 12 0 4238.42 4703.21 215.76 o -3 12 0 3634.78 5899.86 606.44 o -2 12 0 6943.30 6378.52 312.82 o -1 12 0 11170.29 11155.65 294.59 o 0 12 0 813.21 835.18 61.53 o 1 12 0 290.79 211.77 31.45 o 2 12 0 633.43 716.08 48.98 o 3 12 0 1271.21 1283.29 88.44 o 4 12 0 0.54 44.67 43.44 o 5 12 0 19.52 92.54 39.30 o 6 12 0 1832.33 1969.02 87.85 o 7 12 0 454.07 402.68 29.00 o 8 12 0 14.33 47.13 32.01 o 9 12 0 0.01 56.29 49.40 o 10 12 0 1.97 37.78 81.90 o 11 12 0 2.72 27.02 86.25 o 12 12 0 10.33 152.79 99.91 o 13 12 0 7.63 147.53 226.79 o -11 13 0 400.51 598.39 293.24 o -10 13 0 218.07 413.59 162.86 o -9 13 0 267.78 275.05 166.98 o -8 13 0 240.18 166.91 133.86 o -7 13 0 71.56 297.14 247.42 o -6 13 0 414.97 659.78 183.27 o -5 13 0 1234.18 1663.22 142.85 o -4 13 0 2.98 50.27 60.10 o -3 13 0 133.79 470.98 67.75 o -2 13 0 861.77 1283.14 139.54 o -1 13 0 5183.79 5558.76 204.89 o 0 13 0 2885.17 3420.91 220.30 o 1 13 0 195.74 164.33 34.04 o 2 13 0 698.36 669.06 58.41 o 3 13 0 1802.45 1604.10 95.77 o 4 13 0 445.83 589.30 55.68 o 5 13 0 234.98 182.81 51.32 o 6 13 0 1.03 25.05 53.55 o 7 13 0 134.90 101.78 53.34 o 8 13 0 3.10 41.70 65.99 o 9 13 0 40.13 95.73 67.35 o 10 13 0 23.54 126.96 71.69 o 11 13 0 0.01 113.44 99.99 o 12 13 0 14.28 19.24 127.64 o -10 14 0 472.27 377.31 204.03 o -9 14 0 4.20 66.73 182.55 o -8 14 0 836.71 1137.66 404.58 o -7 14 0 1324.64 1417.67 171.62 o -6 14 0 6.11 9.21 129.11 o -5 14 0 428.01 302.00 55.86 o -4 14 0 826.42 883.00 110.95 o -3 14 0 0.62 49.06 63.88 o -2 14 0 753.18 599.41 68.50 o -1 14 0 1319.60 1161.77 118.91 o 0 14 0 22.69 154.01 90.32 o 1 14 0 153.30 344.63 93.74 o 2 14 0 98.12 135.53 58.28 o 3 14 0 16.04 32.25 58.09 o 4 14 0 186.74 400.18 57.70 o 5 14 0 144.18 109.52 60.20 o 6 14 0 224.06 236.61 61.22 o 7 14 0 151.83 183.51 65.76 o 8 14 0 193.76 283.22 69.72 o 9 14 0 0.32 35.84 99.77 o 10 14 0 83.74 143.84 85.41 o 11 14 0 12.53 120.33 129.54 o 12 14 0 0.03 35.22 122.10 o -9 15 0 86.40 80.40 207.05 o -8 15 0 4.01 4.58 190.41 o -7 15 0 432.69 1039.69 190.41 o -6 15 0 324.25 308.15 152.17 o -5 15 0 249.94 182.59 117.87 o -4 15 0 42.81 51.88 83.17 o -3 15 0 660.75 883.51 96.61 o -2 15 0 54.85 96.02 68.70 o -1 15 0 175.01 270.63 71.73 o 0 15 0 2035.16 1973.58 157.32 o 1 15 0 623.17 528.37 112.43 o 2 15 0 136.71 142.43 92.10 o 3 15 0 1.85 46.78 70.78 o 4 15 0 58.67 273.64 139.83 o 5 15 0 7.70 7.41 61.68 o 6 15 0 12.22 61.90 71.99 o 7 15 0 21.53 96.47 72.40 o 8 15 0 351.54 270.98 81.62 o 9 15 0 177.91 278.34 106.71 o 10 15 0 0.06 63.17 101.43 o 11 15 0 17.33 129.52 122.22 o -9 16 0 9.27 20.31 181.08 o -8 16 0 21.44 149.12 171.14 o -7 16 0 94.96 105.57 137.24 o -6 16 0 105.97 63.13 183.90 o -5 16 0 287.95 236.79 158.52 o -4 16 0 861.46 1122.04 133.79 o -3 16 0 83.08 119.60 80.99 o -2 16 0 190.97 407.80 129.22 o -1 16 0 822.38 792.80 81.68 o 0 16 0 0.61 41.65 62.34 o 1 16 0 3072.73 3233.51 217.22 o 2 16 0 605.41 735.88 111.84 o 3 16 0 82.39 0.00 77.86 o 4 16 0 0.50 7.33 92.22 o 5 16 0 2.06 107.13 136.51 o 6 16 0 94.99 218.49 76.74 o 7 16 0 75.85 188.45 96.21 o 8 16 0 71.50 95.23 74.21 o 9 16 0 0.57 63.06 114.17 o 10 16 0 21.55 44.21 117.68 o 11 16 0 1.17 184.42 194.71 o -8 17 0 42.84 190.09 228.98 o -7 17 0 4.25 1.83 208.73 o -6 17 0 280.24 252.00 162.86 o -5 17 0 1116.34 1123.92 220.84 o -4 17 0 994.34 770.32 153.95 o -3 17 0 5.08 124.22 82.17 o -2 17 0 282.98 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255.98 o 2 -2 23 93.76 101.23 180.53 o 3 -2 23 306.60 632.85 425.19 o 4 -2 23 550.78 382.02 233.26 o 1 -1 23 8.22 1.83 160.61 o 2 -1 23 173.91 45.83 207.05 o 3 -1 23 19.28 146.94 202.58 o 4 -1 23 1301.73 1415.26 233.27 o 5 -1 23 574.60 665.74 246.23 o 1 0 23 14.87 4.58 206.14 o 2 0 23 175.56 57.32 216.42 o 3 0 23 420.51 193.38 215.26 o 4 0 23 22.54 138.79 173.28 o 5 0 23 676.59 498.84 261.89 o 0 1 23 7.77 125.54 284.07 o 1 1 23 19.25 38.21 208.73 o 2 1 23 6.84 0.92 208.73 o 3 1 23 239.89 194.49 229.41 o 4 1 23 568.52 1056.95 466.43 o 5 1 23 1.22 60.25 191.49 o 6 1 23 44.64 136.63 184.51 o 0 2 23 43.75 240.52 232.19 o 1 2 23 150.49 121.14 224.30 o 2 2 23 20.37 0.00 194.07 o 3 2 23 79.48 269.87 268.04 o 4 2 23 140.38 177.04 177.61 o 5 2 23 285.58 680.59 237.39 o 6 2 23 29.05 1.83 254.41 o 0 3 23 48.59 298.68 229.41 o 1 3 23 670.08 645.13 215.26 o 2 3 23 334.95 312.96 222.92 o 3 3 23 351.38 441.77 209.16 o 4 3 23 172.70 15.58 236.44 o 5 3 23 20.41 17.49 215.77 o 6 3 23 28.54 130.73 234.85 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