#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/09/2200923.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200923_Fobs loop_ _publ_author_name 'Janczak, Jan' 'Idemori, Ynara Marina' _publ_section_title ; [Phthalocyaninato(2--)]arsenic(III) triiodide ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m36 _journal_page_last m38 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.420 _cell_angle_gamma 90.000 _cell_length_a 8.6520 _cell_length_b 17.5580 _cell_length_c 19.6680 _exptl_crystal_F_000 1824.00 _reflns_d_resolution_high 0.7330 _[local]_cod_data_source_file na6120Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' AsPcI3 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 553.42 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 25260.59 25322.74 205.46 o 6 0 0 9665.50 9615.48 214.96 o 8 0 0 1393.82 1187.14 238.74 o 10 0 0 2209.18 1873.28 385.43 o 3 1 0 5919.84 6145.89 108.50 o 4 1 0 490.44 555.71 61.67 o 5 1 0 3265.17 3177.21 89.97 o 6 1 0 3463.68 3419.30 137.48 o 7 1 0 2937.21 3092.51 148.73 o 8 1 0 5551.35 5389.72 238.89 o 9 1 0 1801.69 1866.31 291.04 o 10 1 0 1256.59 782.86 328.85 o 11 1 0 403.81 436.49 360.15 o 2 2 0 15142.81 14962.88 299.03 o 3 2 0 269.44 292.37 99.21 o 4 2 0 11616.62 11572.50 104.03 o 5 2 0 34738.36 35097.04 190.48 o 6 2 0 1102.64 1049.26 84.84 o 7 2 0 9093.82 9204.11 227.68 o 8 2 0 190.18 507.49 240.07 o 9 2 0 794.59 725.81 238.86 o 10 2 0 335.28 767.32 347.50 o 11 2 0 1351.48 1850.11 331.04 o 1 3 0 933.23 1068.37 134.71 o 2 3 0 92534.26 93667.73 216.78 o 3 3 0 11397.73 11245.94 143.68 o 4 3 0 704.52 740.86 59.69 o 5 3 0 14303.79 14536.41 143.17 o 6 3 0 13679.84 13619.11 210.64 o 7 3 0 964.14 1017.21 191.47 o 8 3 0 3734.79 3559.39 177.73 o 9 3 0 649.09 637.50 240.18 o 10 3 0 47.32 130.22 164.25 o 11 3 0 536.36 1016.28 366.67 o 0 4 0 30977.49 31268.53 305.62 o 1 4 0 3486.94 3662.73 131.02 o 2 4 0 6502.64 6649.94 114.45 o 3 4 0 57983.29 58289.24 212.22 o 4 4 0 17066.38 17333.92 134.17 o 5 4 0 24561.63 24700.39 172.08 o 6 4 0 5445.36 5348.82 205.03 o 7 4 0 2.64 196.90 219.93 o 8 4 0 843.23 655.47 218.59 o 9 4 0 12.29 559.73 278.87 o 10 4 0 621.51 654.29 269.51 o 11 4 0 19.65 663.70 520.92 o 1 5 0 9349.04 9205.69 173.11 o 2 5 0 5489.99 5357.19 120.86 o 3 5 0 45068.69 44797.32 236.96 o 4 5 0 1657.42 1634.47 80.94 o 5 5 0 15969.63 16238.32 203.18 o 6 5 0 3478.11 3419.30 176.72 o 7 5 0 743.31 826.34 193.46 o 8 5 0 221.41 314.89 204.37 o 9 5 0 159.53 167.63 126.24 o 10 5 0 519.55 187.40 416.65 o 11 5 0 1012.43 1258.04 309.55 o 0 6 0 10547.36 10910.85 276.29 o 1 6 0 47612.52 48359.39 294.80 o 2 6 0 13677.75 13463.46 151.30 o 3 6 0 1643.11 1702.86 80.74 o 4 6 0 6450.15 6173.52 134.90 o 5 6 0 29.75 125.00 238.79 o 6 6 0 616.04 849.60 169.39 o 7 6 0 118.30 93.92 345.56 o 8 6 0 376.64 393.45 228.42 o 9 6 0 158.60 352.07 310.18 o 10 6 0 78.12 514.95 309.11 o 11 6 0 14.69 622.67 316.90 o 1 7 0 14748.65 14640.39 155.13 o 2 7 0 41161.58 41625.31 161.49 o 3 7 0 9561.81 9735.37 143.90 o 4 7 0 5935.51 5788.69 138.14 o 5 7 0 1349.90 1381.00 152.38 o 6 7 0 7445.86 7814.62 416.16 o 7 7 0 1781.33 2022.02 225.89 o 8 7 0 8290.00 8498.98 468.14 o 9 7 0 2907.73 3170.40 249.08 o 10 7 0 435.55 491.13 328.83 o 11 7 0 389.54 834.32 325.82 o 0 8 0 74933.25 76230.22 470.43 o 1 8 0 785.96 701.19 73.85 o 2 8 0 1800.32 1699.56 74.30 o 3 8 0 95.30 210.50 74.76 o 4 8 0 5.44 79.63 96.70 o 5 8 0 1468.39 1390.81 129.97 o 6 8 0 365.03 434.10 170.40 o 7 8 0 1308.24 1053.68 181.31 o 8 8 0 83.07 137.98 169.60 o 9 8 0 333.32 344.92 144.61 o 10 8 0 134.98 357.10 252.72 o 11 8 0 105.96 147.33 461.66 o 1 9 0 20518.02 20773.50 200.68 o 2 9 0 4497.30 4731.39 113.24 o 3 9 0 34466.45 34800.97 161.17 o 4 9 0 16.97 49.48 84.89 o 5 9 0 382.64 290.55 136.92 o 6 9 0 2818.92 2660.09 179.01 o 7 9 0 3107.57 3201.86 250.86 o 8 9 0 5338.41 5671.93 248.93 o 9 9 0 249.39 364.54 223.72 o 10 9 0 655.31 680.17 250.04 o 0 10 0 27915.95 28339.96 208.81 o 1 10 0 1096.78 1061.38 73.52 o 2 10 0 12421.30 11992.33 284.42 o 3 10 0 670.29 731.47 92.38 o 4 10 0 193.74 186.80 119.70 o 5 10 0 2560.75 2523.73 126.12 o 6 10 0 1085.77 1061.56 157.22 o 7 10 0 1886.31 2016.73 222.69 o 8 10 0 429.46 133.26 310.59 o 9 10 0 33.65 431.10 251.91 o 10 10 0 655.83 1058.15 319.66 o 1 11 0 1321.66 1375.95 75.56 o 2 11 0 50.68 144.17 118.70 o 3 11 0 7789.49 7728.75 191.51 o 4 11 0 9985.13 10212.46 172.81 o 5 11 0 2.69 398.45 250.01 o 6 11 0 1955.04 1850.95 197.36 o 7 11 0 15.73 232.50 280.11 o 8 11 0 237.53 630.29 311.13 o 9 11 0 489.88 453.22 242.18 o 10 11 0 57.72 55.85 211.37 o 0 12 0 657.60 770.37 192.06 o 1 12 0 1871.04 1891.63 104.74 o 2 12 0 1973.26 1905.58 103.44 o 3 12 0 17427.61 17654.60 205.43 o 4 12 0 1960.70 2086.00 151.33 o 5 12 0 7801.14 8140.44 257.99 o 6 12 0 544.01 487.34 147.16 o 7 12 0 133.62 238.15 182.81 o 8 12 0 30.54 71.83 548.92 o 9 12 0 360.23 616.07 331.59 o 10 12 0 93.62 593.12 523.69 o 1 13 0 3577.67 3607.19 141.87 o 2 13 0 3250.64 3254.02 121.20 o 3 13 0 9.93 243.79 131.74 o 4 13 0 60.15 43.40 104.01 o 5 13 0 4058.95 3757.57 212.63 o 6 13 0 26.09 108.37 229.77 o 7 13 0 2728.30 2620.08 336.01 o 8 13 0 243.97 344.88 323.18 o 9 13 0 726.82 745.56 252.35 o 0 14 0 11164.68 11223.54 216.25 o 1 14 0 4524.41 4314.11 167.20 o 2 14 0 6270.28 6249.67 165.25 o 3 14 0 3392.85 3292.16 137.96 o 4 14 0 1167.74 1280.92 136.32 o 5 14 0 1055.57 1374.70 215.14 o 6 14 0 6621.06 6603.10 218.17 o 7 14 0 96.53 231.49 260.70 o 8 14 0 168.52 275.61 252.12 o 9 14 0 115.44 299.41 262.49 o 1 15 0 348.34 568.28 129.95 o 2 15 0 92.56 210.14 149.31 o 3 15 0 27.11 103.83 134.32 o 4 15 0 101.61 209.78 205.20 o 5 15 0 333.07 550.03 226.28 o 6 15 0 447.14 355.34 145.66 o 7 15 0 256.68 155.85 322.71 o 8 15 0 141.92 259.03 324.78 o 9 15 0 203.82 161.93 427.72 o 0 16 0 7155.73 7515.55 276.32 o 1 16 0 12108.56 11991.71 235.05 o 2 16 0 1756.05 1707.62 145.54 o 3 16 0 20.50 265.38 158.21 o 4 16 0 768.62 763.62 164.82 o 5 16 0 1622.98 1140.68 272.19 o 6 16 0 247.43 203.71 281.82 o 7 16 0 2.20 422.42 369.29 o 8 16 0 32.44 151.61 356.52 o 1 17 0 790.00 834.57 136.75 o 2 17 0 26.81 324.37 150.05 o 3 17 0 159.09 251.80 188.21 o 4 17 0 28.37 308.04 188.79 o 5 17 0 58.99 187.02 265.78 o 6 17 0 897.84 856.44 301.39 o 7 17 0 83.85 112.80 324.18 o 8 17 0 1020.54 1187.29 341.34 o 0 18 0 100.13 143.89 231.79 o 1 18 0 437.48 430.87 157.37 o 2 18 0 331.10 450.20 197.60 o 3 18 0 215.43 562.95 251.11 o 4 18 0 1405.65 1285.23 185.01 o 5 18 0 314.78 298.67 290.85 o 6 18 0 1370.53 1256.08 299.07 o 7 18 0 154.87 737.96 367.56 o 1 19 0 422.08 434.66 146.31 o 2 19 0 19.06 397.55 193.01 o 3 19 0 2238.05 2023.79 247.95 o 4 19 0 523.81 657.67 239.92 o 5 19 0 31.04 775.13 489.02 o 6 19 0 959.03 716.15 312.70 o 7 19 0 93.87 659.96 433.50 o 0 20 0 211.73 345.31 244.21 o 1 20 0 46.13 59.05 177.53 o 2 20 0 452.59 418.90 176.76 o 3 20 0 927.07 1066.81 251.64 o 4 20 0 911.32 1054.83 260.14 o 5 20 0 18.57 44.16 206.03 o 6 20 0 222.30 697.46 468.28 o 1 21 0 64.92 90.51 80.61 o 2 21 0 1255.15 1121.31 298.81 o 4 21 0 668.15 296.75 438.77 o 5 21 0 104.44 174.63 430.05 o 0 22 0 93.92 336.14 327.41 o 1 22 0 237.38 262.47 218.51 o 2 22 0 19.63 97.06 436.56 o 3 22 0 464.44 737.57 322.68 o 4 22 0 130.83 957.19 585.49 o 1 23 0 15.56 459.79 311.42 o 2 23 0 361.31 285.95 329.46 o 3 23 0 76.57 751.19 472.18 o -11 0 1 1086.49 809.01 601.72 o -9 0 1 61.20 356.49 557.31 o -7 0 1 1135.56 855.24 213.21 o -5 0 1 6593.64 6879.84 204.92 o -3 0 1 17147.35 17757.24 599.31 o 3 0 1 33384.95 33830.24 138.90 o 5 0 1 8253.51 8027.07 191.80 o 7 0 1 421.59 469.34 142.47 o 9 0 1 3582.91 3173.92 499.16 o 11 0 1 1658.51 2179.82 601.49 o -11 1 1 497.19 1075.74 387.57 o -10 1 1 583.85 393.88 409.09 o -9 1 1 3604.31 3424.52 649.96 o -8 1 1 155.66 273.85 215.46 o -7 1 1 10613.61 10775.72 287.67 o -6 1 1 12596.64 12766.43 237.87 o -5 1 1 1538.39 1564.52 94.31 o -4 1 1 333.36 286.86 55.49 o -3 1 1 1.70 22.57 52.47 o 2 1 1 25631.23 26215.66 347.47 o 3 1 1 5492.08 5731.35 112.01 o 4 1 1 1409.88 1505.34 62.49 o 5 1 1 1424.41 1414.47 85.32 o 6 1 1 15300.21 15272.55 197.46 o 7 1 1 643.61 688.71 135.47 o 8 1 1 57.75 101.01 302.17 o 9 1 1 476.54 499.55 230.43 o 10 1 1 1623.61 1313.92 529.21 o 11 1 1 1.53 840.82 441.23 o -11 2 1 98.17 201.35 801.54 o -10 2 1 3162.07 3795.53 874.00 o -9 2 1 30.22 67.94 767.96 o -8 2 1 7896.09 7954.19 333.23 o -7 2 1 3687.88 3748.28 209.48 o -6 2 1 4173.57 3940.15 159.93 o -5 2 1 9348.02 9452.80 165.28 o -4 2 1 22517.37 22062.24 313.90 o -3 2 1 307.23 400.07 70.45 o -2 2 1 314.39 486.86 111.12 o 2 2 1 9681.00 10179.34 271.53 o 3 2 1 4135.52 4264.12 95.60 o 4 2 1 2395.14 2548.58 82.58 o 5 2 1 10006.01 10123.04 145.65 o 6 2 1 14620.67 14375.62 327.51 o 7 2 1 2535.33 2529.29 171.25 o 8 2 1 5606.81 5798.65 254.99 o 9 2 1 272.98 438.27 195.90 o 10 2 1 132.85 576.32 319.55 o 11 2 1 564.02 603.84 411.77 o -11 3 1 103.71 615.26 409.41 o -10 3 1 89.00 411.83 253.83 o -9 3 1 43.88 288.68 281.89 o -7 3 1 2176.63 2119.81 191.26 o -6 3 1 7610.35 7629.65 225.65 o -5 3 1 21729.35 21450.91 172.53 o -4 3 1 76196.33 77290.11 210.59 o -3 3 1 11347.11 11138.13 129.46 o -2 3 1 264178.66 264204.25 287.23 o -1 3 1 90110.03 88432.70 295.80 o 0 3 1 530.84 719.77 105.42 o 1 3 1 32.37 23.47 91.48 o 2 3 1 2614.84 2738.94 101.65 o 3 3 1 42476.84 42072.58 256.79 o 4 3 1 331.44 474.65 67.62 o 5 3 1 1239.26 1238.60 87.00 o 6 3 1 1179.74 1217.14 128.28 o 7 3 1 3593.34 3633.01 218.76 o 8 3 1 311.79 299.90 233.04 o 9 3 1 2580.30 2645.94 230.04 o 10 3 1 2548.75 2426.84 311.73 o 11 3 1 840.07 1366.14 581.50 o -11 4 1 39.24 324.14 427.24 o -10 4 1 103.15 23.87 483.53 o -9 4 1 344.31 98.70 389.22 o -8 4 1 1518.03 1365.68 164.04 o -7 4 1 365.32 289.29 245.48 o -6 4 1 0.93 185.10 146.77 o -5 4 1 1209.02 1034.44 93.52 o -4 4 1 1230.31 1314.75 81.45 o -3 4 1 12128.15 11885.45 229.36 o -2 4 1 2335.64 2364.56 83.85 o -1 4 1 9169.44 8986.66 170.58 o 0 4 1 5594.53 5755.49 155.15 o 1 4 1 2608.11 2790.28 117.44 o 2 4 1 181.17 301.55 90.17 o 3 4 1 568.61 641.08 80.03 o 4 4 1 109299.13 109507.23 160.40 o 5 4 1 5281.43 5227.74 121.84 o 6 4 1 15981.47 15924.55 304.32 o 7 4 1 5972.08 5669.92 216.85 o 8 4 1 847.31 521.83 208.42 o 9 4 1 779.88 614.21 226.01 o 10 4 1 46.02 334.57 275.48 o 11 4 1 98.82 231.80 306.83 o -11 5 1 180.82 226.67 311.91 o -10 5 1 656.24 663.07 262.70 o -9 5 1 729.59 536.56 253.15 o -8 5 1 249.42 334.94 134.86 o -7 5 1 244.12 266.62 112.90 o -6 5 1 7.47 21.61 159.86 o -5 5 1 232.50 304.24 88.67 o -4 5 1 25607.42 25166.87 172.80 o -3 5 1 6199.47 6315.01 106.52 o -2 5 1 84419.00 83603.53 241.43 o -1 5 1 21999.29 22171.34 266.38 o 0 5 1 117.80 316.57 167.24 o 1 5 1 11056.80 11117.86 157.33 o 2 5 1 1631.10 1703.46 77.63 o 3 5 1 22829.18 22505.35 180.48 o 4 5 1 6026.32 6150.67 115.92 o 5 5 1 613.86 605.38 99.72 o 6 5 1 2919.99 2644.34 179.22 o 7 5 1 1101.95 1291.34 177.91 o 8 5 1 794.14 799.45 183.33 o 9 5 1 3.39 125.22 230.43 o 10 5 1 43.46 666.73 322.49 o 11 5 1 96.95 375.09 307.21 o -11 6 1 3.89 448.17 308.26 o -10 6 1 1341.39 908.10 321.97 o -9 6 1 66.46 178.75 248.10 o -8 6 1 103.88 214.80 333.07 o -7 6 1 8611.12 8160.46 277.93 o -6 6 1 4120.42 3813.52 209.14 o -5 6 1 14948.30 15117.17 169.85 o -4 6 1 10.83 91.37 95.58 o -3 6 1 25268.79 24846.38 188.72 o -2 6 1 9453.60 9284.97 130.64 o -1 6 1 69550.12 70229.49 203.84 o 0 6 1 10188.93 10362.45 213.85 o 1 6 1 217.36 362.67 88.45 o 2 6 1 54205.83 54082.82 160.05 o 3 6 1 1569.14 1637.72 83.87 o 4 6 1 17684.52 17575.47 157.30 o 5 6 1 987.06 926.76 102.97 o 6 6 1 2344.09 2445.45 180.02 o 7 6 1 2049.15 1883.48 147.05 o 8 6 1 488.09 309.01 238.78 o 9 6 1 702.11 510.42 237.97 o 10 6 1 353.14 339.66 307.86 o 11 6 1 91.32 379.64 463.55 o -11 7 1 217.87 438.72 330.20 o -10 7 1 10.04 609.21 311.82 o -9 7 1 370.80 350.53 336.52 o -8 7 1 2090.84 2075.73 250.51 o -7 7 1 20119.89 20106.77 372.35 o -6 7 1 5121.13 4966.10 260.97 o -5 7 1 9576.09 9409.93 198.24 o -4 7 1 1444.18 1501.90 99.18 o -3 7 1 4326.31 4207.91 105.10 o -2 7 1 14820.74 15183.12 167.98 o -1 7 1 2642.62 2476.34 91.56 o 0 7 1 29965.70 30369.41 302.28 o 1 7 1 6851.96 7027.80 124.14 o 2 7 1 33.27 182.73 86.71 o 3 7 1 27157.23 27322.44 203.47 o 4 7 1 4030.01 4014.90 88.28 o 5 7 1 3457.41 3574.98 132.12 o 6 7 1 2216.12 2274.35 255.01 o 7 7 1 3773.93 3728.35 251.77 o 8 7 1 23.65 291.26 293.40 o 9 7 1 3942.95 4363.87 241.54 o 10 7 1 396.36 836.09 252.01 o 11 7 1 689.73 788.70 317.80 o -11 8 1 16.67 36.62 449.27 o -10 8 1 7.37 0.55 318.11 o -9 8 1 880.27 1246.92 279.56 o -8 8 1 1332.34 1492.73 315.41 o -7 8 1 1842.85 1931.68 218.24 o -6 8 1 95.71 114.72 132.52 o -5 8 1 31.89 105.79 152.82 o -4 8 1 4787.61 4894.04 134.73 o -3 8 1 2246.93 2414.89 99.69 o -2 8 1 2094.42 2175.00 83.71 o -1 8 1 12241.64 12089.72 137.65 o 0 8 1 4614.17 4613.31 119.71 o 1 8 1 71336.82 72213.72 319.51 o 2 8 1 162.65 206.13 82.31 o 3 8 1 150.23 301.90 79.18 o 4 8 1 939.73 1017.35 84.80 o 5 8 1 312.70 266.50 143.67 o 6 8 1 318.48 98.45 253.00 o 7 8 1 10527.38 10909.75 380.65 o 8 8 1 312.73 247.02 311.24 o 9 8 1 2826.38 2983.49 356.39 o 10 8 1 158.47 579.11 298.60 o 11 8 1 20.20 558.77 725.22 o -10 9 1 12.74 317.41 249.44 o -9 9 1 1483.41 987.88 291.34 o -8 9 1 373.13 806.69 254.35 o -7 9 1 4182.99 4519.63 290.63 o -6 9 1 1202.17 1010.41 218.31 o -5 9 1 1503.54 1414.80 178.08 o -4 9 1 1075.33 920.65 82.88 o -3 9 1 39.74 206.43 98.25 o -2 9 1 14294.60 13931.45 154.22 o -1 9 1 19383.48 19255.05 159.66 o 0 9 1 15112.07 15106.40 172.82 o 1 9 1 32653.06 32851.61 218.90 o 2 9 1 15042.61 14621.64 170.87 o 3 9 1 57.22 163.23 81.87 o 4 9 1 19371.85 19622.71 347.29 o 5 9 1 1868.78 2027.58 167.39 o 6 9 1 173.74 198.19 220.77 o 7 9 1 168.42 209.26 240.03 o 8 9 1 2352.27 1908.48 260.97 o 9 9 1 1199.19 1341.15 258.21 o 10 9 1 333.81 451.37 284.87 o -10 10 1 66.58 374.35 371.21 o -9 10 1 214.87 305.01 229.85 o -7 10 1 164.47 677.48 327.99 o -6 10 1 7242.49 7129.02 257.57 o -5 10 1 3714.44 3678.05 159.66 o -4 10 1 37.93 155.64 151.44 o -3 10 1 948.25 954.69 92.27 o -2 10 1 26728.88 26999.18 219.65 o -1 10 1 3504.06 3400.40 160.02 o 0 10 1 2612.69 2678.80 82.65 o 1 10 1 16997.32 17195.54 242.86 o 2 10 1 16215.23 15917.81 188.04 o 3 10 1 14938.20 15003.42 243.89 o 4 10 1 1842.17 1807.94 133.15 o 5 10 1 7166.33 7081.52 263.02 o 6 10 1 146.05 406.67 205.92 o 7 10 1 130.48 277.28 208.09 o 8 10 1 2.11 236.01 295.38 o 9 10 1 52.47 541.09 251.77 o 10 10 1 2.56 6.70 264.64 o -10 11 1 98.74 596.14 328.29 o -9 11 1 366.75 288.25 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