#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:53:41 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180929 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/09/2200950.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200950_Fobs loop_ _publ_author_name 'Krishnakumar, R. V.' 'Subha Nandhini, M.' 'Natarajan, S.' _publ_section_title ; \b-Alaninium oxalate hemihydrate ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o117 _journal_page_last o119 _journal_volume 58 _journal_year 2002 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 115.310 _cell_angle_gamma 90.000 _cell_length_a 22.3735 _cell_length_b 5.6925 _cell_length_c 14.9175 _exptl_crystal_F_000 792.00 _reflns_d_resolution_high 0.8408 _cod_data_source_file ob6102Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' b-ALANINE OXALIC ACID' _shelx_refln_list_code 4 _shelx_f_calc_maximum 274.64 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 780.08 789.16 5.28 o 4 0 0 0.00 2.74 1.83 o 6 0 0 55664.54 53830.66 399.46 o 8 0 0 10155.10 10302.31 41.23 o 10 0 0 2132.80 2128.35 19.18 o 12 0 0 2296.93 2382.07 22.49 o 14 0 0 5371.39 5495.81 38.37 o 16 0 0 453.80 423.02 11.16 o 18 0 0 3.34 0.96 3.01 o 20 0 0 3.20 -1.08 3.20 o 22 0 0 1.75 6.31 4.88 o 24 0 0 54.70 57.88 5.14 o 1 1 0 3458.45 3391.93 15.84 o 3 1 0 1096.58 1124.79 9.32 o 5 1 0 188.92 178.67 4.83 o 7 1 0 16663.03 18178.15 206.53 o 9 1 0 37.05 34.49 2.12 o 11 1 0 344.62 300.12 8.22 o 13 1 0 610.45 615.62 12.93 o 15 1 0 147.04 145.69 4.63 o 17 1 0 125.78 137.56 5.02 o 19 1 0 0.27 -2.74 4.04 o 21 1 0 50.21 33.83 4.19 o 23 1 0 4.28 5.98 5.46 o 0 2 0 2523.88 2360.15 17.09 o 2 2 0 749.58 766.49 10.10 o 4 2 0 10212.31 10403.13 41.38 o 6 2 0 6753.85 7138.46 34.90 o 8 2 0 968.00 1015.51 13.79 o 10 2 0 1102.25 1145.72 16.19 o 12 2 0 2866.40 3019.72 27.91 o 14 2 0 299.31 284.70 8.76 o 16 2 0 419.02 417.01 11.07 o 18 2 0 552.01 530.58 15.10 o 20 2 0 9.08 -2.31 4.15 o 22 2 0 12.00 13.57 5.89 o 1 3 0 266.69 273.74 7.48 o 3 3 0 143.58 134.84 3.94 o 5 3 0 3991.16 3966.75 29.49 o 7 3 0 385.87 395.26 9.90 o 9 3 0 152.05 174.85 5.37 o 11 3 0 2471.32 2610.21 26.99 o 13 3 0 299.55 295.78 8.16 o 15 3 0 4.21 3.94 3.97 o 17 3 0 326.00 329.62 9.84 o 19 3 0 8.94 19.91 5.73 o 21 3 0 0.04 6.49 4.88 o 0 4 0 1246.47 1186.55 17.26 o 2 4 0 28.71 37.72 3.05 o 4 4 0 171.61 183.95 5.51 o 6 4 0 1313.38 1318.88 19.84 o 8 4 0 18.00 12.36 4.99 o 10 4 0 751.23 750.89 16.14 o 12 4 0 19.85 19.02 5.99 o 14 4 0 30.61 47.41 3.89 o 16 4 0 108.13 100.02 5.42 o 18 4 0 60.82 66.23 4.59 o 1 5 0 3046.53 2850.84 30.71 o 3 5 0 67.66 80.72 4.46 o 5 5 0 139.17 139.70 5.33 o 7 5 0 1906.98 1870.12 26.64 o 9 5 0 399.89 429.66 12.17 o 11 5 0 241.81 235.51 7.27 o 13 5 0 380.64 434.08 12.70 o 15 5 0 57.22 52.20 4.89 o 0 6 0 29.38 26.29 4.17 o 2 6 0 912.35 932.82 20.77 o 4 6 0 93.85 95.09 5.27 o 6 6 0 11.56 10.03 6.07 o 8 6 0 1.07 4.34 4.89 o 10 6 0 51.85 58.56 4.83 o -23 1 1 6.09 9.26 4.74 o -21 1 1 2.36 -5.17 5.17 o -19 1 1 46.97 42.29 3.81 o -17 1 1 714.70 636.86 14.87 o -15 1 1 0.07 -4.29 4.29 o -13 1 1 1553.69 1602.14 19.22 o -11 1 1 92.31 89.76 2.99 o -9 1 1 695.01 661.95 10.53 o -7 1 1 6059.98 6225.35 28.97 o -5 1 1 1331.18 1272.37 11.56 o -3 1 1 149.35 141.62 3.51 o -1 1 1 1923.54 1614.65 10.51 o 1 1 1 738.09 625.65 6.90 o 3 1 1 15960.78 15274.74 163.81 o 5 1 1 2292.72 2555.12 17.74 o 7 1 1 2327.32 2451.97 19.57 o 9 1 1 85.85 81.41 2.85 o 11 1 1 253.35 246.88 6.75 o 13 1 1 633.05 718.47 13.96 o 15 1 1 162.65 154.00 5.04 o 17 1 1 249.88 259.06 7.99 o 19 1 1 6.83 1.85 3.94 o 21 1 1 5.59 6.37 4.84 o 23 1 1 10.99 1.42 4.25 o -22 2 1 0.17 6.09 4.84 o -20 2 1 29.49 19.32 5.84 o -18 2 1 135.70 134.93 5.24 o -16 2 1 47.14 43.63 3.72 o -14 2 1 607.84 631.29 13.65 o -12 2 1 378.40 358.21 9.84 o -10 2 1 12269.46 13106.30 57.16 o -8 2 1 246.69 274.43 7.48 o -6 2 1 23.73 27.35 1.88 o -4 2 1 2468.88 2577.61 18.96 o -2 2 1 1269.37 1392.05 12.87 o 0 2 1 1205.72 1224.99 24.92 o 2 2 1 5653.33 5620.94 29.16 o 4 2 1 9987.34 10107.94 43.05 o 6 2 1 1298.65 1314.32 14.93 o 8 2 1 641.31 683.20 11.87 o 10 2 1 15.73 11.12 3.99 o 12 2 1 261.75 259.66 8.01 o 14 2 1 21.18 23.60 3.17 o 16 2 1 261.90 250.09 8.21 o 18 2 1 6.55 12.59 4.88 o 20 2 1 42.99 32.64 4.26 o 22 2 1 7.31 8.52 6.12 o -21 3 1 41.23 35.27 4.42 o -19 3 1 1.80 2.82 3.90 o -17 3 1 20.56 14.59 3.53 o -15 3 1 4.74 0.96 2.89 o -13 3 1 20.67 19.11 3.25 o -11 3 1 721.04 786.28 15.26 o -9 3 1 12.89 13.83 2.51 o -7 3 1 106.57 118.47 3.93 o -5 3 1 270.73 233.38 6.56 o -3 3 1 2089.33 1931.17 19.24 o -1 3 1 2230.33 2323.97 21.14 o 1 3 1 183.53 201.41 5.77 o 3 3 1 486.83 556.03 10.69 o 5 3 1 14.14 17.39 2.16 o 7 3 1 194.00 194.97 5.99 o 9 3 1 5.42 6.54 3.75 o 11 3 1 0.40 -4.20 4.20 o 13 3 1 198.80 181.50 5.47 o 15 3 1 151.69 147.01 5.47 o 17 3 1 6.09 0.00 0.13 o 19 3 1 1.44 15.20 5.18 o -20 4 1 16.97 12.84 7.19 o -18 4 1 0.39 -4.70 4.70 o -16 4 1 16.13 14.08 5.92 o -14 4 1 0.63 7.81 4.47 o -12 4 1 428.31 420.22 11.12 o -10 4 1 0.00 0.29 1.94 o -8 4 1 1836.20 1843.19 23.54 o -6 4 1 21.93 27.81 2.97 o -4 4 1 238.78 237.49 6.96 o -2 4 1 936.95 888.10 15.57 o 0 4 1 10.11 12.98 2.14 o 2 4 1 382.67 373.20 10.48 o 4 4 1 152.75 153.72 4.76 o 6 4 1 1076.32 1074.45 17.88 o 8 4 1 497.61 475.41 12.83 o 10 4 1 7.06 10.97 4.56 o 12 4 1 101.94 99.79 4.73 o 14 4 1 72.97 72.81 4.82 o 16 4 1 3.31 2.93 4.60 o 18 4 1 41.87 38.42 4.61 o -15 5 1 10.72 5.76 5.84 o -13 5 1 73.47 78.11 5.37 o -11 5 1 896.66 921.93 20.64 o -9 5 1 331.93 337.92 9.96 o -7 5 1 331.14 339.22 10.39 o -5 5 1 951.66 920.24 18.58 o -3 5 1 548.65 534.46 14.12 o -1 5 1 931.02 893.65 17.63 o 1 5 1 81.29 88.83 4.46 o 3 5 1 1246.58 1222.56 20.66 o 5 5 1 45.49 67.89 4.27 o 7 5 1 346.92 355.25 11.07 o 9 5 1 135.58 118.42 5.65 o 11 5 1 24.45 25.60 3.87 o 13 5 1 200.77 207.51 7.15 o 15 5 1 0.74 -0.91 3.34 o -10 6 1 10.94 4.98 5.38 o -8 6 1 37.08 46.96 4.48 o -6 6 1 132.60 133.06 5.99 o -4 6 1 10.69 13.33 5.68 o -2 6 1 13.68 15.02 5.59 o 0 6 1 0.37 2.03 5.72 o 2 6 1 25.35 23.15 4.01 o 4 6 1 0.80 -4.82 4.95 o 6 6 1 151.71 160.68 6.58 o 8 6 1 0.26 -5.45 5.45 o 10 6 1 0.12 2.82 4.39 o -24 0 2 28.90 32.38 4.10 o -22 0 2 81.11 81.54 5.10 o -20 0 2 1719.78 1581.48 24.48 o -18 0 2 16.57 20.83 3.19 o -16 0 2 49.55 51.08 3.54 o -14 0 2 4189.39 4371.73 32.46 o -12 0 2 1189.62 1202.78 15.84 o -10 0 2 12.91 3.21 2.46 o -8 0 2 32374.07 34650.06 307.35 o -6 0 2 75424.76 82221.48 505.00 o -4 0 2 2347.73 2263.33 12.57 o -2 0 2 28.73 54.27 1.50 o 0 0 2 8581.90 8433.99 112.94 o 2 0 2 1787.64 1608.28 11.35 o 4 0 2 1920.19 1878.09 14.18 o 6 0 2 810.56 716.06 9.77 o 8 0 2 1360.04 1345.23 15.13 o 10 0 2 77.70 88.66 2.98 o 12 0 2 831.24 816.32 14.26 o 14 0 2 3.53 -0.52 2.16 o 16 0 2 319.35 290.41 8.47 o 18 0 2 391.03 393.90 11.66 o 20 0 2 60.96 68.45 4.66 o 22 0 2 29.02 23.60 3.84 o -23 1 2 81.09 80.51 5.46 o -21 1 2 14.99 28.05 3.94 o -19 1 2 0.31 0.66 2.56 o -17 1 2 139.45 157.03 5.09 o -15 1 2 423.22 406.97 10.95 o -13 1 2 2476.54 2731.76 25.31 o -11 1 2 140.53 148.27 4.67 o -9 1 2 43.29 47.77 2.19 o -7 1 2 249.09 326.45 6.54 o -5 1 2 2449.47 2451.86 15.19 o -3 1 2 2959.08 2849.08 15.41 o -1 1 2 380.43 373.40 5.28 o 1 1 2 19787.84 17137.64 176.91 o 3 1 2 5126.13 4977.59 24.21 o 5 1 2 14885.55 14585.15 186.04 o 7 1 2 157.92 163.06 5.19 o 9 1 2 125.32 106.58 3.26 o 11 1 2 403.32 470.55 10.80 o 13 1 2 157.98 154.02 4.76 o 15 1 2 95.65 107.14 4.44 o 17 1 2 136.23 151.39 5.55 o 19 1 2 110.66 99.80 5.19 o 21 1 2 21.36 27.58 3.91 o -24 2 2 2.92 -3.67 5.05 o -22 2 2 92.41 82.98 4.93 o -20 2 2 93.33 92.70 5.00 o -18 2 2 30.09 30.49 3.73 o -16 2 2 37.70 34.35 3.57 o -14 2 2 7.26 2.74 3.17 o -12 2 2 166.25 165.50 4.65 o -10 2 2 16.92 19.71 2.20 o -8 2 2 560.97 561.39 10.21 o -6 2 2 2401.75 2399.54 19.35 o -4 2 2 1850.96 1859.32 15.96 o -2 2 2 19545.26 19562.63 219.59 o 0 2 2 3962.60 3706.89 26.10 o 2 2 2 2722.99 2384.13 19.40 o 4 2 2 2842.19 2987.47 21.67 o 6 2 2 310.56 277.42 7.91 o 8 2 2 4695.84 4777.22 32.55 o 10 2 2 266.75 263.05 7.69 o 12 2 2 870.26 924.59 16.55 o 14 2 2 253.01 251.54 7.16 o 16 2 2 244.21 231.10 7.21 o 18 2 2 22.53 20.01 3.43 o 20 2 2 8.26 17.85 3.71 o -21 3 2 34.10 31.50 4.18 o -19 3 2 6.45 12.84 4.76 o -17 3 2 48.52 48.36 3.93 o -15 3 2 107.92 118.66 4.91 o -13 3 2 2.07 9.39 4.14 o -11 3 2 31.75 37.59 3.04 o -9 3 2 1035.31 1072.75 16.39 o -7 3 2 3788.41 3833.38 28.90 o -5 3 2 520.10 535.12 10.48 o -3 3 2 5762.30 5716.75 34.25 o -1 3 2 310.05 302.35 7.86 o 1 3 2 1865.00 1879.87 18.93 o 3 3 2 2112.90 2118.09 21.18 o 5 3 2 1332.06 1400.54 17.94 o 7 3 2 1407.44 1500.49 19.44 o 9 3 2 2.52 -3.01 3.63 o 11 3 2 303.44 310.37 9.55 o 13 3 2 70.49 70.15 4.35 o 15 3 2 510.80 485.92 12.46 o 17 3 2 2.37 0.41 2.48 o 19 3 2 11.73 12.20 5.27 o -20 4 2 35.63 36.76 4.51 o -18 4 2 1.53 6.31 5.04 o -16 4 2 60.42 66.23 4.76 o -14 4 2 105.75 127.89 5.10 o -12 4 2 24.81 29.26 3.53 o -10 4 2 351.44 348.27 10.12 o -8 4 2 34.12 32.39 3.47 o -6 4 2 135.65 145.67 4.63 o -4 4 2 1758.83 1776.96 22.16 o -2 4 2 57.69 47.91 3.13 o 0 4 2 286.72 256.19 6.15 o 2 4 2 1438.36 1426.44 19.81 o 4 4 2 217.96 207.43 6.50 o 6 4 2 2285.83 2223.96 25.94 o 8 4 2 34.24 27.94 3.57 o 10 4 2 775.87 744.57 16.69 o 12 4 2 230.57 220.18 6.37 o 14 4 2 106.17 115.69 5.34 o 16 4 2 42.31 59.43 4.69 o -17 5 2 26.73 22.08 6.57 o -15 5 2 14.91 12.13 6.12 o -13 5 2 333.05 349.12 10.54 o -11 5 2 0.45 0.00 0.13 o -9 5 2 357.09 373.38 11.35 o -7 5 2 1650.43 1671.08 25.14 o -5 5 2 636.91 613.63 15.14 o -3 5 2 621.54 626.53 15.29 o -1 5 2 218.18 223.23 6.41 o 1 5 2 701.11 698.89 16.16 o 3 5 2 1638.60 1677.99 25.20 o 5 5 2 104.90 93.59 5.02 o 7 5 2 500.26 498.37 14.63 o 9 5 2 0.11 -4.11 4.62 o 11 5 2 25.43 19.02 6.49 o 13 5 2 3.34 7.14 4.81 o -12 6 2 6.83 16.09 5.88 o -10 6 2 47.41 55.84 4.71 o -8 6 2 88.18 98.64 5.15 o -6 6 2 25.75 14.93 6.45 o -4 6 2 302.66 309.67 9.14 o -2 6 2 7.13 15.55 5.69 o 0 6 2 86.36 74.40 5.53 o 2 6 2 168.82 167.06 6.41 o 4 6 2 11.56 18.44 5.90 o 6 6 2 36.69 32.13 4.34 o 8 6 2 4.43 -5.54 5.54 o -25 1 3 0.02 5.13 5.21 o -23 1 3 0.61 -1.98 3.85 o -21 1 3 186.67 177.50 6.31 o -19 1 3 27.01 13.74 4.85 o -17 1 3 1230.14 1245.52 20.08 o -15 1 3 10.19 12.84 4.36 o -13 1 3 772.88 803.60 13.52 o -11 1 3 2584.39 2745.93 23.07 o -9 1 3 462.35 419.70 8.37 o -7 1 3 234.88 206.00 5.51 o -5 1 3 14171.53 14115.20 164.26 o -3 1 3 981.54 939.39 9.87 o -1 1 3 9948.80 9954.96 126.21 o 1 1 3 71.10 106.35 3.26 o 3 1 3 2174.02 2321.97 17.97 o 5 1 3 80.19 61.81 2.30 o 7 1 3 8.15 9.74 3.02 o 9 1 3 21.80 19.32 2.27 o 11 1 3 0.39 3.33 3.42 o 13 1 3 130.90 132.61 4.68 o 15 1 3 156.80 145.13 5.17 o 17 1 3 113.82 126.89 5.34 o 19 1 3 37.55 22.09 6.67 o 21 1 3 30.51 35.41 4.42 o -24 2 3 5.67 -0.44 2.49 o -22 2 3 4.70 11.58 5.45 o -20 2 3 7.03 6.54 4.61 o -18 2 3 468.05 408.50 10.96 o -16 2 3 504.81 467.19 12.72 o -14 2 3 72.98 68.86 3.74 o -12 2 3 4.02 4.48 3.34 o -10 2 3 30.16 47.57 2.64 o -8 2 3 4415.83 4668.78 29.08 o -6 2 3 17.20 19.03 1.77 o -4 2 3 6473.31 6468.34 31.37 o -2 2 3 2078.77 2059.42 16.84 o 0 2 3 12028.83 11705.10 621.44 o 2 2 3 205.62 221.74 6.40 o 4 2 3 134.56 164.07 4.62 o 6 2 3 3203.15 3371.99 27.02 o 8 2 3 1079.38 1084.15 16.49 o 10 2 3 268.65 261.52 8.03 o 12 2 3 37.20 42.73 3.68 o 14 2 3 252.15 258.70 7.62 o 16 2 3 0.54 0.37 2.22 o 18 2 3 30.75 15.74 6.71 o 20 2 3 7.83 15.82 6.18 o -23 3 3 144.75 173.17 6.83 o -21 3 3 9.30 5.08 5.18 o -19 3 3 12.25 12.28 3.39 o -17 3 3 198.01 158.25 5.68 o -15 3 3 92.08 96.88 4.44 o -13 3 3 106.04 125.89 4.81 o -11 3 3 1309.48 1215.61 18.27 o -9 3 3 1215.33 1247.66 17.70 o -7 3 3 3.96 8.71 3.33 o -5 3 3 57.14 60.34 2.80 o -3 3 3 886.56 913.68 13.75 o -1 3 3 1701.85 1720.00 19.02 o 1 3 3 0.34 4.02 2.72 o 3 3 3 752.45 801.91 13.50 o 5 3 3 1054.15 1015.16 15.94 o 7 3 3 298.31 290.94 8.09 o 9 3 3 1466.21 1496.63 22.05 o 11 3 3 212.01 194.86 5.99 o 13 3 3 309.01 311.03 9.17 o 15 3 3 2.61 -2.21 4.02 o 17 3 3 9.95 19.21 5.83 o 19 3 3 1.56 18.04 5.36 o -20 4 3 3.08 8.19 5.87 o -18 4 3 151.87 145.88 6.27 o -16 4 3 379.17 415.12 11.96 o -14 4 3 285.06 265.71 7.37 o -12 4 3 13.94 13.57 4.81 o -10 4 3 835.13 893.00 17.62 o -8 4 3 74.58 74.58 4.09 o -6 4 3 7.66 9.81 3.95 o -4 4 3 44.85 33.96 3.02 o -2 4 3 505.31 519.80 12.38 o 0 4 3 379.04 358.59 6.94 o 2 4 3 1096.79 1109.08 18.16 o 4 4 3 29.00 22.94 3.24 o 6 4 3 647.96 605.78 15.05 o 8 4 3 617.89 656.95 15.66 o 10 4 3 92.42 85.05 4.58 o 12 4 3 0.05 -5.36 5.36 o 14 4 3 2.86 2.08 4.00 o 16 4 3 0.12 10.52 5.27 o -17 5 3 271.10 254.24 8.28 o -15 5 3 13.82 15.91 6.02 o -13 5 3 11.64 15.55 5.60 o -11 5 3 107.24 108.07 5.16 o -9 5 3 420.39 432.63 11.74 o -7 5 3 1878.03 1814.00 26.23 o -5 5 3 2.62 3.88 4.32 o -3 5 3 489.06 462.36 13.13 o -1 5 3 844.20 866.15 18.01 o 1 5 3 315.96 343.35 10.46 o 3 5 3 286.96 265.73 8.46 o 5 5 3 739.52 787.04 17.79 o 7 5 3 131.49 139.40 5.60 o 9 5 3 189.22 166.82 6.41 o 11 5 3 9.04 6.42 5.14 o 13 5 3 9.58 10.68 6.48 o -12 6 3 0.91 -3.67 5.22 o -10 6 3 1.56 6.72 5.14 o -8 6 3 7.50 9.88 5.31 o -6 6 3 36.15 44.21 4.19 o -4 6 3 72.48 75.15 4.69 o -2 6 3 72.50 63.70 4.68 o 0 6 3 86.87 93.66 3.70 o 2 6 3 17.35 19.02 3.83 o 4 6 3 6.99 -0.43 2.62 o 6 6 3 30.70 29.87 4.31 o 8 6 3 0.85 6.09 4.67 o -26 0 4 70.29 52.04 5.04 o -24 0 4 280.47 269.64 8.15 o -22 0 4 291.70 346.49 11.34 o -20 0 4 58.45 47.13 3.88 o -18 0 4 2814.85 2777.24 30.31 o -16 0 4 417.81 438.06 11.35 o -14 0 4 14187.20 14978.35 64.62 o -12 0 4 5169.20 5119.74 32.27 o -10 0 4 4371.68 4470.25 26.97 o -8 0 4 12688.32 13102.86 170.21 o -6 0 4 2655.95 2482.32 16.44 o -4 0 4 5983.83 5475.53 25.88 o -2 0 4 24303.12 22161.38 218.75 o 0 0 4 2869.75 2288.65 29.52 o 2 0 4 3114.46 2975.87 19.35 o 4 0 4 1032.61 989.22 12.23 o 6 0 4 457.61 458.92 9.23 o 8 0 4 1902.05 1989.61 20.49 o 10 0 4 2127.80 2132.83 23.33 o 12 0 4 1971.09 2155.36 25.50 o 14 0 4 90.97 97.32 4.45 o 16 0 4 21.45 16.92 5.56 o 18 0 4 78.56 74.57 4.87 o 20 0 4 14.44 16.63 6.25 o -25 1 4 92.49 93.56 5.45 o 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