#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2200961.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200961_Fobs loop_ _publ_author_name 'Blake, Alexander J.' 'Felloni, Marina' 'Hubberstey, Peter' 'Wilson, Claire' 'Schr\"oder, Martin' _publ_section_title ; Triaqua(2,6-pyridinedicarboxylato)copper(II) at 150K ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m43 _journal_page_last m46 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.377 _cell_angle_gamma 90.000 _cell_length_a 6.4111 _cell_length_b 23.1690 _cell_length_c 6.8348 _exptl_crystal_F_000 572.00 _reflns_d_resolution_high 0.7385 _[local]_cod_data_source_file om6073Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' CUPICO in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 220.11 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 11076.39 10710.14 221.98 o 4 0 0 4386.02 4334.66 90.98 o 6 0 0 7042.42 6605.07 138.68 o 8 0 0 415.10 377.87 14.86 o 1 1 0 2286.68 2170.62 45.46 o 2 1 0 33.95 36.07 1.06 o 3 1 0 551.58 536.46 8.54 o 4 1 0 71.14 64.64 1.91 o 5 1 0 2975.03 2983.55 44.85 o 6 1 0 156.48 147.67 3.55 o 7 1 0 462.34 446.83 7.19 o 8 1 0 55.96 51.49 3.40 o 1 2 0 2.33 2.90 0.21 o 2 2 0 5312.87 5308.98 72.17 o 3 2 0 55.10 54.43 1.49 o 4 2 0 841.43 799.50 12.58 o 5 2 0 54.76 52.99 1.91 o 6 2 0 950.06 942.19 12.04 o 7 2 0 80.73 67.66 2.27 o 8 2 0 1029.70 981.84 32.90 o 1 3 0 2194.84 2099.53 28.32 o 2 3 0 0.08 0.28 0.28 o 3 3 0 8896.78 9322.04 142.00 o 4 3 0 17.07 15.93 1.06 o 5 3 0 252.85 262.53 4.41 o 6 3 0 14.94 14.16 1.20 o 7 3 0 2242.35 2136.33 28.29 o 0 4 0 2289.03 2371.70 49.78 o 1 4 0 12.72 14.17 0.64 o 2 4 0 200.62 229.32 2.99 o 3 4 0 103.82 103.59 1.70 o 4 4 0 265.68 235.62 3.77 o 5 4 0 13.73 14.80 0.99 o 6 4 0 45.33 39.31 1.63 o 7 4 0 109.60 100.92 2.69 o 1 5 0 26166.77 25385.14 392.81 o 2 5 0 9.81 7.93 0.57 o 3 5 0 2810.05 2826.58 35.83 o 4 5 0 2.64 1.42 0.57 o 5 5 0 247.13 249.56 4.19 o 6 5 0 18.84 19.19 1.27 o 7 5 0 1165.56 1161.83 16.13 o 0 6 0 8074.90 7788.90 162.90 o 1 6 0 4.94 5.10 0.42 o 2 6 0 125.31 183.56 3.69 o 3 6 0 4.60 2.34 0.50 o 4 6 0 1035.67 943.68 12.61 o 5 6 0 11.47 12.04 0.99 o 6 6 0 1924.66 1928.43 25.43 o 7 6 0 43.50 44.54 2.20 o 1 7 0 777.38 742.11 11.41 o 2 7 0 6.17 4.74 0.57 o 3 7 0 1335.01 1466.21 22.26 o 4 7 0 35.61 37.11 1.27 o 5 7 0 87.48 92.84 2.20 o 6 7 0 101.96 93.98 2.48 o 7 7 0 289.47 296.46 7.24 o 0 8 0 10400.68 10221.33 212.04 o 1 8 0 9.84 8.99 0.64 o 2 8 0 1107.91 919.85 14.11 o 3 8 0 17.15 19.97 0.99 o 4 8 0 1586.79 1588.62 24.25 o 5 8 0 3.90 3.11 0.92 o 6 8 0 2141.16 2154.04 38.41 o 7 8 0 0.80 1.77 1.56 o 1 9 0 5926.33 5923.81 87.24 o 2 9 0 25.18 22.38 0.99 o 3 9 0 3093.45 2979.61 44.41 o 4 9 0 33.27 36.76 1.77 o 5 9 0 52.45 33.65 1.70 o 6 9 0 76.02 68.65 2.98 o 7 9 0 313.32 302.91 7.46 o 1 10 0 34.18 26.64 1.06 o 2 10 0 6501.65 6861.06 101.05 o 3 10 0 50.47 51.65 1.70 o 4 10 0 583.43 586.92 9.71 o 5 10 0 23.71 26.13 1.56 o 6 10 0 861.10 778.05 15.23 o 7 10 0 85.93 81.83 3.54 o 1 11 0 11063.73 10931.45 164.22 o 2 11 0 6.78 6.02 0.78 o 3 11 0 4511.09 4611.41 68.40 o 4 11 0 0.02 -0.42 0.78 o 5 11 0 3029.82 2867.81 50.25 o 6 11 0 2.39 2.62 1.42 o 7 11 0 2805.42 2807.11 50.05 o 0 12 0 3996.35 4600.74 96.29 o 1 12 0 24.90 28.40 1.35 o 2 12 0 114.18 125.71 2.70 o 3 12 0 48.04 49.31 1.70 o 4 12 0 1079.90 1087.71 17.11 o 5 12 0 74.98 73.62 2.90 o 6 12 0 431.52 381.57 8.61 o 7 12 0 132.18 132.76 4.54 o 1 13 0 6172.56 5980.74 88.29 o 2 13 0 17.01 15.58 0.99 o 3 13 0 5009.20 5054.74 74.99 o 4 13 0 29.94 32.50 1.98 o 5 13 0 1442.68 1510.99 27.39 o 6 13 0 20.94 20.96 2.05 o 7 13 0 1448.05 1438.78 33.12 o 0 14 0 12704.09 12763.63 273.67 o 1 14 0 10.61 20.74 1.84 o 2 14 0 5616.40 5642.79 83.52 o 3 14 0 7.58 7.50 0.99 o 4 14 0 1535.12 1637.78 29.35 o 5 14 0 24.26 25.77 2.05 o 6 14 0 817.79 852.23 16.71 o 7 14 0 23.19 20.53 4.25 o 1 15 0 4874.11 5035.64 74.63 o 2 15 0 33.44 29.39 1.42 o 3 15 0 142.50 144.99 3.90 o 4 15 0 29.77 30.45 1.98 o 5 15 0 421.28 422.89 9.18 o 6 15 0 56.23 63.25 3.19 o 0 16 0 5346.63 5434.63 113.78 o 1 16 0 0.39 2.76 0.92 o 2 16 0 1563.48 1634.05 25.02 o 3 16 0 21.92 22.80 1.77 o 4 16 0 472.84 456.61 9.54 o 5 16 0 1.23 -0.14 1.34 o 6 16 0 1704.15 1745.80 32.08 o 1 17 0 183.87 171.24 3.62 o 2 17 0 3.71 1.84 1.06 o 3 17 0 3255.02 3242.98 56.42 o 4 17 0 7.44 6.94 1.49 o 5 17 0 156.79 164.59 4.82 o 6 17 0 42.31 42.91 2.83 o 0 18 0 265.95 230.87 6.40 o 1 18 0 6.29 12.25 2.48 o 2 18 0 509.07 509.71 10.20 o 3 18 0 24.73 23.93 1.84 o 4 18 0 189.76 187.59 5.11 o 5 18 0 19.42 20.25 2.19 o 6 18 0 225.51 240.03 6.53 o 1 19 0 4862.33 4863.75 83.62 o 2 19 0 1.66 0.99 1.13 o 3 19 0 561.24 560.64 11.34 o 4 19 0 0.01 -0.07 1.20 o 5 19 0 1152.04 1214.96 22.94 o 6 19 0 0.12 -0.35 1.63 o 0 20 0 664.33 600.85 14.29 o 2 20 0 431.21 416.77 8.76 o 3 20 0 11.04 8.07 1.56 o 4 20 0 115.31 116.03 3.90 o 5 20 0 23.85 23.36 2.27 o 6 20 0 513.18 574.55 21.84 o 1 21 0 1854.64 1973.78 35.11 o 2 21 0 2.50 2.90 1.27 o 3 21 0 172.30 186.06 5.11 o 4 21 0 20.07 22.66 2.19 o 5 21 0 270.62 246.76 6.60 o 0 22 0 1141.06 1264.55 40.30 o 1 22 0 1.01 2.12 1.49 o 2 22 0 3252.01 3158.89 55.35 o 3 22 0 0.51 1.06 1.34 o 4 22 0 1889.54 1939.34 35.19 o 5 22 0 11.39 12.18 2.05 o 1 23 0 348.21 311.95 7.18 o 2 23 0 25.72 24.92 3.97 o 3 23 0 276.17 264.65 6.67 o 4 23 0 46.89 47.95 2.97 o 5 23 0 357.09 383.63 9.16 o 0 24 0 4199.77 4043.35 121.96 o 1 24 0 2.16 9.56 2.05 o 2 24 0 4558.08 4572.97 79.46 o 3 24 0 9.16 7.93 1.77 o 4 24 0 2095.57 2115.59 38.42 o 1 25 0 873.52 814.84 19.66 o 2 25 0 10.01 12.11 1.91 o 3 25 0 815.14 850.23 16.85 o 4 25 0 13.37 12.39 2.19 o 0 26 0 331.34 332.94 13.78 o 2 26 0 289.08 298.81 9.23 o 3 26 0 13.26 12.46 2.05 o 4 26 0 14.73 20.11 2.41 o 1 27 0 1949.82 1849.82 41.42 o 2 27 0 0.16 0.07 2.05 o 3 27 0 840.89 818.89 20.42 o 4 27 0 3.73 -1.98 2.83 o 0 28 0 2.53 -1.13 2.97 o 2 28 0 97.55 86.52 4.82 o 3 28 0 7.28 6.23 2.55 o 1 29 0 1341.39 1326.44 30.93 o 2 29 0 3.11 2.97 2.34 o 0 30 0 620.26 671.56 24.79 o 1 30 0 0.15 4.95 2.34 o -7 0 1 223.55 212.76 5.25 o -5 0 1 218.67 218.69 6.11 o -3 0 1 326.33 306.32 7.35 o -1 0 1 489.87 470.57 7.87 o 1 0 1 55.38 56.56 1.92 o 3 0 1 2.85 0.07 0.92 o 5 0 1 32.17 33.50 2.34 o 7 0 1 13.49 14.80 2.34 o -8 1 1 9.00 8.07 1.20 o -7 1 1 1714.38 1712.27 22.95 o -6 1 1 163.03 154.50 2.91 o -5 1 1 3247.48 3202.96 47.98 o -4 1 1 150.71 150.28 3.12 o -3 1 1 6775.60 6780.51 99.76 o -2 1 1 4.21 12.96 0.64 o -1 1 1 17565.13 19643.46 263.74 o 0 1 1 79.80 78.75 1.42 o 1 1 1 11743.46 10647.05 160.03 o 2 1 1 5.36 4.81 0.42 o 3 1 1 21331.77 18874.43 289.82 o 4 1 1 0.05 0.42 0.64 o 5 1 1 5229.30 5191.42 77.15 o 6 1 1 1.23 1.20 0.99 o 7 1 1 756.36 718.64 12.42 o -8 2 1 196.62 181.93 3.62 o -7 2 1 134.13 131.15 3.05 o -6 2 1 5311.54 5344.96 67.94 o -5 2 1 155.85 153.62 2.91 o -4 2 1 9002.17 9441.97 109.06 o -3 2 1 317.57 309.63 4.42 o -2 2 1 12.69 16.08 0.50 o -1 2 1 111.68 113.76 1.78 o 0 2 1 22522.93 19618.72 361.23 o 1 2 1 35.88 34.24 0.78 o 2 2 1 6751.62 6289.52 84.36 o 3 2 1 3.30 1.56 0.57 o 4 2 1 168.08 160.43 3.34 o 5 2 1 0.07 -0.35 0.85 o 6 2 1 491.44 470.04 8.40 o 7 2 1 7.62 6.51 1.35 o -8 3 1 70.74 74.94 3.40 o -7 3 1 622.45 620.00 9.27 o -6 3 1 235.71 227.85 4.05 o -5 3 1 1780.72 1799.11 23.41 o -4 3 1 521.95 508.50 7.15 o -3 3 1 5535.70 5965.90 74.95 o -2 3 1 12.58 15.51 0.71 o -1 3 1 52.75 71.47 1.42 o 0 3 1 148.56 144.94 2.43 o 1 3 1 5325.75 5137.92 65.65 o 2 3 1 29.90 25.08 0.92 o 3 3 1 1406.41 1344.03 18.58 o 4 3 1 0.02 -0.07 0.64 o 5 3 1 722.08 720.65 11.80 o 6 3 1 6.93 7.43 1.06 o 7 3 1 115.68 124.52 3.47 o -8 4 1 542.56 564.52 11.96 o -7 4 1 0.59 0.07 0.99 o -6 4 1 623.99 636.93 9.20 o -5 4 1 33.07 32.22 1.35 o -4 4 1 8132.15 8417.43 105.60 o -3 4 1 1.15 0.99 0.42 o -2 4 1 95.23 159.05 2.84 o -1 4 1 6.13 18.76 1.42 o 0 4 1 2282.53 2155.19 45.05 o 1 4 1 1.11 3.47 0.28 o 2 4 1 30635.96 28920.06 535.48 o 3 4 1 1.47 2.62 0.50 o 4 4 1 2004.52 2053.97 31.00 o 5 4 1 2.66 2.48 0.78 o 6 4 1 2087.23 2074.34 27.21 o 7 4 1 0.68 0.00 1.13 o -8 5 1 22.72 23.72 2.83 o -7 5 1 383.87 381.27 6.33 o -6 5 1 43.52 43.91 1.70 o -5 5 1 3.17 4.74 0.85 o -4 5 1 184.70 177.84 3.05 o -3 5 1 4285.80 4630.42 68.43 o -2 5 1 7.35 5.24 0.57 o -1 5 1 387.32 398.34 5.75 o 0 5 1 21.35 20.55 0.57 o 1 5 1 77.31 115.27 1.92 o 2 5 1 24.46 20.19 0.78 o 3 5 1 3609.30 3865.55 45.63 o 4 5 1 2.05 2.05 0.64 o 5 5 1 91.18 94.26 2.27 o 6 5 1 10.33 11.75 1.35 o 7 5 1 266.81 273.16 5.61 o -8 6 1 9.57 11.04 3.47 o -7 6 1 150.20 149.68 3.90 o -6 6 1 333.79 337.02 5.47 o -5 6 1 95.19 92.08 2.20 o -4 6 1 519.16 447.42 7.50 o -3 6 1 140.53 137.11 2.77 o -2 6 1 287.57 390.04 6.21 o -1 6 1 75.37 75.95 1.42 o 0 6 1 468.51 477.07 6.70 o 1 6 1 9.87 8.00 0.57 o 2 6 1 1243.52 1134.76 13.72 o 3 6 1 0.01 0.14 0.42 o 4 6 1 2468.19 2512.61 32.22 o 5 6 1 0.04 0.21 0.71 o 6 6 1 622.86 598.85 9.91 o 7 6 1 1.87 1.49 1.20 o -7 7 1 2079.07 2020.50 31.43 o -6 7 1 33.27 31.44 1.77 o -5 7 1 3600.82 3631.05 54.33 o -4 7 1 16.71 17.21 1.06 o -3 7 1 1664.64 1509.35 22.86 o -2 7 1 29.21 31.52 1.13 o -1 7 1 2314.94 2376.45 32.16 o 0 7 1 1.79 2.69 0.35 o 1 7 1 950.68 697.04 11.06 o 2 7 1 2.50 1.63 0.42 o 3 7 1 3293.21 3065.73 36.43 o 4 7 1 0.05 0.50 0.57 o 5 7 1 24.55 36.47 1.70 o 6 7 1 0.12 -0.07 0.99 o 7 7 1 14.77 14.37 1.63 o -7 8 1 227.10 217.07 4.97 o -6 8 1 414.72 384.99 7.19 o -5 8 1 256.74 250.22 4.90 o -4 8 1 29.82 51.13 1.98 o -3 8 1 82.08 79.06 1.99 o -2 8 1 774.88 876.77 13.49 o -1 8 1 100.57 99.33 2.06 o 0 8 1 522.61 521.89 7.41 o 1 8 1 39.58 31.04 1.06 o 2 8 1 193.67 173.19 2.91 o 3 8 1 0.01 0.35 0.50 o 4 8 1 145.43 141.11 2.70 o 5 8 1 0.23 -0.99 0.85 o 6 8 1 542.68 528.55 9.05 o 7 8 1 5.09 3.82 1.70 o -7 9 1 1314.90 1325.77 24.77 o -6 9 1 4.41 5.52 1.20 o -5 9 1 2647.18 2647.79 40.07 o -4 9 1 79.46 76.41 2.20 o -3 9 1 1411.58 1397.55 21.31 o -2 9 1 2.49 2.83 0.57 o -1 9 1 2132.83 2113.33 31.50 o 0 9 1 112.98 147.77 5.61 o 1 9 1 11943.57 11439.39 170.49 o 2 9 1 3.56 4.03 0.50 o 3 9 1 10351.03 10681.00 150.79 o 4 9 1 2.64 1.42 0.99 o 5 9 1 1844.86 1771.18 31.74 o 6 9 1 17.07 17.63 1.91 o 7 9 1 764.58 772.13 15.63 o -7 10 1 17.83 17.91 2.05 o -6 10 1 1198.77 1176.95 18.81 o -5 10 1 94.39 91.93 2.62 o -4 10 1 6803.52 6954.86 102.75 o -3 10 1 28.39 31.09 1.35 o -2 10 1 3376.44 3289.19 48.82 o -1 10 1 18.37 16.85 0.85 o 0 10 1 10537.74 10200.65 152.88 o 1 10 1 25.88 21.74 0.85 o 2 10 1 6744.86 6813.53 91.81 o 3 10 1 0.05 0.71 0.57 o 4 10 1 1979.02 1964.78 34.74 o 5 10 1 3.09 2.19 1.27 o 6 10 1 2858.87 2807.15 49.69 o 7 10 1 8.66 7.22 1.84 o -7 11 1 133.56 134.26 4.47 o -6 11 1 285.47 272.53 5.61 o -5 11 1 379.76 379.57 6.90 o -4 11 1 483.59 485.37 8.27 o -3 11 1 66.18 80.58 2.34 o -2 11 1 134.62 139.91 2.91 o -1 11 1 243.35 306.03 5.20 o 1 11 1 1612.64 1744.20 23.89 o 2 11 1 13.93 11.68 0.71 o 3 11 1 580.60 572.81 9.65 o 4 11 1 2.69 2.83 1.13 o 5 11 1 457.43 430.15 9.11 o 6 11 1 14.43 15.43 1.91 o 7 11 1 129.17 109.08 7.23 o -7 12 1 42.77 44.90 2.83 o -6 12 1 4700.01 4599.84 79.83 o -5 12 1 1.48 2.90 0.99 o -4 12 1 8955.55 9271.25 136.76 o -3 12 1 1.56 2.69 0.78 o -2 12 1 4266.66 4210.44 62.45 o -1 12 1 30.15 38.67 1.84 o 0 12 1 11648.84 11820.58 177.98 o 1 12 1 0.07 -0.50 0.50 o 2 12 1 9448.39 9784.48 143.83 o 3 12 1 0.08 -0.07 0.92 o 4 12 1 2049.21 2118.41 37.42 o 5 12 1 3.77 4.18 1.42 o 6 12 1 546.99 543.58 11.47 o -7 13 1 431.65 437.73 9.88 o -6 13 1 207.44 205.34 5.53 o -5 13 1 51.54 51.00 2.05 o -4 13 1 235.64 233.04 4.69 o -3 13 1 44.49 45.97 1.70 o -2 13 1 82.69 83.94 2.27 o -1 13 1 4030.31 4266.46 63.22 o 0 13 1 70.51 89.53 2.62 o 1 13 1 671.83 631.24 10.04 o 2 13 1 9.75 9.13 1.20 o 3 13 1 4000.40 4200.71 72.36 o 4 13 1 0.48 -0.71 1.13 o 5 13 1 1921.37 1831.50 33.03 o 6 13 1 0.69 0.14 1.49 o -7 14 1 95.41 91.26 3.83 o -6 14 1 731.94 777.18 15.42 o -5 14 1 37.40 40.37 2.34 o -4 14 1 976.78 962.65 15.36 o -3 14 1 123.99 120.50 2.91 o -2 14 1 1090.55 1106.04 17.17 o -1 14 1 107.34 110.01 2.62 o 0 14 1 960.19 868.19 13.55 o 1 14 1 22.35 23.65 1.20 o 2 14 1 11803.21 11933.82 202.62 o 3 14 1 0.20 1.34 1.13 o 4 14 1 2075.95 2172.60 38.47 o 5 14 1 8.34 8.78 1.63 o 6 14 1 102.53 112.67 4.18 o -7 15 1 961.65 1001.24 34.10 o -6 15 1 12.35 14.09 1.84 o -5 15 1 1225.11 1276.34 23.57 o -4 15 1 2.11 0.50 0.92 o -3 15 1 9268.22 9570.73 141.09 o -2 15 1 3.07 2.97 0.85 o -1 15 1 2779.64 2647.57 39.71 o 0 15 1 1.27 3.11 0.71 o 1 15 1 3759.82 3686.39 63.54 o 2 15 1 0.26 1.63 0.99 o 3 15 1 7263.08 7299.97 124.92 o 4 15 1 0.05 0.07 1.20 o 5 15 1 1159.79 1243.86 23.17 o 6 15 1 0.64 1.42 1.63 o -7 16 1 78.40 84.94 6.52 o -6 16 1 3.41 4.67 1.63 o -5 16 1 196.82 191.00 5.18 o -4 16 1 1564.82 1566.35 28.25 o -3 16 1 128.28 126.30 3.05 o -2 16 1 121.60 99.36 2.55 o -1 16 1 73.82 87.46 2.62 o 0 16 1 124.40 123.85 2.84 o 1 16 1 24.00 38.88 4.25 o 2 16 1 1401.16 1405.30 25.23 o 3 16 1 0.03 0.57 1.06 o 4 16 1 606.94 573.82 11.63 o 5 16 1 1.79 1.20 1.42 o 6 16 1 198.28 237.05 6.45 o -7 17 1 263.50 226.40 11.21 o -6 17 1 23.23 22.87 2.27 o -5 17 1 3760.21 3771.22 65.89 o -4 17 1 25.95 29.39 2.05 o -3 17 1 115.23 122.37 3.47 o -2 17 1 0.60 0.71 0.78 o -1 17 1 1208.27 1179.10 18.40 o 1 17 1 1739.73 1823.96 32.28 o 2 17 1 3.89 4.96 1.27 o 3 17 1 50.94 61.62 4.96 o 4 17 1 1.52 1.98 1.34 o 5 17 1 480.61 496.60 10.68 o 6 17 1 6.84 2.34 1.70 o -6 18 1 737.74 742.35 15.12 o -5 18 1 118.15 112.27 3.97 o -4 18 1 42.60 47.17 2.55 o -3 18 1 2.50 2.12 0.92 o -2 18 1 64.76 54.77 1.98 o -1 18 1 0.45 0.35 1.06 o 0 18 1 3359.83 3270.20 57.49 o 1 18 1 10.62 11.33 2.41 o 2 18 1 895.36 948.99 17.70 o 3 18 1 0.21 0.92 1.20 o 4 18 1 1363.53 1400.53 25.83 o 5 18 1 0.27 -1.27 1.34 o 6 18 1 647.25 693.14 25.01 o -6 19 1 71.77 72.47 3.40 o -5 19 1 245.54 226.92 5.96 o -4 19 1 42.16 43.27 2.48 o -3 19 1 1.59 6.30 1.27 o -2 19 1 35.73 39.73 2.12 o -1 19 1 1134.94 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