#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:57:33 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180930 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/10/2201002.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201002_Fobs loop_ _publ_author_name 'van Albada, Gerard A.' 'Mutikainen, Ilpo' 'Turpeinen, Urho' 'Reedijk, Jan' _publ_section_title ; Redetermination of bis(2-aminopyrimidine)bis(nitrato)copper(II) ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m55 _journal_page_last m57 _journal_volume 58 _journal_year 2002 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 81.020 _cell_angle_beta 81.460 _cell_angle_gamma 69.510 _cell_length_a 5.6910 _cell_length_b 7.0910 _cell_length_c 8.9830 _exptl_crystal_F_000 191.00 _reflns_d_resolution_high 0.8383 _cod_data_source_file ya6082Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 84.58 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 700.99 1105.41 22.38 o 2 0 0 1321.55 1275.02 521.84 o 3 0 0 454.83 545.65 6.02 o 4 0 0 141.65 164.11 1.21 o 5 0 0 36.64 36.34 0.68 o 6 0 0 34.35 33.13 0.66 o -6 1 0 33.38 28.92 0.53 o -5 1 0 61.27 57.23 0.74 o -4 1 0 126.57 128.01 9.00 o -3 1 0 222.07 265.08 7.00 o -2 1 0 21.49 8.97 0.38 o -1 1 0 170.77 193.08 5.62 o 0 1 0 1619.95 1943.77 23.11 o 1 1 0 4325.97 4593.93 78.96 o 2 1 0 69.25 58.21 0.37 o 3 1 0 1294.77 1284.21 47.87 o 4 1 0 71.15 95.77 8.85 o 5 1 0 88.67 88.01 2.69 o 6 1 0 12.14 8.36 0.28 o -5 2 0 1.55 1.12 0.13 o -4 2 0 199.20 196.87 2.97 o -3 2 0 125.46 144.36 0.99 o -2 2 0 134.17 150.13 1.34 o -1 2 0 11.65 30.06 1.32 o 0 2 0 1.55 4.78 0.07 o 1 2 0 4.47 2.13 0.07 o 2 2 0 483.96 510.39 1.65 o 3 2 0 207.38 183.98 3.92 o 4 2 0 334.73 395.55 1.55 o 5 2 0 419.76 467.80 2.58 o 6 2 0 6.46 8.70 0.28 o -5 3 0 5.02 5.42 0.14 o -4 3 0 0.35 0.40 0.14 o -3 3 0 362.40 376.45 1.74 o -2 3 0 8.05 9.74 0.21 o -1 3 0 1308.80 1259.80 39.79 o 0 3 0 300.02 261.60 1.88 o 1 3 0 1123.34 1288.47 503.70 o 2 3 0 179.06 268.03 5.43 o 3 3 0 360.94 332.72 7.23 o 4 3 0 103.80 110.44 5.88 o 5 3 0 721.74 765.59 29.78 o 6 3 0 258.41 282.30 1.56 o -4 4 0 17.26 17.43 0.36 o -3 4 0 23.39 24.77 0.94 o -2 4 0 40.31 40.69 0.70 o -1 4 0 59.11 53.86 0.82 o 0 4 0 360.92 344.12 0.88 o 1 4 0 448.13 435.21 1.36 o 2 4 0 1423.42 1830.37 730.07 o 3 4 0 0.73 0.86 0.09 o 4 4 0 163.71 160.05 9.43 o 5 4 0 69.86 77.95 6.85 o 6 4 0 175.31 168.53 4.08 o -3 5 0 101.06 103.19 0.84 o -2 5 0 13.52 15.89 0.32 o -1 5 0 85.82 81.65 1.71 o 0 5 0 18.47 19.33 0.26 o 1 5 0 2.91 2.74 0.10 o 2 5 0 494.21 535.32 6.05 o 3 5 0 44.04 53.16 0.63 o 4 5 0 23.46 19.04 0.47 o 5 5 0 90.15 89.38 3.17 o 6 5 0 7.86 6.68 0.18 o -2 6 0 113.03 121.33 1.46 o -1 6 0 46.54 48.13 1.98 o 0 6 0 116.88 117.62 1.99 o 1 6 0 36.83 44.91 2.57 o 2 6 0 71.84 69.74 1.41 o 3 6 0 33.17 38.18 0.56 o 4 6 0 25.29 25.88 0.44 o 5 6 0 111.44 108.08 2.69 o 6 6 0 53.89 55.49 8.44 o -1 7 0 52.50 54.14 0.52 o 0 7 0 59.06 52.03 0.55 o 1 7 0 177.20 175.83 9.64 o 2 7 0 0.19 0.27 0.12 o 3 7 0 25.57 26.31 2.28 o 4 7 0 0.99 1.03 0.26 o 5 7 0 13.81 14.02 0.86 o 1 8 0 135.22 123.63 4.33 o 2 8 0 113.80 113.29 5.66 o 3 8 0 14.57 16.04 0.61 o -3 -8 1 24.90 23.20 1.28 o -2 -8 1 25.98 24.09 1.07 o -1 -8 1 11.63 11.87 0.44 o -5 -7 1 19.78 19.28 1.67 o -4 -7 1 15.60 18.19 0.34 o -3 -7 1 69.06 66.90 3.81 o -2 -7 1 7.44 7.82 0.56 o -1 -7 1 184.31 184.58 14.65 o 0 -7 1 0.78 1.11 0.07 o 1 -7 1 35.38 34.26 0.42 o -5 -6 1 59.29 50.59 0.53 o -4 -6 1 1.60 2.02 0.25 o -3 -6 1 0.74 0.72 0.13 o -2 -6 1 7.01 8.64 0.35 o -1 -6 1 37.96 40.85 2.72 o 0 -6 1 122.13 118.73 3.32 o 1 -6 1 1.37 0.95 0.15 o 2 -6 1 134.34 134.63 0.97 o -6 -5 1 14.14 17.39 0.42 o -5 -5 1 344.80 305.42 18.44 o -4 -5 1 465.37 472.26 21.79 o -3 -5 1 29.55 25.98 0.44 o -2 -5 1 131.06 148.39 0.97 o -1 -5 1 184.61 224.09 7.01 o 0 -5 1 54.32 51.97 0.43 o 1 -5 1 73.35 75.62 1.06 o 2 -5 1 11.00 11.66 0.25 o 3 -5 1 57.91 59.14 0.65 o -6 -4 1 8.63 8.40 0.26 o -5 -4 1 78.95 77.10 3.10 o -4 -4 1 1531.00 1427.65 36.36 o -3 -4 1 240.92 248.86 4.34 o -2 -4 1 746.22 759.48 1.89 o -1 -4 1 747.01 848.55 13.61 o 0 -4 1 485.89 494.08 2.56 o 1 -4 1 36.08 29.91 1.17 o 2 -4 1 131.68 125.26 2.78 o 3 -4 1 0.70 0.70 0.42 o 4 -4 1 25.75 29.46 0.69 o -6 -3 1 14.56 20.37 0.54 o -5 -3 1 27.33 31.62 0.53 o -4 -3 1 179.57 193.70 1.11 o -3 -3 1 237.84 275.18 1.13 o -2 -3 1 52.09 28.52 0.87 o -1 -3 1 1023.43 1131.54 518.56 o 0 -3 1 220.59 229.11 2.29 o 1 -3 1 704.95 646.07 20.85 o 2 -3 1 21.33 29.18 1.59 o 3 -3 1 212.63 212.77 7.13 o 4 -3 1 1.30 1.09 0.15 o 5 -3 1 11.16 14.33 0.93 o -6 -2 1 11.69 12.53 0.37 o -5 -2 1 79.76 97.00 0.97 o -4 -2 1 29.08 25.40 0.46 o -3 -2 1 118.02 167.02 4.96 o -2 -2 1 128.14 110.58 2.34 o -1 -2 1 50.15 37.80 1.28 o 0 -2 1 472.00 526.75 7.99 o 2 -2 1 125.31 111.88 4.07 o 3 -2 1 65.82 62.29 3.97 o 4 -2 1 617.32 610.71 30.09 o 5 -2 1 3.33 3.36 0.16 o -6 -1 1 6.62 6.26 0.23 o -5 -1 1 169.59 181.86 6.08 o -4 -1 1 351.00 352.00 10.54 o -3 -1 1 965.38 1067.84 18.06 o -2 -1 1 1166.52 1265.48 557.28 o -1 -1 1 1519.14 2185.08 28.15 o 0 -1 1 435.76 360.54 6.85 o 1 -1 1 7153.77 9366.41 441.42 o 2 -1 1 911.71 847.97 53.32 o 3 -1 1 65.29 52.18 3.26 o 4 -1 1 490.70 508.25 32.42 o 5 -1 1 246.78 231.10 4.27 o 6 -1 1 31.35 31.14 0.58 o -6 0 1 1.20 2.24 0.16 o -5 0 1 34.31 36.78 1.09 o -4 0 1 0.29 1.02 0.20 o -3 0 1 453.53 450.94 17.47 o -1 0 1 3.33 1.05 0.30 o 0 0 1 1221.68 1701.81 11.67 o 1 0 1 464.58 342.47 18.52 o 3 0 1 0.70 6.23 0.77 o 4 0 1 93.54 80.22 2.13 o 5 0 1 34.58 36.43 1.02 o 6 0 1 45.89 41.42 0.76 o -5 1 1 44.06 43.77 1.17 o -4 1 1 0.19 0.25 0.20 o -3 1 1 100.26 145.36 2.43 o -2 1 1 885.78 978.11 5.88 o -1 1 1 329.75 323.45 4.73 o 0 1 1 30.67 18.77 0.30 o 1 1 1 1269.52 1643.24 44.67 o 2 1 1 63.67 105.55 1.01 o 3 1 1 1170.49 1247.33 21.30 o 4 1 1 35.82 24.45 1.13 o 5 1 1 146.65 150.20 2.98 o 6 1 1 36.48 41.33 0.88 o -5 2 1 113.85 95.79 1.19 o -4 2 1 192.60 199.51 7.76 o -3 2 1 17.75 12.67 0.74 o -2 2 1 174.44 178.96 5.23 o -1 2 1 65.54 70.98 1.96 o 0 2 1 0.70 0.42 0.03 o 1 2 1 909.39 755.43 342.37 o 2 2 1 701.05 674.83 20.45 o 3 2 1 1028.32 1164.58 70.69 o 4 2 1 403.58 395.00 20.09 o 5 2 1 384.17 415.94 12.18 o 6 2 1 407.07 491.51 2.74 o -5 3 1 7.30 7.15 0.15 o -4 3 1 138.76 132.93 1.05 o -3 3 1 384.89 400.97 2.60 o -2 3 1 145.67 132.76 3.71 o -1 3 1 301.24 307.54 1.99 o 0 3 1 134.36 137.67 0.89 o 1 3 1 54.74 45.97 1.11 o 2 3 1 20.40 24.54 1.39 o 3 3 1 878.13 1012.98 57.98 o 4 3 1 0.84 1.92 0.11 o 5 3 1 76.89 76.05 6.28 o 6 3 1 323.49 338.23 2.13 o -4 4 1 0.89 1.07 0.12 o -3 4 1 354.11 361.42 1.72 o -2 4 1 213.63 208.75 2.89 o -1 4 1 227.45 214.87 1.12 o 0 4 1 488.21 477.31 4.26 o 1 4 1 70.67 66.63 0.55 o 2 4 1 12.80 1.03 0.08 o 3 4 1 177.94 186.57 8.70 o 4 4 1 65.35 82.47 5.42 o 5 4 1 104.85 114.36 8.09 o 6 4 1 78.74 85.49 0.86 o -3 5 1 23.70 26.55 0.65 o -2 5 1 176.17 180.34 2.58 o -1 5 1 53.68 56.40 1.75 o 0 5 1 214.95 213.36 1.59 o 1 5 1 62.41 63.76 0.64 o 2 5 1 199.62 191.66 1.55 o 3 5 1 84.55 75.51 0.89 o 4 5 1 204.01 210.86 3.67 o 5 5 1 35.41 38.35 0.84 o 6 5 1 9.76 11.18 0.62 o -2 6 1 37.99 37.60 1.11 o -1 6 1 59.07 60.55 1.26 o 0 6 1 103.66 99.73 1.17 o 1 6 1 1.03 0.65 0.20 o 2 6 1 141.99 155.28 5.51 o 3 6 1 46.68 45.49 1.74 o 4 6 1 6.57 10.48 0.50 o 5 6 1 116.44 111.41 5.32 o 6 6 1 16.91 21.04 3.46 o -1 7 1 76.06 74.97 2.07 o 0 7 1 164.94 162.96 2.45 o 1 7 1 57.79 55.99 3.82 o 2 7 1 63.63 64.14 2.81 o 3 7 1 150.93 152.35 13.06 o 4 7 1 0.95 0.85 0.10 o 5 7 1 30.15 30.03 2.36 o 1 8 1 95.15 92.03 2.55 o 2 8 1 79.30 79.46 3.41 o 3 8 1 126.14 111.74 5.05 o 4 8 1 39.97 40.81 1.16 o -4 -7 2 34.71 31.11 1.35 o -3 -7 2 35.34 37.45 0.45 o -2 -7 2 4.14 5.45 0.29 o -1 -7 2 104.13 103.66 6.13 o 0 -7 2 26.77 25.70 0.41 o 1 -7 2 16.73 19.32 0.31 o -5 -6 2 32.55 32.84 1.53 o -4 -6 2 56.56 52.46 1.43 o -3 -6 2 351.38 368.85 1.55 o -2 -6 2 0.13 0.38 0.20 o -1 -6 2 73.23 82.04 4.62 o 0 -6 2 356.05 369.89 11.41 o 1 -6 2 52.84 52.20 1.35 o 2 -6 2 92.61 101.01 1.38 o -6 -5 2 118.69 118.41 2.87 o -5 -5 2 81.37 77.36 5.37 o -4 -5 2 214.80 204.85 5.46 o -3 -5 2 654.44 703.72 5.42 o -2 -5 2 374.03 398.19 6.22 o -1 -5 2 0.66 1.72 0.27 o 0 -5 2 344.68 375.10 5.83 o 1 -5 2 124.84 127.54 0.98 o 2 -5 2 59.95 65.27 1.14 o 3 -5 2 84.37 85.71 0.76 o -6 -4 2 35.02 36.23 1.41 o -5 -4 2 0.75 1.23 0.11 o -4 -4 2 59.51 58.71 1.37 o -3 -4 2 250.91 273.61 4.43 o -2 -4 2 542.33 626.30 13.05 o -1 -4 2 195.40 149.60 7.94 o 0 -4 2 68.22 66.44 1.24 o 1 -4 2 57.21 56.10 0.86 o 2 -4 2 31.91 36.17 1.26 o 3 -4 2 3.61 2.43 0.21 o 4 -4 2 33.23 33.91 0.50 o -6 -3 2 94.43 99.45 10.74 o -5 -3 2 55.24 61.30 2.39 o -4 -3 2 42.28 45.89 0.58 o -3 -3 2 32.70 28.54 0.41 o -2 -3 2 204.80 280.61 13.30 o -1 -3 2 700.24 730.63 38.41 o 0 -3 2 625.76 551.48 9.40 o 1 -3 2 583.62 595.15 11.06 o 2 -3 2 432.76 391.17 14.39 o 3 -3 2 61.16 64.81 1.54 o 4 -3 2 11.94 11.50 0.53 o 5 -3 2 134.14 114.60 3.43 o -6 -2 2 74.11 82.62 0.97 o -5 -2 2 118.27 124.22 2.83 o -4 -2 2 18.00 21.91 0.96 o -3 -2 2 469.43 408.75 5.62 o -2 -2 2 39.35 57.08 1.05 o 0 -2 2 145.02 105.55 1.89 o 2 -2 2 2149.81 1997.81 779.12 o 3 -2 2 775.68 729.56 37.22 o 4 -2 2 117.98 115.33 1.04 o 5 -2 2 34.24 33.17 3.16 o -6 -1 2 35.92 41.20 0.70 o -5 -1 2 90.00 91.92 3.45 o -4 -1 2 252.55 295.81 3.95 o -3 -1 2 54.74 34.92 1.02 o -2 -1 2 362.85 303.68 0.94 o 0 -1 2 379.32 417.35 7.50 o 1 -1 2 83.63 105.56 1.91 o 2 -1 2 1393.09 1282.70 30.17 o 3 -1 2 165.74 182.48 6.47 o 4 -1 2 362.49 357.48 24.53 o 5 -1 2 69.74 67.72 3.92 o -6 0 2 23.45 26.54 0.49 o -5 0 2 58.01 55.65 2.90 o -4 0 2 46.95 58.74 2.01 o -3 0 2 192.87 199.88 8.10 o -2 0 2 8.89 32.00 0.57 o 0 0 2 105.47 94.07 0.68 o 1 0 2 832.45 722.09 15.75 o 2 0 2 355.73 248.93 0.89 o 3 0 2 0.24 0.74 0.23 o 4 0 2 102.02 97.21 8.26 o 5 0 2 90.53 91.80 3.53 o 6 0 2 105.74 111.76 1.28 o -5 1 2 39.67 38.22 1.40 o -4 1 2 167.73 165.45 1.22 o -3 1 2 0.40 2.38 0.13 o -2 1 2 622.29 564.88 33.52 o 1 1 2 504.67 353.90 9.18 o 2 1 2 985.33 807.16 29.52 o 3 1 2 627.56 639.40 6.79 o 4 1 2 179.42 202.89 3.56 o 5 1 2 54.57 54.13 2.72 o 6 1 2 68.89 79.00 1.21 o -5 2 2 132.76 119.91 2.44 o -4 2 2 185.08 180.08 4.52 o -3 2 2 55.34 65.40 0.94 o -2 2 2 285.75 310.70 5.65 o -1 2 2 196.50 148.44 3.33 o 0 2 2 477.01 496.65 7.69 o 2 2 2 12.64 5.99 0.14 o 3 2 2 866.48 818.83 30.56 o 4 2 2 582.23 695.20 35.40 o 5 2 2 67.78 67.25 2.05 o 6 2 2 0.26 0.32 0.21 o -4 3 2 306.00 294.43 3.10 o -3 3 2 128.40 136.69 1.31 o -2 3 2 728.56 836.00 13.71 o -1 3 2 951.08 929.92 14.56 o 0 3 2 32.52 24.81 0.73 o 1 3 2 74.21 74.22 1.00 o 2 3 2 26.60 41.14 0.41 o 3 3 2 0.75 4.70 0.12 o 4 3 2 241.96 243.17 1.29 o 5 3 2 115.41 122.34 2.74 o 6 3 2 2.32 1.98 0.21 o -4 4 2 10.57 10.50 0.45 o -3 4 2 174.16 182.79 6.33 o -2 4 2 117.91 134.23 4.00 o -1 4 2 1005.39 1013.52 6.36 o 0 4 2 310.81 291.99 1.51 o 1 4 2 981.88 942.58 2.27 o 2 4 2 0.66 0.70 0.34 o 3 4 2 15.85 6.83 0.31 o 4 4 2 50.71 42.02 0.68 o 5 4 2 2.72 3.18 0.24 o 6 4 2 93.09 94.24 9.73 o -3 5 2 4.08 3.37 0.13 o -2 5 2 63.69 70.19 1.78 o -1 5 2 22.91 21.06 0.41 o 0 5 2 241.51 226.51 1.23 o 1 5 2 302.96 274.62 1.43 o 2 5 2 498.33 509.03 4.41 o 3 5 2 47.72 56.08 0.82 o 4 5 2 238.81 232.05 1.35 o 5 5 2 13.08 11.29 0.71 o 6 5 2 14.48 15.24 3.09 o -2 6 2 12.16 13.94 0.50 o -1 6 2 112.37 110.17 3.14 o 0 6 2 110.94 113.16 0.63 o 1 6 2 64.97 62.56 1.10 o 2 6 2 160.82 149.85 2.67 o 3 6 2 275.15 278.02 9.27 o 4 6 2 201.18 190.39 12.10 o 5 6 2 83.68 88.41 8.06 o 6 6 2 8.00 8.88 2.43 o -1 7 2 19.48 18.96 0.45 o 0 7 2 391.40 376.33 1.08 o 1 7 2 65.85 74.99 0.83 o 2 7 2 8.70 8.67 0.20 o 3 7 2 145.91 151.60 10.14 o 4 7 2 76.16 66.67 3.41 o 5 7 2 84.10 84.55 7.28 o 1 8 2 186.08 175.68 2.16 o 2 8 2 1.19 0.81 0.08 o 3 8 2 29.11 30.63 1.86 o 4 8 2 7.35 5.75 0.37 o -4 -7 3 47.05 44.81 0.37 o -3 -7 3 136.19 125.69 2.94 o -2 -7 3 247.59 248.53 7.35 o -1 -7 3 36.40 36.89 2.05 o 0 -7 3 8.38 8.35 0.18 o -5 -6 3 79.22 68.40 2.09 o -4 -6 3 0.08 0.76 0.49 o -3 -6 3 227.69 225.82 1.95 o -2 -6 3 261.20 281.31 5.31 o -1 -6 3 387.37 396.58 13.40 o 0 -6 3 60.40 65.25 1.42 o 1 -6 3 140.76 144.84 0.97 o 2 -6 3 88.22 89.04 0.68 o -5 -5 3 134.53 126.26 6.18 o -4 -5 3 11.83 10.55 0.56 o -3 -5 3 2.62 3.39 0.12 o -2 -5 3 185.20 200.37 1.16 o -1 -5 3 0.20 0.66 0.14 o 0 -5 3 260.98 246.18 2.80 o 1 -5 3 18.68 22.34 0.56 o 2 -5 3 173.18 173.91 2.58 o 3 -5 3 40.00 48.27 0.83 o -5 -4 3 132.39 129.08 2.64 o -4 -4 3 52.50 53.42 0.86 o -3 -4 3 9.03 8.91 0.19 o -2 -4 3 210.27 222.99 5.63 o -1 -4 3 54.08 67.34 3.51 o 0 -4 3 13.65 13.45 0.61 o 1 -4 3 156.89 151.36 1.11 o 2 -4 3 79.88 86.68 1.47 o 3 -4 3 253.06 251.42 8.83 o 4 -4 3 32.30 39.41 0.50 o -6 -3 3 30.85 34.03 2.52 o -5 -3 3 0.09 0.11 0.14 o -4 -3 3 231.22 235.83 1.25 o -3 -3 3 97.53 107.17 2.44 o -2 -3 3 745.82 716.67 24.84 o -1 -3 3 613.54 701.02 36.76 o 0 -3 3 1064.93 1074.43 25.58 o 1 -3 3 44.51 32.32 0.44 o 2 -3 3 425.98 404.37 3.28 o 3 -3 3 441.98 398.18 14.83 o 4 -3 3 76.06 71.93 3.94 o -6 -2 3 182.46 190.72 15.98 o -5 -2 3 48.70 56.75 2.77 o -4 -2 3 3.72 4.44 0.14 o -3 -2 3 223.50 249.83 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224.66 204.07 5.23 o 1 1 3 287.92 260.80 2.13 o 2 1 3 893.21 778.05 26.94 o 3 1 3 2.68 2.02 0.24 o 4 1 3 47.74 42.83 0.71 o 5 1 3 136.31 135.85 5.25 o 6 1 3 14.04 12.21 0.38 o -5 2 3 111.74 98.53 3.62 o -4 2 3 243.67 252.70 4.70 o -3 2 3 46.56 43.18 0.62 o -2 2 3 209.84 234.50 2.45 o -1 2 3 744.49 899.73 18.33 o 0 2 3 848.98 728.31 7.90 o 1 2 3 1527.65 1251.76 16.60 o 2 2 3 125.46 117.66 4.10 o 3 2 3 305.91 281.86 11.41 o 4 2 3 0.95 4.05 0.19 o 5 2 3 189.18 199.69 14.00 o 6 2 3 2.37 2.52 0.28 o -4 3 3 479.79 458.41 6.09 o -3 3 3 187.13 196.03 1.68 o -2 3 3 69.58 66.86 0.71 o -1 3 3 534.73 648.27 11.49 o 0 3 3 231.25 251.19 1.29 o 1 3 3 175.62 138.83 1.36 o 2 3 3 755.21 637.45 341.54 o 3 3 3 56.93 56.22 0.66 o 4 3 3 81.52 71.32 5.91 o 5 3 3 191.28 191.50 21.59 o 6 3 3 42.48 53.57 1.02 o -4 4 3 17.34 15.03 0.31 o -3 4 3 266.58 272.16 11.62 o -2 4 3 1.05 0.62 0.13 o -1 4 3 390.69 410.36 10.06 o 0 4 3 126.14 126.68 0.58 o 1 4 3 223.06 205.11 2.51 o 2 4 3 69.41 54.74 1.35 o 3 4 3 188.61 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90.31 96.64 0.78 o 0 4 7 1.68 1.14 0.08 o 1 4 7 79.18 87.76 0.82 o 2 4 7 170.15 176.52 1.17 o 3 4 7 155.38 141.47 3.10 o 4 4 7 4.95 5.26 0.18 o 5 4 7 20.92 19.49 0.56 o -1 5 7 246.13 225.67 5.08 o 0 5 7 81.30 82.81 1.51 o 1 5 7 0.37 0.64 0.11 o 2 5 7 178.49 173.90 3.34 o 3 5 7 242.24 227.74 1.28 o 4 5 7 33.59 32.33 0.70 o 5 5 7 65.09 71.40 0.67 o 0 6 7 184.17 169.58 1.44 o 1 6 7 54.65 58.96 1.87 o 2 6 7 45.52 53.89 1.34 o 3 6 7 48.50 43.61 0.53 o 4 6 7 30.67 32.04 0.80 o 2 7 7 150.42 171.71 2.13 o 3 7 7 10.60 14.10 0.25 o -2 -4 8 3.73 1.96 0.08 o -1 -4 8 80.20 72.00 0.53 o 0 -4 8 87.80 84.00 1.30 o 1 -4 8 46.54 46.70 2.11 o -3 -3 8 27.36 22.04 0.59 o -2 -3 8 69.22 74.01 0.56 o -1 -3 8 0.33 0.74 0.16 o 0 -3 8 216.04 207.52 3.31 o 1 -3 8 102.29 106.11 2.93 o 2 -3 8 103.60 105.36 2.74 o -3 -2 8 47.67 43.39 0.48 o -2 -2 8 119.64 123.78 0.79 o -1 -2 8 24.65 26.46 0.59 o 0 -2 8 0.23 1.04 0.12 o 1 -2 8 254.86 268.58 5.36 o 2 -2 8 31.10 34.94 1.06 o 3 -2 8 13.41 14.98 0.67 o -3 -1 8 6.50 7.20 0.32 o -2 -1 8 97.30 92.80 1.61 o -1 -1 8 8.90 11.27 0.24 o 0 -1 8 11.31 14.61 0.28 o 1 -1 8 40.44 44.11 0.64 o 2 -1 8 79.55 85.62 0.90 o 3 -1 8 0.12 0.43 0.17 o 4 -1 8 0.19 0.94 0.13 o -3 0 8 25.03 24.01 0.67 o -2 0 8 106.81 96.60 1.05 o -1 0 8 171.96 168.32 2.27 o 0 0 8 4.64 5.38 0.10 o 1 0 8 226.32 239.29 1.42 o 2 0 8 82.08 89.74 1.21 o 3 0 8 154.08 165.58 2.38 o 4 0 8 28.46 32.26 2.75 o -3 1 8 13.64 15.26 0.60 o -2 1 8 286.58 263.11 8.16 o -1 1 8 211.73 213.82 1.18 o 0 1 8 55.02 58.63 0.56 o 1 1 8 77.17 76.37 1.43 o 2 1 8 239.03 263.60 1.58 o 3 1 8 39.44 40.29 1.48 o 4 1 8 183.84 190.57 15.21 o -3 2 8 86.45 79.94 2.20 o -2 2 8 83.90 85.13 3.66 o -1 2 8 181.72 180.98 3.43 o 0 2 8 72.16 85.26 0.80 o 1 2 8 4.21 4.35 0.16 o 2 2 8 37.35 42.60 0.67 o 3 2 8 16.95 17.44 0.68 o 4 2 8 1.39 2.05 0.16 o 5 2 8 0.74 0.31 0.15 o -2 3 8 187.53 189.03 3.79 o -1 3 8 14.43 15.47 0.31 o 0 3 8 391.93 415.65 4.00 o 1 3 8 30.34 37.06 0.56 o 2 3 8 18.81 22.83 0.42 o 3 3 8 189.30 192.90 1.72 o 4 3 8 9.61 9.12 0.21 o 5 3 8 22.29 19.93 0.39 o -1 4 8 57.58 57.30 0.52 o 0 4 8 115.51 105.91 0.75 o 1 4 8 381.70 381.66 6.38 o 2 4 8 2.41 2.45 0.13 o 3 4 8 378.85 367.38 1.63 o 4 4 8 220.40 202.40 3.91 o 5 4 8 30.93 31.61 0.45 o -1 5 8 37.02 35.09 0.51 o 0 5 8 64.10 60.10 0.56 o 1 5 8 104.95 100.09 1.77 o 2 5 8 38.40 37.82 1.07 o 3 5 8 49.69 52.34 0.58 o 4 5 8 96.51 86.68 1.10 o 1 6 8 49.30 53.95 0.76 o 2 6 8 35.51 40.70 0.44 o 3 6 8 68.86 83.54 0.61 o -1 -3 9 3.02 3.88 0.10 o 0 -3 9 68.97 75.76 1.18 o 1 -3 9 3.17 3.82 0.19 o -2 -2 9 29.61 30.47 0.33 o -1 -2 9 16.38 14.88 0.33 o 0 -2 9 24.30 22.44 0.27 o 1 -2 9 5.90 4.50 0.24 o 2 -2 9 3.49 3.95 0.25 o -2 -1 9 31.24 32.81 0.61 o -1 -1 9 321.44 315.46 4.95 o 0 -1 9 78.06 76.40 0.49 o 1 -1 9 10.02 9.98 0.22 o 2 -1 9 26.23 28.50 0.49 o 3 -1 9 22.01 20.32 0.35 o -2 0 9 1.91 3.83 0.11 o -1 0 9 367.22 353.25 1.93 o 0 0 9 325.67 331.70 2.34 o 1 0 9 179.49 191.04 6.01 o 2 0 9 27.20 30.36 0.54 o 3 0 9 152.73 157.23 6.67 o -2 1 9 22.98 25.04 0.96 o -1 1 9 38.87 41.44 2.01 o 0 1 9 57.66 58.64 0.45 o 1 1 9 86.40 93.07 2.01 o 2 1 9 73.51 81.00 2.51 o 3 1 9 12.24 13.35 0.30 o 4 1 9 152.79 143.90 5.65 o -2 2 9 74.99 71.85 2.08 o -1 2 9 155.07 167.29 5.40 o 0 2 9 23.49 25.40 0.50 o 1 2 9 28.77 32.46 1.65 o 2 2 9 58.89 66.32 1.72 o 3 2 9 0.16 0.52 0.25 o 4 2 9 141.39 135.66 3.41 o -1 3 9 98.87 92.95 2.27 o 0 3 9 259.80 258.76 3.29 o 1 3 9 120.46 112.72 3.06 o 2 3 9 152.02 148.61 4.23 o 3 3 9 5.63 6.50 0.16 o 4 3 9 62.32 66.29 1.31 o -1 4 9 8.57 6.83 0.17 o 0 4 9 25.51 25.75 0.25 o 1 4 9 319.59 300.73 1.24 o 2 4 9 102.57 94.14 1.02 o 3 4 9 95.63 92.88 1.25 o 4 4 9 24.93 28.14 0.39 o 1 5 9 60.01 63.11 0.50 o 2 5 9 63.35 64.66 0.54 o 3 5 9 69.21 67.81 1.49 o -1 -1 10 40.18 46.35 0.38 o 0 -1 10 85.93 86.82 0.54 o 1 -1 10 166.41 160.34 1.13 o -1 0 10 77.54 85.34 0.54 o 0 0 10 100.66 110.23 0.66 o 1 0 10 77.76 76.85 1.25 o 2 0 10 27.58 28.78 0.41 o -1 1 10 54.56 55.45 1.40 o 0 1 10 87.36 102.99 0.63 o 1 1 10 118.70 125.06 2.58 o 2 1 10 66.48 67.15 0.89 o 3 1 10 40.08 40.75 0.46 o -1 2 10 17.87 12.24 0.31 o 0 2 10 54.71 57.55 1.05 o 1 2 10 36.99 39.01 1.06 o 2 2 10 243.84 234.25 5.86 o 3 2 10 37.95 33.28 0.42 o 0 3 10 66.37 59.27 0.31 o 1 3 10 0.15 0.22 0.11 o 2 3 10 142.47 137.16 2.08 o 3 3 10 74.77 67.57 0.85 o 1 4 10 23.75 31.94 0.33 o 2 4 10 27.23 31.87 0.75 o