#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:57:33 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180930 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/10/2201012.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201012_Fobs loop_ _publ_author_name 'Reynoso-Paz, C. Mariuska' 'Olmstead, Marilyn M.' 'Kurth, Mark J.' 'Schore, Neil E.' _publ_section_title ; A solution phase catalyst for an enantioselective Diels--Alder reaction ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m310 _journal_page_last m312 _journal_volume 58 _journal_year 2002 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.5996 _cell_length_b 17.9326 _cell_length_c 19.5746 _exptl_crystal_F_000 1764.00 _reflns_d_resolution_high 0.6800 _cod_data_source_file ac60054sup2.hkl _cod_data_source_block 4 #BEGIN Tags that were not found in dictionaries: _shelx_title ' mn1347 in P2(1)2(1)2(1); Mariuska's Cat1.THF' _shelx_refln_list_code 4 _shelx_f_calc_maximum 294.73 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3252.46 3507.68 107.13 o 4 0 0 984.30 1116.29 45.21 o 6 0 0 30847.01 32387.88 954.31 o 8 0 0 368.00 442.74 33.74 o 10 0 0 546.21 538.49 40.92 o 12 0 0 18.67 19.92 25.55 o 14 0 0 1853.09 1919.23 72.67 o 1 1 0 16452.40 15900.01 443.85 o 2 1 0 15576.23 15717.11 292.18 o 3 1 0 1145.36 1097.26 52.74 o 4 1 0 7582.41 7921.39 168.76 o 5 1 0 1456.30 1497.76 40.42 o 6 1 0 890.16 739.95 31.72 o 7 1 0 313.36 343.05 24.80 o 8 1 0 7525.89 7811.09 172.35 o 9 1 0 349.76 330.96 23.25 o 10 1 0 105.36 97.52 19.14 o 11 1 0 14.96 43.19 18.47 o 12 1 0 890.91 777.64 40.79 o 13 1 0 35.74 26.30 17.15 o 14 1 0 290.78 320.14 25.71 o 15 1 0 312.96 326.58 24.64 o 1 2 0 505.36 547.40 11.44 o 2 2 0 36536.21 38049.67 629.46 o 3 2 0 19924.42 20481.28 346.52 o 4 2 0 561.71 655.93 49.18 o 5 2 0 1603.16 1699.53 44.35 o 6 2 0 8510.16 8669.88 187.41 o 7 2 0 962.61 834.28 32.42 o 8 2 0 35.51 -0.53 14.20 o 9 2 0 2617.58 2550.14 67.64 o 10 2 0 2574.63 2587.55 69.95 o 11 2 0 982.09 1000.72 40.41 o 12 2 0 181.97 189.23 20.38 o 13 2 0 758.07 783.85 35.08 o 14 2 0 1353.00 1321.69 45.71 o 15 2 0 154.94 146.02 25.35 o 1 3 0 91.59 78.75 4.43 o 2 3 0 12161.96 12382.44 230.84 o 3 3 0 1388.72 1254.01 33.04 o 4 3 0 15674.34 16349.76 257.31 o 5 3 0 3968.71 3535.90 73.16 o 6 3 0 144.46 174.19 11.61 o 7 3 0 1670.86 1908.65 52.10 o 8 3 0 320.23 346.01 22.13 o 9 3 0 4354.25 4237.53 101.34 o 10 3 0 311.23 257.55 20.29 o 11 3 0 92.06 102.49 17.58 o 12 3 0 94.77 100.12 18.42 o 13 3 0 370.24 386.91 26.34 o 14 3 0 1.06 -6.49 17.85 o 15 3 0 265.14 234.59 32.42 o 1 4 0 8278.09 8456.68 125.58 o 2 4 0 31.27 18.93 5.31 o 3 4 0 4115.80 3841.76 62.30 o 4 4 0 3114.69 2517.43 189.96 o 5 4 0 7761.83 8238.35 132.36 o 6 4 0 1085.32 1136.08 25.16 o 7 4 0 5389.00 5238.99 95.43 o 8 4 0 5165.87 5575.66 113.69 o 9 4 0 380.95 381.01 21.78 o 10 4 0 2358.43 2390.75 58.82 o 11 4 0 2074.36 2001.86 53.56 o 12 4 0 137.05 155.78 19.65 o 13 4 0 220.81 204.44 22.57 o 14 4 0 355.11 355.89 33.30 o 15 4 0 8.80 -12.72 24.53 o 1 5 0 6611.77 6581.52 105.44 o 2 5 0 189.41 159.18 7.14 o 3 5 0 703.79 741.80 19.30 o 4 5 0 13066.26 13125.15 191.89 o 5 5 0 1502.86 1745.10 33.70 o 6 5 0 8219.53 8240.59 144.08 o 7 5 0 736.99 769.09 23.57 o 8 5 0 1579.71 1421.76 39.59 o 9 5 0 442.87 449.64 22.53 o 10 5 0 913.07 866.44 32.99 o 11 5 0 8.44 -15.73 15.73 o 12 5 0 2320.84 2363.75 61.33 o 13 5 0 421.65 434.15 27.58 o 14 5 0 88.41 84.46 22.59 o 15 5 0 384.95 442.93 67.64 o 1 6 0 120.83 145.34 7.05 o 2 6 0 18.49 58.25 6.95 o 3 6 0 4921.14 5324.19 81.44 o 4 6 0 1285.92 1046.09 30.23 o 5 6 0 1507.22 1467.21 28.17 o 7 6 0 676.12 701.36 25.30 o 8 6 0 1689.95 1741.05 45.11 o 9 6 0 1657.83 1723.39 50.88 o 10 6 0 163.98 172.55 17.88 o 11 6 0 131.60 111.99 18.35 o 12 6 0 25.44 32.19 16.77 o 13 6 0 16.61 32.95 19.42 o 14 6 0 166.19 171.72 29.95 o 15 6 0 4.13 -39.85 44.48 o 1 7 0 43.29 55.57 6.10 o 2 7 0 22.77 15.11 5.76 o 3 7 0 831.03 770.10 18.31 o 4 7 0 3126.50 3066.43 57.72 o 5 7 0 2174.88 1998.66 35.23 o 6 7 0 8979.00 8984.68 134.57 o 7 7 0 557.43 545.81 23.47 o 8 7 0 483.46 453.47 24.58 o 9 7 0 335.77 384.57 21.05 o 10 7 0 2199.40 2161.26 54.57 o 11 7 0 723.75 629.98 29.21 o 12 7 0 719.24 760.29 36.90 o 13 7 0 1.45 -2.29 25.89 o 14 7 0 221.98 250.02 33.42 o 0 8 0 37.15 24.59 6.67 o 1 8 0 5998.03 5906.18 90.10 o 2 8 0 1321.18 1369.89 26.23 o 3 8 0 11516.95 11568.07 172.84 o 4 8 0 30.30 26.69 7.72 o 5 8 0 1427.40 1339.41 29.07 o 6 8 0 2091.45 2127.79 38.21 o 7 8 0 702.39 729.06 25.81 o 8 8 0 261.67 293.99 21.48 o 9 8 0 115.74 69.15 23.67 o 10 8 0 210.82 212.78 21.78 o 11 8 0 138.82 121.40 24.78 o 12 8 0 330.84 372.19 33.51 o 13 8 0 146.79 133.17 28.82 o 14 8 0 31.08 25.31 24.89 o 1 9 0 7217.18 7406.40 112.23 o 2 9 0 4648.34 4676.45 73.30 o 3 9 0 198.04 255.80 11.85 o 4 9 0 1049.30 974.78 24.04 o 5 9 0 7445.33 7206.01 103.27 o 6 9 0 3711.01 3591.84 58.66 o 7 9 0 465.49 483.70 18.60 o 8 9 0 46.35 47.73 13.52 o 9 9 0 1545.26 1641.10 44.10 o 10 9 0 56.08 48.01 22.35 o 11 9 0 56.07 42.65 23.53 o 12 9 0 0.36 -6.90 22.43 o 13 9 0 8.54 4.42 22.92 o 14 9 0 10.31 6.83 31.08 o 1 10 0 11402.72 11690.54 186.96 o 2 10 0 229.90 271.27 11.03 o 3 10 0 1275.49 1249.24 26.55 o 4 10 0 3069.25 3103.25 59.70 o 5 10 0 3514.29 3443.66 61.10 o 6 10 0 1036.49 950.48 25.58 o 7 10 0 6410.62 6261.76 113.20 o 8 10 0 24.54 54.89 16.78 o 9 10 0 103.93 148.20 23.18 o 10 10 0 442.38 468.37 33.16 o 11 10 0 337.98 357.33 31.54 o 12 10 0 87.05 100.01 35.15 o 13 10 0 632.75 701.07 45.29 o 14 10 0 1249.23 1328.78 107.49 o 1 11 0 1473.03 1625.43 31.33 o 2 11 0 10751.90 10745.31 187.25 o 3 11 0 4388.18 4290.87 68.89 o 4 11 0 21.06 10.06 8.59 o 5 11 0 802.05 824.28 26.45 o 6 11 0 36.76 30.78 10.99 o 7 11 0 1.21 2.17 13.62 o 8 11 0 4036.97 3794.72 108.78 o 9 11 0 1247.55 1347.35 54.39 o 10 11 0 216.19 210.74 30.67 o 11 11 0 34.63 44.43 23.53 o 12 11 0 547.16 600.67 45.38 o 13 11 0 149.58 111.04 28.49 o 14 11 0 53.63 36.14 44.48 o 0 12 0 6841.62 6456.79 163.19 o 1 12 0 4190.49 4323.58 69.72 o 2 12 0 41.65 56.82 10.24 o 3 12 0 325.74 350.22 18.98 o 4 12 0 1962.68 2001.28 48.43 o 5 12 0 1009.27 963.54 29.77 o 6 12 0 1928.69 2010.42 41.71 o 7 12 0 43.70 41.94 18.51 o 8 12 0 42.61 51.57 18.94 o 9 12 0 754.49 686.24 40.29 o 10 12 0 2175.99 2142.79 74.00 o 11 12 0 138.39 141.83 26.18 o 12 12 0 305.64 297.64 32.27 o 13 12 0 25.47 50.71 25.26 o 1 13 0 475.63 460.39 18.20 o 2 13 0 4530.68 4495.73 78.27 o 3 13 0 264.93 298.99 17.96 o 4 13 0 5211.85 5040.42 94.41 o 5 13 0 2694.28 2726.56 56.89 o 6 13 0 7.52 -1.76 11.77 o 7 13 0 109.28 111.88 16.23 o 8 13 0 353.62 372.45 25.92 o 9 13 0 2.45 2.01 20.50 o 10 13 0 745.42 715.58 42.07 o 11 13 0 1225.08 1229.53 55.81 o 12 13 0 480.06 541.01 40.67 o 13 13 0 1044.28 1014.66 95.44 o 0 14 0 14139.16 14265.62 351.17 o 1 14 0 60.58 65.82 13.18 o 2 14 0 407.95 422.03 18.32 o 3 14 0 3482.46 3397.51 67.39 o 4 14 0 21.87 29.40 12.70 o 5 14 0 739.15 751.07 30.45 o 6 14 0 175.37 186.57 21.13 o 7 14 0 172.42 195.08 18.73 o 8 14 0 16.56 13.41 17.08 o 9 14 0 113.21 132.58 25.14 o 10 14 0 823.17 903.82 46.71 o 11 14 0 62.42 47.13 24.95 o 12 14 0 21.47 31.24 28.68 o 13 14 0 75.58 67.64 49.11 o 1 15 0 1122.77 1051.89 41.73 o 2 15 0 405.50 402.21 19.40 o 3 15 0 37.10 25.84 11.46 o 4 15 0 340.69 358.38 21.33 o 5 15 0 4240.42 4241.82 91.11 o 6 15 0 594.65 542.73 31.64 o 7 15 0 429.79 430.97 23.96 o 8 15 0 0.02 24.33 17.82 o 9 15 0 329.82 371.68 28.20 o 10 15 0 103.52 101.37 25.58 o 11 15 0 1430.20 1459.30 62.93 o 12 15 0 59.50 104.35 28.43 o 0 16 0 1040.96 983.87 47.26 o 1 16 0 67.61 64.37 12.10 o 2 16 0 5668.08 5851.23 109.45 o 3 16 0 321.63 354.80 22.17 o 4 16 0 41.52 43.56 18.33 o 5 16 0 36.67 32.60 15.51 o 6 16 0 106.71 88.48 16.99 o 7 16 0 1043.23 996.56 50.99 o 8 16 0 134.63 187.27 22.51 o 9 16 0 238.82 247.08 25.75 o 10 16 0 101.77 117.74 26.84 o 11 16 0 565.88 611.91 57.74 o 12 16 0 99.19 133.19 36.25 o 1 17 0 516.76 525.30 26.12 o 2 17 0 823.16 825.36 33.05 o 3 17 0 47.42 34.50 15.83 o 4 17 0 1570.99 1479.40 49.87 o 5 17 0 1247.33 1234.51 45.46 o 6 17 0 1823.05 1745.83 55.21 o 7 17 0 79.02 103.71 17.95 o 8 17 0 1337.97 1343.88 48.65 o 9 17 0 56.02 40.16 20.60 o 10 17 0 747.51 784.37 47.93 o 11 17 0 286.88 297.83 33.31 o 0 18 0 185.46 157.28 31.08 o 1 18 0 107.85 98.96 21.22 o 2 18 0 1153.82 1230.92 40.05 o 3 18 0 883.02 881.42 34.79 o 4 18 0 2248.44 2231.67 65.15 o 5 18 0 0.16 7.98 18.30 o 6 18 0 535.16 591.04 32.73 o 7 18 0 6.65 29.96 19.19 o 8 18 0 224.06 276.18 42.62 o 9 18 0 397.17 427.14 36.60 o 10 18 0 95.57 107.02 28.72 o 11 18 0 59.34 48.35 31.43 o 1 19 0 326.90 311.12 26.92 o 2 19 0 98.06 100.38 18.47 o 3 19 0 8.34 20.74 16.01 o 4 19 0 576.95 591.15 32.67 o 5 19 0 381.08 415.58 29.58 o 6 19 0 920.10 914.62 41.22 o 7 19 0 18.06 15.35 26.30 o 8 19 0 709.55 876.29 48.33 o 9 19 0 55.04 64.21 26.88 o 10 19 0 35.85 101.00 47.26 o 0 20 0 4.04 -8.91 27.04 o 1 20 0 430.36 483.06 31.50 o 2 20 0 1691.85 1747.80 93.22 o 3 20 0 472.26 484.79 30.71 o 4 20 0 228.28 169.50 23.14 o 5 20 0 18.86 4.96 18.73 o 6 20 0 444.92 452.04 31.01 o 7 20 0 1620.33 1649.49 56.97 o 8 20 0 98.39 97.67 27.76 o 9 20 0 2.19 8.20 26.27 o 1 21 0 1464.43 1445.87 51.88 o 2 21 0 854.08 888.08 41.09 o 3 21 0 293.92 283.53 27.09 o 4 21 0 354.00 312.77 27.62 o 5 21 0 335.91 325.70 28.61 o 6 21 0 200.24 183.94 24.76 o 7 21 0 43.87 28.47 20.79 o 8 21 0 10.57 -8.71 29.65 o 9 21 0 710.93 737.60 82.47 o 0 22 0 694.25 661.56 53.06 o 1 22 0 192.83 245.36 27.28 o 2 22 0 97.90 96.14 23.15 o 3 22 0 7.99 7.71 19.78 o 4 22 0 285.08 271.10 28.60 o 5 22 0 1.06 -9.68 19.81 o 6 22 0 10.49 8.99 20.92 o 7 22 0 1719.86 1838.25 62.58 o 8 22 0 155.51 113.98 50.96 o 1 23 0 43.19 42.22 21.77 o 2 23 0 1006.58 992.93 69.77 o 3 23 0 19.71 23.35 22.10 o 4 23 0 24.67 21.96 22.35 o 5 23 0 189.66 205.56 27.20 o 6 23 0 57.04 76.27 27.10 o 7 23 0 124.49 50.96 45.40 o 0 24 0 2023.46 2085.44 96.64 o 1 24 0 120.44 128.66 24.71 o 2 24 0 4.18 7.60 21.54 o 3 24 0 0.51 -21.58 21.58 o 4 24 0 470.32 520.84 36.32 o 5 24 0 370.65 341.32 34.93 o 1 25 0 357.57 334.90 31.61 o 2 25 0 538.62 518.78 36.63 o 3 25 0 7.61 34.65 37.99 o 4 25 0 62.47 39.85 46.33 o 1 0 1 19475.08 19482.61 441.23 o 2 0 1 9561.38 9281.42 158.58 o 3 0 1 3494.85 3401.14 75.40 o 4 0 1 8801.38 9168.02 194.36 o 5 0 1 926.72 989.79 30.92 o 6 0 1 1325.72 1578.05 45.63 o 7 0 1 2708.51 2700.90 67.41 o 8 0 1 1691.35 1684.40 49.57 o 9 0 1 3774.48 3791.74 92.43 o 10 0 1 1718.52 1841.48 55.12 o 11 0 1 286.05 332.70 26.35 o 12 0 1 244.23 175.28 22.22 o 13 0 1 918.51 883.96 36.55 o 14 0 1 72.86 91.73 20.07 o 15 0 1 676.95 738.41 33.28 o -15 1 1 411.01 365.39 25.38 o -14 1 1 333.56 346.53 26.80 o -13 1 1 258.09 253.35 23.45 o -12 1 1 532.02 566.25 28.69 o -11 1 1 839.29 770.73 39.99 o -10 1 1 249.35 237.97 21.95 o -9 1 1 2515.01 2557.84 67.18 o -8 1 1 4279.29 4229.86 101.23 o -7 1 1 926.64 1009.42 35.32 o -6 1 1 3111.06 3049.27 76.33 o -5 1 1 4593.09 4865.24 133.75 o -4 1 1 2633.19 2639.47 63.82 o -3 1 1 26518.36 26768.40 561.29 o -2 1 1 3810.51 3770.83 72.27 o -1 1 1 20127.56 19608.89 356.96 o 1 1 1 19696.54 19696.77 472.38 o 2 1 1 3768.83 3768.84 92.72 o 3 1 1 27187.03 27265.48 501.43 o 4 1 1 2869.69 2910.10 64.28 o 5 1 1 5518.42 5744.79 134.82 o 6 1 1 3323.37 3354.12 76.79 o 7 1 1 888.45 932.33 34.74 o 8 1 1 4395.63 4407.16 101.57 o 9 1 1 2406.37 2459.42 66.83 o 10 1 1 258.72 265.26 22.44 o 11 1 1 938.47 921.80 37.99 o 12 1 1 471.05 458.29 40.79 o 13 1 1 277.60 300.85 26.94 o 14 1 1 326.43 353.78 24.41 o 15 1 1 370.00 360.71 25.55 o -15 2 1 83.52 48.32 23.04 o -14 2 1 279.05 257.57 24.64 o -13 2 1 195.74 211.11 22.24 o -12 2 1 167.01 153.61 19.82 o -11 2 1 399.42 392.87 27.15 o -10 2 1 1766.93 1924.91 54.32 o -9 2 1 170.40 174.93 19.95 o -8 2 1 2682.87 2705.42 72.27 o -7 2 1 928.46 1060.93 36.58 o -6 2 1 6948.84 7048.57 155.32 o -5 2 1 4854.34 4995.17 96.46 o -4 2 1 25184.63 26018.02 518.11 o -3 2 1 4801.43 5018.65 78.00 o -2 2 1 25422.90 25499.22 426.08 o -1 2 1 16166.18 16714.51 311.10 o 0 2 1 48981.71 49631.33 782.01 o 1 2 1 16251.23 16844.70 304.79 o 2 2 1 25999.07 26655.38 1069.33 o 3 2 1 4291.45 4503.95 91.46 o 4 2 1 23037.87 24272.46 464.71 o 5 2 1 4595.54 4860.02 96.38 o 6 2 1 6981.88 7173.05 155.32 o 7 2 1 1030.77 1082.96 36.36 o 8 2 1 2996.47 3046.45 73.19 o 9 2 1 211.73 206.11 20.91 o 10 2 1 1481.72 1582.04 52.47 o 11 2 1 344.42 362.71 26.21 o 12 2 1 167.70 170.29 22.28 o 13 2 1 242.58 261.30 23.44 o 14 2 1 391.69 366.56 26.63 o 15 2 1 104.43 75.35 21.16 o -15 3 1 138.56 107.18 28.68 o -14 3 1 74.31 85.89 20.49 o -13 3 1 190.73 180.67 21.59 o -12 3 1 3076.85 3154.83 74.03 o -11 3 1 521.43 540.92 31.63 o -10 3 1 1293.01 1257.87 39.63 o -9 3 1 1323.44 1365.52 40.36 o -8 3 1 1667.95 1641.32 43.27 o -7 3 1 1634.22 1694.01 42.07 o -6 3 1 2752.38 2532.53 56.23 o -5 3 1 4977.49 5111.74 83.88 o -4 3 1 5351.32 5581.22 93.88 o -3 3 1 15040.48 15400.05 238.65 o -2 3 1 32499.83 31778.13 965.08 o -1 3 1 57.53 71.32 8.74 o 0 3 1 8577.20 8736.01 149.63 o 1 3 1 45.11 66.70 5.65 o 2 3 1 33094.18 33075.06 1331.56 o 3 3 1 15169.06 15403.22 223.55 o 4 3 1 5954.45 6206.85 123.83 o 5 3 1 5030.46 5108.26 90.36 o 6 3 1 2914.90 2750.59 57.02 o 7 3 1 1483.13 1547.86 46.68 o 8 3 1 1521.21 1539.26 47.36 o 9 3 1 1342.54 1373.14 45.28 o 10 3 1 1332.07 1240.72 43.76 o 11 3 1 473.90 497.64 26.32 o 12 3 1 2999.95 2971.06 73.14 o 13 3 1 219.10 214.56 22.13 o 14 3 1 62.89 65.03 20.52 o 15 3 1 126.88 110.56 28.08 o -15 4 1 76.76 67.29 27.27 o -14 4 1 540.07 545.51 31.03 o -13 4 1 376.97 358.61 25.50 o -12 4 1 795.19 793.01 34.20 o -11 4 1 299.52 331.18 22.96 o -10 4 1 673.38 711.49 30.50 o -9 4 1 156.75 166.41 17.56 o -8 4 1 1637.75 1673.94 48.68 o -7 4 1 1793.17 1756.87 38.13 o -6 4 1 5340.51 5296.14 87.03 o -5 4 1 94.36 110.52 8.07 o -4 4 1 5862.13 5559.66 95.17 o -3 4 1 10878.65 11290.86 166.33 o -2 4 1 4815.25 4854.08 92.56 o -1 4 1 17078.38 17266.33 510.42 o 0 4 1 16201.45 16528.19 281.25 o 1 4 1 17444.69 17339.06 718.14 o 2 4 1 4822.03 4785.32 72.94 o 3 4 1 10673.39 11182.08 177.80 o 4 4 1 5604.50 5409.27 82.20 o 5 4 1 79.05 78.83 8.55 o 6 4 1 5209.74 5182.27 93.44 o 7 4 1 1635.14 1652.78 47.42 o 8 4 1 1758.33 1799.05 45.38 o 9 4 1 138.89 137.96 16.48 o 10 4 1 617.69 640.74 29.49 o 11 4 1 301.46 303.86 22.78 o 12 4 1 767.13 802.25 34.30 o 13 4 1 310.47 281.47 23.85 o 14 4 1 541.50 587.38 35.67 o 15 4 1 94.92 106.02 28.92 o -15 5 1 308.92 335.44 60.23 o -14 5 1 91.22 89.91 22.41 o -13 5 1 145.60 150.72 21.48 o -12 5 1 733.32 719.06 34.24 o -11 5 1 200.11 215.37 20.45 o -10 5 1 34.44 39.47 15.44 o -9 5 1 2431.18 2425.69 60.20 o -8 5 1 724.38 684.08 28.16 o -7 5 1 253.51 281.84 13.71 o -6 5 1 1936.89 2084.50 42.59 o -4 5 1 5340.07 5561.54 87.51 o -3 5 1 307.81 383.14 15.81 o -2 5 1 3058.35 2924.92 54.23 o -1 5 1 5007.41 4922.92 94.91 o 0 5 1 123.65 100.19 6.42 o 1 5 1 5507.07 4945.41 213.12 o 2 5 1 3132.99 2998.70 46.66 o 3 5 1 304.49 358.03 13.01 o 4 5 1 5789.49 6078.16 87.63 o 5 5 1 7611.13 7299.57 109.42 o 6 5 1 2157.97 2221.13 111.20 o 7 5 1 236.21 231.94 12.78 o 8 5 1 641.98 594.86 33.57 o 9 5 1 2689.48 2676.88 60.67 o 10 5 1 13.99 17.10 14.02 o 11 5 1 125.66 144.68 18.59 o 12 5 1 706.85 703.03 31.54 o 13 5 1 195.59 178.70 24.26 o 14 5 1 73.22 68.41 22.17 o 15 5 1 351.18 346.39 45.51 o -15 6 1 100.67 101.93 49.11 o -14 6 1 16.40 13.70 25.67 o -13 6 1 246.53 271.22 23.46 o -12 6 1 944.51 937.36 35.95 o -11 6 1 1319.74 1355.03 45.34 o -10 6 1 42.63 57.59 15.46 o -9 6 1 66.58 63.92 14.76 o -8 6 1 168.94 181.23 16.32 o -7 6 1 10340.06 10182.23 178.65 o -6 6 1 788.81 808.29 24.03 o -5 6 1 899.87 1058.55 22.83 o -4 6 1 159.18 158.97 9.35 o -3 6 1 1464.62 1238.06 41.51 o -2 6 1 4182.81 4394.44 73.36 o -1 6 1 2927.92 3101.62 62.39 o 0 6 1 2232.13 2340.08 37.97 o 2 6 1 4375.42 4520.79 68.67 o 3 6 1 1979.06 1728.16 75.06 o 4 6 1 181.43 169.23 10.42 o 5 6 1 914.46 1041.15 22.67 o 6 6 1 866.37 881.84 23.32 o 8 6 1 160.78 176.88 17.74 o 9 6 1 111.88 106.07 15.03 o 10 6 1 40.14 51.15 14.92 o 11 6 1 1287.74 1288.95 40.93 o 12 6 1 878.19 828.12 39.12 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45.25 o -4 7 16 734.77 719.13 31.48 o -3 7 16 1052.20 1016.61 51.07 o -2 7 16 978.28 972.72 52.28 o -1 7 16 160.21 163.57 27.67 o 0 7 16 211.40 202.69 20.77 o 1 7 16 235.79 269.21 18.66 o 2 7 16 1060.61 1057.29 32.86 o 3 7 16 1048.38 1022.97 29.86 o 4 7 16 713.11 699.70 29.86 o 5 7 16 1241.03 1265.34 39.03 o 6 7 16 722.60 690.70 31.54 o 7 7 16 403.38 427.49 24.98 o 8 7 16 63.17 73.30 21.18 o 9 7 16 426.21 440.56 30.90 o 10 7 16 8.37 6.27 25.27 o 11 7 16 267.57 251.66 34.03 o -11 8 16 149.14 98.76 25.85 o -10 8 16 261.96 244.82 29.21 o -9 8 16 86.89 90.25 24.13 o -8 8 16 336.17 329.75 29.27 o -7 8 16 843.89 856.76 39.85 o -6 8 16 33.70 17.81 17.27 o -5 8 16 719.55 643.23 45.88 o -4 8 16 975.91 886.42 48.28 o -3 8 16 429.79 430.38 35.41 o -2 8 16 976.33 931.18 50.67 o -1 8 16 1555.84 1547.40 60.95 o 0 8 16 259.60 229.06 19.69 o 1 8 16 1334.25 1407.68 39.66 o 2 8 16 938.23 944.36 40.86 o 3 8 16 569.26 543.08 26.71 o 4 8 16 984.73 967.69 32.10 o 5 8 16 837.46 837.49 32.44 o 6 8 16 59.16 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237.21 206.64 21.16 o -5 10 16 52.51 18.94 18.97 o -4 10 16 344.11 314.30 36.30 o -3 10 16 653.13 632.98 48.73 o -2 10 16 228.88 193.76 29.11 o -1 10 16 1244.80 1221.62 44.84 o 0 10 16 384.17 465.61 29.26 o 1 10 16 1059.28 1073.67 43.32 o 2 10 16 270.49 285.91 25.61 o 3 10 16 909.44 912.88 34.93 o 4 10 16 371.86 375.07 24.45 o 5 10 16 74.98 70.51 17.93 o 6 10 16 211.63 198.88 22.82 o 7 10 16 1705.43 1714.84 50.12 o 8 10 16 327.90 324.94 27.84 o 9 10 16 50.62 29.68 21.29 o 10 10 16 73.47 64.82 28.26 o 11 10 16 648.60 613.24 55.65 o -11 11 16 57.37 30.58 45.40 o -10 11 16 260.06 297.71 40.47 o -9 11 16 989.44 1008.22 64.33 o -8 11 16 1377.44 1344.94 52.86 o -7 11 16 138.67 93.52 22.92 o -6 11 16 263.02 217.43 22.30 o -5 11 16 375.90 398.65 37.74 o -4 11 16 160.75 126.18 28.14 o -3 11 16 175.18 187.14 28.20 o -2 11 16 678.63 696.33 43.23 o -1 11 16 598.91 574.40 31.40 o 0 11 16 72.05 60.69 17.18 o 1 11 16 628.70 640.18 33.50 o 2 11 16 631.80 676.75 35.78 o 3 11 16 125.67 136.40 22.90 o 4 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o 0 10 26 650.08 746.86 87.10 o 1 10 26 298.68 340.07 67.64 o 2 10 26 200.43 232.58 62.08 o 1 0 27 80.53 96.71 32.02 o 2 0 27 182.06 169.94 43.19 o 3 0 27 407.61 359.17 59.30 o 4 0 27 2.08 -47.26 47.26 o 5 0 27 34.57 56.52 55.60 o -4 1 27 164.73 102.86 57.45 o -3 1 27 7.59 5.23 28.69 o -2 1 27 124.80 119.82 32.81 o -1 1 27 141.38 104.80 33.73 o 0 1 27 50.26 26.27 30.16 o 1 1 27 94.73 99.87 32.30 o 2 1 27 114.31 104.24 33.20 o 3 1 27 12.50 -27.70 27.70 o 4 1 27 174.16 166.19 40.56 o 5 1 27 86.82 72.28 52.82 o -5 2 27 125.05 72.28 63.01 o -4 2 27 231.40 281.77 48.65 o -3 2 27 83.54 53.13 32.21 o -2 2 27 55.37 65.94 31.41 o -1 2 27 44.26 3.40 29.68 o 0 2 27 1264.07 1226.17 62.41 o 1 2 27 48.03 61.93 30.90 o 2 2 27 72.13 86.61 31.15 o 3 2 27 124.69 87.50 30.98 o -4 3 27 360.43 323.39 50.96 o -3 3 27 13.70 -5.81 25.68 o -2 3 27 226.45 216.85 34.38 o -1 3 27 129.98 85.07 31.45 o 0 3 27 36.06 22.47 29.37 o 1 3 27 128.50 100.26 31.41 o 2 3 27 196.58 180.55 34.43 o 3 3 27 13.09 14.83 44.48 o -4 4 27 70.48 36.14 41.70 o -3 4 27 170.48 224.52 35.40 o -2 4 27 25.00 20.55 25.82 o -1 4 27 36.37 10.31 29.51 o 0 4 27 198.43 210.04 35.72 o 1 4 27 46.32 21.80 35.40 o 2 4 27 27.54 -9.44 36.26 o -4 5 27 104.52 75.06 42.62 o -3 5 27 20.28 25.02 37.99 o -2 5 27 103.17 102.86 40.77 o -1 5 27 433.27 527.53 44.43 o 0 5 27 1.66 -8.01 36.41 o -4 6 27 125.30 132.51 60.23 o -3 6 27 395.66 439.22 76.91 o -2 6 27 10.09 6.49 55.60 o -1 6 27 120.74 143.63 57.45 o 0 6 27 72.02 148.26 55.60 o -2 7 27 104.32 91.74 56.52 o -1 7 27 144.61 222.39 63.01 o 0 7 27 43.30 144.55 53.74 o 1 7 27 143.78 208.49 55.60 o -1 8 27 35.71 51.89 55.60 o 0 8 27 865.79 1033.19 101.00 o 1 8 27 30.92 100.08 52.82 o 2 8 27 19.19 31.51 43.55 o 0 0 28 216.75 183.47 67.64 o 1 0 28 336.47 255.89 58.84 o 2 0 28 67.58 51.89 58.38 o -1 1 28 145.63 87.69 43.11 o 0 1 28 226.10 178.80 47.82 o 1 1 28 181.10 123.24 58.38 o 2 1 28 158.78 195.52 63.94 o 3 1 28 40.67 0.00 54.67 o -2 2 28 71.87 75.98 59.30 o -1 2 28 58.00 67.64 58.38 o 0 2 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