#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/10/2201035.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201035_Fobs loop_ _publ_author_name 'Zhu, Miaoli' 'Lu, Liping' 'Yang, Pin' 'Jin, Xianglin' _publ_section_title ; Bis(1,1-dimethylbiguanido)nickel(II) ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m272 _journal_page_last m274 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.050 _cell_angle_gamma 90.000 _cell_length_a 6.4120 _cell_length_b 9.0320 _cell_length_c 11.2390 _exptl_crystal_F_000 332.00 _reflns_d_resolution_high 0.7702 _[local]_cod_data_source_file bt6135Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' j277 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 100.16 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 4772.29 4928.50 10.53 o 2 0 0 9105.13 9283.97 34.31 o 3 0 0 1487.47 1375.68 18.96 o 5 0 0 2684.50 2533.17 17.15 o 6 0 0 471.61 468.89 20.47 o 7 0 0 591.69 544.13 14.15 o 8 0 0 23.39 45.14 13.54 o 1 1 0 3474.42 3631.67 37.32 o 2 1 0 675.24 711.16 15.05 o 3 1 0 440.27 462.57 6.92 o 4 1 0 116.91 113.16 4.82 o 5 1 0 0.58 1.20 4.21 o 6 1 0 74.25 70.42 6.62 o 7 1 0 2.13 -1.50 6.32 o 8 1 0 51.74 43.34 8.13 o 0 2 0 251.77 245.58 4.82 o 1 2 0 9685.16 9062.46 32.50 o 2 2 0 6749.43 6842.89 93.00 o 3 2 0 4519.86 4582.70 30.70 o 4 2 0 1361.17 1272.15 11.14 o 5 2 0 523.52 520.36 13.24 o 6 2 0 715.47 688.89 19.86 o 7 2 0 108.57 104.73 7.52 o 8 2 0 278.48 278.99 12.04 o 1 3 0 328.14 337.37 3.01 o 2 3 0 9.19 15.05 3.91 o 3 3 0 24.08 25.88 3.91 o 4 3 0 21.71 22.87 4.82 o 5 3 0 3.89 6.62 4.21 o 6 3 0 45.86 38.22 6.62 o 7 3 0 6.09 11.44 5.42 o 0 4 0 428.74 415.02 17.76 o 1 4 0 2586.11 2526.25 57.78 o 2 4 0 288.24 272.07 7.22 o 3 4 0 1329.30 1227.31 14.15 o 4 4 0 386.97 359.95 6.32 o 5 4 0 299.96 313.00 7.52 o 6 4 0 285.47 291.63 12.04 o 7 4 0 316.64 306.07 11.74 o 1 5 0 20.33 25.58 3.91 o 2 5 0 4.33 4.82 4.51 o 3 5 0 11.23 9.63 3.91 o 4 5 0 0.09 1.50 5.12 o 5 5 0 0.03 3.01 6.02 o 6 5 0 136.72 111.66 9.93 o 7 5 0 0.90 6.32 6.02 o 0 6 0 1745.66 1706.13 25.28 o 1 6 0 225.32 214.88 6.62 o 2 6 0 1116.66 1154.78 29.79 o 3 6 0 295.35 282.00 9.63 o 4 6 0 297.55 282.90 33.11 o 5 6 0 553.48 479.43 57.78 o 6 6 0 74.42 58.08 10.53 o 7 6 0 162.01 158.30 14.15 o 1 7 0 5.56 -1.81 3.01 o 2 7 0 34.80 44.84 5.72 o 3 7 0 0.10 9.33 4.82 o 4 7 0 61.27 51.46 5.12 o 5 7 0 21.21 14.75 6.92 o 6 7 0 20.14 16.25 6.92 o 0 8 0 940.00 928.16 26.48 o 1 8 0 1231.47 1178.25 83.06 o 2 8 0 545.23 571.22 13.84 o 3 8 0 562.84 601.92 31.60 o 4 8 0 649.36 644.35 30.40 o 5 8 0 202.75 221.81 9.93 o 6 8 0 249.05 252.20 10.23 o 1 9 0 1.92 -4.51 12.34 o 2 9 0 0.28 5.72 8.73 o 3 9 0 38.02 34.61 7.52 o 4 9 0 9.64 17.46 10.53 o 5 9 0 10.54 3.91 11.14 o 0 10 0 810.95 747.58 15.95 o 1 10 0 639.86 698.52 14.45 o 2 10 0 715.26 803.86 16.85 o 3 10 0 472.78 481.83 24.68 o 4 10 0 345.02 371.98 33.11 o 1 11 0 0.61 -0.30 7.52 o 2 11 0 5.10 7.22 9.03 o -8 1 1 75.45 80.66 9.63 o -7 1 1 159.88 149.28 12.94 o -6 1 1 298.30 301.86 5.12 o -5 1 1 692.42 706.35 9.93 o -4 1 1 771.33 794.53 15.05 o -3 1 1 780.41 760.22 6.92 o -2 1 1 306.10 295.54 6.32 o -1 1 1 6086.48 6232.85 13.24 o 0 1 1 2791.32 2823.59 29.79 o 1 1 1 4167.49 4243.52 24.68 o 2 1 1 797.85 732.53 10.23 o 3 1 1 1751.05 1727.80 17.15 o 4 1 1 1824.28 1749.47 22.87 o 5 1 1 759.86 710.56 8.73 o 6 1 1 610.70 550.15 14.15 o 7 1 1 72.67 72.83 11.14 o 8 1 1 240.90 233.84 8.43 o -8 2 1 21.20 24.08 9.93 o -7 2 1 26.08 23.17 10.53 o -6 2 1 14.30 15.95 7.82 o -5 2 1 10.47 18.96 6.62 o -4 2 1 277.85 280.19 4.21 o -3 2 1 971.37 1059.98 12.64 o -2 2 1 220.81 230.84 4.82 o -1 2 1 1863.42 1872.56 18.66 o 0 2 1 246.70 241.07 3.91 o 1 2 1 9898.08 9889.20 70.12 o 2 2 1 42.98 43.94 4.21 o 3 2 1 54.85 51.46 6.02 o 4 2 1 16.97 15.95 7.52 o 5 2 1 154.37 158.30 8.43 o 6 2 1 88.42 79.15 5.72 o 7 2 1 4.89 5.72 8.13 o 8 2 1 4.35 11.44 9.93 o -8 3 1 52.86 55.08 10.53 o -7 3 1 182.87 189.30 7.22 o -6 3 1 144.02 162.22 8.43 o -4 3 1 570.42 593.79 12.64 o -3 3 1 1853.73 1896.64 9.03 o -2 3 1 3969.36 3975.36 19.56 o -1 3 1 54.63 43.64 4.51 o 0 3 1 3730.79 3644.61 34.31 o 1 3 1 2268.59 2263.21 34.91 o 2 3 1 10031.80 9904.54 88.48 o 3 3 1 1692.59 1642.03 27.69 o 4 3 1 909.00 924.54 15.05 o 5 3 1 953.57 930.86 15.65 o 6 3 1 385.53 407.50 7.52 o 7 3 1 966.51 962.77 17.76 o -7 4 1 33.05 31.90 9.93 o -6 4 1 14.22 14.45 4.51 o -5 4 1 83.42 94.20 7.82 o -4 4 1 0.17 -1.81 3.61 o -3 4 1 51.22 43.34 3.01 o -2 4 1 1051.13 1160.50 11.74 o -1 4 1 112.36 131.82 5.72 o 0 4 1 59.33 64.71 3.91 o 1 4 1 106.91 123.99 2.11 o 2 4 1 466.14 468.59 10.23 o 3 4 1 494.77 524.27 7.22 o 4 4 1 21.33 15.65 3.91 o 5 4 1 0.19 0.60 5.12 o 6 4 1 11.19 14.75 6.62 o 7 4 1 2.01 4.82 7.22 o -7 5 1 58.57 52.37 5.12 o -6 5 1 351.92 338.88 25.28 o -5 5 1 60.47 72.23 6.02 o -4 5 1 620.67 553.76 41.23 o -3 5 1 631.64 613.96 22.27 o -2 5 1 1200.25 1201.13 19.26 o -1 5 1 4286.52 4260.37 33.11 o 0 5 1 1691.46 1304.35 270.26 o 1 5 1 2237.77 2179.84 43.64 o 2 5 1 708.11 649.17 33.11 o 3 5 1 3173.49 3040.28 65.01 o 4 5 1 1466.63 1451.52 22.27 o 5 5 1 947.33 901.37 41.53 o 6 5 1 592.11 545.94 24.38 o 7 5 1 339.33 335.87 8.13 o -7 6 1 28.19 18.06 10.23 o -6 6 1 84.55 79.15 11.14 o -5 6 1 1.55 -0.60 4.51 o -4 6 1 0.73 1.20 3.91 o -3 6 1 121.59 122.49 5.42 o -2 6 1 24.28 33.71 3.91 o -1 6 1 16.01 18.06 3.01 o 0 6 1 98.65 103.23 3.31 o 1 6 1 68.39 59.59 7.22 o 2 6 1 209.23 222.71 10.53 o 3 6 1 205.92 187.20 18.36 o 4 6 1 2.71 2.41 4.51 o 5 6 1 14.88 9.33 6.32 o 6 6 1 19.46 11.74 8.73 o 7 6 1 12.81 -4.82 8.73 o -6 7 1 143.37 141.75 6.92 o -5 7 1 568.08 548.95 13.24 o -4 7 1 403.24 425.25 16.55 o -3 7 1 611.73 637.73 13.84 o -2 7 1 448.28 427.96 28.59 o -1 7 1 567.23 561.59 8.73 o 0 7 1 1148.72 1096.69 19.26 o 1 7 1 2039.36 2047.12 32.50 o 2 7 1 1197.00 1194.20 30.40 o 3 7 1 366.18 367.47 9.03 o 4 7 1 561.48 575.43 14.15 o 5 7 1 548.51 455.05 84.27 o 6 7 1 446.40 435.49 8.43 o -6 8 1 0.89 4.21 9.63 o -5 8 1 5.42 3.91 12.64 o -4 8 1 3.85 4.51 7.22 o -3 8 1 0.73 5.42 5.42 o -2 8 1 4.45 10.53 4.82 o -1 8 1 23.24 23.17 6.62 o 0 8 1 337.24 340.08 10.53 o 1 8 1 78.48 66.81 5.72 o 2 8 1 3.56 3.01 9.03 o 3 8 1 24.63 22.87 6.32 o 4 8 1 95.28 85.17 12.34 o 5 8 1 118.01 110.75 7.22 o -5 9 1 212.70 227.52 12.94 o -4 9 1 144.35 145.96 9.33 o -3 9 1 260.78 247.99 9.63 o -2 9 1 395.67 441.51 8.43 o -1 9 1 586.73 621.18 15.35 o 0 9 1 825.68 788.81 27.99 o 1 9 1 34.12 29.19 4.82 o 2 9 1 372.31 397.27 14.45 o 3 9 1 314.30 331.66 15.65 o 4 9 1 506.75 541.73 31.60 o 5 9 1 112.49 102.33 8.73 o -4 10 1 4.30 6.32 8.73 o -3 10 1 19.48 3.61 6.92 o -2 10 1 9.64 14.75 6.92 o -1 10 1 1.99 6.02 9.93 o 0 10 1 95.53 80.05 9.33 o 1 10 1 68.01 60.49 6.62 o 2 10 1 27.92 32.80 9.33 o 3 10 1 26.16 27.69 6.92 o 4 10 1 3.93 4.21 9.03 o -2 11 1 222.90 231.74 14.15 o -1 11 1 99.39 102.93 11.14 o 0 11 1 15.68 28.29 9.63 o 1 11 1 554.07 575.43 25.88 o 2 11 1 245.81 246.79 20.47 o -8 0 2 313.48 278.99 14.75 o -7 0 2 92.21 91.79 11.14 o -6 0 2 85.09 70.73 6.32 o -5 0 2 896.61 916.12 10.53 o -4 0 2 258.62 215.19 6.32 o -3 0 2 437.99 487.85 6.02 o -2 0 2 23.01 20.77 3.01 o -1 0 2 2327.37 2436.56 37.02 o 0 0 2 170.20 169.44 7.52 o 1 0 2 378.16 355.73 3.61 o 2 0 2 295.69 295.84 4.21 o 3 0 2 1627.81 1571.30 10.83 o 4 0 2 1419.69 1420.83 16.85 o 5 0 2 407.92 401.78 12.94 o 6 0 2 176.18 173.35 10.23 o 7 0 2 347.40 336.77 12.64 o 8 0 2 100.92 103.53 8.73 o -8 1 2 15.20 6.02 7.82 o -7 1 2 92.14 90.89 9.33 o -6 1 2 93.94 89.69 6.62 o -5 1 2 0.48 0.30 6.02 o -4 1 2 0.77 3.01 4.51 o -3 1 2 0.16 3.01 3.31 o -2 1 2 139.73 138.74 4.21 o -1 1 2 735.04 744.27 4.51 o 0 1 2 2021.51 2011.61 40.03 o 1 1 2 1578.91 1621.26 15.95 o 2 1 2 546.01 598.00 7.22 o 3 1 2 525.66 553.16 8.43 o 4 1 2 4.67 7.82 5.12 o 5 1 2 17.97 9.93 7.52 o 6 1 2 113.39 112.56 7.82 o 7 1 2 0.08 -4.82 12.34 o 8 1 2 91.78 81.56 15.65 o -8 2 2 36.56 40.03 7.82 o -7 2 2 225.68 226.32 12.04 o -6 2 2 530.82 551.96 10.83 o -4 2 2 457.07 443.31 4.21 o -3 2 2 520.27 468.29 9.93 o -2 2 2 300.11 267.55 5.12 o -1 2 2 489.01 528.78 11.44 o 0 2 2 931.22 990.15 16.85 o 1 2 2 5673.73 5693.53 56.58 o 2 2 2 366.60 356.03 6.92 o 3 2 2 582.26 562.79 4.82 o 4 2 2 586.66 527.88 11.44 o 5 2 2 1160.59 1187.58 9.33 o 6 2 2 621.53 611.55 8.13 o 7 2 2 252.91 256.72 15.05 o -8 3 2 1.67 -0.90 9.03 o -7 3 2 87.83 88.78 11.14 o -6 3 2 14.61 15.35 7.82 o -5 3 2 0.19 3.01 5.42 o -4 3 2 92.35 92.70 6.02 o -3 3 2 8.23 7.22 3.61 o -2 3 2 35.71 41.23 3.61 o -1 3 2 834.94 935.08 9.93 o 0 3 2 1025.51 1000.39 41.23 o 1 3 2 55.01 68.62 2.41 o 2 3 2 0.33 3.61 4.21 o 3 3 2 122.18 133.02 4.51 o 4 3 2 740.92 751.19 11.14 o 5 3 2 31.46 32.20 5.42 o 6 3 2 11.99 15.05 8.43 o 7 3 2 17.52 10.83 7.52 o -7 4 2 133.38 132.42 9.63 o -6 4 2 31.12 43.94 9.33 o -5 4 2 95.78 96.31 6.62 o -4 4 2 663.77 649.47 10.23 o -3 4 2 774.19 790.62 20.16 o -2 4 2 3053.59 3064.96 12.64 o -1 4 2 974.47 973.30 13.24 o 0 4 2 947.85 924.54 23.17 o 1 4 2 778.23 767.14 12.04 o 2 4 2 4172.55 3972.35 23.47 o 3 4 2 2816.62 2791.99 25.88 o 4 4 2 1075.62 1013.63 18.66 o 5 4 2 339.13 347.01 8.13 o 6 4 2 638.32 650.07 20.47 o 7 4 2 462.81 480.03 22.57 o -7 5 2 5.45 2.41 6.62 o -6 5 2 17.77 16.85 4.82 o -5 5 2 49.07 38.22 4.82 o -4 5 2 35.28 30.40 6.62 o -3 5 2 7.03 4.21 6.32 o -2 5 2 0.10 4.21 2.41 o -1 5 2 491.87 545.94 3.61 o 0 5 2 27.54 19.56 10.83 o 1 5 2 65.97 75.54 7.22 o 2 5 2 205.25 193.52 6.02 o 3 5 2 87.38 81.86 5.72 o 4 5 2 149.65 136.64 6.62 o 5 5 2 32.00 23.47 7.52 o 6 5 2 8.33 15.65 7.22 o 7 5 2 18.35 14.45 6.92 o -7 6 2 56.66 53.87 12.04 o -6 6 2 211.41 213.38 6.92 o -5 6 2 295.03 247.99 33.71 o -4 6 2 250.10 257.32 13.84 o -3 6 2 408.58 451.74 7.22 o -2 6 2 450.16 486.95 12.64 o -1 6 2 834.57 889.03 9.63 o 0 6 2 2206.31 2182.85 33.11 o 1 6 2 993.04 1004.30 8.73 o 2 6 2 1358.53 1322.11 40.63 o 3 6 2 267.05 232.04 18.66 o 4 6 2 1286.57 1178.55 104.43 o 5 6 2 696.68 595.90 60.79 o 6 6 2 385.75 402.38 15.05 o -6 7 2 68.54 72.23 13.24 o -5 7 2 80.35 80.96 9.33 o -4 7 2 49.96 41.83 9.63 o -3 7 2 20.54 27.09 5.72 o -2 7 2 47.92 51.16 4.51 o -1 7 2 1.75 6.62 6.62 o 0 7 2 150.18 134.83 6.32 o 1 7 2 0.01 3.01 8.43 o 2 7 2 310.27 309.99 17.15 o 3 7 2 1.42 3.31 5.72 o 4 7 2 59.76 58.69 12.04 o 5 7 2 13.93 10.83 10.53 o 6 7 2 25.81 34.61 12.34 o -6 8 2 156.69 144.46 11.14 o -5 8 2 182.85 187.20 14.15 o -4 8 2 187.65 184.49 7.52 o -3 8 2 128.12 150.78 7.82 o -2 8 2 74.36 69.22 11.44 o -1 8 2 607.97 629.61 9.63 o 0 8 2 184.55 191.71 9.03 o 1 8 2 630.60 594.09 40.93 o 2 8 2 32.04 28.59 7.82 o 3 8 2 503.51 535.41 27.09 o 4 8 2 162.25 158.00 9.03 o 5 8 2 332.43 342.79 18.66 o -5 9 2 1.98 0.30 7.22 o -4 9 2 124.63 115.57 11.44 o -3 9 2 8.83 6.62 8.73 o -2 9 2 0.73 7.82 5.12 o -1 9 2 0.01 -4.82 5.42 o 0 9 2 10.92 12.34 6.02 o 1 9 2 229.37 210.07 20.16 o 2 9 2 4.95 2.41 5.72 o 3 9 2 25.27 31.00 6.32 o 4 9 2 17.00 11.44 6.92 o 5 9 2 27.89 31.30 7.82 o -4 10 2 60.81 66.81 10.53 o -3 10 2 178.82 189.30 13.54 o -2 10 2 192.39 207.06 9.03 o -1 10 2 50.79 55.08 8.13 o 0 10 2 24.05 23.17 8.43 o 1 10 2 64.02 65.61 18.06 o 2 10 2 191.90 191.41 9.33 o 3 10 2 243.65 242.87 17.15 o 4 10 2 53.26 47.85 9.33 o -2 11 2 13.36 17.15 9.03 o -1 11 2 41.14 31.30 9.33 o 0 11 2 3.46 -3.31 8.43 o 1 11 2 5.50 -4.51 9.33 o 2 11 2 25.93 27.09 9.93 o -7 1 3 102.20 111.05 11.74 o -6 1 3 390.41 390.64 19.86 o -5 1 3 621.83 597.40 14.45 o -4 1 3 901.44 869.17 15.95 o -3 1 3 213.35 221.81 4.51 o -2 1 3 1081.97 1043.12 10.23 o -1 1 3 1422.35 1428.05 9.03 o 0 1 3 2473.51 2433.85 23.78 o 1 1 3 1993.64 2014.01 33.11 o 2 1 3 955.34 951.03 5.72 o 3 1 3 1983.95 2013.41 31.90 o 4 1 3 931.99 934.18 20.77 o 5 1 3 1227.14 1220.39 13.84 o 6 1 3 441.38 445.72 14.75 o 7 1 3 448.14 469.50 9.03 o -8 2 3 82.51 93.60 15.35 o -7 2 3 5.68 12.64 7.22 o -6 2 3 8.61 9.93 9.93 o -5 2 3 49.05 45.75 4.51 o -4 2 3 667.70 674.75 7.82 o -3 2 3 50.92 62.60 4.21 o -1 2 3 499.74 508.62 5.72 o 0 2 3 6.69 6.02 1.81 o 1 2 3 40.98 53.27 4.82 o 2 2 3 172.68 185.99 5.72 o 3 2 3 31.22 36.12 3.31 o 4 2 3 36.06 40.03 5.42 o 5 2 3 6.00 5.72 6.62 o 6 2 3 3.94 8.73 8.43 o 7 2 3 13.63 19.26 10.23 o -8 3 3 299.25 271.16 13.24 o -7 3 3 542.47 549.55 13.24 o -6 3 3 346.83 355.73 11.14 o -5 3 3 176.79 164.93 5.42 o -4 3 3 334.44 319.02 8.13 o -3 3 3 1527.84 1409.09 5.42 o -2 3 3 699.81 660.30 12.94 o -1 3 3 553.14 535.10 45.14 o 0 3 3 289.50 238.96 15.35 o 1 3 3 369.01 331.05 10.83 o 2 3 3 837.25 864.05 14.15 o 3 3 3 155.30 131.22 4.51 o 4 3 3 710.29 692.20 18.36 o 5 3 3 135.23 133.32 8.73 o 6 3 3 314.92 316.31 14.15 o 7 3 3 129.65 138.14 11.14 o -7 4 3 50.59 55.08 9.33 o -6 4 3 2.48 8.13 9.63 o -5 4 3 167.29 161.92 9.33 o -4 4 3 242.04 268.45 5.42 o -3 4 3 15.50 13.54 3.61 o -2 4 3 0.07 1.50 3.61 o -1 4 3 11.04 15.05 3.61 o 0 4 3 177.08 213.98 6.92 o 1 4 3 158.03 170.94 3.91 o 2 4 3 230.32 212.18 5.42 o 3 4 3 490.19 507.12 5.72 o 4 4 3 15.22 9.03 4.51 o 5 4 3 0.58 -0.30 8.13 o 6 4 3 3.54 2.71 11.44 o 7 4 3 0.05 -0.90 10.83 o -7 5 3 169.23 169.44 10.83 o -6 5 3 147.68 166.13 10.53 o -5 5 3 742.64 706.35 12.64 o -4 5 3 441.95 423.15 10.23 o -3 5 3 558.02 529.69 12.94 o -2 5 3 403.10 372.89 5.42 o -1 5 3 102.31 98.11 7.22 o 0 5 3 36.21 27.09 2.41 o 1 5 3 323.08 301.26 11.44 o 2 5 3 586.17 586.27 7.52 o 3 5 3 271.42 255.81 7.82 o 4 5 3 3.54 2.11 6.02 o 5 5 3 8.28 15.65 9.63 o 6 5 3 183.11 168.24 17.15 o 7 5 3 76.57 79.75 12.34 o -7 6 3 7.35 5.72 12.04 o -6 6 3 8.84 8.73 12.04 o -5 6 3 77.76 68.32 8.73 o -4 6 3 1.01 1.81 7.22 o -3 6 3 9.83 11.14 5.72 o -2 6 3 22.20 24.08 7.52 o -1 6 3 332.29 371.38 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