#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/10/2201040.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201040_Fobs loop_ _publ_author_name 'Okabe, Nobuo' 'Kyoyama, Hasuyo' _publ_section_title ; A polynuclear lanthanum(III) complex of dipicolinic acid ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m226 _journal_page_last m227 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yab' _symmetry_space_group_name_H-M 'P 1 21/a 1' _[local]_cod_data_source_file bt6140Isup2.hkl _[local]_cod_data_source_block I loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma _refln_F_squared_calc _refln_observed_status 1 1 -1 5665.83 278.05 5244.15 o 0 0 2 13636.10 707.14 14154.09 o 1 1 1 1379.48 79.76 1308.13 o 2 0 0 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372.43 o 9 2 14 891.17 97.59 920.07 o 2 5 -18 167.16 172.65 152.09 o 7 4 15 2047.89 194.51 2085.98 o 3 1 18 116.29 189.19 169.71 o 4 12 -10 659.92 83.75 516.62 o 4 11 -12 1097.50 112.08 1108.57 o 3 14 -2 404.68 82.26 454.40 o 7 12 -8 1112.47 114.19 1188.60 o 9 12 0 998.35 102.63 918.94 o 14 4 -12 -84.06 165.93 200.94 o 1 12 10 1321.84 128.38 1197.08 o 2 3 18 600.76 84.47 517.75 o 3 11 11 1033.22 110.17 1058.28 o 14 8 -3 2158.77 236.96 2013.23 o 7 8 -15 -24.95 164.16 43.01 o 12 10 -1 2110.61 186.19 1922.72 o 10 8 9 3615.64 313.02 3575.30 o 10 8 -13 3695.47 319.09 3767.78 o 12 5 -14 222.80 161.25 105.05 o 12 7 -12 1041.65 111.00 1033.34 o 3 14 1 2374.41 266.17 2544.10 o 6 8 13 2406.57 264.32 2164.34 o 4 5 -18 192.97 139.65 66.37 o 7 13 -1 438.12 77.15 433.30 o 11 5 -15 1409.82 142.78 1515.39 o 14 7 -8 25.46 155.10 1.95 o 14 8 -2 1706.97 179.52 1965.07 o 12 10 -4 137.23 153.72 140.60 o 15 4 4 749.27 96.71 936.48 o 15 4 -10 1614.23 176.80 1718.65 o 6 12 -9 641.23 81.39 473.13 o 7 13 -2 2409.40 243.93 2243.20 o 1 13 -8 1576.42 177.09 1799.00 o 2 7 16 1552.14 164.66 1419.55 o 16 0 3 481.91 84.95 542.30 o 16 4 0 118.01 166.45 103.69 o 4 10 12 1090.40 112.98 1079.92 o 1 4 18 576.17 87.75 590.38 o 1 6 17 2636.84 269.42 2336.78 o 9 12 -4 2502.01 258.90 2325.37 o 16 3 -8 487.70 80.96 468.67 o 6 10 -13 1235.99 132.44 1277.35 o