#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/10/2201077.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201077_Fobs loop_ _publ_author_name 'Maderov\'a, Jana' 'Pavel\N-(Carboxymethyl)aspartic acid ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o469 _journal_page_last o470 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.384 _cell_angle_gamma 90.000 _cell_length_a 5.3430 _cell_length_b 16.0330 _cell_length_c 9.0895 _exptl_crystal_F_000 400.00 _reflns_d_resolution_high 0.8387 _[local]_cod_data_source_file ci6101Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' cma, CI6101, TEMP 120 K, fp (Brno) in P2(1)/n, C6 H9 N O6' _shelx_refln_list_code 4 _shelx_f_calc_maximum 94.83 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 46.31 68.73 3.42 o 4 0 0 1207.33 1284.18 18.00 o 6 0 0 133.35 126.41 5.50 o 1 1 0 841.16 669.98 4.28 o 2 1 0 933.96 995.67 7.38 o 3 1 0 199.26 213.11 6.83 o 4 1 0 132.92 146.99 4.86 o 5 1 0 412.07 403.58 8.73 o 6 1 0 41.99 38.62 5.19 o 1 2 0 3745.91 3422.35 102.85 o 2 2 0 455.85 514.62 11.11 o 3 2 0 340.19 358.92 20.16 o 4 2 0 3.10 5.51 0.80 o 5 2 0 5.15 6.51 3.25 o 6 2 0 449.31 427.67 32.11 o 1 3 0 137.37 104.60 6.58 o 2 3 0 663.22 627.63 24.70 o 3 3 0 948.24 965.94 26.09 o 4 3 0 264.67 269.22 6.28 o 5 3 0 208.86 212.55 14.19 o 6 3 0 1.08 1.44 1.23 o 0 4 0 2157.49 1872.01 10.71 o 1 4 0 1222.67 1112.77 46.05 o 2 4 0 1044.37 974.61 37.68 o 3 4 0 1002.13 1012.90 31.06 o 4 4 0 120.03 115.80 7.12 o 5 4 0 0.19 -0.92 3.03 o 6 4 0 41.22 40.97 3.13 o 1 5 0 2.01 2.58 1.29 o 2 5 0 5264.21 5214.56 119.82 o 3 5 0 240.31 243.47 10.89 o 4 5 0 130.98 134.34 5.18 o 5 5 0 0.41 0.08 2.40 o 6 5 0 29.07 26.50 6.01 o 0 6 0 1150.62 1061.15 7.48 o 1 6 0 1866.74 1711.86 44.58 o 2 6 0 76.03 80.88 3.02 o 3 6 0 20.16 24.63 1.32 o 4 6 0 0.12 -0.92 4.24 o 5 6 0 446.66 416.71 56.74 o 6 6 0 60.78 61.45 14.62 o 1 7 0 327.12 311.62 6.39 o 2 7 0 1.89 0.51 1.74 o 3 7 0 280.53 274.19 8.09 o 4 7 0 18.69 17.37 0.99 o 5 7 0 10.08 2.30 3.47 o 0 8 0 94.85 93.75 6.20 o 1 8 0 78.38 74.96 4.93 o 2 8 0 24.73 25.16 1.36 o 3 8 0 118.59 131.63 7.85 o 4 8 0 370.53 341.48 20.23 o 5 8 0 99.54 84.68 8.21 o 1 9 0 12.52 13.83 1.45 o 2 9 0 373.12 370.70 6.85 o 3 9 0 229.05 202.36 9.12 o 4 9 0 65.59 57.25 7.52 o 5 9 0 30.43 28.84 8.28 o 0 10 0 875.25 873.90 11.44 o 1 10 0 327.71 307.11 6.60 o 2 10 0 304.58 288.35 6.30 o 3 10 0 111.46 99.25 7.39 o 4 10 0 339.26 262.33 53.92 o 5 10 0 51.55 40.83 13.92 o 1 11 0 930.70 885.29 16.81 o 2 11 0 254.11 237.80 6.19 o 3 11 0 310.04 294.60 21.21 o 4 11 0 306.45 267.48 38.05 o 5 11 0 40.01 41.21 13.00 o 0 12 0 24.55 25.26 1.27 o 1 12 0 418.62 419.61 7.57 o 2 12 0 84.11 78.58 4.11 o 3 12 0 260.44 243.09 18.79 o 4 12 0 29.56 24.62 4.57 o 1 13 0 69.46 65.42 2.97 o 2 13 0 75.99 76.18 3.47 o 3 13 0 337.28 297.26 47.95 o 4 13 0 240.16 150.56 40.62 o 0 14 0 0.03 2.13 2.35 o 1 14 0 0.22 0.76 2.28 o 2 14 0 20.42 19.88 0.85 o 3 14 0 342.09 323.38 40.89 o 4 14 0 22.31 29.35 4.74 o 1 15 0 65.70 70.08 5.19 o 2 15 0 1595.03 1491.83 56.32 o 3 15 0 275.68 262.79 34.44 o 0 16 0 372.93 394.15 8.83 o 1 16 0 18.99 22.72 2.37 o 2 16 0 17.08 15.30 2.31 o 3 16 0 34.40 40.74 14.17 o 1 17 0 379.30 385.94 36.19 o 2 17 0 18.47 19.58 1.06 o 0 18 0 50.56 61.79 5.93 o 1 18 0 36.74 35.47 2.06 o 2 18 0 14.62 19.28 2.80 o -5 0 1 1202.23 1253.99 20.62 o -3 0 1 0.00 2.46 2.45 o -1 0 1 154.40 155.37 3.21 o 1 0 1 3623.87 4014.53 45.12 o 3 0 1 236.75 227.11 6.93 o 5 0 1 7.58 6.29 4.63 o -6 1 1 160.21 160.53 21.97 o -5 1 1 143.47 142.17 6.95 o -4 1 1 477.97 497.21 8.10 o -3 1 1 448.19 496.76 6.68 o -2 1 1 1.39 3.75 3.11 o -1 1 1 112.29 90.90 1.86 o 1 1 1 329.58 296.52 4.50 o 2 1 1 72.60 77.56 2.59 o 3 1 1 150.00 154.55 5.18 o 4 1 1 648.91 657.74 18.00 o 5 1 1 13.01 15.95 0.75 o 6 1 1 68.67 81.74 6.88 o -6 2 1 268.76 279.91 31.64 o -5 2 1 269.24 291.02 7.85 o -4 2 1 55.35 59.79 2.53 o -3 2 1 1320.15 1389.71 11.05 o -2 2 1 67.33 70.25 2.52 o -1 2 1 3326.23 3200.65 94.39 o 1 2 1 5625.73 6342.07 311.66 o 2 2 1 1094.84 1180.16 12.01 o 3 2 1 164.05 159.34 6.17 o 4 2 1 117.14 124.23 4.70 o 5 2 1 9.30 11.41 0.73 o 6 2 1 39.45 39.75 3.08 o -6 3 1 17.60 15.31 1.81 o -5 3 1 0.50 -0.19 2.88 o -4 3 1 53.04 63.17 3.20 o -3 3 1 763.78 808.53 38.56 o -2 3 1 1432.09 1470.23 55.30 o -1 3 1 3871.29 3741.45 132.58 o 0 3 1 19.89 21.45 0.84 o 1 3 1 132.44 137.89 2.66 o 2 3 1 39.31 45.29 2.64 o 3 3 1 1394.24 1421.84 11.79 o 4 3 1 224.81 225.81 13.75 o 5 3 1 96.13 95.96 4.12 o 6 3 1 33.13 37.25 2.91 o -6 4 1 12.76 14.23 5.98 o -5 4 1 233.24 207.17 15.85 o -4 4 1 0.21 3.88 2.59 o -3 4 1 288.98 283.62 10.87 o -2 4 1 42.77 46.70 2.63 o -1 4 1 81.48 68.71 2.82 o 0 4 1 1591.75 1535.44 18.91 o 1 4 1 1137.88 1154.72 23.24 o 2 4 1 83.32 89.25 2.87 o 3 4 1 461.42 467.88 13.53 o 4 4 1 26.12 28.95 1.36 o 5 4 1 166.75 163.64 15.21 o 6 4 1 55.44 56.96 4.66 o -6 5 1 7.79 14.24 8.11 o -5 5 1 37.61 39.27 5.99 o -4 5 1 300.50 272.76 19.33 o -3 5 1 985.08 959.38 34.74 o -2 5 1 129.93 148.41 8.19 o -1 5 1 258.94 256.03 9.39 o 0 5 1 1161.86 1012.85 9.06 o 1 5 1 997.29 943.23 20.09 o 2 5 1 6.65 11.00 0.69 o 3 5 1 448.36 456.97 7.28 o 4 5 1 940.76 891.25 33.89 o 5 5 1 7.55 1.92 3.69 o 6 5 1 2.02 -2.91 4.02 o -6 6 1 131.46 124.31 47.50 o -5 6 1 202.61 198.32 15.25 o -4 6 1 6.55 2.91 2.81 o -3 6 1 154.04 126.28 4.36 o -2 6 1 1144.78 1135.93 53.58 o -1 6 1 17.57 15.53 0.90 o 0 6 1 306.40 307.16 3.00 o 1 6 1 68.88 63.44 2.44 o 2 6 1 632.52 596.49 17.54 o 3 6 1 9.42 8.01 3.11 o 4 6 1 1.51 3.88 2.68 o 5 6 1 6.51 5.99 1.02 o -5 7 1 3.66 0.64 3.31 o -4 7 1 16.02 16.89 0.95 o -3 7 1 224.63 237.47 12.49 o -2 7 1 0.09 0.06 1.86 o -1 7 1 13.37 13.96 2.49 o 0 7 1 2758.84 2787.17 26.37 o 1 7 1 736.74 708.79 7.26 o 2 7 1 379.15 347.86 6.09 o 3 7 1 105.20 86.35 8.32 o 4 7 1 102.07 99.02 3.98 o 5 7 1 197.17 149.41 32.77 o -5 8 1 0.00 -0.81 8.52 o -4 8 1 104.21 90.24 8.26 o -3 8 1 135.99 140.82 5.12 o -2 8 1 336.41 349.85 16.87 o -1 8 1 9.32 8.79 0.41 o 0 8 1 1445.88 1456.46 19.43 o 1 8 1 365.33 333.67 5.46 o 2 8 1 281.10 262.35 5.60 o 3 8 1 23.05 26.39 1.29 o 4 8 1 30.05 27.26 5.04 o 5 8 1 167.59 122.81 27.99 o -5 9 1 95.71 98.37 14.62 o -4 9 1 4.40 0.98 3.20 o -3 9 1 80.61 73.45 3.32 o -2 9 1 45.87 47.50 4.11 o -1 9 1 15.28 18.89 0.81 o 0 9 1 4.99 6.14 0.37 o 1 9 1 7.85 6.82 1.31 o 2 9 1 420.18 399.40 11.14 o 3 9 1 51.87 54.34 2.86 o 4 9 1 1.35 0.54 2.84 o 5 9 1 16.07 15.09 4.82 o -5 10 1 49.96 33.30 10.52 o -4 10 1 10.73 11.07 0.94 o -3 10 1 311.10 273.87 27.47 o -2 10 1 231.06 220.51 8.41 o -1 10 1 69.71 81.70 3.72 o 0 10 1 403.33 410.05 4.92 o 1 10 1 5.58 2.82 1.15 o 2 10 1 760.81 697.32 26.24 o 3 10 1 530.40 473.89 41.16 o 4 10 1 0.14 -2.68 3.14 o 5 10 1 9.10 10.92 4.77 o -5 11 1 30.05 22.24 3.71 o -4 11 1 9.25 7.44 1.04 o -3 11 1 271.63 245.13 12.66 o -2 11 1 3.52 3.47 1.94 o -1 11 1 315.41 303.52 6.22 o 0 11 1 23.21 22.87 0.84 o 1 11 1 163.93 166.67 4.90 o 2 11 1 408.40 389.69 20.90 o 3 11 1 7.94 6.51 2.69 o 4 11 1 88.03 70.97 9.13 o 5 11 1 1.74 -0.32 3.85 o -4 12 1 66.87 49.48 12.22 o -3 12 1 669.08 609.71 46.36 o -2 12 1 60.61 60.05 2.71 o -1 12 1 4.83 2.52 1.61 o 0 12 1 36.64 48.63 2.64 o 1 12 1 1496.13 1465.61 39.30 o 2 12 1 263.89 259.93 13.57 o 3 12 1 394.42 373.40 43.19 o 4 12 1 58.43 48.17 9.83 o -4 13 1 3.20 4.91 7.18 o -3 13 1 378.67 348.41 61.46 o -2 13 1 39.52 38.67 1.79 o -1 13 1 490.44 484.35 8.62 o 0 13 1 1.00 0.43 1.53 o 1 13 1 197.65 193.48 9.60 o 2 13 1 44.47 44.28 2.33 o 3 13 1 265.72 241.61 26.27 o 4 13 1 120.66 94.91 20.33 o -4 14 1 28.76 26.38 7.08 o -3 14 1 2.38 -0.45 2.96 o -2 14 1 33.70 32.29 1.48 o -1 14 1 434.55 431.91 8.63 o 0 14 1 34.26 38.54 1.46 o 1 14 1 5.15 3.12 2.39 o 2 14 1 6.89 7.48 3.04 o 3 14 1 0.61 -1.84 2.83 o 4 14 1 53.70 39.62 11.03 o -3 15 1 1.62 2.08 3.33 o -2 15 1 166.30 172.38 13.51 o -1 15 1 396.11 367.04 14.87 o 0 15 1 0.31 1.94 0.71 o 1 15 1 73.38 76.57 3.17 o 2 15 1 18.96 26.29 8.51 o 3 15 1 6.70 6.68 3.24 o -3 16 1 21.23 25.32 4.03 o -2 16 1 6.83 6.96 0.88 o -1 16 1 10.97 14.55 1.17 o 0 16 1 196.64 195.96 5.93 o 1 16 1 11.63 14.88 0.69 o 2 16 1 1.03 0.88 4.82 o 3 16 1 18.86 19.13 3.19 o -2 17 1 21.48 23.44 1.25 o -1 17 1 701.82 695.86 28.37 o 0 17 1 0.05 0.74 2.04 o 1 17 1 12.61 13.07 0.79 o 2 17 1 23.33 26.61 3.53 o -2 18 1 0.63 3.89 3.31 o -1 18 1 2.06 -2.48 3.58 o 0 18 1 31.42 33.46 0.90 o 1 18 1 157.16 155.70 11.73 o 2 18 1 79.22 95.68 6.75 o 0 19 1 0.31 0.99 2.39 o -6 0 2 149.29 164.28 7.69 o -4 0 2 348.88 374.62 10.42 o -2 0 2 6631.28 8206.72 89.23 o 0 0 2 3151.28 2605.15 35.05 o 2 0 2 679.15 647.57 9.40 o 4 0 2 427.31 432.78 11.32 o 6 0 2 125.67 135.87 6.67 o -6 1 2 10.27 10.28 0.86 o -5 1 2 215.39 218.48 7.92 o -4 1 2 156.45 172.14 5.28 o -3 1 2 3.65 5.86 1.47 o -2 1 2 1921.27 2017.78 11.57 o -1 1 2 4588.66 5431.61 85.34 o 0 1 2 1825.43 1842.10 16.46 o 1 1 2 2028.96 2006.72 10.43 o 2 1 2 764.54 809.32 7.38 o 3 1 2 296.92 316.74 8.08 o 4 1 2 48.42 50.64 2.20 o 5 1 2 464.27 473.78 9.83 o 6 1 2 234.33 225.94 10.86 o -6 2 2 42.48 39.74 5.08 o -5 2 2 123.58 125.25 5.06 o -4 2 2 34.09 42.47 2.14 o -3 2 2 152.23 167.83 4.32 o -2 2 2 816.09 816.20 11.07 o -1 2 2 2.54 2.55 1.79 o 0 2 2 4027.14 3620.87 254.43 o 1 2 2 1744.02 1799.38 9.39 o 2 2 2 768.90 840.18 16.72 o 3 2 2 440.26 473.77 7.04 o 4 2 2 393.69 404.79 11.61 o 5 2 2 110.37 107.80 10.52 o 6 2 2 33.38 34.08 3.73 o -6 3 2 1.91 -3.93 3.93 o -5 3 2 306.63 300.19 8.22 o -4 3 2 77.71 91.10 4.19 o -3 3 2 244.51 264.93 8.55 o -2 3 2 758.68 846.48 40.47 o -1 3 2 197.53 181.11 11.66 o 0 3 2 2911.90 2654.09 35.62 o 1 3 2 1424.26 1441.89 35.38 o 2 3 2 30.32 39.59 2.61 o 3 3 2 436.54 436.23 6.88 o 4 3 2 69.50 81.75 3.60 o 5 3 2 525.68 504.61 30.78 o 6 3 2 10.91 9.60 3.44 o -6 4 2 0.74 2.10 3.49 o -5 4 2 207.11 200.19 10.58 o -4 4 2 0.19 -2.62 2.75 o -3 4 2 729.15 773.08 12.12 o -2 4 2 1.93 4.58 0.36 o -1 4 2 366.05 400.00 20.33 o 0 4 2 43.55 43.84 2.32 o 1 4 2 8992.51 10453.77 367.58 o 2 4 2 46.97 59.55 5.58 o 3 4 2 130.84 142.23 4.49 o 4 4 2 269.13 279.97 9.35 o 5 4 2 233.69 229.50 19.20 o -6 5 2 18.39 18.74 6.22 o -5 5 2 39.88 36.19 2.73 o -4 5 2 525.33 508.76 16.08 o -3 5 2 374.52 358.47 7.33 o -2 5 2 1561.70 1624.03 75.00 o -1 5 2 1231.43 1164.19 14.03 o 0 5 2 177.90 200.44 5.44 o 1 5 2 1806.21 1870.02 10.77 o 2 5 2 472.38 453.98 12.50 o 3 5 2 105.68 106.82 9.51 o 4 5 2 7.49 7.86 0.88 o 5 5 2 50.25 53.39 6.57 o -6 6 2 6.31 7.28 5.83 o -5 6 2 127.61 103.08 13.42 o -4 6 2 15.56 18.39 4.87 o -3 6 2 1.40 0.94 3.32 o -2 6 2 459.27 480.56 14.93 o -1 6 2 255.88 266.00 16.12 o 0 6 2 244.63 243.41 2.88 o 1 6 2 49.07 48.97 2.34 o 2 6 2 4.73 -0.69 1.88 o 3 6 2 212.26 206.62 5.48 o 4 6 2 413.06 406.69 8.59 o 5 6 2 133.52 91.77 30.16 o -5 7 2 10.04 6.17 3.52 o -4 7 2 0.43 1.23 3.76 o -3 7 2 56.42 58.09 2.87 o -2 7 2 780.23 788.71 22.92 o -1 7 2 417.73 398.00 5.71 o 0 7 2 1170.09 1218.40 23.54 o 1 7 2 70.54 71.42 3.30 o 2 7 2 434.59 430.70 6.85 o 3 7 2 84.91 94.66 3.74 o 4 7 2 375.24 361.54 20.75 o 5 7 2 209.82 170.51 39.50 o -5 8 2 51.73 45.77 9.70 o -4 8 2 43.79 43.10 3.76 o -3 8 2 310.41 280.35 6.69 o -2 8 2 99.68 99.87 3.80 o -1 8 2 536.01 542.16 56.16 o 0 8 2 409.62 406.04 9.73 o 1 8 2 503.10 491.09 6.79 o 2 8 2 56.88 54.12 2.62 o 3 8 2 548.79 532.39 18.92 o 4 8 2 168.46 160.06 16.68 o 5 8 2 0.16 -0.97 5.02 o -5 9 2 0.71 -0.11 4.71 o -4 9 2 10.08 11.67 1.34 o -3 9 2 61.19 57.41 2.61 o -2 9 2 1.75 1.98 1.37 o -1 9 2 827.11 822.04 25.19 o 0 9 2 148.92 150.23 5.71 o 1 9 2 490.87 484.90 18.36 o 2 9 2 584.39 562.79 11.97 o 3 9 2 325.86 304.35 31.03 o 4 9 2 816.61 725.96 109.78 o 5 9 2 22.35 21.55 5.46 o -5 10 2 62.06 52.13 11.35 o -4 10 2 518.55 447.02 56.06 o -3 10 2 438.86 412.80 14.47 o -2 10 2 869.42 800.78 10.39 o -1 10 2 847.20 850.96 34.98 o 0 10 2 92.56 99.78 2.58 o 1 10 2 136.53 130.92 4.32 o 2 10 2 596.01 562.23 21.93 o 3 10 2 249.81 231.70 20.88 o 4 10 2 183.22 159.35 5.39 o 5 10 2 22.60 18.64 3.93 o -5 11 2 2.79 -3.74 3.84 o -4 11 2 27.53 27.76 3.04 o -3 11 2 56.03 60.96 6.73 o -2 11 2 0.29 0.47 2.44 o -1 11 2 177.96 189.93 12.88 o 0 11 2 84.32 90.91 2.73 o 1 11 2 16.80 17.46 0.76 o 2 11 2 188.15 176.62 18.55 o 3 11 2 611.43 566.61 75.66 o 4 11 2 7.17 10.18 1.62 o -4 12 2 344.31 332.92 32.54 o -3 12 2 732.05 672.95 23.44 o -2 12 2 326.56 326.30 7.60 o -1 12 2 118.14 112.07 5.67 o 0 12 2 29.43 29.90 1.13 o 1 12 2 212.99 207.45 5.87 o 2 12 2 479.73 457.14 17.84 o 3 12 2 56.04 47.60 8.17 o 4 12 2 0.61 -0.94 3.52 o -4 13 2 42.31 35.90 4.62 o -3 13 2 20.93 23.11 1.08 o -2 13 2 15.49 15.42 0.87 o -1 13 2 439.85 416.90 8.15 o 0 13 2 2.72 5.01 0.72 o 1 13 2 252.31 244.62 6.58 o 2 13 2 752.82 731.22 51.71 o 3 13 2 22.63 17.83 1.72 o 4 13 2 26.05 28.07 8.54 o -4 14 2 16.38 18.13 7.40 o -3 14 2 24.23 22.09 2.50 o -2 14 2 23.52 22.63 1.31 o -1 14 2 32.78 33.18 1.35 o 0 14 2 222.84 219.66 4.43 o 1 14 2 8.24 10.40 0.70 o 2 14 2 1050.75 998.71 58.38 o 3 14 2 11.21 10.39 5.89 o 4 14 2 43.96 53.92 15.28 o -3 15 2 0.16 5.44 3.03 o -2 15 2 239.41 237.16 22.81 o -1 15 2 61.29 59.70 2.68 o 0 15 2 1028.48 1047.07 17.53 o 1 15 2 113.30 117.05 8.55 o 2 15 2 1.54 2.37 2.92 o 3 15 2 0.00 6.49 3.17 o -3 16 2 36.36 31.38 4.78 o -2 16 2 4.88 2.39 3.12 o -1 16 2 146.70 159.18 8.05 o 0 16 2 25.24 26.98 0.88 o 1 16 2 0.90 1.40 4.45 o 2 16 2 13.63 15.24 3.16 o 3 16 2 6.25 8.37 1.08 o -2 17 2 45.64 46.12 3.56 o -1 17 2 76.40 76.14 3.75 o 0 17 2 119.38 123.29 3.90 o 1 17 2 11.90 12.19 0.88 o 2 17 2 98.61 92.79 14.78 o -1 18 2 55.82 59.89 2.93 o 0 18 2 99.01 107.99 3.61 o 1 18 2 1.61 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