#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2201112.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201112_Fobs loop_ _publ_author_name 'Guo, Rongwei' 'Ao-Yueng, Terry T. L.' 'Choi, Michael C. K.' 'Zhou, Zhongyuan' _publ_section_title ; (R)-2,2'-Bis[bis(3,5-dimethylphenyl)phosphinoamino]-5,5',6,6',7,7',8,8'-octahydro-1,1'-binaphthyl ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o544 _journal_page_last o545 _journal_volume 58 _journal_year 2002 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.1595 _cell_length_b 19.9611 _cell_length_c 22.3596 _exptl_crystal_F_000 1656.00 _reflns_d_resolution_high 0.7673 _[local]_cod_data_source_file cv6105Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' GRW4 in P2(1)2(1)2(1) C52H58N2P2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 275.83 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 24479.95 22218.75 199.96 o 4 0 0 616.36 642.77 42.95 o 6 0 0 314.50 157.41 44.44 o 8 0 0 23.25 -16.98 80.89 o 10 0 0 163.80 177.43 134.49 o 12 0 0 177.96 328.90 199.41 o 1 1 0 1427.65 1270.02 29.90 o 2 1 0 515.82 481.54 19.27 o 3 1 0 175.70 168.26 17.91 o 4 1 0 35.09 29.10 14.93 o 5 1 0 7.66 14.31 17.21 o 6 1 0 2082.21 1782.21 54.32 o 7 1 0 225.68 215.01 31.85 o 8 1 0 23.81 -29.44 51.28 o 9 1 0 130.68 87.33 78.64 o 10 1 0 48.02 44.18 83.26 o 11 1 0 31.51 -28.44 89.75 o 12 1 0 32.36 -69.74 101.12 o 13 1 0 0.80 -94.96 150.30 o 1 2 0 15097.39 14604.34 242.94 o 2 2 0 10833.32 11541.67 235.73 o 3 2 0 2262.08 2017.64 89.95 o 4 2 0 6655.46 6593.51 71.44 o 5 2 0 476.06 559.98 27.67 o 6 2 0 232.49 222.39 25.13 o 7 2 0 343.95 377.26 55.56 o 8 2 0 0.14 9.53 62.02 o 9 2 0 5.76 -67.20 67.20 o 10 2 0 190.66 197.73 95.10 o 11 2 0 45.74 46.63 97.80 o 12 2 0 54.95 -18.88 112.95 o 13 2 0 0.03 55.02 131.05 o 1 3 0 8333.30 7643.21 81.56 o 2 3 0 8574.45 8261.11 111.31 o 3 3 0 667.92 647.74 26.75 o 4 3 0 265.40 262.86 37.32 o 5 3 0 2977.86 2788.50 91.75 o 6 3 0 95.10 107.21 36.45 o 7 3 0 13.10 20.91 39.28 o 8 3 0 1321.13 1412.18 180.39 o 9 3 0 461.55 427.18 106.56 o 10 3 0 103.07 8.86 83.42 o 11 3 0 69.58 40.25 94.39 o 12 3 0 24.34 57.09 107.51 o 13 3 0 51.35 -30.64 125.52 o 0 4 0 52702.82 54710.56 389.86 o 1 4 0 20090.20 20470.67 114.73 o 2 4 0 17.82 7.87 12.19 o 3 4 0 449.87 419.46 42.38 o 4 4 0 4996.80 5176.93 111.91 o 5 4 0 95.54 202.95 40.49 o 6 4 0 12.62 4.22 32.76 o 7 4 0 839.44 884.61 77.52 o 8 4 0 553.60 555.94 75.55 o 9 4 0 61.58 60.45 77.81 o 10 4 0 8.45 -65.76 76.56 o 11 4 0 4.48 4.82 91.60 o 12 4 0 10.26 -16.80 113.23 o 13 4 0 1.92 0.27 127.82 o 1 5 0 54540.91 57226.30 339.36 o 2 5 0 9473.42 8978.92 106.26 o 3 5 0 1385.69 1291.38 39.40 o 4 5 0 0.73 14.14 17.03 o 5 5 0 45.61 42.13 32.70 o 6 5 0 40.68 16.94 32.58 o 7 5 0 63.29 75.68 45.72 o 8 5 0 383.34 417.70 70.61 o 9 5 0 598.00 447.49 114.24 o 10 5 0 55.47 53.88 90.02 o 11 5 0 84.68 44.14 80.99 o 12 5 0 6.44 1.03 106.11 o 0 6 0 31328.42 30076.19 309.61 o 1 6 0 1145.18 1128.75 29.23 o 2 6 0 2027.55 2131.02 48.13 o 3 6 0 8618.45 8873.06 105.04 o 4 6 0 4310.32 4658.94 84.75 o 5 6 0 1121.44 1181.88 62.67 o 6 6 0 848.98 861.85 83.57 o 7 6 0 1199.44 1255.48 94.69 o 8 6 0 41.56 -3.50 46.25 o 9 6 0 6.97 -19.69 54.75 o 10 6 0 40.58 -22.51 64.57 o 11 6 0 55.73 -32.69 69.88 o 12 6 0 11.66 -9.32 106.82 o 1 7 0 4437.63 4506.52 95.35 o 2 7 0 58.43 76.98 17.50 o 3 7 0 4374.12 4166.36 84.57 o 4 7 0 422.11 377.56 34.95 o 5 7 0 796.99 678.54 60.84 o 6 7 0 42.47 38.85 35.18 o 7 7 0 178.10 251.87 52.90 o 8 7 0 37.68 46.03 47.81 o 9 7 0 84.93 60.42 51.79 o 10 7 0 48.15 39.52 71.47 o 11 7 0 22.48 22.79 79.76 o 12 7 0 99.33 110.58 114.84 o 0 8 0 4077.37 3848.71 122.56 o 1 8 0 1494.39 1675.51 41.76 o 2 8 0 3670.60 3636.74 61.80 o 3 8 0 4993.32 5536.52 99.71 o 4 8 0 699.93 649.72 41.39 o 5 8 0 62.82 64.17 23.60 o 6 8 0 53.01 41.44 38.96 o 7 8 0 274.68 283.80 54.81 o 8 8 0 31.71 -39.28 44.52 o 9 8 0 1.52 -24.94 46.99 o 10 8 0 79.63 43.30 70.81 o 11 8 0 49.34 -20.28 79.23 o 12 8 0 49.45 83.66 121.88 o 1 9 0 6531.06 6645.91 86.32 o 2 9 0 2177.02 2252.13 54.68 o 3 9 0 43.62 23.30 19.86 o 4 9 0 98.67 80.56 25.91 o 5 9 0 1690.37 1671.23 59.64 o 6 9 0 123.60 151.42 46.46 o 7 9 0 370.72 453.74 63.93 o 8 9 0 43.17 11.79 45.04 o 9 9 0 3.24 -48.87 48.87 o 10 9 0 13.71 -10.80 69.21 o 11 9 0 14.16 -75.43 75.43 o 12 9 0 42.93 36.94 115.35 o 0 10 0 25.69 21.80 33.57 o 1 10 0 84.97 45.96 24.68 o 2 10 0 5880.58 5886.84 94.07 o 3 10 0 1.65 -19.99 19.99 o 4 10 0 589.21 679.76 46.68 o 5 10 0 339.20 320.76 39.43 o 6 10 0 9.47 15.72 37.62 o 7 10 0 332.56 448.01 66.04 o 8 10 0 0.42 -0.56 44.75 o 9 10 0 65.48 102.33 61.09 o 10 10 0 26.01 23.43 72.94 o 11 10 0 57.49 105.10 91.18 o 12 10 0 3.66 -32.98 94.16 o 1 11 0 1607.39 1309.98 61.84 o 2 11 0 842.86 880.48 35.61 o 3 11 0 1956.57 2148.38 62.47 o 4 11 0 770.49 786.60 49.47 o 5 11 0 2675.88 2574.12 96.85 o 6 11 0 1374.66 1385.53 109.84 o 7 11 0 280.09 283.82 59.85 o 8 11 0 3.54 8.55 49.65 o 9 11 0 17.18 12.49 58.02 o 10 11 0 0.40 -37.48 73.26 o 11 11 0 0.56 -62.54 81.69 o 0 12 0 640.29 563.06 78.99 o 1 12 0 125.62 181.95 37.58 o 2 12 0 0.13 4.56 17.71 o 3 12 0 408.92 447.85 37.46 o 4 12 0 322.62 336.26 42.04 o 5 12 0 234.07 180.69 46.05 o 6 12 0 542.73 567.92 79.56 o 7 12 0 3.29 -10.99 47.55 o 8 12 0 0.74 11.25 52.45 o 9 12 0 7.15 -19.14 58.00 o 10 12 0 1.01 -61.69 69.91 o 11 12 0 8.52 38.29 89.84 o 1 13 0 1451.24 1463.35 71.99 o 2 13 0 884.55 927.72 59.01 o 3 13 0 232.56 325.47 40.32 o 4 13 0 51.41 11.33 31.45 o 5 13 0 57.02 7.15 46.29 o 6 13 0 181.58 182.67 51.27 o 7 13 0 26.94 0.73 47.45 o 8 13 0 27.22 37.33 64.49 o 9 13 0 0.16 48.56 74.24 o 10 13 0 9.71 -48.62 76.69 o 11 13 0 10.48 48.82 116.04 o 0 14 0 10.38 8.78 43.65 o 1 14 0 43.27 66.99 36.10 o 2 14 0 833.04 940.11 75.48 o 3 14 0 2022.54 1996.23 88.47 o 4 14 0 427.27 517.17 73.35 o 5 14 0 2.26 -10.77 58.78 o 6 14 0 52.58 60.77 74.93 o 7 14 0 42.16 -67.43 67.43 o 8 14 0 34.00 -13.85 80.15 o 9 14 0 126.83 185.99 104.93 o 10 14 0 0.11 -45.38 108.16 o 11 14 0 8.43 72.90 170.11 o 1 15 0 51.61 26.97 35.45 o 2 15 0 1211.40 1245.53 82.68 o 3 15 0 1451.62 1423.87 85.97 o 4 15 0 52.68 4.19 42.61 o 5 15 0 12.88 21.75 66.79 o 6 15 0 10.79 77.59 74.78 o 7 15 0 0.18 -17.67 76.16 o 8 15 0 326.09 393.67 116.91 o 9 15 0 168.41 224.24 118.50 o 10 15 0 0.83 -93.43 105.81 o 0 16 0 82.94 45.80 57.11 o 1 16 0 11.70 20.88 36.71 o 2 16 0 64.97 60.46 41.12 o 3 16 0 14.55 34.17 40.96 o 4 16 0 7.94 15.71 46.37 o 5 16 0 110.50 188.90 85.18 o 6 16 0 43.71 -0.88 74.55 o 7 16 0 72.26 79.64 93.12 o 8 16 0 21.37 18.84 91.35 o 9 16 0 17.12 -50.39 101.19 o 10 16 0 36.70 -38.78 121.65 o 1 17 0 20.20 34.92 42.34 o 2 17 0 745.05 736.85 76.15 o 3 17 0 46.77 34.45 40.01 o 4 17 0 69.84 60.79 68.70 o 5 17 0 1.02 36.23 68.85 o 6 17 0 0.89 -41.79 69.44 o 7 17 0 27.35 96.85 97.31 o 8 17 0 73.97 135.86 98.63 o 9 17 0 2.43 -73.48 101.73 o 10 17 0 57.52 -32.96 182.10 o 0 18 0 16.61 16.64 58.14 o 1 18 0 81.43 74.21 43.10 o 2 18 0 44.63 70.46 44.70 o 3 18 0 1.73 -11.03 42.39 o 4 18 0 270.29 288.76 91.68 o 5 18 0 7.59 8.09 73.94 o 6 18 0 2.09 -59.72 75.55 o 7 18 0 1.60 -2.43 88.71 o 8 18 0 29.51 -47.46 91.44 o 9 18 0 4.78 -25.64 114.03 o 1 19 0 3.58 -40.11 40.11 o 2 19 0 305.69 295.06 72.62 o 3 19 0 22.60 53.88 50.70 o 4 19 0 42.24 52.83 78.97 o 5 19 0 1.00 14.46 81.60 o 6 19 0 142.78 172.62 106.41 o 7 19 0 6.71 31.04 92.78 o 8 19 0 12.13 -96.33 96.33 o 9 19 0 0.11 35.00 122.45 o 0 20 0 156.69 205.28 79.99 o 1 20 0 56.62 29.12 47.73 o 2 20 0 6.70 28.94 46.59 o 3 20 0 20.61 -9.76 49.11 o 4 20 0 8.81 -15.92 75.17 o 5 20 0 9.62 -49.52 78.43 o 6 20 0 26.39 12.40 94.12 o 7 20 0 16.34 -52.50 97.66 o 8 20 0 4.96 3.83 104.25 o 1 21 0 1.08 15.17 48.16 o 2 21 0 26.02 -15.53 50.79 o 3 21 0 65.70 115.49 57.69 o 4 21 0 41.46 30.73 84.10 o 5 21 0 159.66 98.47 94.81 o 6 21 0 209.50 133.55 143.81 o 7 21 0 1.07 -104.98 104.98 o 0 22 0 180.77 142.20 82.79 o 1 22 0 14.94 1.75 51.31 o 2 22 0 1.08 -45.48 52.52 o 3 22 0 0.90 -10.80 67.38 o 4 22 0 9.87 -16.11 90.86 o 5 22 0 4.83 -84.71 90.99 o 6 22 0 15.64 -47.50 127.00 o 7 22 0 7.43 52.60 118.80 o 1 23 0 0.82 10.39 56.81 o 2 23 0 28.18 18.75 59.95 o 3 23 0 21.36 -30.98 84.72 o 4 23 0 11.79 -6.33 91.29 o 5 23 0 207.51 157.37 109.74 o 6 23 0 4.06 -106.72 108.13 o 0 24 0 17.14 -47.21 83.80 o 1 24 0 14.31 6.13 60.85 o 2 24 0 0.30 -45.07 58.79 o 3 24 0 0.12 -37.64 96.03 o 4 24 0 115.23 108.40 108.84 o 5 24 0 0.98 -104.56 109.03 o 1 25 0 6.05 -44.55 64.34 o 2 25 0 1.13 3.48 77.75 o 3 25 0 0.05 -5.69 95.33 o 1 0 1 11.92 20.62 5.49 o 2 0 1 4938.60 4954.05 76.74 o 3 0 1 302.79 254.10 21.72 o 4 0 1 164.60 163.93 20.94 o 5 0 1 1099.51 1150.81 43.45 o 6 0 1 38.67 35.29 20.37 o 7 0 1 0.52 6.01 21.53 o 8 0 1 149.87 122.80 66.13 o 9 0 1 6.89 -18.85 72.74 o 10 0 1 121.51 159.41 102.00 o 11 0 1 167.96 135.18 103.61 o 12 0 1 22.98 37.11 112.09 o 13 0 1 2.82 -112.65 112.65 o -13 1 1 46.54 42.72 134.55 o -12 1 1 47.06 -8.06 109.73 o -11 1 1 3.26 45.82 91.19 o -10 1 1 181.61 35.87 83.21 o -9 1 1 126.43 50.09 82.37 o -8 1 1 557.65 427.96 91.84 o -7 1 1 22.44 25.55 22.13 o -6 1 1 175.10 262.51 31.14 o -5 1 1 1654.16 1477.19 85.05 o -4 1 1 140.89 224.72 21.87 o -3 1 1 3876.77 3464.99 77.45 o -2 1 1 1771.78 1658.03 44.10 o -1 1 1 22593.29 23327.02 425.24 o 1 1 1 22550.71 22832.32 135.79 o 2 1 1 1780.59 1571.53 44.43 o 3 1 1 3807.60 3619.67 60.46 o 4 1 1 152.48 222.06 27.68 o 5 1 1 1660.98 1588.21 50.04 o 6 1 1 176.83 295.23 36.74 o 7 1 1 24.50 17.75 24.06 o 8 1 1 545.51 470.70 94.39 o 9 1 1 134.96 96.91 82.03 o 10 1 1 181.33 66.38 87.50 o 11 1 1 3.02 -29.35 94.34 o 12 1 1 47.45 19.47 115.59 o 13 1 1 46.51 -20.13 118.74 o -13 2 1 4.50 42.15 131.39 o -12 2 1 57.59 82.66 117.33 o -11 2 1 65.20 72.28 97.40 o -10 2 1 73.64 15.84 81.10 o -9 2 1 159.67 151.65 87.07 o -8 2 1 103.99 69.64 42.85 o -7 2 1 455.45 538.98 64.29 o -6 2 1 309.40 284.21 29.16 o -5 2 1 2244.08 2353.51 52.41 o -4 2 1 506.11 579.80 27.27 o -3 2 1 1255.80 1261.82 46.21 o -2 2 1 3244.85 3236.89 52.79 o -1 2 1 1599.15 1624.29 38.25 o 0 2 1 3328.96 3152.28 78.82 o 1 2 1 1581.86 1476.79 22.10 o 2 2 1 3230.62 3305.39 67.20 o 3 2 1 1271.62 1255.78 51.48 o 4 2 1 507.87 514.66 43.64 o 5 2 1 2255.17 2351.56 83.95 o 6 2 1 311.99 275.23 48.20 o 7 2 1 458.19 505.26 68.64 o 8 2 1 101.83 41.86 65.48 o 9 2 1 162.18 196.78 88.44 o 10 2 1 74.03 57.51 85.32 o 11 2 1 65.32 -19.28 97.43 o 12 2 1 58.76 127.59 116.03 o 13 2 1 4.54 -99.26 119.11 o -13 3 1 6.03 80.58 135.75 o -12 3 1 19.99 36.11 112.66 o -11 3 1 28.93 9.19 90.48 o -10 3 1 27.19 44.21 88.92 o -9 3 1 164.58 95.75 82.04 o -8 3 1 313.87 390.53 69.22 o -7 3 1 1491.55 1400.30 81.60 o -6 3 1 340.57 380.19 37.63 o -5 3 1 3504.98 3812.74 97.84 o -4 3 1 1623.64 1616.69 48.89 o -3 3 1 1872.14 1820.73 47.24 o -2 3 1 12752.84 12375.69 117.67 o -1 3 1 935.05 935.93 27.07 o 0 3 1 3167.54 3176.58 49.08 o 1 3 1 921.71 965.45 21.85 o 2 3 1 12709.52 12261.19 145.73 o 3 3 1 1888.84 1765.09 62.02 o 4 3 1 1641.57 1648.12 68.98 o 5 3 1 3503.37 3778.62 165.12 o 6 3 1 344.66 287.88 47.62 o 7 3 1 1484.53 1362.98 83.00 o 8 3 1 313.90 419.59 100.78 o 9 3 1 163.54 105.73 86.22 o 10 3 1 29.44 45.74 87.80 o 11 3 1 28.65 31.62 102.46 o 12 3 1 20.37 87.49 115.76 o 13 3 1 6.04 1.58 112.64 o -13 4 1 44.72 64.71 134.69 o -12 4 1 12.74 -33.85 106.05 o -11 4 1 81.26 88.41 96.82 o -10 4 1 0.84 76.87 86.12 o -9 4 1 60.63 33.11 78.86 o -8 4 1 122.52 122.00 49.82 o -7 4 1 102.59 106.27 46.90 o -6 4 1 590.56 647.83 46.37 o -5 4 1 504.55 524.88 35.93 o -4 4 1 688.55 767.92 37.14 o -3 4 1 361.46 376.54 28.87 o -2 4 1 142.19 153.64 20.96 o -1 4 1 12013.57 12167.88 190.68 o 0 4 1 5423.19 5184.63 72.42 o 1 4 1 12061.55 12361.03 84.99 o 2 4 1 139.81 128.70 16.90 o 3 4 1 364.92 384.15 29.43 o 4 4 1 686.08 757.05 52.05 o 5 4 1 511.03 643.28 61.60 o 6 4 1 584.52 707.82 71.30 o 7 4 1 106.13 79.96 42.44 o 8 4 1 119.67 92.13 51.36 o 9 4 1 62.19 40.34 78.36 o 10 4 1 0.87 4.26 80.15 o 11 4 1 82.85 105.19 101.43 o 12 4 1 12.89 -13.98 112.98 o 13 4 1 44.03 -43.13 123.92 o -12 5 1 9.46 -39.38 103.40 o -11 5 1 27.53 31.69 90.55 o -10 5 1 108.78 30.18 85.28 o -9 5 1 170.08 131.25 77.87 o -8 5 1 128.82 124.85 52.03 o -7 5 1 896.60 927.33 89.16 o -6 5 1 1780.77 1753.48 125.80 o -5 5 1 2334.44 2460.58 63.70 o -4 5 1 125.59 122.05 25.97 o -3 5 1 227.35 174.92 25.09 o -2 5 1 4344.95 4245.64 81.15 o -1 5 1 4596.88 4832.43 110.58 o 0 5 1 8747.71 9266.94 108.99 o 1 5 1 4606.81 4633.84 70.64 o 2 5 1 4316.20 4134.22 61.48 o 3 5 1 229.36 201.89 21.59 o 4 5 1 134.04 144.89 31.84 o 5 5 1 2339.20 2419.32 81.58 o 6 5 1 1784.02 1748.58 88.88 o 7 5 1 900.04 850.48 84.65 o 8 5 1 130.69 146.45 55.68 o 9 5 1 171.62 61.66 66.03 o 10 5 1 107.33 69.01 66.38 o 11 5 1 27.01 10.49 101.19 o 12 5 1 9.64 -22.85 116.68 o -12 6 1 33.63 -21.74 110.39 o -11 6 1 30.83 6.63 74.79 o -10 6 1 80.98 174.33 100.10 o -9 6 1 84.34 42.74 59.46 o -8 6 1 61.45 28.25 47.58 o -7 6 1 35.42 -1.79 44.54 o -6 6 1 184.94 219.84 51.07 o -5 6 1 2135.25 2129.89 63.71 o -4 6 1 1280.66 1394.99 65.15 o -3 6 1 5176.99 5420.04 84.37 o -2 6 1 324.74 290.74 25.74 o -1 6 1 2101.91 2146.62 39.56 o 0 6 1 2033.47 1972.11 56.22 o 1 6 1 2079.64 2109.29 37.38 o 2 6 1 323.11 286.82 22.48 o 3 6 1 5203.62 5297.32 78.84 o 4 6 1 1276.50 1245.38 40.72 o 5 6 1 2128.13 2072.71 78.84 o 6 6 1 181.04 154.57 39.13 o 7 6 1 38.66 66.05 39.65 o 8 6 1 61.58 12.99 41.08 o 9 6 1 84.13 85.16 61.77 o 10 6 1 84.39 78.62 71.04 o 11 6 1 30.92 64.73 74.75 o 12 6 1 34.82 -2.99 110.94 o -12 7 1 11.71 55.15 111.07 o -11 7 1 40.46 -4.49 75.96 o -10 7 1 2.75 3.66 68.99 o -9 7 1 8.13 -1.95 47.21 o -8 7 1 74.36 31.11 51.63 o -7 7 1 69.11 25.60 44.47 o -6 7 1 598.68 698.67 73.93 o -5 7 1 70.19 46.17 24.13 o -4 7 1 688.62 774.64 53.90 o -3 7 1 2996.23 3092.72 67.63 o -2 7 1 4664.95 4791.45 78.06 o -1 7 1 2492.32 2469.16 52.36 o 0 7 1 746.71 754.78 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