#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:58:04 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180932 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/12/2201224.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201224_Fobs loop_ _publ_author_name 'Wang, Shun' 'Hu, Mao-Lin' 'Ng, Seik Weng' _publ_section_title ; catena-Poly[[tetra-\m-acetatodinickel(II)]\m-N,N'-hexamethylenetetramine] ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m242 _journal_page_last m244 _journal_volume 58 _journal_year 2002 _space_group_IT_number 67 _symmetry_space_group_name_Hall '-C 2a 2' _symmetry_space_group_name_H-M 'C m m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 15.4800 _cell_length_b 15.6380 _cell_length_c 8.0480 _exptl_crystal_F_000 1024.00 _reflns_d_resolution_high 0.8396 _cod_data_source_file ya6102Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' S37 in Cmma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 408.26 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y+1/2, z' '-x, y+1/2, -z' 'x, -y, -z' 'x+1/2, y+1/2, z' '-x+1/2, -y+1, z' '-x+1/2, y+1, -z' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x, y-1/2, -z' 'x, -y-1/2, z' '-x, y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, y, -z' 'x+1/2, -y, z' '-x+1/2, y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 166675.70 137563.95 2752.38 o 4 0 0 2846.01 3144.26 81.21 o 6 0 0 130.58 152.08 25.19 o 8 0 0 17535.63 18142.31 387.23 o 10 0 0 67630.58 64636.06 1316.09 o 12 0 0 24548.28 25940.22 836.15 o 14 0 0 11020.78 10880.84 398.41 o 16 0 0 4266.15 4308.81 208.85 o 18 0 0 769.35 580.85 102.17 o 0 2 0 29619.29 27376.17 752.73 o 2 2 0 5016.34 5453.90 163.27 o 4 2 0 48.74 116.26 28.64 o 6 2 0 1631.95 1700.68 39.50 o 8 2 0 12766.63 13927.00 343.54 o 10 2 0 10603.40 11035.70 211.37 o 12 2 0 1712.15 1857.04 63.01 o 14 2 0 389.72 244.49 51.09 o 16 2 0 671.12 543.85 113.94 o 18 2 0 924.54 903.71 88.57 o 0 4 0 3150.33 2920.31 104.33 o 2 4 0 13042.27 12527.77 255.51 o 4 4 0 385.55 353.83 24.10 o 6 4 0 30.98 5.83 23.60 o 8 4 0 633.03 773.13 46.35 o 10 4 0 99.66 117.62 30.41 o 12 4 0 1088.31 1096.40 51.96 o 14 4 0 80.50 86.98 35.27 o 16 4 0 2.34 -11.02 47.31 o 18 4 0 101.35 46.28 55.64 o 0 6 0 14532.20 13025.63 379.39 o 2 6 0 3539.81 3948.95 233.99 o 4 6 0 6151.01 5796.36 131.34 o 6 6 0 9148.59 8978.55 161.94 o 8 6 0 9630.40 9406.70 220.81 o 10 6 0 3820.77 3840.53 115.49 o 12 6 0 116.06 192.05 51.89 o 14 6 0 588.51 542.62 48.24 o 16 6 0 1548.18 1476.42 125.63 o 0 8 0 2949.09 2918.83 114.68 o 2 8 0 16011.17 14434.80 298.51 o 4 8 0 20383.00 20640.44 416.28 o 6 8 0 30099.87 26397.89 717.94 o 8 8 0 20981.15 21260.16 621.58 o 10 8 0 2135.59 2020.68 103.25 o 12 8 0 2003.34 1998.77 69.96 o 14 8 0 3307.52 3241.00 96.59 o 16 8 0 4393.34 4614.88 125.40 o 0 10 0 2855.25 3409.40 140.62 o 2 10 0 13486.65 12791.55 272.54 o 4 10 0 19737.88 20062.68 332.66 o 6 10 0 17415.64 17630.74 528.08 o 8 10 0 7184.96 7371.28 260.41 o 10 10 0 1288.49 1533.29 117.37 o 12 10 0 2838.81 2608.14 139.15 o 14 10 0 3441.31 3357.25 120.38 o 0 12 0 2826.47 2726.71 121.33 o 2 12 0 943.68 845.28 64.30 o 4 12 0 1848.98 2099.95 124.02 o 6 12 0 1705.96 1889.15 124.29 o 8 12 0 38.31 30.11 56.60 o 10 12 0 24.36 85.84 59.29 o 12 12 0 93.25 -14.59 65.14 o 14 12 0 6.16 -3.73 99.42 o 0 14 0 155.66 181.83 62.38 o 2 14 0 80.39 64.50 35.84 o 4 14 0 197.51 156.82 65.54 o 6 14 0 1715.13 1599.23 111.72 o 8 14 0 2429.51 2455.82 141.16 o 10 14 0 17.91 -43.63 54.25 o 12 14 0 137.36 18.28 68.09 o 0 16 0 9063.29 8352.97 290.05 o 2 16 0 5136.94 4898.59 203.07 o 4 16 0 2722.04 2459.78 146.00 o 6 16 0 2050.10 2145.87 141.70 o 8 16 0 2115.50 2045.57 146.27 o 2 18 0 2250.29 2134.03 147.62 o 4 18 0 1602.26 1649.98 129.73 o 0 0 1 39195.82 34588.62 946.12 o 2 0 1 13562.68 14392.77 242.79 o 4 0 1 3595.50 4014.52 79.45 o 6 0 1 9105.79 9418.38 161.54 o 8 0 1 21946.72 23074.96 344.13 o 10 0 1 13560.62 14464.63 225.43 o 12 0 1 2491.10 2418.36 95.55 o 14 0 1 509.87 512.94 62.72 o 16 0 1 1016.86 1073.92 83.02 o 18 0 1 1487.49 1620.94 155.14 o 1 1 1 8041.16 7957.33 124.82 o 3 1 1 25250.74 26016.52 284.23 o 5 1 1 661.71 693.41 18.72 o 7 1 1 4295.87 4665.82 58.89 o 9 1 1 767.54 789.32 22.80 o 11 1 1 1524.12 1467.13 53.16 o 13 1 1 3076.03 3213.16 95.52 o 15 1 1 356.94 293.89 42.24 o 17 1 1 349.33 397.88 57.02 o 0 2 1 80059.37 72841.73 1393.91 o 2 2 1 33759.49 32841.67 380.28 o 4 2 1 1386.17 1443.43 28.57 o 6 2 1 402.59 428.06 16.50 o 8 2 1 4784.13 4832.17 79.31 o 10 2 1 7713.89 7662.61 99.49 o 12 2 1 5224.95 5384.60 95.61 o 14 2 1 2415.32 2308.70 71.62 o 16 2 1 975.35 1012.59 58.06 o 18 2 1 298.45 307.25 47.22 o 1 3 1 99.24 172.79 17.58 o 3 3 1 34415.85 33877.97 386.69 o 5 3 1 11344.41 11214.89 129.78 o 7 3 1 11992.34 11955.60 139.12 o 9 3 1 1323.16 1355.40 32.96 o 11 3 1 2471.09 2330.58 56.46 o 13 3 1 3917.35 3766.87 69.43 o 15 3 1 411.34 386.27 44.07 o 17 3 1 753.72 742.08 55.24 o 0 4 1 8577.28 8443.08 179.03 o 2 4 1 317.58 368.20 19.11 o 4 4 1 3274.00 3498.56 55.34 o 6 4 1 4278.09 4423.72 102.66 o 8 4 1 104.43 74.94 16.39 o 10 4 1 491.33 422.94 27.72 o 12 4 1 138.77 146.34 23.28 o 14 4 1 29.19 35.35 26.66 o 16 4 1 136.97 142.40 40.34 o 1 5 1 934.87 1043.86 29.26 o 3 5 1 7454.34 6685.02 104.24 o 5 5 1 23177.57 23108.91 295.83 o 7 5 1 5018.10 4770.31 76.37 o 9 5 1 2507.39 2473.11 54.14 o 11 5 1 2613.79 2669.19 55.06 o 13 5 1 1061.57 1034.83 43.15 o 15 5 1 962.34 1010.88 46.79 o 17 5 1 399.58 304.85 45.27 o 0 6 1 22807.53 20943.44 419.01 o 2 6 1 9460.23 9470.39 157.02 o 4 6 1 664.68 638.53 35.70 o 6 6 1 1210.35 1208.27 47.89 o 8 6 1 4597.17 4551.31 88.53 o 10 6 1 3654.70 3550.90 80.03 o 12 6 1 1449.33 1453.75 46.11 o 14 6 1 785.02 716.11 37.13 o 16 6 1 682.94 588.55 48.32 o 1 7 1 9754.75 9776.89 148.32 o 3 7 1 1643.96 1499.40 37.79 o 5 7 1 6595.85 6517.15 118.85 o 7 7 1 1072.89 1141.03 46.45 o 9 7 1 2784.05 2592.23 81.93 o 11 7 1 1783.63 1761.23 50.81 o 13 7 1 626.75 569.18 32.07 o 15 7 1 1475.60 1448.52 49.77 o 0 8 1 5164.16 5423.28 105.43 o 2 8 1 8318.02 7808.72 123.25 o 4 8 1 10163.35 10347.81 157.40 o 6 8 1 12361.28 12221.73 212.88 o 8 8 1 7858.45 8039.65 160.19 o 10 8 1 2389.11 2221.76 61.10 o 12 8 1 1116.72 1015.13 58.50 o 14 8 1 1476.60 1442.17 55.80 o 16 8 1 1895.37 1865.67 63.81 o 1 9 1 750.63 728.04 30.85 o 3 9 1 718.66 664.52 34.12 o 5 9 1 145.37 142.64 24.35 o 7 9 1 240.24 258.46 41.69 o 9 9 1 3.71 -12.08 34.79 o 11 9 1 807.09 695.19 77.68 o 13 9 1 543.31 422.88 61.20 o 15 9 1 33.19 16.77 31.68 o 0 10 1 107.39 131.33 35.82 o 2 10 1 2095.79 1926.83 53.06 o 4 10 1 10108.65 10163.66 158.02 o 6 10 1 11194.69 11521.20 533.96 o 8 10 1 3766.05 3934.64 118.96 o 10 10 1 603.96 509.71 53.09 o 12 10 1 371.08 402.78 48.09 o 14 10 1 895.68 865.09 56.22 o 1 11 1 8974.64 9056.19 130.33 o 3 11 1 4256.10 4394.08 100.19 o 5 11 1 4474.98 4455.01 177.26 o 7 11 1 250.33 210.80 42.68 o 9 11 1 1678.37 1533.96 75.04 o 11 11 1 3985.21 4020.60 126.59 o 13 11 1 2129.42 2112.01 92.16 o 0 12 1 2079.74 1913.47 150.40 o 2 12 1 1224.14 1250.37 43.65 o 4 12 1 383.17 341.38 36.68 o 6 12 1 36.29 17.16 35.88 o 8 12 1 89.29 -6.74 71.02 o 10 12 1 263.99 179.71 52.28 o 12 12 1 1009.19 1127.31 57.27 o 1 13 1 1902.39 2009.89 82.94 o 3 13 1 1747.11 1825.52 276.58 o 5 13 1 1435.49 1280.07 96.66 o 7 13 1 953.58 1031.49 96.60 o 9 13 1 1084.10 1031.57 141.20 o 11 13 1 907.92 985.87 110.64 o 13 13 1 529.47 519.03 61.56 o 0 14 1 1846.72 1788.17 233.49 o 2 14 1 1304.97 1386.94 66.44 o 4 14 1 537.54 593.66 50.16 o 6 14 1 454.75 454.58 57.90 o 8 14 1 396.69 416.73 58.39 o 10 14 1 236.57 240.35 52.51 o 12 14 1 271.88 72.33 114.88 o 1 15 1 2964.52 3049.07 79.26 o 3 15 1 1605.31 1619.06 84.88 o 5 15 1 64.68 46.58 40.38 o 7 15 1 956.43 985.92 89.14 o 9 15 1 936.95 1028.79 68.32 o 0 16 1 1289.02 1182.16 117.90 o 2 16 1 1386.06 1475.84 124.46 o 4 16 1 2056.88 2279.32 111.75 o 6 16 1 2215.14 2492.18 167.31 o 8 16 1 1495.52 1757.34 109.74 o 1 17 1 277.07 213.50 58.25 o 3 17 1 10.14 26.20 51.37 o 5 17 1 211.17 212.54 101.87 o 7 17 1 0.37 122.01 61.37 o 2 18 1 1358.40 1223.60 123.79 o 4 18 1 755.72 703.33 84.00 o 0 0 2 7014.94 6509.79 201.93 o 2 0 2 5869.95 5846.18 109.32 o 4 0 2 1461.62 1699.74 58.48 o 6 0 2 4705.50 4800.69 96.78 o 8 0 2 171.39 213.86 22.97 o 10 0 2 577.09 541.14 31.78 o 12 0 2 1101.25 1009.34 58.08 o 14 0 2 7.60 72.84 48.10 o 16 0 2 200.66 207.97 58.58 o 18 0 2 0.86 -9.56 52.69 o 1 1 2 121.32 93.28 15.27 o 3 1 2 11098.79 11057.46 136.61 o 5 1 2 19286.48 19070.85 213.77 o 7 1 2 8379.97 9005.07 109.24 o 9 1 2 1553.92 1422.78 32.84 o 11 1 2 523.24 581.14 26.30 o 13 1 2 378.85 369.07 37.88 o 15 1 2 211.49 204.76 40.01 o 17 1 2 469.76 467.39 51.48 o 0 2 2 9254.96 9804.67 205.81 o 2 2 2 113.53 81.01 12.29 o 4 2 2 9089.81 9136.92 108.18 o 6 2 2 12488.95 13298.51 154.45 o 8 2 2 2099.70 2134.96 37.61 o 10 2 2 33.30 50.95 17.27 o 12 2 2 34.39 55.09 23.28 o 14 2 2 13.26 19.76 29.00 o 16 2 2 175.32 207.47 41.37 o 1 3 2 4528.71 5036.81 74.20 o 3 3 2 25865.21 26312.95 309.17 o 5 3 2 27537.42 27187.00 299.65 o 7 3 2 10012.52 10134.52 121.37 o 9 3 2 4501.22 4567.58 71.16 o 11 3 2 5992.27 6422.96 98.27 o 13 3 2 5629.17 5599.34 102.56 o 15 3 2 1968.45 1969.40 67.94 o 17 3 2 981.10 1029.46 59.99 o 0 4 2 2690.98 2788.06 77.50 o 2 4 2 7179.28 7116.13 100.63 o 4 4 2 8194.38 8740.81 112.13 o 6 4 2 9204.15 9826.81 117.69 o 8 4 2 170.89 167.26 17.35 o 10 4 2 451.87 409.96 29.21 o 12 4 2 1399.18 1373.93 42.18 o 14 4 2 172.59 191.02 32.93 o 16 4 2 621.93 610.09 81.11 o 1 5 2 43631.14 41520.46 571.97 o 3 5 2 37749.41 38386.09 530.47 o 5 5 2 25648.86 25856.97 306.16 o 7 5 2 9646.44 9678.02 117.08 o 9 5 2 9009.63 9569.39 145.05 o 11 5 2 11615.55 11784.13 176.48 o 13 5 2 9299.29 9290.89 153.50 o 15 5 2 4107.43 4089.72 98.51 o 17 5 2 1290.74 1135.63 61.27 o 0 6 2 17923.21 18012.74 366.13 o 2 6 2 8958.12 9257.67 141.82 o 4 6 2 874.14 918.02 35.03 o 6 6 2 2528.97 2437.72 51.92 o 8 6 2 68.32 65.17 24.24 o 10 6 2 2314.81 2341.27 56.12 o 12 6 2 2793.87 2616.68 63.19 o 14 6 2 71.26 35.80 26.77 o 16 6 2 112.76 34.91 43.18 o 1 7 2 893.93 915.85 36.22 o 3 7 2 1380.23 1368.95 41.72 o 5 7 2 3228.64 3059.52 60.34 o 7 7 2 3107.23 3337.59 61.56 o 9 7 2 2309.05 2134.65 66.87 o 11 7 2 711.32 707.69 36.04 o 13 7 2 128.43 98.56 29.89 o 15 7 2 203.83 194.78 32.45 o 0 8 2 15.63 -7.93 24.04 o 2 8 2 527.02 524.95 34.85 o 4 8 2 490.26 390.55 26.36 o 6 8 2 318.19 442.94 60.93 o 8 8 2 67.92 98.88 30.14 o 10 8 2 279.97 202.30 31.62 o 12 8 2 14.47 -17.18 31.77 o 14 8 2 1.18 15.85 31.84 o 16 8 2 1.51 -13.16 41.20 o 1 9 2 165.42 182.09 23.28 o 3 9 2 357.79 435.58 28.95 o 5 9 2 1085.24 997.98 42.48 o 7 9 2 1.71 19.24 35.80 o 9 9 2 4.16 -17.40 58.74 o 11 9 2 164.96 137.51 33.18 o 13 9 2 138.01 119.45 40.51 o 15 9 2 0.75 20.41 38.26 o 0 10 2 845.94 871.23 87.65 o 2 10 2 3.97 46.74 22.83 o 4 10 2 63.49 23.88 22.41 o 6 10 2 16.00 44.77 37.98 o 8 10 2 183.09 151.61 42.77 o 10 10 2 69.49 38.48 34.59 o 12 10 2 15.80 7.70 42.15 o 14 10 2 106.05 45.21 41.15 o 1 11 2 6005.35 6141.96 107.79 o 3 11 2 8410.67 8539.28 139.43 o 5 11 2 8226.43 8006.08 195.19 o 7 11 2 3396.35 3261.63 109.21 o 9 11 2 2909.70 2908.39 106.75 o 11 11 2 3452.26 3488.58 100.40 o 13 11 2 2259.88 2244.20 83.69 o 0 12 2 368.22 418.90 48.07 o 2 12 2 555.20 503.46 35.19 o 4 12 2 22.92 -21.95 27.24 o 6 12 2 0.94 -0.43 42.71 o 8 12 2 677.69 685.10 68.49 o 10 12 2 140.38 127.43 55.19 o 12 12 2 117.73 138.48 48.80 o 1 13 2 9466.64 10194.33 165.19 o 3 13 2 6308.31 6440.57 204.18 o 5 13 2 2834.04 2764.83 144.86 o 7 13 2 2296.12 2425.70 116.36 o 9 13 2 2782.25 2735.94 109.50 o 11 13 2 3527.81 3739.95 122.80 o 0 14 2 604.59 517.84 54.14 o 2 14 2 110.89 139.63 41.07 o 4 14 2 2281.11 2213.54 95.39 o 6 14 2 2602.25 2632.16 160.08 o 8 14 2 90.56 41.74 100.76 o 10 14 2 6.89 -28.62 51.26 o 1 15 2 2033.55 2071.01 74.80 o 3 15 2 1852.46 1889.56 92.63 o 5 15 2 1933.04 1947.03 132.29 o 7 15 2 2910.60 3082.30 120.06 o 9 15 2 1693.17 1636.95 97.61 o 0 16 2 6.69 72.51 52.93 o 2 16 2 126.93 210.49 113.50 o 4 16 2 146.03 227.28 73.00 o 6 16 2 9.23 -2.47 114.68 o 8 16 2 5.92 -51.16 51.16 o 1 17 2 17.30 30.42 51.06 o 3 17 2 227.76 78.44 75.99 o 5 17 2 124.93 119.19 63.86 o 2 18 2 25.55 -8.32 62.15 o 0 0 3 15088.32 14181.21 412.73 o 2 0 3 4792.40 4402.12 107.32 o 4 0 3 3534.64 3875.25 82.34 o 6 0 3 5178.68 4969.75 127.46 o 8 0 3 6056.46 6221.05 109.65 o 10 0 3 2285.68 2348.19 59.63 o 12 0 3 288.09 369.08 38.07 o 14 0 3 1017.85 1140.82 79.68 o 16 0 3 1903.50 1907.17 141.30 o 1 1 3 2044.14 1818.14 41.70 o 3 1 3 53.15 28.54 14.20 o 5 1 3 928.08 865.88 25.32 o 7 1 3 553.86 575.39 22.19 o 9 1 3 14.40 0.10 15.06 o 11 1 3 473.46 454.07 27.23 o 13 1 3 193.66 195.09 35.54 o 15 1 3 495.99 547.42 48.32 o 17 1 3 1.93 44.17 38.76 o 0 2 3 11452.73 10877.32 369.17 o 2 2 3 5082.50 5064.85 76.81 o 4 2 3 1086.35 1089.04 42.51 o 6 2 3 3275.22 3498.40 52.13 o 8 2 3 5778.38 5960.70 79.47 o 10 2 3 2525.62 2612.05 51.13 o 12 2 3 520.54 477.00 30.44 o 14 2 3 410.68 328.41 67.12 o 16 2 3 671.49 626.08 50.81 o 1 3 3 13779.31 13566.08 199.22 o 3 3 3 11714.92 11367.97 142.05 o 5 3 3 26899.40 26711.95 316.78 o 7 3 3 8138.01 8350.39 103.97 o 9 3 3 6494.48 6710.11 97.26 o 11 3 3 4374.58 4515.76 83.92 o 13 3 3 2044.17 2192.52 60.95 o 15 3 3 2930.93 2977.34 85.51 o 17 3 3 952.60 884.55 95.03 o 0 4 3 13633.12 13773.51 286.39 o 2 4 3 6721.74 6794.72 98.65 o 4 4 3 1406.50 1437.24 31.17 o 6 4 3 3289.10 3253.29 54.84 o 8 4 3 9.38 3.50 15.95 o 10 4 3 1684.94 1687.50 46.61 o 12 4 3 2100.12 2049.79 55.88 o 14 4 3 85.12 103.97 35.79 o 16 4 3 110.90 124.17 41.57 o 1 5 3 12235.68 12554.61 168.82 o 3 5 3 16367.25 16006.68 212.06 o 5 5 3 8006.16 8234.64 114.18 o 7 5 3 10441.97 10904.12 140.54 o 9 5 3 6674.01 7320.11 117.94 o 11 5 3 4154.49 4326.30 82.57 o 13 5 3 3129.91 3163.90 88.10 o 15 5 3 1055.26 921.25 47.98 o 0 6 3 8123.52 8966.59 214.47 o 2 6 3 4915.60 5291.41 91.32 o 4 6 3 2426.49 2200.84 44.71 o 6 6 3 3270.02 3445.78 56.02 o 8 6 3 2618.25 2806.46 103.50 o 10 6 3 539.40 494.90 36.10 o 12 6 3 374.82 342.32 34.47 o 14 6 3 1403.17 1314.05 51.49 o 16 6 3 1526.28 1338.98 74.42 o 1 7 3 9351.47 9062.62 142.30 o 3 7 3 3604.49 3829.31 72.33 o 5 7 3 694.81 771.98 38.18 o 7 7 3 126.20 112.24 28.41 o 9 7 3 664.21 690.02 55.11 o 11 7 3 2007.15 1971.06 88.39 o 13 7 3 2347.27 2415.18 81.29 o 15 7 3 141.66 171.94 40.69 o 0 8 3 1253.86 1225.49 55.59 o 2 8 3 2268.72 1763.46 72.44 o 4 8 3 1172.88 1227.15 43.92 o 6 8 3 3581.68 3726.63 100.34 o 8 8 3 4704.40 4797.47 176.78 o 10 8 3 1027.92 1218.57 57.17 o 12 8 3 137.88 115.10 48.44 o 14 8 3 128.10 66.72 41.17 o 1 9 3 64.73 81.92 23.16 o 3 9 3 913.77 962.37 50.19 o 5 9 3 939.36 910.38 43.22 o 7 9 3 535.88 508.74 56.52 o 9 9 3 88.09 61.50 33.10 o 11 9 3 59.97 69.26 35.79 o 13 9 3 211.45 251.33 52.90 o 15 9 3 91.69 42.05 43.98 o 0 10 3 6750.03 6801.89 164.65 o 2 10 3 4518.00 4562.72 86.89 o 4 10 3 1271.39 1319.25 49.78 o 6 10 3 689.81 686.87 63.78 o 8 10 3 1211.69 1190.84 56.83 o 10 10 3 1909.82 1943.32 73.77 o 12 10 3 1461.51 1461.57 67.95 o 14 10 3 596.34 579.09 69.08 o 1 11 3 2506.63 2512.86 70.91 o 3 11 3 3763.18 3913.92 85.46 o 5 11 3 758.55 754.38 45.05 o 7 11 3 1831.10 1833.73 93.54 o 9 11 3 901.06 771.81 95.25 o 11 11 3 972.10 1110.19 79.51 o 13 11 3 1344.61 1575.77 94.67 o 0 12 3 37.37 5.99 37.34 o 2 12 3 16.43 -0.91 37.80 o 4 12 3 1494.39 1432.15 93.98 o 6 12 3 893.80 858.06 93.64 o 8 12 3 14.76 52.56 48.96 o 10 12 3 32.25 75.01 140.42 o 12 12 3 78.87 244.56 88.50 o 1 13 3 3160.50 3368.38 77.40 o 3 13 3 4992.69 5098.12 115.54 o 5 13 3 6787.92 6805.28 180.68 o 7 13 3 6567.35 7069.13 271.77 o 9 13 3 3434.93 3660.01 131.14 o 11 13 3 1382.68 1496.22 98.72 o 0 14 3 2378.86 2478.31 93.34 o 2 14 3 608.43 668.18 50.94 o 4 14 3 146.60 180.33 50.47 o 6 14 3 2.21 -88.83 88.83 o 8 14 3 682.69 816.05 100.36 o 10 14 3 642.59 790.85 84.63 o 1 15 3 540.81 457.63 46.07 o 3 15 3 275.75 163.79 55.31 o 5 15 3 1210.63 1270.00 84.86 o 7 15 3 411.55 446.49 79.72 o 9 15 3 363.04 260.16 147.14 o 0 16 3 2833.81 2859.34 158.24 o 2 16 3 1240.89 1346.98 162.98 o 4 16 3 349.48 434.39 69.48 o 6 16 3 302.59 157.36 68.13 o 1 17 3 69.73 296.52 186.43 o 3 17 3 11.09 66.00 56.23 o 0 0 4 1763.22 1649.45 84.63 o 2 0 4 14979.68 13644.97 579.44 o 4 0 4 21089.47 20916.26 519.88 o 6 0 4 22750.66 23523.16 400.74 o 8 0 4 17100.49 17717.20 346.05 o 10 0 4 997.56 1103.68 43.75 o 12 0 4 1949.90 1903.20 67.11 o 14 0 4 3051.63 2914.93 114.69 o 16 0 4 3567.12 3433.17 247.27 o 1 1 4 12.59 21.61 17.89 o 3 1 4 60.37 40.73 19.17 o 5 1 4 1843.69 1916.99 42.69 o 7 1 4 1678.69 1703.77 35.83 o 9 1 4 459.56 467.63 36.09 o 11 1 4 25.99 57.44 20.71 o 13 1 4 54.17 42.51 33.86 o 15 1 4 138.11 84.53 43.63 o 0 2 4 3313.02 3114.90 130.34 o 2 2 4 5625.99 5852.28 130.46 o 4 2 4 11540.94 11233.54 155.40 o 6 2 4 13665.88 14747.17 184.49 o 8 2 4 7677.19 8359.74 106.91 o 10 2 4 1934.50 1949.95 48.84 o 12 2 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8 597.45 603.47 58.43 o 0 4 8 5.26 50.17 47.83 o 2 4 8 132.84 94.26 34.21 o 4 4 8 3.49 -8.99 36.63 o 6 4 8 31.04 29.01 43.25 o 8 4 8 2.15 5.30 39.56 o 1 5 8 1457.15 1390.81 57.35 o 3 5 8 536.25 490.78 43.74 o 5 5 8 636.01 675.27 47.17 o 7 5 8 634.64 762.69 65.72 o 0 6 8 737.13 685.84 67.24 o 2 6 8 429.84 487.77 45.20 o 4 6 8 505.96 517.24 44.76 o 6 6 8 576.94 632.70 55.07 o 8 6 8 463.14 436.58 61.49 o 1 7 8 371.26 371.47 41.81 o 3 7 8 3.60 35.53 34.25 o 5 7 8 522.80 543.62 47.75 o 7 7 8 128.12 104.98 67.08 o 0 8 8 1156.04 1019.69 94.34 o 2 8 8 1847.40 1720.05 74.80 o 4 8 8 1765.11 1688.99 64.07 o 6 8 8 1437.87 1513.65 71.56 o 1 9 8 132.49 107.16 44.34 o 3 9 8 20.01 29.78 45.47 o 0 10 8 683.67 491.24 65.05 o 2 10 8 1158.70 1175.91 60.62 o 0 0 9 639.13 447.82 84.50 o 2 0 9 524.88 484.90 65.39 o 4 0 9 1288.31 1243.02 82.16 o 6 0 9 1173.71 1253.23 87.22 o 1 1 9 37.18 -10.52 65.61 o 3 1 9 35.95 55.33 42.61 o 5 1 9 34.42 27.14 36.84 o 0 2 9 3132.82 3151.18 118.97 o 2 2 9 2338.31 2459.93 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