#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/12/2201299.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2201299_Fobs
loop_
_publ_author_name
'Nockemann, Peter'
'Meyer, Gerd'
_publ_section_title
;
 Bis(tetraethylammonium) decachloro- tetramercurate(II),
 (Et~4~N)~2~[Hg~4~Cl~10~]
;
_journal_issue                   10
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m534
_journal_page_last               m536
_journal_volume                  58
_journal_year                    2002
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                105.537
_cell_angle_beta                 96.467
_cell_angle_gamma                109.182
_cell_length_a                   8.3409
_cell_length_b                   10.5043
_cell_length_c                   11.0390
_exptl_crystal_F_000             640.00
_reflns_d_resolution_high        0.7828
_[local]_cod_data_source_file    bt6188Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' TEN16                           P-1'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            320.80
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 0 0 19909.47 15982.31 984.78 o
2 0 0 618.51 501.93 190.24 o
3 0 0 9329.18 8288.76 254.67 o
4 0 0 32940.30 29496.63 901.12 o
5 0 0 188.43 149.12 118.53 o
6 0 0 670.73 784.82 148.59 o
7 0 0 78.83 155.09 119.05 o
8 0 0 442.00 508.10 135.62 o
9 0 0 733.12 852.70 119.16 o
-10 1 0 494.96 485.76 155.69 o
-9 1 0 724.46 744.65 134.88 o
-8 1 0 680.63 649.18 119.74 o
-7 1 0 125.36 293.99 132.38 o
-6 1 0 557.56 568.73 116.56 o
-5 1 0 601.44 578.47 154.64 o
-4 1 0 43729.70 36935.48 1225.28 o
-3 1 0 21320.67 17793.13 420.84 o
-2 1 0 204.12 217.17 216.24 o
1 1 0 18862.51 16757.62 949.78 o
2 1 0 198.62 227.61 197.93 o
3 1 0 3920.15 3489.79 201.49 o
4 1 0 6776.98 6351.46 175.15 o
5 1 0 237.59 82.40 129.66 o
6 1 0 3750.89 4162.26 182.75 o
7 1 0 3.78 90.68 119.02 o
8 1 0 405.14 305.52 151.24 o
9 1 0 485.83 407.09 129.48 o
-10 2 0 642.27 627.02 141.58 o
-9 2 0 366.26 564.92 133.28 o
-8 2 0 1900.67 1979.97 123.96 o
-7 2 0 1198.24 1227.61 137.84 o
-6 2 0 2003.47 1990.51 159.55 o
-5 2 0 4787.81 4483.46 156.33 o
-4 2 0 56673.54 50600.45 2172.58 o
-3 2 0 7937.26 7023.20 395.87 o
-2 2 0 2010.14 2165.78 275.83 o
-1 2 0 26398.38 23800.66 1049.98 o
0 2 0 50451.65 43041.55 2776.97 o
1 2 0 2682.23 2584.73 247.74 o
2 2 0 2853.26 2682.09 199.93 o
3 2 0 1014.78 891.21 154.76 o
4 2 0 1212.47 1098.71 128.77 o
5 2 0 1164.78 1309.32 156.29 o
6 2 0 6810.65 7398.40 224.94 o
7 2 0 59.61 51.82 124.93 o
8 2 0 241.78 215.56 125.40 o
9 2 0 431.13 471.42 157.13 o
-10 3 0 475.07 526.81 141.67 o
-9 3 0 3.25 53.53 184.46 o
-8 3 0 3210.20 3345.26 272.71 o
-7 3 0 2228.83 2347.63 155.46 o
-6 3 0 2724.99 2570.71 150.95 o
-5 3 0 3163.25 2671.49 183.47 o
-4 3 0 28765.41 24757.96 989.90 o
-3 3 0 13920.41 12274.89 298.56 o
-2 3 0 6590.57 6482.07 702.28 o
-1 3 0 3752.70 3326.80 223.76 o
0 3 0 3251.08 2895.17 225.32 o
1 3 0 174.24 215.06 194.55 o
2 3 0 17606.01 15646.60 426.34 o
3 3 0 149.49 39.07 139.06 o
4 3 0 937.24 713.82 126.37 o
5 3 0 2297.43 2422.18 141.66 o
6 3 0 9306.72 10232.92 315.71 o
7 3 0 3.08 -26.09 123.57 o
8 3 0 74.45 73.98 125.69 o
-10 4 0 461.49 698.63 200.76 o
-9 4 0 176.24 362.98 189.52 o
-8 4 0 4981.76 5427.47 283.43 o
-7 4 0 1835.80 1713.81 202.17 o
-6 4 0 708.84 551.94 211.50 o
-5 4 0 4601.63 4377.13 226.34 o
-4 4 0 16183.48 14576.14 824.91 o
-3 4 0 5314.59 4562.58 214.74 o
-2 4 0 1924.91 1774.40 184.76 o
-1 4 0 1300.25 1204.55 190.00 o
0 4 0 8984.45 7953.58 1007.02 o
1 4 0 282.80 299.59 128.91 o
2 4 0 13797.74 12539.57 439.67 o
3 4 0 9.60 78.37 123.62 o
4 4 0 1250.81 1110.53 131.64 o
5 4 0 4773.87 4954.71 272.82 o
6 4 0 5341.74 5691.92 240.03 o
7 4 0 119.82 283.96 119.13 o
8 4 0 5.30 51.04 140.17 o
-10 5 0 234.84 146.70 168.41 o
-9 5 0 235.34 78.23 162.74 o
-8 5 0 5502.86 5485.96 308.89 o
-7 5 0 1716.84 1810.03 168.30 o
-6 5 0 76.50 -0.16 146.71 o
-5 5 0 722.44 463.40 175.19 o
-4 5 0 15760.17 14041.45 958.72 o
-3 5 0 2793.99 2700.58 287.28 o
-2 5 0 539.76 529.85 159.14 o
-1 5 0 502.87 429.85 162.59 o
0 5 0 13084.61 12041.61 1642.79 o
1 5 0 4217.39 3817.95 240.72 o
2 5 0 13386.87 12729.53 582.71 o
3 5 0 145.68 222.22 132.93 o
4 5 0 1179.01 1155.16 133.25 o
5 5 0 4784.25 4837.80 185.08 o
6 5 0 2989.08 3030.33 226.26 o
7 5 0 124.30 137.96 133.64 o
-10 6 0 62.01 18.38 143.17 o
-9 6 0 55.73 280.48 193.67 o
-8 6 0 4298.04 3938.75 256.37 o
-7 6 0 1811.58 1705.99 168.67 o
-6 6 0 125.98 139.17 203.08 o
-5 6 0 1529.87 1328.38 173.86 o
-4 6 0 15376.96 14665.06 1382.94 o
-3 6 0 889.04 838.18 161.13 o
-2 6 0 1787.32 1743.92 170.89 o
-1 6 0 1301.07 1239.81 146.60 o
0 6 0 10099.01 8826.82 955.14 o
1 6 0 3192.12 2764.39 147.31 o
2 6 0 8396.12 7690.33 153.54 o
3 6 0 533.13 597.07 148.62 o
4 6 0 83.00 0.87 118.37 o
5 6 0 2136.43 2331.52 139.50 o
6 6 0 1562.92 1723.50 140.59 o
-10 7 0 46.94 -16.29 170.73 o
-9 7 0 47.71 279.62 318.70 o
-8 7 0 2587.93 2344.72 246.03 o
-7 7 0 1736.56 1571.48 175.41 o
-6 7 0 77.53 218.39 147.93 o
-5 7 0 943.08 976.72 214.98 o
-4 7 0 10506.62 9431.63 221.63 o
-3 7 0 6.14 88.06 149.01 o
-2 7 0 5376.47 4636.09 352.52 o
-1 7 0 382.38 548.55 169.44 o
0 7 0 1993.53 1866.06 184.93 o
1 7 0 5604.96 5189.53 415.41 o
2 7 0 7257.22 6895.25 220.83 o
3 7 0 328.74 358.27 147.71 o
4 7 0 31.02 38.19 141.16 o
5 7 0 837.18 916.56 157.45 o
6 7 0 644.45 730.43 135.29 o
-10 8 0 33.38 -11.34 174.58 o
-9 8 0 78.93 41.28 201.19 o
-8 8 0 1675.93 1563.46 170.95 o
-7 8 0 544.10 461.84 213.83 o
-6 8 0 504.28 568.04 178.85 o
-5 8 0 1144.60 1175.39 165.66 o
-4 8 0 3237.30 3087.91 262.43 o
-3 8 0 587.47 546.84 125.93 o
-2 8 0 10305.11 9038.50 523.59 o
-1 8 0 249.95 175.54 203.83 o
0 8 0 1.87 17.15 157.80 o
1 8 0 1909.04 1791.84 190.27 o
2 8 0 6810.97 6735.32 392.60 o
3 8 0 161.41 129.59 141.18 o
4 8 0 1.96 30.13 163.55 o
5 8 0 350.81 359.58 147.76 o
-9 9 0 132.09 49.63 175.45 o
-8 9 0 1206.16 1120.45 178.99 o
-7 9 0 13.93 121.02 211.64 o
-6 9 0 2155.61 2243.27 223.82 o
-5 9 0 57.72 8.30 187.95 o
-4 9 0 282.08 346.61 199.48 o
-3 9 0 2277.91 1966.70 155.60 o
-2 9 0 7549.06 6816.27 248.94 o
-1 9 0 1511.35 1208.21 191.13 o
0 9 0 463.02 448.74 144.44 o
1 9 0 2077.13 1790.81 208.05 o
2 9 0 3052.18 3157.04 202.40 o
3 9 0 111.80 80.94 148.38 o
4 9 0 40.28 -77.40 171.32 o
-9 10 0 38.01 -259.59 218.07 o
-8 10 0 644.75 403.15 212.25 o
-7 10 0 120.14 435.49 216.59 o
-6 10 0 1735.24 2055.30 241.25 o
-5 10 0 192.92 270.64 184.04 o
-4 10 0 80.89 103.63 174.84 o
-3 10 0 1841.74 1758.68 148.56 o
-2 10 0 5268.44 4667.89 395.47 o
-1 10 0 1014.21 773.61 172.58 o
0 10 0 14.86 26.74 206.11 o
1 10 0 1289.72 1371.02 150.73 o
2 10 0 1409.76 1735.57 182.26 o
3 10 0 24.76 180.28 222.98 o
-8 11 0 324.57 264.47 226.03 o
-7 11 0 180.59 99.41 306.67 o
-6 11 0 1187.88 1329.39 190.68 o
-5 11 0 545.13 642.54 191.60 o
-4 11 0 13.63 41.93 202.34 o
-3 11 0 726.02 511.38 279.50 o
-2 11 0 1739.25 1624.50 174.25 o
-1 11 0 248.51 110.76 213.15 o
0 11 0 94.88 121.98 211.10 o
1 11 0 761.52 604.64 222.68 o
-7 12 0 52.22 93.70 249.22 o
-6 12 0 548.86 547.91 179.95 o
-5 12 0 86.13 61.96 207.57 o
-4 12 0 118.81 -43.42 316.49 o
-3 12 0 251.38 360.69 211.55 o
-2 12 0 708.37 617.65 215.46 o
-1 12 0 12.41 113.21 182.01 o
3 -13 1 1.69 55.40 315.07 o
4 -13 1 435.54 555.37 326.30 o
5 -13 1 82.81 181.78 212.60 o
0 -12 1 181.40 380.94 176.62 o
1 -12 1 3.81 -187.18 214.63 o
2 -12 1 181.84 130.36 200.11 o
3 -12 1 86.91 104.55 296.90 o
4 -12 1 1867.44 1859.86 199.72 o
5 -12 1 428.06 416.05 174.77 o
6 -12 1 1.52 24.93 175.22 o
7 -12 1 113.41 196.87 242.53 o
-2 -11 1 525.47 412.97 183.20 o
-1 -11 1 311.19 235.95 181.02 o
0 -11 1 924.38 874.28 199.85 o
1 -11 1 62.70 -245.49 201.97 o
2 -11 1 28.02 5.66 279.32 o
3 -11 1 62.87 110.81 183.09 o
4 -11 1 3920.59 3592.80 184.71 o
5 -11 1 1119.48 1219.07 182.89 o
6 -11 1 2.24 67.19 170.52 o
7 -11 1 110.19 -105.24 296.24 o
8 -11 1 1055.19 858.32 196.99 o
-3 -10 1 71.36 121.37 139.71 o
-2 -10 1 814.99 724.91 142.80 o
-1 -10 1 45.53 88.48 142.66 o
0 -10 1 2031.48 2128.87 352.93 o
1 -10 1 786.57 1036.58 207.21 o
2 -10 1 206.49 264.90 189.20 o
3 -10 1 674.20 635.18 167.20 o
4 -10 1 5387.40 4743.03 220.17 o
5 -10 1 1165.33 1195.40 146.16 o
6 -10 1 163.41 202.49 208.87 o
7 -10 1 198.31 189.62 171.95 o
8 -10 1 559.81 735.12 178.38 o
9 -10 1 10.20 36.75 200.53 o
-4 -9 1 102.24 -29.54 169.61 o
-3 -9 1 207.84 121.68 127.47 o
-2 -9 1 812.44 668.16 145.80 o
-1 -9 1 38.85 110.29 149.57 o
0 -9 1 5981.79 6074.79 331.53 o
1 -9 1 4974.63 4702.86 363.21 o
2 -9 1 860.55 857.76 138.06 o
3 -9 1 460.25 480.96 167.22 o
4 -9 1 5421.62 4868.41 233.20 o
5 -9 1 731.88 665.65 176.67 o
6 -9 1 963.32 868.93 182.45 o
7 -9 1 279.02 392.05 147.23 o
8 -9 1 312.88 319.16 216.92 o
9 -9 1 97.74 110.11 166.66 o
-5 -8 1 16.37 38.61 139.36 o
-4 -8 1 898.86 833.48 143.32 o
-3 -8 1 1634.49 1670.59 144.54 o
-2 -8 1 550.28 455.19 129.75 o
-1 -8 1 944.77 860.45 127.12 o
0 -8 1 8796.08 9089.67 975.74 o
1 -8 1 5849.46 5434.59 311.37 o
2 -8 1 524.65 581.65 128.97 o
3 -8 1 1873.15 1704.09 209.52 o
4 -8 1 4292.96 3438.66 210.60 o
5 -8 1 393.94 403.55 163.34 o
6 -8 1 964.47 720.66 177.00 o
7 -8 1 200.27 31.78 210.88 o
8 -8 1 473.77 477.39 210.05 o
9 -8 1 81.17 41.69 379.94 o
10 -8 1 684.92 623.38 177.26 o
-6 -7 1 344.48 283.28 131.58 o
-5 -7 1 13.05 16.64 156.50 o
-4 -7 1 4861.94 4948.60 263.90 o
-3 -7 1 4514.65 4420.46 149.55 o
-2 -7 1 1155.87 1074.14 122.53 o
-1 -7 1 1750.06 1747.79 145.42 o
0 -7 1 21846.84 20666.76 1862.80 o
1 -7 1 5619.57 5378.41 488.43 o
2 -7 1 171.32 148.03 138.44 o
3 -7 1 3079.60 2972.50 413.65 o
4 -7 1 7201.18 6799.66 398.64 o
5 -7 1 8.84 9.79 151.27 o
6 -7 1 778.98 873.50 213.07 o
7 -7 1 61.75 268.01 202.00 o
8 -7 1 1143.16 1237.42 203.85 o
9 -7 1 153.32 375.79 200.17 o
10 -7 1 790.90 792.48 147.80 o
-7 -6 1 230.55 153.49 157.58 o
-6 -6 1 323.71 404.64 151.82 o
-5 -6 1 65.09 211.19 147.68 o
-4 -6 1 8673.46 8945.03 315.27 o
-3 -6 1 4641.50 4684.02 160.17 o
-2 -6 1 41.39 29.44 133.85 o
-1 -6 1 1055.33 1104.05 141.88 o
0 -6 1 25722.88 23554.13 758.78 o
1 -6 1 3633.14 3336.75 213.85 o
2 -6 1 683.10 622.42 182.78 o
3 -6 1 2606.78 2406.63 234.20 o
4 -6 1 16512.43 15722.75 1205.03 o
5 -6 1 26.25 124.48 165.27 o
6 -6 1 1785.66 1612.51 180.93 o
7 -6 1 7.06 17.78 199.86 o
8 -6 1 1860.46 1909.32 167.14 o
9 -6 1 347.10 215.87 199.28 o
10 -6 1 884.59 908.36 185.72 o
-7 -5 1 297.49 425.57 125.12 o
-6 -5 1 652.35 825.26 123.33 o
-5 -5 1 12.14 58.04 132.28 o
-4 -5 1 12869.78 12808.20 291.45 o
-3 -5 1 2719.14 2849.90 146.72 o
-2 -5 1 82.13 134.41 138.30 o
-1 -5 1 4894.97 4803.45 336.08 o
0 -5 1 29278.99 27692.71 1592.77 o
1 -5 1 4358.47 4282.60 383.19 o
2 -5 1 47.93 150.64 206.92 o
3 -5 1 1917.71 2088.30 199.68 o
4 -5 1 13478.56 13128.43 772.39 o
5 -5 1 78.17 221.67 175.74 o
6 -5 1 6788.49 6303.28 192.63 o
7 -5 1 206.97 80.57 162.49 o
8 -5 1 736.53 724.66 138.99 o
9 -5 1 776.15 846.69 159.40 o
10 -5 1 968.71 1010.33 151.13 o
-8 -4 1 1029.06 1025.08 124.95 o
-7 -4 1 480.45 426.79 147.65 o
-6 -4 1 1006.34 1336.29 118.06 o
-5 -4 1 20.15 76.58 118.06 o
-4 -4 1 11586.18 11607.91 604.43 o
-3 -4 1 5291.03 5207.33 272.16 o
-2 -4 1 357.00 384.53 161.15 o
-1 -4 1 4640.53 4628.08 358.22 o
0 -4 1 33922.88 31446.45 1909.14 o
1 -4 1 2154.26 2162.18 175.54 o
2 -4 1 7597.48 7738.10 412.71 o
3 -4 1 106.30 93.08 179.90 o
4 -4 1 12685.36 13097.36 454.75 o
5 -4 1 1369.46 1314.70 134.86 o
6 -4 1 15021.96 13824.14 601.20 o
7 -4 1 372.77 426.72 165.14 o
8 -4 1 9.72 138.30 133.09 o
9 -4 1 1093.31 1150.47 168.29 o
10 -4 1 1161.98 1320.17 193.99 o
-8 -3 1 1341.26 1392.50 151.79 o
-7 -3 1 1145.07 1197.04 121.69 o
-6 -3 1 152.86 207.89 133.29 o
-5 -3 1 1872.00 1951.31 140.58 o
-4 -3 1 11905.68 11667.15 661.93 o
-3 -3 1 10463.57 10089.73 638.00 o
-2 -3 1 1511.92 1521.32 194.79 o
-1 -3 1 8599.90 8530.62 363.63 o
0 -3 1 24430.85 23826.42 975.32 o
1 -3 1 3532.89 3894.87 223.06 o
2 -3 1 57594.83 64279.20 1914.46 o
3 -3 1 846.15 900.62 158.91 o
4 -3 1 53.73 41.11 136.66 o
5 -3 1 5367.11 5006.13 213.42 o
6 -3 1 20016.93 18621.05 269.17 o
7 -3 1 850.66 1020.30 157.28 o
8 -3 1 376.92 447.74 137.29 o
9 -3 1 964.47 994.24 136.72 o
10 -3 1 1004.05 1059.93 140.48 o
-9 -2 1 19.64 158.79 106.78 o
-8 -2 1 1900.29 1996.40 155.24 o
-7 -2 1 2953.35 3150.45 132.87 o
-6 -2 1 4.08 49.68 123.45 o
-5 -2 1 2812.62 2827.56 184.41 o
-4 -2 1 18814.88 18390.43 813.10 o
-3 -2 1 12699.44 11954.03 712.82 o
-2 -2 1 7214.04 7199.13 509.18 o
-1 -2 1 2342.71 2612.06 173.84 o
0 -2 1 33953.43 35388.94 905.92 o
1 -2 1 5716.87 6336.49 303.96 o
2 -2 1 77344.59 83161.76 1548.83 o
3 -2 1 4111.37 4219.33 225.77 o
4 -2 1 22.19 71.30 151.05 o
5 -2 1 13454.18 11824.19 308.40 o
6 -2 1 12011.33 10832.62 411.86 o
7 -2 1 393.70 309.19 146.06 o
8 -2 1 50.30 130.65 128.21 o
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10 -2 1 743.10 764.44 154.24 o
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-8 -1 1 3671.60 4051.72 200.57 o
-7 -1 1 4245.90 4464.72 252.39 o
-6 -1 1 227.77 289.22 155.21 o
-5 -1 1 4096.66 4335.96 223.11 o
-4 -1 1 34884.84 32490.18 963.76 o
-3 -1 1 5379.92 5243.17 302.68 o
-2 -1 1 25270.54 24470.24 964.29 o
-1 -1 1 743.75 935.86 230.00 o
1 -1 1 4998.35 5412.54 280.11 o
2 -1 1 58857.96 62289.75 2609.36 o
3 -1 1 12952.32 12173.63 204.71 o
4 -1 1 736.47 607.92 164.97 o
5 -1 1 9746.57 8905.18 289.07 o
6 -1 1 10538.65 10175.28 512.87 o
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-8 0 1 6103.39 6626.93 259.24 o
-7 0 1 3345.27 3461.20 138.99 o
-6 0 1 354.80 467.71 136.32 o
-5 0 1 981.06 1146.75 146.07 o
-4 0 1 34566.48 30506.03 1062.78 o
-3 0 1 81.11 84.18 179.60 o
-2 0 1 22070.39 22967.14 442.40 o
-1 0 1 372.50 378.64 622.78 o
1 0 1 27610.12 29030.02 617.67 o
2 0 1 15261.98 14681.95 336.64 o
3 0 1 4577.38 4245.80 171.50 o
4 0 1 85.80 87.15 139.67 o
5 0 1 6506.06 6169.28 285.97 o
6 0 1 4172.56 4017.86 129.78 o
7 0 1 6.84 118.95 118.10 o
8 0 1 1277.30 1351.34 133.76 o
9 0 1 428.91 436.82 151.96 o
-10 1 1 3.37 52.07 139.72 o
-9 1 1 108.47 264.66 182.09 o
-8 1 1 5763.23 6429.17 200.75 o
-7 1 1 1318.91 1366.83 139.40 o
-6 1 1 2507.36 2501.24 146.48 o
-5 1 1 113.22 134.01 141.22 o
-4 1 1 22123.72 19981.24 597.48 o
-3 1 1 816.26 806.69 185.56 o
-2 1 1 37459.25 38283.59 2353.74 o
-1 1 1 13573.81 14840.74 480.17 o
0 1 1 3458.04 3099.97 349.51 o
1 1 1 13826.11 12993.74 418.25 o
2 1 1 31383.66 27358.12 1008.94 o
3 1 1 1697.62 1731.15 141.36 o
4 1 1 2058.61 1976.58 144.27 o
5 1 1 5453.25 5314.06 162.99 o
6 1 1 8110.99 8434.89 178.72 o
7 1 1 274.20 421.04 113.78 o
8 1 1 1063.23 1212.05 154.25 o
9 1 1 164.16 59.88 137.37 o
-10 2 1 327.10 145.78 184.57 o
-9 2 1 42.96 110.44 153.35 o
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