#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:58:21 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180933 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/13/2201319.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201319_Fobs loop_ _publ_author_name 'Li, Jian-Rong' 'Cai, Li-Zhen' 'Zou, Ru-Qiang' 'Zhou, Guo-Wei' 'Guo, Guo-Cong' 'Bu, Xian-He' 'Huang, Jin-Shun' _publ_section_title ; Pentacyanoferrate(III)-\m-cyano-triaquatetrakis(dimethylformamide)europium(III) hydrate ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m686 _journal_page_last m687 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.116 _cell_angle_gamma 90.000 _cell_length_a 17.6332 _cell_length_b 8.8791 _cell_length_c 19.8309 _exptl_crystal_F_000 1468.00 _reflns_d_resolution_high 0.6896 _cod_data_source_file bt6208Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 14 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 385.77 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 42411.90 41174.45 280.20 o 4 0 0 25838.78 24152.94 102.09 o 6 0 0 17211.94 17354.33 212.48 o 8 0 0 13922.42 14507.10 112.42 o 10 0 0 19707.46 20375.75 150.44 o 12 0 0 4066.04 4641.33 80.82 o 14 0 0 264.61 333.22 33.10 o 16 0 0 10040.58 10563.15 144.71 o 18 0 0 6944.14 7169.82 129.46 o 20 0 0 1281.45 1376.33 68.07 o 22 0 0 9284.20 9590.79 171.97 o 24 0 0 1749.39 1906.70 80.91 o 1 1 0 1771.12 1521.07 20.15 o 2 1 0 91.63 14.69 7.44 o 3 1 0 4344.39 4265.08 41.68 o 4 1 0 57330.64 62047.73 513.75 o 6 1 0 7099.66 7715.68 42.33 o 7 1 0 16465.28 15460.96 111.18 o 8 1 0 14163.20 15362.23 118.22 o 9 1 0 15477.66 13984.24 120.08 o 10 1 0 13325.57 14911.59 131.48 o 11 1 0 15271.29 15099.27 139.56 o 12 1 0 8337.87 7937.79 110.23 o 13 1 0 12361.07 12242.87 140.98 o 14 1 0 9377.17 9725.42 133.91 o 15 1 0 7739.21 8000.64 123.57 o 16 1 0 235.31 54.11 51.51 o 17 1 0 4383.24 3788.85 104.62 o 18 1 0 5386.51 5533.35 121.77 o 19 1 0 1820.45 1752.47 79.99 o 20 1 0 197.76 29.01 52.81 o 21 1 0 670.61 660.72 61.93 o 22 1 0 271.64 178.51 52.62 o 23 1 0 28.35 12.83 39.05 o 24 1 0 4.24 -45.00 45.00 o 25 1 0 245.31 198.96 51.13 o 2 2 0 20980.28 20899.60 93.42 o 3 2 0 34161.33 33150.44 244.84 o 4 2 0 508.97 795.29 21.95 o 5 2 0 26978.08 25920.81 363.99 o 6 2 0 156.07 138.35 16.36 o 7 2 0 12701.96 12369.25 105.60 o 8 2 0 3952.93 3672.95 62.97 o 9 2 0 4963.64 5041.66 76.41 o 10 2 0 2284.97 2560.34 58.63 o 11 2 0 456.35 506.39 31.80 o 12 2 0 230.55 151.73 25.66 o 13 2 0 120.48 132.20 27.89 o 14 2 0 4230.19 4456.46 89.37 o 15 2 0 982.34 896.46 49.47 o 16 2 0 320.86 305.70 36.82 o 17 2 0 2611.41 2557.27 80.19 o 18 2 0 773.50 682.88 56.91 o 19 2 0 4400.20 4271.24 110.94 o 20 2 0 2740.07 2736.11 98.24 o 21 2 0 3455.21 3487.88 108.11 o 22 2 0 182.94 160.65 52.62 o 23 2 0 2284.98 2395.43 99.89 o 24 2 0 2244.69 2078.96 92.64 o 25 2 0 2103.43 1996.47 90.77 o 1 3 0 542.21 571.96 13.75 o 2 3 0 4479.73 5568.49 41.51 o 3 3 0 1310.38 1674.12 38.34 o 5 3 0 1816.13 1817.91 42.81 o 6 3 0 59244.20 63161.16 249.78 o 7 3 0 2005.69 2153.91 50.44 o 8 3 0 6509.10 7571.09 93.99 o 9 3 0 2015.70 2250.02 56.39 o 10 3 0 18430.95 19413.41 162.17 o 11 3 0 116.55 75.31 26.03 o 12 3 0 16193.49 17084.18 164.90 o 13 3 0 994.00 1063.88 49.29 o 14 3 0 5629.46 5989.87 106.54 o 15 3 0 39.44 -20.45 33.28 o 16 3 0 8628.98 8980.46 140.15 o 17 3 0 0.15 5.95 35.70 o 18 3 0 1574.41 1573.62 68.82 o 19 3 0 12.70 -27.15 35.51 o 20 3 0 1796.20 2015.61 83.89 o 21 3 0 45.96 -53.36 53.36 o 22 3 0 93.58 52.43 44.62 o 23 3 0 138.37 143.36 41.84 o 24 3 0 116.40 121.23 42.58 o 0 4 0 11130.99 11748.43 122.74 o 1 4 0 15548.91 17432.19 130.72 o 2 4 0 25179.27 25926.89 159.27 o 3 4 0 17342.75 16476.96 129.84 o 4 4 0 2291.42 3049.49 59.94 o 5 4 0 15036.51 15069.43 130.15 o 6 4 0 1037.98 1148.86 40.92 o 7 4 0 4584.49 4834.60 79.18 o 8 4 0 4085.47 3689.58 72.26 o 9 4 0 704.95 580.64 36.64 o 10 4 0 5836.78 6600.63 102.10 o 11 4 0 158.10 215.14 30.31 o 12 4 0 2920.37 3045.83 77.79 o 13 4 0 96.32 153.96 27.89 o 14 4 0 1668.34 1868.23 66.78 o 15 4 0 1603.84 1627.82 68.64 o 16 4 0 164.52 219.78 38.12 o 17 4 0 1524.79 1652.65 72.36 o 18 4 0 816.43 761.92 58.02 o 19 4 0 2953.87 2988.54 97.87 o 20 4 0 1478.13 1567.38 81.47 o 21 4 0 3038.87 2948.27 103.63 o 22 4 0 7.70 -45.37 45.37 o 23 4 0 3274.32 3109.43 106.80 o 24 4 0 1982.16 1919.04 91.89 o 1 5 0 430.91 393.14 30.13 o 2 5 0 225.97 236.34 27.15 o 3 5 0 2844.64 3217.66 66.65 o 4 5 0 13870.86 13553.82 133.54 o 5 5 0 11918.53 12465.24 131.16 o 6 5 0 71.42 149.12 25.47 o 7 5 0 5936.08 5546.26 93.73 o 8 5 0 9831.01 9832.29 124.64 o 9 5 0 7243.23 7479.27 112.96 o 10 5 0 4656.23 4832.87 94.41 o 11 5 0 10413.96 10780.58 142.51 o 12 5 0 2553.64 2693.43 79.83 o 13 5 0 10448.14 10359.26 148.07 o 14 5 0 6224.56 6308.12 121.99 o 15 5 0 7589.21 7634.40 136.75 o 16 5 0 537.27 551.92 51.14 o 17 5 0 2255.73 2142.20 85.95 o 18 5 0 3768.07 3878.48 110.73 o 19 5 0 1284.32 1314.37 73.28 o 20 5 0 29.58 15.80 45.93 o 21 5 0 220.30 201.93 46.67 o 22 5 0 131.30 180.36 47.23 o 23 5 0 171.71 95.20 51.69 o 0 6 0 48435.30 47679.75 309.79 o 1 6 0 371.01 406.69 35.33 o 2 6 0 4455.17 4432.66 85.11 o 3 6 0 900.78 875.11 43.89 o 4 6 0 19972.75 20227.86 178.86 o 5 6 0 94.80 87.95 15.62 o 6 6 0 9971.12 10444.83 133.59 o 7 6 0 116.26 85.35 16.92 o 8 6 0 934.19 1093.24 50.77 o 9 6 0 324.92 246.01 21.01 o 10 6 0 609.24 686.22 46.49 o 11 6 0 319.84 386.40 30.12 o 12 6 0 68.96 27.70 35.89 o 13 6 0 35.72 28.45 34.77 o 14 6 0 95.75 185.19 39.60 o 15 6 0 9.90 -1.86 38.30 o 16 6 0 3920.29 4193.79 112.22 o 17 6 0 25.61 -6.51 48.16 o 18 6 0 4061.11 4097.47 116.32 o 19 6 0 58.46 36.82 49.64 o 20 6 0 1580.59 1611.66 74.21 o 21 6 0 4.12 -50.20 50.20 o 1 7 0 782.16 628.80 38.87 o 2 7 0 23.86 47.97 13.76 o 3 7 0 2772.57 2646.91 60.85 o 4 7 0 8386.50 8695.57 105.71 o 5 7 0 2143.28 2361.26 59.54 o 6 7 0 147.37 146.34 16.36 o 7 7 0 7199.32 7565.54 103.60 o 8 7 0 1662.67 1724.25 55.99 o 9 7 0 11899.14 11595.63 132.27 o 10 7 0 1471.60 1604.88 55.80 o 11 7 0 7125.98 7066.99 133.01 o 12 7 0 1710.57 1818.12 78.13 o 13 7 0 3954.31 4076.17 108.32 o 14 7 0 3355.88 3483.15 107.37 o 15 7 0 2855.95 2869.59 97.87 o 16 7 0 50.15 61.92 45.74 o 17 7 0 1318.57 1432.11 74.95 o 18 7 0 2316.86 2337.25 87.25 o 19 7 0 893.67 741.08 61.18 o 20 7 0 17.47 2.23 41.65 o 0 8 0 132.72 155.63 21.38 o 1 8 0 6510.43 6422.12 106.00 o 2 8 0 11037.50 10827.86 127.59 o 3 8 0 7672.32 7095.15 103.98 o 4 8 0 725.39 689.02 40.54 o 5 8 0 3644.50 3426.55 75.19 o 6 8 0 698.60 690.69 41.84 o 7 8 0 2067.72 1990.60 75.90 o 8 8 0 2139.15 2166.80 81.30 o 9 8 0 1018.02 873.74 60.44 o 10 8 0 38.09 -2.60 39.42 o 11 8 0 36.83 36.44 41.46 o 12 8 0 1051.50 1029.96 70.30 o 13 8 0 516.14 546.52 58.39 o 14 8 0 662.72 643.05 65.27 o 15 8 0 656.51 601.58 63.97 o 16 8 0 246.47 188.36 48.16 o 17 8 0 1076.18 984.19 68.63 o 18 8 0 594.48 518.82 56.72 o 1 9 0 0.01 -33.65 40.91 o 2 9 0 1682.88 1502.45 71.80 o 3 9 0 24.90 -36.63 36.63 o 4 9 0 358.14 315.37 44.81 o 5 9 0 936.82 788.92 61.37 o 6 9 0 8212.96 8338.79 151.85 o 7 9 0 67.51 46.86 41.84 o 8 9 0 1019.45 951.29 65.84 o 9 9 0 1.31 18.22 39.98 o 10 9 0 6063.73 6154.86 140.40 o 11 9 0 93.80 45.00 48.53 o 12 9 0 5912.74 6006.48 142.99 o 13 9 0 158.89 186.50 42.39 o 14 9 0 2348.15 2353.82 87.99 o 15 9 0 0.58 15.62 43.32 o 16 9 0 3690.71 3860.55 112.02 o 0 10 0 693.00 692.16 73.46 o 1 10 0 8995.43 7721.93 171.06 o 2 10 0 2229.04 2120.04 88.74 o 3 10 0 3165.23 2921.19 104.20 o 4 10 0 166.79 177.94 50.02 o 5 10 0 3244.32 2958.99 105.13 o 6 10 0 307.27 280.96 56.34 o 7 10 0 1207.63 1123.91 77.00 o 8 10 0 1169.19 1057.13 65.28 o 9 10 0 900.55 887.08 66.02 o 10 10 0 265.66 201.38 49.46 o 11 10 0 14.74 47.60 43.14 o 12 10 0 380.06 301.24 58.39 o 1 11 0 29.48 47.60 49.46 o 2 11 0 1.35 35.33 43.14 o 3 11 0 378.14 375.06 53.37 o 4 11 0 1479.67 1258.07 76.07 o 5 11 0 1838.47 1601.16 78.87 o 6 11 0 2.92 -32.72 44.07 o 7 11 0 1591.26 1348.30 74.21 o -25 0 1 252.51 261.62 48.35 o -23 0 1 63.41 58.38 46.48 o -21 0 1 7122.08 6962.81 142.85 o -19 0 1 1403.79 1536.16 68.63 o -17 0 1 20348.84 20751.24 206.80 o -15 0 1 8199.68 8300.62 121.72 o -13 0 1 24328.93 24528.51 189.59 o -11 0 1 30912.29 31066.69 194.32 o -9 0 1 21106.83 21932.66 146.18 o -5 0 1 9088.52 10828.26 167.09 o -3 0 1 5235.66 4180.79 36.91 o 1 0 1 19780.08 19778.14 66.04 o 7 0 1 32350.81 34158.29 526.27 o 9 0 1 45791.38 44997.89 215.35 o 11 0 1 23389.27 23465.21 172.68 o 13 0 1 9815.33 10369.66 126.68 o 15 0 1 18790.72 18622.51 184.57 o 17 0 1 128.25 103.94 32.17 o 19 0 1 5824.12 5948.84 125.32 o 21 0 1 97.47 136.85 42.21 o 23 0 1 163.01 128.48 49.09 o 25 0 1 240.42 232.43 50.02 o -25 1 1 1644.26 1356.47 81.84 o -24 1 1 2291.14 2177.21 91.71 o -23 1 1 66.95 25.29 51.32 o -22 1 1 2599.76 2799.92 98.97 o -21 1 1 3002.21 2944.25 105.68 o -20 1 1 1854.29 1785.01 84.27 o -19 1 1 396.02 296.78 50.39 o -18 1 1 2511.00 2549.71 80.75 o -17 1 1 3.98 -33.47 33.47 o -16 1 1 3501.17 3605.56 87.85 o -15 1 1 1405.54 1326.09 55.99 o -14 1 1 1156.55 1172.75 49.29 o -13 1 1 3343.64 3203.83 71.30 o -12 1 1 138.16 116.96 23.80 o -11 1 1 17.75 29.01 21.38 o -10 1 1 3735.67 3488.86 64.63 o -9 1 1 7894.73 8274.79 91.83 o -8 1 1 8910.91 9205.75 91.18 o -7 1 1 7607.33 9526.95 86.86 o -6 1 1 14790.60 13322.16 230.03 o -5 1 1 7206.55 6414.40 110.55 o -4 1 1 25332.69 26384.63 113.57 o -3 1 1 83788.92 88710.17 565.10 o -2 1 1 50944.10 52793.54 391.47 o 0 1 1 71277.06 71019.55 645.46 o 1 1 1 37721.05 45650.05 381.14 o 2 1 1 71941.98 70229.70 489.69 o 3 1 1 6284.81 5168.67 48.32 o 4 1 1 27065.90 26664.63 119.37 o 5 1 1 12360.54 11181.49 184.57 o 6 1 1 9789.10 8860.13 58.75 o 7 1 1 3340.43 3239.68 53.28 o 8 1 1 2843.13 2941.46 54.93 o 9 1 1 833.88 1288.66 40.92 o 10 1 1 0.98 -14.50 19.89 o 11 1 1 9191.06 9736.19 113.46 o 12 1 1 128.31 111.57 26.78 o 13 1 1 6398.92 6845.88 104.35 o 14 1 1 3174.51 2941.31 75.94 o 15 1 1 345.37 248.25 44.26 o 16 1 1 6206.80 6177.66 113.44 o 18 1 1 4942.50 4515.98 119.71 o 21 1 1 12.45 -82.37 82.37 o 22 1 1 3070.70 2744.38 118.71 o 23 1 1 3263.61 2872.26 128.20 o 24 1 1 2246.96 1890.15 102.13 o 25 1 1 288.29 35.70 65.64 o -25 2 1 2.70 72.89 38.12 o -24 2 1 8.64 15.99 39.05 o -23 2 1 195.40 230.38 48.34 o -22 2 1 159.05 205.65 45.00 o -21 2 1 10.91 -8.92 41.09 o -20 2 1 848.66 747.23 62.86 o -19 2 1 3100.10 3248.14 95.46 o -18 2 1 3855.00 3974.75 99.20 o -17 2 1 93.68 35.33 36.26 o -16 2 1 5357.81 5545.16 108.19 o -15 2 1 7138.92 7405.39 120.18 o -14 2 1 9123.73 9215.30 126.62 o -13 2 1 4638.09 5111.33 92.18 o -12 2 1 12461.59 12137.19 132.79 o -11 2 1 2671.62 3125.25 67.56 o -10 2 1 25759.84 25741.79 175.92 o -9 2 1 13568.32 13586.89 122.73 o -8 2 1 25481.01 28689.96 168.54 o -7 2 1 2644.53 3267.94 55.86 o -6 2 1 13122.95 15513.49 110.97 o -5 2 1 2395.57 2499.05 25.05 o -4 2 1 6467.88 5583.17 87.32 o -3 2 1 19.04 85.58 11.82 o -2 2 1 3.70 2.89 8.39 o -1 2 1 606.44 485.60 20.28 o 0 2 1 723.43 485.68 16.05 o 1 2 1 1684.77 1852.58 36.88 o 2 2 1 1865.82 999.97 19.52 o 3 2 1 54907.23 56382.34 455.24 o 4 2 1 26579.12 24887.81 153.61 o 6 2 1 24890.12 23860.22 141.74 o 7 2 1 11532.67 11532.53 104.22 o 8 2 1 21209.49 21991.99 150.87 o 9 2 1 700.60 661.95 32.92 o 10 2 1 14712.92 14411.87 135.44 o 11 2 1 4394.20 4420.95 80.83 o 12 2 1 9928.39 9951.00 122.96 o 13 2 1 5716.87 5796.01 101.15 o 14 2 1 5370.87 5479.40 101.32 o 15 2 1 21.47 -12.27 30.31 o 16 2 1 3311.93 3580.14 91.56 o 17 2 1 7964.64 7914.77 138.63 o 18 2 1 1605.48 1232.50 93.56 o 19 2 1 130.74 -53.18 53.18 o 20 2 1 420.83 417.46 51.51 o 21 2 1 130.12 129.23 46.30 o 22 2 1 85.46 -26.22 48.53 o 23 2 1 40.94 -32.35 39.98 o 24 2 1 266.23 212.90 51.88 o 25 2 1 459.77 424.52 58.02 o -24 3 1 0.87 -46.48 46.48 o -23 3 1 5956.51 5942.86 133.11 o -22 3 1 172.28 19.34 57.64 o -21 3 1 3284.83 3177.72 105.32 o -20 3 1 17.62 -19.34 42.58 o -19 3 1 4938.07 4987.86 118.40 o -18 3 1 4.14 -19.52 39.60 o -17 3 1 3201.62 3200.38 87.09 o -16 3 1 0.27 -14.32 30.68 o -15 3 1 83.57 116.40 30.12 o -14 3 1 0.24 19.15 23.61 o -13 3 1 2340.77 2237.54 64.20 o -12 3 1 946.87 952.84 45.38 o -11 3 1 7910.78 9004.14 115.80 o -10 3 1 246.12 262.00 27.15 o -9 3 1 326.90 401.30 28.08 o -8 3 1 0.24 10.23 17.48 o -7 3 1 18133.63 19409.87 142.37 o -6 3 1 7.70 8.74 17.29 o -5 3 1 46861.07 48902.77 209.79 o -4 3 1 19.68 28.08 14.87 o -3 3 1 27148.72 30553.80 154.64 o -2 3 1 7567.59 7271.44 48.11 o -1 3 1 13546.56 13118.74 151.19 o 0 3 1 1963.54 1942.50 36.05 o 2 3 1 269.26 265.77 15.52 o 3 3 1 36922.78 40268.89 182.80 o 4 3 1 137.40 122.54 19.15 o 5 3 1 17156.99 16887.20 125.97 o 6 3 1 38.07 43.70 19.52 o 7 3 1 1596.77 1484.52 42.61 o 8 3 1 1001.81 1150.14 41.30 o 9 3 1 4874.65 4728.90 79.74 o 10 3 1 942.27 984.50 42.78 o 11 3 1 8920.00 9578.81 120.50 o 12 3 1 505.71 526.47 37.19 o 13 3 1 297.29 297.34 32.54 o 14 3 1 49.91 88.69 29.19 o 15 3 1 3700.47 3997.35 92.69 o 16 3 1 33.56 29.38 32.72 o 17 3 1 4405.25 4554.28 104.06 o 18 3 1 7.59 -18.04 37.37 o 19 3 1 2999.37 3141.75 97.13 o 20 3 1 64.84 67.87 39.79 o 21 3 1 9460.93 9703.01 177.20 o 22 3 1 11.27 -53.92 53.92 o 23 3 1 482.12 491.66 51.32 o 24 3 1 125.26 32.91 47.60 o -24 4 1 0.10 13.20 39.98 o -23 4 1 108.49 93.71 47.60 o -22 4 1 437.29 398.31 53.93 o -21 4 1 155.26 60.24 50.58 o -20 4 1 696.23 639.90 61.18 o -19 4 1 1634.75 1888.32 80.35 o -18 4 1 2928.75 3213.00 96.94 o -17 4 1 557.07 601.58 49.84 o -16 4 1 7058.88 7251.58 130.58 o -15 4 1 5701.28 5908.44 116.21 o -14 4 1 7517.98 7557.01 124.47 o -13 4 1 514.53 575.74 42.77 o -12 4 1 13112.98 13604.93 153.29 o -11 4 1 40.15 75.68 27.89 o -10 4 1 10632.60 11282.91 131.40 o -9 4 1 12830.32 13475.07 138.82 o -8 4 1 10040.44 10303.39 117.43 o -7 4 1 1573.91 1437.67 46.14 o -6 4 1 11624.93 10587.73 111.59 o -5 4 1 256.24 273.91 24.36 o -4 4 1 3526.13 3010.97 58.67 o -3 4 1 506.44 493.78 28.46 o -2 4 1 652.19 819.33 33.48 o -1 4 1 5.78 7.81 17.11 o 1 4 1 2221.33 1902.03 49.15 o 3 4 1 2376.64 2303.42 52.13 o 4 4 1 5383.54 5411.64 78.68 o 5 4 1 83.22 113.98 21.01 o 6 4 1 24212.05 23830.47 170.47 o 7 4 1 13641.60 14353.45 136.70 o 8 4 1 18428.69 19000.97 161.45 o 9 4 1 771.40 743.39 42.96 o 10 4 1 17817.95 18854.11 171.95 o 11 4 1 1693.27 1693.70 58.97 o 12 4 1 13249.23 13353.07 155.35 o 13 4 1 3273.69 3378.03 85.61 o 14 4 1 10085.74 10154.60 145.26 o 15 4 1 772.86 622.64 53.75 o 16 4 1 4629.12 4429.49 106.30 o 17 4 1 3828.63 3854.96 102.55 o 18 4 1 1617.37 1632.39 75.33 o 19 4 1 119.03 94.27 42.02 o 20 4 1 600.37 630.77 55.97 o 21 4 1 75.77 89.25 44.81 o 22 4 1 4.61 0.56 40.72 o 23 4 1 22.49 -30.31 45.74 o -23 5 1 201.30 37.75 55.60 o -22 5 1 2906.09 2818.79 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