#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:58:21 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180933 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/13/2201334.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201334_Fobs loop_ _publ_author_name 'Kang, Yao' 'Li, Zhao-Ji' 'Qin, Ye-Yan' 'Chen, Yu-Biao' 'Hu, Rui-Feng' 'Wen, Yi-Hang' 'Cheng, Jian-Kai' 'Yao, Yuan-Gen' _publ_section_title ; A trinuclear molybdenum cluster coordinated by N-phenylanthranilate ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m420 _journal_page_last m422 _journal_volume 58 _journal_year 2002 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 74.787 _cell_angle_beta 76.232 _cell_angle_gamma 80.688 _cell_length_a 12.4661 _cell_length_b 14.1240 _cell_length_c 14.8507 _exptl_crystal_F_000 1264.00 _reflns_d_resolution_high 0.8389 _cod_data_source_file cf6191Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 364.60 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 88266.46 42208.71 20351.79 o 2 0 0 11308.94 11219.90 433.76 o 3 0 0 16604.44 16325.31 1032.13 o 4 0 0 1923.78 2145.14 90.33 o 5 0 0 2120.39 2005.17 60.82 o 6 0 0 7512.19 7203.43 518.55 o 7 0 0 6.15 3.37 11.93 o 8 0 0 712.30 645.78 82.29 o 9 0 0 39.95 17.17 30.82 o 10 0 0 456.11 433.04 26.29 o 11 0 0 357.94 339.80 26.39 o 12 0 0 106.22 94.91 22.75 o 13 0 0 231.91 267.02 46.94 o 14 0 0 104.28 121.95 44.20 o -14 1 0 97.42 32.61 38.55 o -13 1 0 189.20 204.24 47.69 o -12 1 0 367.74 329.42 31.86 o -11 1 0 6.23 2.34 17.77 o -10 1 0 203.50 216.92 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5902.06 87.93 o 2 3 0 760.75 638.84 43.46 o 3 3 0 2522.21 2586.14 136.34 o 4 3 0 5629.77 5743.25 95.30 o 5 3 0 21929.90 22317.81 329.16 o 6 3 0 2141.34 2189.96 55.03 o 7 3 0 8.22 3.48 11.02 o 8 3 0 1253.18 1136.49 26.65 o 9 3 0 433.01 449.64 24.86 o 10 3 0 382.96 341.25 23.83 o 11 3 0 202.45 95.25 37.56 o 12 3 0 34.72 39.77 32.61 o 13 3 0 496.56 537.82 56.66 o 14 3 0 443.59 366.50 49.02 o -13 4 0 1.34 -26.43 26.43 o -12 4 0 710.55 792.99 72.93 o -11 4 0 253.82 279.02 56.18 o -10 4 0 246.25 148.54 64.42 o -9 4 0 57.46 118.83 25.82 o -8 4 0 734.96 681.33 114.11 o -7 4 0 24.36 57.43 12.03 o -6 4 0 9222.35 9991.50 833.87 o -5 4 0 834.53 870.48 98.17 o -4 4 0 933.46 1027.50 90.51 o -3 4 0 9073.75 9664.83 206.42 o -2 4 0 1152.47 1080.74 53.81 o -1 4 0 366.04 581.42 14.06 o 0 4 0 41.40 93.24 10.37 o 1 4 0 1668.38 1444.41 31.58 o 2 4 0 6190.08 7106.20 473.02 o 3 4 0 31748.92 33383.96 487.16 o 4 4 0 22564.88 21864.30 1094.18 o 5 4 0 0.60 -8.61 8.61 o 6 4 0 440.23 367.39 21.31 o 7 4 0 49.36 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o -4 7 0 170.07 170.22 11.12 o -3 7 0 0.30 -6.12 6.12 o -2 7 0 7073.50 7478.12 115.20 o -1 7 0 13687.86 13853.65 255.09 o 0 7 0 7837.93 7874.77 149.29 o 1 7 0 3448.21 3715.55 75.90 o 2 7 0 1632.69 1481.33 36.53 o 3 7 0 5008.39 5371.73 527.01 o 4 7 0 8941.82 9124.12 723.79 o 5 7 0 4236.35 4239.61 145.65 o 6 7 0 359.04 372.30 16.63 o 7 7 0 215.25 201.82 14.36 o 8 7 0 12.91 7.10 16.09 o 9 7 0 15.36 -20.24 22.54 o 10 7 0 988.79 930.39 107.57 o 11 7 0 894.12 816.13 41.59 o 12 7 0 378.55 361.50 41.10 o 13 7 0 69.62 173.12 40.52 o -11 8 0 182.18 149.72 25.20 o -10 8 0 98.38 101.58 21.09 o -9 8 0 2174.44 2275.68 61.97 o -8 8 0 2460.79 2703.67 67.44 o -7 8 0 53.86 37.17 14.22 o -6 8 0 298.93 234.96 19.63 o -5 8 0 3.20 -9.13 9.13 o -4 8 0 1813.29 1797.68 79.22 o -3 8 0 21040.41 22280.33 330.42 o -2 8 0 21278.80 22024.09 389.86 o -1 8 0 677.50 644.31 23.99 o 0 8 0 140.38 148.44 13.52 o 1 8 0 10.92 0.24 17.39 o 2 8 0 0.53 11.17 9.08 o 3 8 0 98.81 94.44 26.58 o 4 8 0 237.96 270.89 37.75 o 5 8 0 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