#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2201349.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201349_Fobs loop_ _publ_author_name 'Batsanov, Andrei S.' 'Bryce, Martin R.' 'Lyubchik, Svetlana B.' 'Perepichka, Igor F.' _publ_section_title ; An unexpected TTFAQ donor--fluorene acceptor reaction resulting in a novel salt: 2,6-dihexyloxy-9,10-bis(4,5-dimethyl-1,3-dithiol-2-ylium)-anthracene bis(2,5,7-trinitro-4-bromo-9-cyanofluorenide) dioxane trisolvate ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1106 _journal_page_last o1110 _journal_volume 58 _journal_year 2002 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 77.920 _cell_angle_beta 78.490 _cell_angle_gamma 60.260 _cell_length_a 14.1360 _cell_length_b 14.2440 _cell_length_c 22.3830 _exptl_crystal_F_000 1764.00 _reflns_d_resolution_high 0.7316 _[local]_cod_data_source_file cf6206Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 01srv059 noabs in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 600.87 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 12783.90 394.54 29.32 o 2 0 0 17410.62 19249.50 705.57 o 3 0 0 253.49 131.47 80.35 o 4 0 0 1724.43 2037.68 68.42 o 5 0 0 929.10 979.82 47.73 o 6 0 0 653.06 413.61 31.56 o 7 0 0 2720.68 2547.96 160.09 o 8 0 0 1832.04 1919.07 83.46 o 9 0 0 4567.78 4213.46 212.41 o 10 0 0 42.08 55.09 35.82 o 11 0 0 1422.56 1195.89 127.43 o 12 0 0 637.98 615.81 99.70 o 13 0 0 1114.02 1262.54 138.09 o 14 0 0 52.48 78.38 73.58 o 15 0 0 2448.89 2743.67 235.13 o 16 0 0 433.91 630.20 116.23 o -16 1 0 77.28 3.73 83.71 o -15 1 0 25.58 91.17 81.04 o -14 1 0 130.16 81.04 76.78 o -13 1 0 2083.07 2233.43 196.21 o -12 1 0 778.49 737.90 108.77 o -11 1 0 200.09 215.40 71.44 o -10 1 0 2812.88 2948.40 158.87 o -9 1 0 3664.29 3601.00 271.38 o -8 1 0 4757.15 4053.93 161.70 o -7 1 0 2673.15 3104.10 125.64 o -6 1 0 2397.62 2101.46 88.00 o -5 1 0 874.41 616.89 83.32 o -4 1 0 5231.71 5241.63 200.41 o -3 1 0 167653.27 184062.95 6843.39 o -2 1 0 34713.63 31171.48 960.60 o -1 1 0 4186.83 4879.81 151.87 o 0 1 0 8356.64 181.10 12.37 o 1 1 0 10088.75 1704.48 351.89 o 2 1 0 13113.99 12266.25 834.37 o 3 1 0 62566.55 70085.32 2464.14 o 4 1 0 369.93 574.70 146.62 o 5 1 0 6681.10 6849.23 246.84 o 6 1 0 74.81 71.16 34.62 o 7 1 0 3301.59 3233.11 124.34 o 8 1 0 6650.73 6561.34 240.00 o 9 1 0 1375.33 1389.06 67.72 o 10 1 0 77.66 6.22 34.04 o 11 1 0 32.11 23.98 36.14 o 12 1 0 44.94 -0.47 37.95 o 13 1 0 314.81 405.74 85.31 o 14 1 0 458.34 460.66 91.70 o 15 1 0 662.28 769.89 122.63 o 16 1 0 120.07 154.08 84.24 o 17 1 0 100.53 192.47 92.24 o -15 2 0 467.09 650.46 117.30 o -14 2 0 1830.35 2240.36 203.14 o -13 2 0 1986.04 2356.59 206.34 o -12 2 0 137.58 187.14 78.91 o -11 2 0 456.10 443.06 84.77 o -10 2 0 276.25 108.23 67.71 o -9 2 0 298.08 174.04 40.53 o -8 2 0 1069.00 1247.72 112.23 o -7 2 0 2376.50 1736.27 78.82 o -6 2 0 6649.79 6653.50 255.41 o -5 2 0 319.40 251.59 22.76 o -4 2 0 271.36 13.09 32.52 o -3 2 0 4942.77 4913.54 154.44 o -2 2 0 361049.28 391357.31 12028.08 o -1 2 0 27593.53 23424.28 1368.10 o 0 2 0 9579.98 10253.87 642.05 o 1 2 0 20702.25 16015.48 599.63 o 2 2 0 1722.65 1966.40 109.69 o 3 2 0 20460.79 19928.45 607.97 o 4 2 0 204.25 299.25 28.81 o 5 2 0 72.51 128.64 18.20 o 6 2 0 15962.04 17286.64 613.64 o 7 2 0 2205.26 2457.52 285.98 o 8 2 0 6078.97 6402.00 234.05 o 9 2 0 104.90 105.74 26.78 o 10 2 0 1311.31 1198.32 64.52 o 11 2 0 570.37 594.49 49.12 o 12 2 0 52.09 3.45 38.91 o 13 2 0 198.53 121.88 46.85 o 14 2 0 467.75 266.79 54.88 o 15 2 0 333.80 336.96 90.11 o 16 2 0 280.84 196.74 84.77 o 17 2 0 1445.78 1642.15 177.01 o -14 3 0 69.27 11.73 76.78 o -13 3 0 243.69 256.99 89.57 o -12 3 0 181.57 -14.93 69.31 o -11 3 0 443.39 505.44 94.90 o -10 3 0 238.73 87.44 65.05 o -9 3 0 277.42 316.70 76.24 o -8 3 0 146.51 29.86 54.92 o -7 3 0 2766.91 2407.70 102.82 o -6 3 0 4433.86 4064.89 160.87 o -5 3 0 31486.63 36211.16 1352.79 o -4 3 0 710.84 497.42 36.20 o -3 3 0 11526.94 12776.88 452.10 o -2 3 0 2068.39 1556.47 77.83 o -1 3 0 139646.33 147691.67 6728.78 o 0 3 0 2147.62 1845.64 90.12 o 1 3 0 66930.63 70147.32 2617.06 o 2 3 0 20538.85 18313.84 825.66 o 3 3 0 4372.93 4891.01 173.13 o 4 3 0 1123.87 1276.79 47.17 o 5 3 0 616.09 918.91 37.63 o 6 3 0 964.97 1163.26 53.90 o 7 3 0 8323.58 9592.04 345.05 o 8 3 0 8806.67 8623.26 310.83 o 9 3 0 4812.85 4469.62 273.56 o 10 3 0 2152.13 2060.36 89.25 o 11 3 0 126.24 180.80 34.66 o 12 3 0 17.55 12.09 31.69 o 13 3 0 139.56 143.94 37.05 o 14 3 0 29.25 4.20 43.73 o 15 3 0 13.49 20.80 45.47 o 16 3 0 288.05 123.69 81.04 o 17 3 0 2368.50 2486.15 223.40 o -14 4 0 201.82 256.99 93.84 o -13 4 0 1659.95 1836.22 183.94 o -12 4 0 841.23 1033.28 132.76 o -11 4 0 472.47 599.28 104.50 o -10 4 0 18.91 13.86 65.05 o -9 4 0 193.27 149.82 69.31 o -8 4 0 2725.49 2253.16 189.27 o -7 4 0 189.02 299.40 41.06 o -6 4 0 637.11 684.23 46.03 o -5 4 0 6184.43 4920.86 192.53 o -4 4 0 56943.98 63773.97 2374.03 o -3 4 0 1882.69 1712.47 59.25 o -2 4 0 2351.84 2553.01 128.42 o -1 4 0 1554.51 1371.54 285.24 o 0 4 0 236.91 128.82 22.82 o 1 4 0 3050.82 2757.94 107.60 o 2 4 0 693.91 755.42 37.94 o 3 4 0 1648.87 1528.94 78.73 o 4 4 0 31378.43 36866.10 1278.79 o 5 4 0 2184.55 3086.75 100.51 o 6 4 0 3114.46 3804.70 122.48 o 7 4 0 1820.38 2917.58 197.15 o 8 4 0 2274.43 3953.98 285.01 o 9 4 0 3473.92 3909.09 246.96 o 10 4 0 1371.48 1308.16 66.96 o 11 4 0 1754.02 1771.37 82.58 o 12 4 0 2748.20 2679.99 113.84 o 13 4 0 471.90 554.86 58.65 o 14 4 0 134.42 123.88 39.68 o 15 4 0 286.54 157.96 42.16 o 16 4 0 215.75 137.27 53.88 o 17 4 0 1315.48 1515.79 163.68 o 18 4 0 4.41 -38.39 84.77 o -13 5 0 308.99 478.25 110.37 o -12 5 0 90.66 114.63 81.57 o -11 5 0 27.62 84.77 78.38 o -10 5 0 529.93 296.44 83.71 o -9 5 0 1343.12 1480.07 153.02 o -8 5 0 438.10 544.36 93.84 o -7 5 0 8120.43 9383.52 444.78 o -6 5 0 155.69 152.20 37.02 o -5 5 0 6712.05 6396.79 306.00 o -4 5 0 9990.99 9515.38 446.68 o -3 5 0 22996.81 23773.62 1095.20 o -2 5 0 121.29 79.01 26.20 o -1 5 0 4332.52 4901.39 233.16 o 0 5 0 270.66 203.06 18.67 o 1 5 0 3665.86 3484.84 135.68 o 2 5 0 156.21 92.16 15.65 o 3 5 0 2240.11 2656.30 128.53 o 4 5 0 12018.31 11399.29 517.87 o 5 5 0 13491.44 15875.15 553.48 o 6 5 0 26.33 23.30 16.49 o 7 5 0 2159.42 3848.95 124.82 o 8 5 0 773.02 1263.88 96.45 o 9 5 0 4280.89 4612.50 173.26 o 10 5 0 1957.62 1756.25 80.27 o 11 5 0 5277.20 4889.59 184.94 o 12 5 0 4553.20 4335.11 168.57 o 13 5 0 99.09 111.33 36.98 o 14 5 0 79.18 73.56 36.52 o 15 5 0 1466.70 1533.25 83.89 o 16 5 0 235.02 183.11 46.18 o 17 5 0 18.58 14.78 56.25 o 18 5 0 1650.37 1723.19 180.21 o -12 6 0 35.12 -29.86 75.71 o -11 6 0 1639.81 2247.83 206.87 o -10 6 0 241.10 467.59 94.90 o -9 6 0 798.89 786.42 117.30 o -8 6 0 445.02 511.84 90.64 o -7 6 0 82.30 -18.67 37.40 o -6 6 0 12025.07 12633.81 592.30 o -5 6 0 178.35 162.69 37.66 o -4 6 0 154.13 120.47 34.19 o -3 6 0 5022.57 4398.81 216.15 o -2 6 0 4983.65 4802.49 232.58 o -1 6 0 1972.45 1731.91 95.75 o 0 6 0 2454.38 2676.68 107.88 o 1 6 0 228.95 198.50 21.28 o 2 6 0 4973.93 3369.04 282.31 o 3 6 0 225.74 178.63 44.36 o 4 6 0 362.53 596.58 47.68 o 5 6 0 83.18 62.98 27.72 o 6 6 0 9331.01 11937.49 419.35 o 7 6 0 474.45 616.01 39.31 o 8 6 0 81.03 94.64 32.99 o 9 6 0 2879.62 3285.42 110.25 o 10 6 0 5828.02 5485.52 205.83 o 11 6 0 1279.09 1374.23 75.21 o 12 6 0 2793.24 3112.57 143.90 o 13 6 0 135.89 163.90 37.24 o 14 6 0 168.52 238.75 41.99 o 15 6 0 1154.80 1243.30 75.47 o 16 6 0 952.40 1018.67 72.05 o 17 6 0 270.64 70.00 48.29 o 18 6 0 196.09 283.85 52.46 o -12 7 0 487.25 757.63 124.76 o -11 7 0 972.02 1143.64 148.75 o -10 7 0 436.54 579.55 106.63 o -9 7 0 2101.76 1943.39 187.14 o -8 7 0 45.03 50.12 67.18 o -7 7 0 968.44 1106.88 134.36 o -6 7 0 688.03 803.62 74.75 o -5 7 0 5451.51 5520.45 271.78 o -4 7 0 76.78 55.77 35.13 o -3 7 0 4665.31 4771.77 234.79 o -2 7 0 5009.24 4628.85 226.57 o -1 7 0 500.11 171.64 70.91 o 0 7 0 485.62 177.97 34.53 o 1 7 0 2283.99 2038.08 86.26 o 2 7 0 8001.73 7990.66 303.74 o 3 7 0 3718.87 4269.04 201.69 o 4 7 0 15017.79 14873.15 559.01 o 5 7 0 18334.10 20389.94 922.71 o 6 7 0 1609.01 1681.76 71.72 o 7 7 0 235.54 248.62 40.63 o 8 7 0 153.12 174.21 23.68 o 9 7 0 2456.93 2610.30 102.55 o 10 7 0 4680.01 5022.44 223.85 o 11 7 0 1951.67 2261.14 114.99 o 12 7 0 5052.98 4788.03 184.73 o 13 7 0 843.19 887.22 61.85 o 14 7 0 383.75 529.49 51.51 o 15 7 0 143.06 162.56 40.91 o 16 7 0 2037.48 1918.42 110.32 o 17 7 0 1143.29 1056.28 75.75 o 18 7 0 21.84 -21.08 45.22 o -11 8 0 1688.74 1859.68 191.94 o -10 8 0 217.30 346.02 97.04 o -9 8 0 1053.61 1329.72 155.15 o -8 8 0 11177.34 10819.54 757.63 o -7 8 0 197.15 340.78 56.33 o -6 8 0 52.17 -7.84 43.45 o -5 8 0 1078.60 1276.49 91.59 o -4 8 0 8272.61 9179.55 437.17 o -3 8 0 1227.12 1322.87 88.59 o -2 8 0 126.94 -26.35 32.79 o -1 8 0 6778.63 6569.44 314.73 o 0 8 0 299.03 182.27 48.25 o 1 8 0 1025.42 541.96 62.90 o 2 8 0 4621.50 4702.41 183.99 o 3 8 0 2164.74 1736.47 310.14 o 4 8 0 18727.74 20344.66 760.80 o 5 8 0 6574.34 6730.30 258.45 o 6 8 0 144.57 128.43 30.64 o 7 8 0 663.69 740.61 46.29 o 8 8 0 1142.49 1019.66 54.88 o 9 8 0 621.73 666.50 45.34 o 10 8 0 34.00 21.85 22.75 o 11 8 0 256.20 313.05 46.25 o 12 8 0 2162.03 2506.36 129.40 o 13 8 0 774.57 767.75 72.25 o 14 8 0 279.00 295.71 53.52 o 15 8 0 16.30 17.58 36.84 o 16 8 0 399.90 417.32 50.88 o 17 8 0 14.01 81.98 56.63 o 18 8 0 207.02 253.52 65.21 o -10 9 0 2021.36 2232.90 212.20 o -9 9 0 821.76 1062.60 142.36 o -8 9 0 379.69 527.30 102.37 o -7 9 0 2708.52 2644.50 223.93 o -6 9 0 230.20 91.94 49.58 o -5 9 0 159.52 38.49 45.05 o -4 9 0 1366.94 1465.75 100.45 o -3 9 0 107.17 49.39 41.27 o -2 9 0 901.33 847.04 73.96 o -1 9 0 3189.40 3014.44 159.46 o 0 9 0 4841.33 4330.74 233.53 o 1 9 0 541.55 472.82 50.88 o 2 9 0 62.00 41.29 24.07 o 3 9 0 6154.32 6445.02 248.63 o 4 9 0 11759.03 11812.56 447.11 o 5 9 0 7287.08 7225.40 277.85 o 6 9 0 8198.62 8058.96 308.59 o 7 9 0 2620.20 2915.81 148.07 o 8 9 0 234.04 331.76 31.79 o 9 9 0 2758.01 2975.05 117.36 o 10 9 0 1041.50 1011.88 56.60 o 11 9 0 1782.14 2310.08 120.64 o 12 9 0 149.15 219.85 45.53 o 13 9 0 599.91 662.19 64.06 o 14 9 0 119.13 150.69 51.15 o 15 9 0 1866.93 1737.48 224.46 o 16 9 0 144.38 136.06 52.82 o 17 9 0 180.85 172.48 58.45 o 18 9 0 433.49 500.23 73.00 o -9 10 0 1089.28 1413.42 164.22 o -8 10 0 223.98 390.28 102.37 o -7 10 0 410.75 579.02 104.50 o -6 10 0 157.57 124.80 51.84 o -5 10 0 2228.11 2395.21 143.96 o -4 10 0 149.00 174.63 51.63 o -3 10 0 1945.70 2257.48 132.51 o -2 10 0 1966.54 2175.72 127.80 o -1 10 0 765.85 541.44 60.89 o 0 10 0 34.10 81.39 38.56 o 1 10 0 539.32 664.70 60.13 o 2 10 0 2491.11 2488.84 134.14 o 3 10 0 309.44 105.87 25.88 o 4 10 0 1059.26 981.94 55.41 o 5 10 0 414.50 335.52 59.48 o 6 10 0 3448.95 3555.37 144.98 o 7 10 0 4541.64 4558.22 181.56 o 8 10 0 98.17 114.01 28.85 o 9 10 0 459.63 482.24 39.17 o 10 10 0 6304.07 6447.12 236.08 o 11 10 0 1034.87 1022.11 76.58 o 12 10 0 453.30 450.32 54.91 o 13 10 0 2007.39 1806.60 106.35 o 14 10 0 950.96 1040.12 132.23 o 15 10 0 742.52 715.23 74.68 o 16 10 0 246.66 245.35 59.95 o 17 10 0 102.47 181.96 56.63 o 18 10 0 46.68 -4.96 55.72 o -8 11 0 2066.42 2306.48 221.80 o -7 11 0 690.20 769.89 120.50 o -6 11 0 359.08 301.54 64.27 o -5 11 0 163.02 200.44 56.16 o -4 11 0 449.75 535.81 68.23 o -3 11 0 368.60 482.96 63.14 o -2 11 0 323.00 316.63 54.05 o -1 11 0 38.42 -5.33 41.13 o 0 11 0 3518.32 3549.15 186.04 o 1 11 0 228.03 213.04 53.58 o 2 11 0 733.88 749.45 83.97 o 3 11 0 71.13 40.02 55.98 o 4 11 0 2451.25 2210.11 98.00 o 5 11 0 2224.45 1969.09 90.76 o 6 11 0 1922.42 1866.75 88.06 o 7 11 0 2471.35 2531.58 110.08 o 8 11 0 717.46 676.61 50.62 o 9 11 0 8698.62 8071.38 292.26 o 10 11 0 410.08 464.62 40.93 o 11 11 0 10.95 19.31 40.22 o 12 11 0 120.29 197.10 47.00 o 13 11 0 995.88 976.07 76.78 o 14 11 0 606.22 630.64 70.11 o 15 11 0 63.34 50.27 49.43 o 16 11 0 1638.08 1443.94 101.73 o 17 11 0 2355.97 2126.64 126.88 o 18 11 0 6.82 -22.58 54.66 o -7 12 0 176.57 291.11 99.70 o -6 12 0 59.38 136.49 85.84 o -5 12 0 27.87 -30.60 50.96 o -4 12 0 137.58 109.16 55.98 o -3 12 0 1440.00 1746.42 119.27 o -2 12 0 55.57 14.32 48.28 o -1 12 0 1452.80 1498.46 105.27 o 0 12 0 821.05 1015.61 84.56 o 1 12 0 391.36 399.40 55.01 o 2 12 0 454.73 515.68 57.47 o 3 12 0 41.75 -19.68 36.38 o 4 12 0 353.32 114.53 38.50 o 5 12 0 971.91 777.35 68.92 o 6 12 0 5941.35 5868.86 282.19 o 7 12 0 610.53 397.00 149.82 o 8 12 0 6099.98 5978.98 287.41 o 9 12 0 1091.57 995.35 69.73 o 10 12 0 178.38 251.36 36.40 o 11 12 0 21.02 -3.62 41.12 o 12 12 0 3695.95 3508.59 170.74 o 13 12 0 535.87 555.99 60.92 o 14 12 0 93.33 43.39 48.03 o 15 12 0 1564.41 1355.13 116.50 o 16 12 0 238.94 335.12 61.72 o 17 12 0 1412.18 1214.75 96.45 o 18 12 0 235.51 291.03 74.91 o -6 13 0 40.22 77.31 79.97 o -5 13 0 440.17 455.81 72.56 o -4 13 0 786.57 846.05 88.77 o -3 13 0 275.66 416.34 67.46 o -2 13 0 232.41 -34.20 49.87 o -1 13 0 751.45 632.28 76.14 o 0 13 0 192.25 29.21 47.68 o 1 13 0 107.03 66.74 46.10 o 2 13 0 179.21 148.22 80.51 o 3 13 0 253.10 266.05 82.11 o 4 13 0 322.02 219.13 79.44 o 5 13 0 303.95 400.94 85.31 o 6 13 0 454.33 456.92 82.64 o 7 13 0 1481.64 1343.48 92.05 o 8 13 0 1528.02 1690.45 104.79 o 9 13 0 69.20 14.35 46.12 o 10 13 0 266.76 334.48 57.35 o 11 13 0 498.65 591.54 49.29 o 12 13 0 72.89 53.38 47.58 o 13 13 0 652.48 639.90 69.63 o 14 13 0 1064.15 923.52 82.11 o 15 13 0 1653.68 1586.75 104.93 o 16 13 0 276.63 422.09 90.90 o 17 13 0 129.12 164.85 61.94 o 18 13 0 31.11 37.85 74.11 o -4 14 0 83.66 58.12 84.24 o -3 14 0 547.48 704.31 121.03 o -2 14 0 337.27 162.08 93.30 o -1 14 0 979.65 1294.53 150.89 o 0 14 0 16.84 -39.45 76.24 o 1 14 0 1421.98 1549.91 163.68 o 2 14 0 2460.97 2856.70 233.53 o 3 14 0 153.47 152.49 82.64 o 4 14 0 364.63 491.05 98.10 o 5 14 0 681.30 621.67 98.64 o 6 14 0 93.51 55.45 70.91 o 7 14 0 159.29 194.07 75.71 o 8 14 0 155.32 157.82 69.84 o 9 14 0 153.64 137.76 48.07 o 10 14 0 1662.12 1736.53 87.00 o 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421.73 86.91 o -7 -14 3 332.26 377.48 84.77 o -6 -14 3 1242.00 1175.10 134.89 o -5 -14 3 514.41 549.16 99.17 o -4 -14 3 2051.59 2023.90 185.54 o -3 -14 3 241.00 319.37 90.64 o -2 -14 3 237.81 204.20 89.04 o -1 -14 3 118.45 142.89 89.04 o 0 -14 3 141.90 181.89 58.90 o 1 -14 3 79.57 80.94 55.70 o 2 -14 3 400.26 599.92 76.63 o 3 -14 3 419.28 486.09 74.25 o 4 -14 3 99.53 142.42 66.30 o -17 -13 3 57.29 28.38 79.97 o -16 -13 3 273.98 271.36 62.47 o -15 -13 3 321.81 386.90 63.32 o -14 -13 3 76.35 87.90 52.78 o -13 -13 3 115.88 94.42 68.25 o -12 -13 3 382.50 649.00 67.10 o -11 -13 3 3039.70 2952.82 150.30 o -10 -13 3 67.61 121.63 36.93 o -9 -13 3 200.87 165.50 38.50 o -8 -13 3 204.70 240.09 70.11 o -7 -13 3 1729.48 1633.09 152.49 o -6 -13 3 4464.36 4684.40 332.16 o -5 -13 3 421.22 215.96 47.51 o -4 -13 3 244.56 101.00 44.55 o -3 -13 3 215.25 -13.70 41.61 o -2 -13 3 1007.04 816.78 79.28 o -1 -13 3 1017.10 1142.55 112.76 o 0 -13 3 1045.95 939.10 87.60 o 1 -13 3 889.95 959.62 89.95 o 2 -13 3 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129.83 o -16 -11 3 530.91 631.18 73.26 o -15 -11 3 72.33 47.40 51.61 o -14 -11 3 187.53 184.67 71.44 o -13 -11 3 882.66 996.79 78.01 o -12 -11 3 359.17 541.79 58.98 o -11 -11 3 181.06 174.04 44.70 o -10 -11 3 1656.08 2211.03 96.11 o -9 -11 3 2402.69 2583.87 108.17 o -8 -11 3 1453.34 1820.05 83.28 o -7 -11 3 525.56 529.61 45.83 o -6 -11 3 3125.09 2932.42 125.58 o -5 -11 3 3494.43 3194.67 134.98 o -4 -11 3 1897.10 1922.76 112.57 o -3 -11 3 2895.87 2659.34 145.32 o -2 -11 3 743.44 748.84 71.58 o -1 -11 3 1856.49 1353.03 363.09 o 0 -11 3 246.53 78.66 59.18 o 1 -11 3 32.50 -14.56 43.48 o 2 -11 3 107.75 122.27 49.37 o 3 -11 3 103.04 37.58 47.84 o 4 -11 3 495.62 757.22 78.95 o 5 -11 3 1343.26 1519.81 113.88 o 6 -11 3 258.94 412.09 66.73 o 7 -11 3 49.78 21.33 82.11 o 8 -11 3 218.99 175.94 91.70 o -18 -10 3 796.81 705.03 83.54 o -17 -10 3 2203.14 2278.34 131.87 o -16 -10 3 812.96 739.18 84.24 o -15 -10 3 421.64 450.57 62.75 o -14 -10 3 132.18 134.13 50.12 o -13 -10 3 428.80 468.80 57.51 o -12 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62.47 o -8 -9 3 4656.04 4279.91 161.40 o -7 -9 3 1822.44 2021.19 85.67 o -6 -9 3 135.98 154.29 34.21 o -5 -9 3 1913.31 1961.38 88.24 o -4 -9 3 574.36 510.48 79.48 o -3 -9 3 10439.10 9474.57 447.58 o -2 -9 3 4172.15 3683.98 181.42 o -1 -9 3 302.51 335.89 59.18 o 0 -9 3 100.27 53.85 48.52 o 1 -9 3 269.39 18.93 67.45 o 2 -9 3 484.89 135.48 44.20 o 3 -9 3 59.37 71.93 41.28 o 4 -9 3 95.51 57.91 54.65 o 5 -9 3 1768.78 1928.37 121.33 o 6 -9 3 93.96 98.24 50.75 o 7 -9 3 111.25 78.29 52.17 o 8 -9 3 2.32 -29.32 75.18 o 9 -9 3 101.43 29.86 81.57 o 10 -9 3 14.28 4.27 77.84 o -18 -8 3 225.97 134.89 79.97 o -17 -8 3 130.17 14.27 53.98 o -16 -8 3 1199.98 1083.45 89.34 o -15 -8 3 1576.18 1595.32 102.46 o -14 -8 3 2904.28 2595.46 136.78 o -13 -8 3 385.24 400.96 54.69 o -12 -8 3 244.09 250.74 45.85 o -11 -8 3 5200.62 4895.20 221.49 o -10 -8 3 350.20 410.26 61.05 o -9 -8 3 1213.38 1532.81 74.91 o -8 -8 3 6145.22 6274.62 226.33 o -7 -8 3 2212.77 3433.87 131.18 o -6 -8 3 90.67 134.20 31.05 o -5 -8 3 988.14 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