#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/13/2201350.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201350_Fobs loop_ _publ_author_name 'Sun, Yan-Qiong' 'Zhang, Jie' 'Yang, Guo-Yu' _publ_section_title ; Hexaaquazinc(II) dihydrogen-1,2,4,5-benzenetetracarboxylate ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m548 _journal_page_last m550 _journal_volume 58 _journal_year 2002 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.562 _cell_angle_gamma 90.000 _cell_length_a 21.9723 _cell_length_b 9.7717 _cell_length_c 7.3036 _exptl_crystal_F_000 872.00 _reflns_d_resolution_high 0.8390 _[local]_cod_data_source_file cf6207Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' CF6207 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 295.03 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 502.32 421.10 10.91 o 4 0 0 10583.71 9067.86 227.17 o 6 0 0 17234.92 14568.98 365.06 o 8 0 0 1533.40 1388.80 36.21 o 10 0 0 17337.60 18106.95 454.34 o 12 0 0 19276.55 19454.57 488.56 o 14 0 0 20722.98 20975.80 526.75 o 16 0 0 923.41 946.86 26.29 o 18 0 0 7377.62 8156.21 207.33 o 20 0 0 7244.65 7757.92 197.41 o 22 0 0 3715.69 3729.91 97.22 o 24 0 0 461.53 529.73 17.36 o 1 1 0 1966.51 1850.83 50.56 o 3 1 0 2136.98 2132.99 188.48 o 5 1 0 7950.98 7906.91 259.66 o 7 1 0 769.67 676.33 12.63 o 9 1 0 3385.19 3402.36 228.16 o 11 1 0 2779.87 3463.78 62.25 o 13 1 0 2106.20 2399.61 44.01 o 15 1 0 4603.57 5315.96 95.92 o 17 1 0 363.49 310.05 9.67 o 19 1 0 232.84 209.09 11.41 o 21 1 0 1068.83 1063.64 21.39 o 23 1 0 14.77 38.90 3.72 o 25 1 0 15.61 -3.47 3.47 o 0 2 0 80.91 52.45 4.22 o 2 2 0 17064.58 15171.51 219.25 o 4 2 0 12192.80 12974.64 187.66 o 6 2 0 4331.24 4148.89 222.46 o 8 2 0 873.10 1000.57 19.34 o 10 2 0 5045.60 4656.62 83.44 o 12 2 0 1683.59 1385.76 33.73 o 14 2 0 1638.19 1753.65 32.61 o 16 2 0 7759.78 8549.87 153.04 o 18 2 0 1060.64 1148.43 22.62 o 20 2 0 35.30 25.31 5.21 o 22 2 0 1743.21 1996.40 54.56 o 24 2 0 1092.45 1066.40 31.25 o 1 3 0 13566.85 12350.28 154.88 o 3 3 0 11962.49 12157.72 175.96 o 5 3 0 22.95 48.77 14.77 o 7 3 0 933.21 1200.19 17.94 o 9 3 0 1972.93 1642.97 65.97 o 11 3 0 855.13 705.50 24.06 o 13 3 0 6844.97 6459.19 115.71 o 15 3 0 62.93 42.39 3.97 o 17 3 0 5858.66 6133.65 110.65 o 19 3 0 665.31 726.14 21.82 o 21 3 0 624.72 545.10 17.36 o 23 3 0 1313.31 1518.25 42.66 o 0 4 0 1277.55 1066.13 46.62 o 2 4 0 9177.81 9791.27 122.91 o 4 4 0 2856.14 3235.36 53.32 o 6 4 0 9994.42 10895.84 157.88 o 8 4 0 37.18 22.09 2.98 o 10 4 0 29.21 30.87 2.98 o 12 4 0 1817.64 1715.24 31.74 o 14 4 0 1126.53 1098.64 29.76 o 16 4 0 3057.84 3083.13 80.35 o 18 4 0 1949.31 1973.08 53.07 o 20 4 0 2468.61 2489.92 65.97 o 22 4 0 6.46 4.96 3.97 o 1 5 0 52344.15 43853.33 548.77 o 3 5 0 2469.20 2274.70 62.57 o 5 5 0 5848.35 6280.05 125.04 o 7 5 0 8393.86 8483.03 123.26 o 9 5 0 550.26 497.17 32.24 o 11 5 0 18148.44 17240.93 433.50 o 13 5 0 4834.42 4738.78 121.02 o 15 5 0 8205.46 7387.91 187.49 o 17 5 0 1698.91 1854.54 50.10 o 19 5 0 4054.84 3987.34 103.66 o 21 5 0 3923.92 3950.14 103.17 o 0 6 0 332.93 304.95 19.84 o 2 6 0 225.88 276.74 5.80 o 4 6 0 1020.43 1061.13 20.90 o 6 6 0 512.83 513.14 18.35 o 8 6 0 97.79 87.56 2.81 o 10 6 0 403.92 434.84 18.60 o 12 6 0 1013.93 945.37 25.79 o 14 6 0 3502.95 3114.87 80.35 o 16 6 0 376.46 319.42 11.41 o 18 6 0 57.67 58.53 5.46 o 20 6 0 1058.85 1135.84 32.74 o 1 7 0 563.86 562.03 11.12 o 3 7 0 7788.40 7999.87 116.90 o 5 7 0 930.67 934.58 14.98 o 7 7 0 90.49 79.67 2.65 o 9 7 0 193.77 222.60 16.12 o 11 7 0 2636.77 2391.00 134.17 o 13 7 0 218.47 221.71 7.94 o 15 7 0 4586.87 4437.70 114.58 o 17 7 0 734.51 768.80 23.31 o 19 7 0 67.81 87.79 6.94 o 0 8 0 20.37 30.26 2.98 o 2 8 0 13495.79 13971.13 249.54 o 4 8 0 48.08 41.65 4.56 o 6 8 0 176.17 228.60 4.89 o 8 8 0 644.18 608.21 26.92 o 10 8 0 501.47 518.57 11.75 o 12 8 0 3157.64 2658.56 69.44 o 14 8 0 17.51 14.88 3.47 o 16 8 0 1422.54 1481.55 41.17 o 18 8 0 1253.46 1310.93 37.20 o 1 9 0 2575.92 2520.55 47.15 o 3 9 0 462.81 441.36 28.27 o 5 9 0 1358.65 1408.20 37.20 o 7 9 0 10.40 32.01 3.16 o 9 9 0 1601.32 1541.06 33.21 o 11 9 0 161.66 167.87 14.88 o 13 9 0 1226.55 1179.26 24.06 o 15 9 0 379.03 380.98 10.24 o 0 10 0 7370.16 7171.16 183.52 o 2 10 0 3221.96 2997.79 55.94 o 4 10 0 1317.21 1273.20 25.43 o 6 10 0 2359.13 2391.34 53.57 o 8 10 0 1224.44 1135.21 61.75 o 10 10 0 890.69 875.44 27.28 o 12 10 0 3285.57 3245.32 87.30 o 1 11 0 84.42 91.80 13.89 o 3 11 0 43.83 32.00 7.94 o 5 11 0 6.40 9.54 2.97 o 7 11 0 193.59 189.68 6.48 o -25 1 1 1828.23 1985.48 54.56 o -23 1 1 426.07 478.03 11.39 o -21 1 1 17.42 29.65 12.90 o -19 1 1 6102.25 6741.87 121.34 o -17 1 1 4571.95 5234.43 121.77 o -15 1 1 12613.53 13478.42 240.00 o -13 1 1 17504.48 18368.00 326.17 o -11 1 1 1615.27 1372.11 79.86 o -9 1 1 7682.55 7876.85 140.11 o -7 1 1 1398.93 1593.66 28.76 o -5 1 1 6106.49 6046.94 107.29 o -3 1 1 23222.60 21942.22 388.43 o -1 1 1 8740.48 8266.42 119.67 o 1 1 1 29529.63 23629.75 341.39 o 3 1 1 15570.91 13981.78 247.76 o 5 1 1 15325.91 14106.43 298.10 o 7 1 1 12182.03 10929.79 194.24 o 9 1 1 6875.19 5884.76 127.97 o 11 1 1 7472.71 7497.07 133.97 o 13 1 1 3140.14 3007.48 54.89 o 15 1 1 875.35 903.02 17.89 o 17 1 1 3453.49 3673.10 67.16 o 19 1 1 2076.10 2233.88 41.90 o 21 1 1 3720.89 4006.12 155.00 o 23 1 1 5155.02 5457.42 99.76 o -24 2 1 131.16 129.46 7.94 o -22 2 1 275.61 319.92 12.40 o -20 2 1 664.86 717.72 27.03 o -18 2 1 152.81 160.82 8.68 o -16 2 1 3215.72 3472.58 72.42 o -14 2 1 2878.80 2925.47 160.46 o -12 2 1 1810.52 2219.95 40.68 o -10 2 1 6340.32 5960.98 126.73 o -8 2 1 5982.98 6772.40 120.43 o -6 2 1 1063.01 1127.15 20.52 o -4 2 1 1491.70 1640.80 65.48 o -2 2 1 3517.64 3682.28 63.83 o 0 2 1 5276.80 5380.00 78.03 o 2 2 1 25.19 49.80 11.66 o 4 2 1 611.05 555.09 10.07 o 6 2 1 49.77 41.54 5.95 o 8 2 1 12994.81 12043.21 503.44 o 10 2 1 126.77 152.86 9.67 o 12 2 1 69.96 82.70 10.17 o 14 2 1 670.36 610.67 32.74 o 16 2 1 810.48 674.39 18.10 o 18 2 1 4118.27 3985.03 97.71 o 20 2 1 712.62 813.36 17.01 o 22 2 1 460.66 429.94 10.34 o -25 3 1 136.17 163.18 9.42 o -23 3 1 218.34 259.90 11.41 o -21 3 1 1318.29 1354.57 37.70 o -19 3 1 10.14 19.34 3.47 o -17 3 1 395.84 365.06 11.90 o -15 3 1 4380.53 4344.40 78.36 o -13 3 1 2839.51 3075.76 55.77 o -11 3 1 3469.71 3536.32 63.65 o -9 3 1 1016.46 1019.23 27.03 o -7 3 1 2998.06 3517.51 122.55 o -5 3 1 473.35 532.35 14.14 o -3 3 1 21405.66 20182.88 313.15 o -1 3 1 2332.22 2526.62 37.01 o 1 3 1 4016.71 4231.56 53.41 o 3 3 1 67.41 61.29 2.72 o 5 3 1 1342.31 1704.47 41.10 o 7 3 1 15966.19 16267.23 288.82 o 9 3 1 3847.88 3595.05 64.86 o 11 3 1 381.30 351.22 32.24 o 13 3 1 650.66 576.36 14.38 o 15 3 1 146.28 138.02 4.37 o 17 3 1 621.20 699.28 29.76 o 19 3 1 2961.63 2753.29 72.42 o 21 3 1 390.12 471.70 15.38 o 23 3 1 217.34 190.46 8.93 o -24 4 1 1162.97 1175.02 34.22 o -22 4 1 32.34 36.21 5.46 o -20 4 1 1198.05 1107.57 31.25 o -18 4 1 6600.95 6000.60 153.26 o -16 4 1 7653.25 7817.94 198.40 o -14 4 1 10806.52 10753.26 271.31 o -12 4 1 6621.36 7280.77 184.51 o -10 4 1 2495.39 2282.26 41.39 o -8 4 1 6084.21 5879.63 85.58 o -6 4 1 10758.80 11366.64 202.18 o -4 4 1 7031.58 6887.80 122.90 o -2 4 1 10161.99 9828.92 123.36 o 0 4 1 12223.41 11917.72 149.58 o 2 4 1 21904.56 21708.42 272.00 o 4 4 1 22384.66 21906.78 274.56 o 6 4 1 7714.87 7600.42 110.53 o 8 4 1 6519.63 6686.07 97.44 o 10 4 1 5472.08 5854.48 105.02 o 12 4 1 4970.26 4761.17 107.63 o 14 4 1 2241.26 2141.96 39.81 o 16 4 1 2222.49 2249.85 59.52 o 18 4 1 1773.76 1837.18 49.60 o 20 4 1 1594.39 1459.73 40.18 o 22 4 1 6227.58 6384.01 164.18 o -23 5 1 337.33 367.04 13.89 o -21 5 1 11.96 1.49 2.98 o -19 5 1 81.32 69.44 4.96 o -17 5 1 136.84 118.05 5.95 o -15 5 1 25.07 18.85 2.98 o -13 5 1 500.18 466.24 14.38 o -11 5 1 7.28 6.94 1.98 o -9 5 1 130.30 144.94 3.97 o -7 5 1 643.38 699.89 17.86 o -5 5 1 1188.73 1304.52 47.37 o -3 5 1 76.85 79.94 3.60 o -1 5 1 463.13 472.00 25.72 o 1 5 1 20.57 36.69 1.21 o 3 5 1 452.50 562.24 7.74 o 5 5 1 794.08 933.30 13.53 o 7 5 1 9.02 17.60 3.22 o 9 5 1 29.43 40.34 9.51 o 11 5 1 71.76 80.85 4.96 o 13 5 1 565.43 510.88 15.38 o 15 5 1 39.38 41.17 3.97 o 17 5 1 52.94 69.94 5.46 o 19 5 1 79.19 78.86 5.95 o 21 5 1 7.38 47.62 4.46 o -22 6 1 506.79 523.28 17.86 o -20 6 1 834.84 733.58 22.32 o -18 6 1 1780.66 1604.06 43.65 o -16 6 1 2403.00 2472.56 64.98 o -14 6 1 8522.28 8325.84 211.30 o -12 6 1 3498.44 3581.61 92.26 o -10 6 1 572.69 551.42 11.39 o -8 6 1 3645.89 3852.92 69.79 o -6 6 1 281.13 229.69 5.58 o -4 6 1 4795.16 4903.73 88.03 o -2 6 1 10421.79 10238.51 128.86 o 0 6 1 4560.25 4871.40 135.86 o 2 6 1 3459.83 3627.86 57.85 o 4 6 1 1240.50 1206.01 18.18 o 6 6 1 9595.48 9767.51 142.27 o 8 6 1 2181.33 2242.11 75.71 o 10 6 1 4523.11 4685.25 84.35 o 12 6 1 3875.43 4123.74 106.14 o 14 6 1 18.63 13.39 3.47 o 16 6 1 1814.61 1595.63 43.15 o 18 6 1 1300.06 1341.18 37.70 o 20 6 1 2925.77 2892.17 76.38 o -19 7 1 52.24 50.10 4.96 o -17 7 1 1624.47 1611.01 44.14 o -15 7 1 431.17 376.96 12.40 o -13 7 1 279.61 298.10 10.42 o -11 7 1 3037.71 2933.82 53.81 o -9 7 1 16.78 24.51 1.91 o -7 7 1 405.79 406.88 8.94 o -5 7 1 605.50 607.33 38.44 o -3 7 1 75.15 96.24 9.01 o -1 7 1 56.11 60.06 2.18 o 1 7 1 2095.10 2230.67 37.73 o 3 7 1 1572.99 1629.36 24.80 o 5 7 1 93.13 100.65 3.40 o 7 7 1 1023.19 1023.38 20.14 o 9 7 1 798.51 830.17 33.64 o 11 7 1 64.46 52.76 13.39 o 13 7 1 40.12 58.32 7.44 o 15 7 1 578.01 564.94 17.36 o 17 7 1 19.60 35.71 4.46 o 19 7 1 497.10 429.54 14.88 o -18 8 1 727.86 704.32 21.82 o -16 8 1 693.72 670.09 20.34 o -14 8 1 979.70 931.98 26.78 o -12 8 1 982.64 956.81 28.52 o -10 8 1 1150.50 1113.49 21.74 o -8 8 1 86.58 115.72 15.13 o -6 8 1 8.85 2.69 1.44 o -4 8 1 9121.17 9277.62 135.62 o -2 8 1 1111.15 1125.68 22.27 o 0 8 1 459.64 484.11 10.69 o 2 8 1 4381.81 4485.77 109.12 o 4 8 1 950.81 900.17 18.06 o 6 8 1 779.45 776.53 25.32 o 8 8 1 5038.67 5167.15 76.43 o 10 8 1 741.55 742.63 15.53 o 12 8 1 551.34 495.28 11.36 o 14 8 1 428.98 396.45 9.80 o 16 8 1 135.54 126.71 5.43 o -15 9 1 3564.41 3370.81 87.79 o -13 9 1 3368.30 3132.93 57.84 o -11 9 1 1185.89 1105.29 21.90 o -9 9 1 922.20 987.80 16.38 o -7 9 1 6739.85 6612.74 119.75 o -5 9 1 763.35 819.31 17.36 o -3 9 1 1492.30 1530.46 29.81 o -1 9 1 7001.35 6798.78 122.93 o 1 9 1 1517.77 1487.62 28.75 o 3 9 1 5606.29 5802.45 105.39 o 5 9 1 6868.10 6513.14 117.82 o 7 9 1 1397.48 1429.12 73.41 o 9 9 1 1201.74 1165.60 33.73 o 11 9 1 3191.34 3146.15 79.11 o 13 9 1 1319.78 1432.54 28.38 o -12 10 1 638.66 667.67 20.58 o -10 10 1 23.91 3.40 15.38 o -8 10 1 270.34 247.58 7.53 o -6 10 1 626.77 638.18 39.43 o -4 10 1 22.41 27.98 6.20 o -2 10 1 83.91 74.81 3.81 o 0 10 1 23.29 24.37 5.95 o 2 10 1 401.10 387.50 9.45 o 4 10 1 180.06 175.75 18.85 o 6 10 1 38.38 38.19 4.46 o 8 10 1 81.26 79.86 5.95 o 10 10 1 120.51 123.50 6.94 o -7 11 1 109.55 116.70 6.70 o -5 11 1 1424.01 1466.70 29.46 o -3 11 1 1190.49 1155.63 28.27 o -1 11 1 2166.33 2105.33 106.64 o 1 11 1 783.83 754.23 18.60 o 3 11 1 279.74 267.19 18.60 o 5 11 1 736.25 689.93 21.82 o -26 0 2 2113.30 2414.52 65.47 o -24 0 2 1185.81 1361.52 38.69 o -22 0 2 2985.03 2989.88 78.37 o -20 0 2 2863.17 2816.78 73.41 o -18 0 2 1377.51 1365.98 36.70 o -16 0 2 7494.40 8274.26 209.31 o -14 0 2 21200.72 22467.27 563.95 o -12 0 2 9122.46 9623.87 242.54 o -10 0 2 12930.29 13268.47 333.31 o -8 0 2 13328.17 13331.96 334.80 o -6 0 2 87042.91 69729.05 1744.93 o -4 0 2 2616.69 2381.79 60.51 o -2 0 2 66260.02 51968.31 1300.51 o 0 0 2 3189.33 3549.37 89.78 o 2 0 2 2900.82 3037.55 127.72 o 4 0 2 70630.79 53575.71 947.95 o 6 0 2 17997.52 14966.32 265.32 o 8 0 2 65454.20 56929.79 1425.50 o 10 0 2 4456.41 3902.03 99.70 o 12 0 2 637.71 639.34 18.35 o 14 0 2 1875.91 1964.65 52.08 o 16 0 2 9439.27 8985.02 228.16 o 18 0 2 1289.96 1463.20 40.18 o 20 0 2 4748.73 4783.91 124.00 o 22 0 2 2760.06 2816.78 74.90 o -25 1 2 29.32 47.12 6.45 o -23 1 2 15.03 18.72 2.97 o -21 1 2 16.90 13.91 3.97 o -19 1 2 4271.93 4675.17 167.65 o -17 1 2 11.64 19.60 5.21 o -15 1 2 94.66 107.58 5.21 o -13 1 2 50.97 35.71 10.17 o -11 1 2 7237.29 7516.68 133.97 o -9 1 2 155.78 244.66 31.00 o -7 1 2 6380.85 6420.82 93.45 o -5 1 2 20099.07 20714.68 367.03 o -3 1 2 49492.57 43393.61 767.91 o -1 1 2 10779.02 11724.74 228.51 o 1 1 2 7843.43 7950.00 115.39 o 3 1 2 166.45 156.99 6.60 o 5 1 2 124.71 186.11 4.24 o 7 1 2 7194.13 7308.57 106.39 o 9 1 2 646.81 567.56 33.48 o 11 1 2 11.21 61.64 38.44 o 13 1 2 2641.10 2815.52 51.73 o 15 1 2 84.59 77.84 13.14 o 17 1 2 896.89 873.50 45.88 o 19 1 2 593.13 629.41 13.85 o 21 1 2 1288.81 1350.18 68.20 o -24 2 2 982.89 899.74 26.29 o -22 2 2 319.27 346.21 11.90 o -20 2 2 57.51 50.10 4.46 o -18 2 2 6270.49 6746.91 121.16 o -16 2 2 914.86 916.94 17.69 o -14 2 2 78.38 63.55 2.26 o -12 2 2 2627.30 3080.49 86.06 o -10 2 2 2055.26 2124.51 38.56 o -8 2 2 12141.10 12397.87 220.06 o -6 2 2 2897.53 2812.53 50.50 o -4 2 2 405.84 354.33 9.16 o -2 2 2 267.84 272.86 4.48 o 0 2 2 1697.68 1879.24 38.44 o 2 2 2 1364.21 1275.36 19.18 o 4 2 2 5251.48 5188.23 84.19 o 6 2 2 8367.31 8296.19 120.79 o 8 2 2 5103.70 4864.63 142.43 o 10 2 2 1694.31 1585.65 29.63 o 12 2 2 2591.57 2512.64 130.94 o 14 2 2 14.92 41.56 14.63 o 16 2 2 14.14 18.22 14.38 o 18 2 2 2007.43 2003.06 54.81 o 20 2 2 1783.96 1882.03 41.66 o 22 2 2 568.51 623.81 18.60 o -25 3 2 79.24 94.24 6.94 o -23 3 2 3126.68 3119.83 82.34 o -21 3 2 263.76 225.18 8.93 o -19 3 2 1521.96 1575.29 42.66 o -17 3 2 536.74 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407.71 14.38 o -2 6 7 667.65 629.92 20.34 o 0 6 7 40.60 11.41 4.96 o -16 0 8 14.58 54.56 5.46 o -14 0 8 994.21 1063.92 31.25 o -12 0 8 956.89 926.53 27.28 o -10 0 8 2682.47 2829.68 75.39 o -8 0 8 808.69 973.65 28.77 o -6 0 8 1560.41 1658.62 46.62 o -4 0 8 1873.39 2077.74 57.04 o -2 0 8 312.01 397.79 14.88 o 0 0 8 253.92 269.33 11.41 o 2 0 8 1532.44 1474.61 42.66 o -15 1 8 8.11 19.17 3.16 o -13 1 8 209.81 214.55 15.38 o -11 1 8 127.73 147.64 6.45 o -9 1 8 270.90 276.84 7.72 o -7 1 8 292.25 289.81 9.18 o -5 1 8 2.98 26.63 12.65 o -3 1 8 82.24 88.86 5.08 o -1 1 8 195.58 164.17 6.13 o 1 1 8 2.23 16.41 6.94 o 3 1 8 400.96 401.34 10.69 o -14 2 8 211.91 229.15 9.92 o -12 2 8 513.16 521.79 17.36 o -10 2 8 510.49 568.57 12.98 o -8 2 8 1019.20 1052.40 21.74 o -6 2 8 861.12 961.74 36.21 o -4 2 8 70.44 47.19 8.68 o -2 2 8 426.12 427.64 11.21 o 0 2 8 929.44 978.99 21.04 o 2 2 8 9.35 3.06 2.97 o -13 3 8 50.99 86.30 6.45 o -11 3 8 1145.04 1039.61 30.75 o -9 3 8 320.91 337.78 12.40 o -7 3 8 889.22 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