#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:58:21 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180933 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/13/2201393.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201393_Fobs loop_ _publ_author_name 'Yadav, Bishwa Nath' 'Prasad, Shambhu' 'Prasad, Satya Murti' _publ_section_title ; 2-(2-Nitrophenyl)-4,5-benz-1,3-oxazin-6-one ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1111 _journal_page_last o1112 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.260 _cell_angle_gamma 90.000 _cell_length_a 4.1824 _cell_length_b 22.1910 _cell_length_c 12.7670 _exptl_crystal_F_000 552.00 _reflns_d_resolution_high 0.8323 _cod_data_source_file ci6155Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ; 2-(2'-Nitrophenyl)-4,5-benz-1,3-oxazin-6-one, C14 H8 N2 O4 ; _shelx_refln_list_code 4 _shelx_f_calc_maximum 154.22 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y+1/2, z+1/2' '-x, -y, -z' '-x, y-1/2, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 245.49 232.72 3.60 o 3 0 0 238.74 228.81 5.04 o 4 0 0 73.19 65.07 2.36 o 5 0 0 0.00 0.16 1.40 o 1 1 0 1581.46 1494.42 6.07 o 2 1 0 701.99 654.56 6.05 o 3 1 0 46.47 53.51 1.90 o 4 1 0 18.53 24.48 1.73 o 5 1 0 20.49 18.41 1.29 o 0 2 0 229.46 180.65 1.21 o 1 2 0 5923.79 5767.32 62.18 o 2 2 0 7.74 7.71 0.86 o 3 2 0 89.65 92.44 2.81 o 4 2 0 13.39 15.98 1.65 o 5 2 0 11.59 9.64 1.21 o 1 3 0 656.79 702.53 4.33 o 2 3 0 122.51 120.07 2.94 o 3 3 0 25.55 24.76 1.66 o 4 3 0 1.49 0.00 1.47 o 0 4 0 3593.67 3260.71 38.08 o 1 4 0 6895.91 6935.30 73.93 o 2 4 0 1459.51 1430.71 9.29 o 3 4 0 5.55 6.62 2.07 o 4 4 0 11.38 14.52 1.70 o 1 5 0 4328.50 4347.44 60.49 o 2 5 0 548.80 557.28 5.96 o 3 5 0 0.04 1.12 1.58 o 4 5 0 2.47 0.59 1.99 o 0 6 0 4342.99 4048.00 52.30 o 1 6 0 914.46 915.21 5.69 o 2 6 0 56.45 61.26 1.78 o 3 6 0 0.00 4.91 1.96 o 4 6 0 4.03 4.04 2.02 o 1 7 0 186.79 205.12 3.03 o 2 7 0 43.57 61.06 1.78 o 3 7 0 81.20 78.55 2.45 o 4 7 0 2.63 2.60 2.01 o 0 8 0 98.68 89.41 1.84 o 1 8 0 2508.92 2486.80 10.70 o 2 8 0 58.04 56.65 1.65 o 3 8 0 6.68 6.37 2.32 o 4 8 0 8.11 9.51 1.68 o 1 9 0 30.46 26.79 0.97 o 2 9 0 26.82 30.79 1.58 o 3 9 0 56.82 53.75 2.32 o 4 9 0 1.36 2.01 1.90 o 0 10 0 202.45 188.01 3.01 o 1 10 0 10.34 9.17 0.79 o 2 10 0 25.05 17.27 1.42 o 3 10 0 2.32 2.89 2.02 o 4 10 0 5.62 4.93 2.25 o 1 11 0 81.50 93.78 2.67 o 2 11 0 46.36 52.74 1.83 o 3 11 0 91.60 96.70 2.95 o 4 11 0 107.98 117.89 3.44 o 0 12 0 1.79 1.89 0.90 o 1 12 0 195.43 220.13 4.10 o 2 12 0 44.31 41.60 1.78 o 3 12 0 19.69 21.45 1.73 o 4 12 0 5.34 8.00 1.42 o 1 13 0 151.63 150.15 3.68 o 2 13 0 0.37 0.00 0.63 o 3 13 0 13.41 11.73 1.67 o 4 13 0 2.74 0.89 1.46 o 0 14 0 8.56 5.00 0.82 o 1 14 0 238.49 255.12 4.93 o 2 14 0 117.98 121.81 3.59 o 3 14 0 7.80 8.52 1.44 o 4 14 0 8.26 8.92 1.53 o 1 15 0 4.47 6.29 1.12 o 2 15 0 29.93 31.42 1.91 o 3 15 0 30.08 24.60 1.81 o 4 15 0 2.49 4.23 1.55 o 0 16 0 3.78 2.29 1.30 o 1 16 0 38.14 34.98 1.68 o 2 16 0 139.29 141.28 4.15 o 3 16 0 6.29 6.85 2.10 o 4 16 0 5.66 6.01 1.21 o 1 17 0 11.97 13.43 1.40 o 2 17 0 62.47 63.44 2.33 o 3 17 0 4.65 4.95 2.06 o 0 18 0 215.02 223.24 5.22 o 1 18 0 35.12 32.38 1.80 o 2 18 0 337.33 335.71 6.70 o 3 18 0 2.73 6.37 1.84 o 1 19 0 11.11 8.95 1.41 o 2 19 0 58.42 56.22 2.13 o 3 19 0 106.83 110.26 3.16 o 0 20 0 110.55 112.48 3.10 o 1 20 0 1.86 2.43 1.53 o 2 20 0 128.31 130.11 3.71 o 3 20 0 94.15 86.16 2.64 o 1 21 0 0.33 5.07 1.48 o 2 21 0 16.63 16.54 1.55 o 3 21 0 0.02 0.00 0.41 o 0 22 0 579.74 593.43 8.52 o 1 22 0 183.31 208.27 5.28 o 2 22 0 46.82 44.59 1.90 o 1 23 0 319.10 330.52 6.06 o 2 23 0 3.07 3.75 1.40 o 0 24 0 6.30 7.11 1.26 o 1 24 0 85.68 85.32 2.40 o 2 24 0 2.21 2.10 1.20 o 1 25 0 58.72 57.32 1.91 o 0 26 0 0.13 1.04 1.03 o 1 26 0 137.10 129.72 3.05 o -5 1 1 0.01 0.83 1.06 o -4 1 1 103.77 105.77 3.34 o -3 1 1 36.43 36.92 1.78 o -2 1 1 64.45 55.26 1.63 o -1 1 1 2444.80 2471.18 7.88 o 0 1 1 283.69 234.44 2.57 o 1 1 1 1342.34 1313.14 5.67 o 2 1 1 73.57 72.56 2.01 o 3 1 1 118.85 107.05 3.19 o 4 1 1 16.87 22.20 1.76 o -5 2 1 1.37 0.71 1.04 o -4 2 1 66.41 66.05 2.38 o -3 2 1 437.40 453.08 6.93 o -2 2 1 497.87 446.44 5.16 o -1 2 1 6300.71 6104.20 65.43 o 0 2 1 4262.64 4288.69 28.68 o 1 2 1 4415.02 4336.32 55.28 o 2 2 1 737.69 668.10 6.32 o 3 2 1 52.63 45.63 1.92 o 4 2 1 9.38 11.68 1.61 o -4 3 1 39.64 55.84 2.18 o -3 3 1 354.55 365.37 6.37 o -2 3 1 76.05 70.64 1.98 o -1 3 1 2718.76 2695.79 8.66 o 0 3 1 3227.93 2953.77 23.86 o 1 3 1 14.15 0.00 0.10 o 2 3 1 5.26 5.43 0.89 o 3 3 1 167.46 173.17 4.60 o 4 3 1 34.86 33.13 1.96 o -4 4 1 0.62 2.15 1.93 o -3 4 1 1.93 3.22 1.79 o -2 4 1 1955.36 1954.99 10.89 o -1 4 1 9781.38 9720.89 91.02 o 0 4 1 270.24 247.74 1.67 o 1 4 1 378.36 356.20 3.38 o 2 4 1 1090.46 1116.68 8.19 o 3 4 1 195.62 215.87 5.25 o 4 4 1 23.40 19.36 1.86 o -4 5 1 1.30 1.06 1.73 o -3 5 1 90.85 93.77 2.83 o -2 5 1 1761.16 1732.18 10.24 o -1 5 1 77.15 80.63 1.82 o 0 5 1 510.82 492.11 2.31 o 1 5 1 639.39 648.42 4.99 o 2 5 1 7.10 7.96 0.94 o 3 5 1 19.36 12.47 1.55 o 4 5 1 5.77 4.32 2.19 o -4 6 1 0.70 2.78 1.88 o -3 6 1 87.04 89.33 2.69 o -2 6 1 573.07 599.22 6.38 o -1 6 1 617.76 585.58 4.74 o 0 6 1 1741.60 1554.01 8.30 o 1 6 1 1534.14 1493.96 7.62 o 2 6 1 117.15 131.15 3.26 o 3 6 1 65.68 63.31 2.26 o 4 6 1 29.92 25.50 1.89 o -4 7 1 0.91 0.90 1.60 o -3 7 1 0.99 4.32 2.02 o -2 7 1 805.88 850.95 7.61 o -1 7 1 342.23 339.27 3.75 o 0 7 1 728.06 681.28 3.32 o 1 7 1 1540.14 1529.40 8.02 o 2 7 1 666.06 677.23 7.00 o 3 7 1 67.22 67.38 2.33 o 4 7 1 0.02 0.00 2.28 o -4 8 1 0.00 0.00 1.29 o -3 8 1 0.10 0.00 0.62 o -2 8 1 2171.24 2239.42 12.82 o -1 8 1 211.55 227.00 3.31 o 0 8 1 899.18 795.22 13.60 o 1 8 1 193.50 184.23 3.09 o 2 8 1 19.35 19.46 1.18 o 3 8 1 82.76 97.41 2.80 o 4 8 1 14.11 11.76 1.84 o -4 9 1 5.39 0.00 0.33 o -3 9 1 537.96 551.38 8.22 o -2 9 1 119.15 104.64 2.82 o -1 9 1 647.34 627.55 5.72 o 0 9 1 724.59 728.66 3.89 o 1 9 1 187.91 200.52 3.45 o 2 9 1 61.44 60.44 1.64 o 3 9 1 4.93 0.00 1.80 o 4 9 1 36.31 35.55 2.13 o -4 10 1 5.45 5.46 2.16 o -3 10 1 99.97 94.56 2.68 o -2 10 1 47.55 51.16 1.57 o -1 10 1 69.64 77.91 2.01 o 0 10 1 1669.27 1692.39 31.39 o 1 10 1 122.05 138.72 3.06 o 2 10 1 3.58 2.85 1.51 o 3 10 1 52.76 53.75 2.32 o 4 10 1 8.87 8.59 1.59 o -4 11 1 32.57 39.79 2.00 o -3 11 1 0.64 2.49 1.92 o -2 11 1 5.13 6.81 1.14 o -1 11 1 19.06 17.85 0.96 o 0 11 1 278.00 275.78 5.13 o 1 11 1 364.27 392.57 5.16 o 2 11 1 53.93 56.03 1.88 o 3 11 1 2.89 3.81 2.19 o 4 11 1 46.03 46.56 2.16 o -4 12 1 45.00 41.50 1.99 o -3 12 1 61.94 63.37 2.39 o -2 12 1 73.52 75.48 2.26 o -1 12 1 24.33 30.29 1.12 o 0 12 1 0.00 0.14 0.42 o 1 12 1 33.68 35.46 1.26 o 2 12 1 88.31 96.06 2.79 o 3 12 1 35.89 36.33 2.01 o 4 12 1 2.04 0.77 1.43 o -4 13 1 31.83 32.57 1.76 o -3 13 1 0.69 0.00 4.68 o -2 13 1 58.84 56.16 2.01 o -1 13 1 4.29 2.35 1.28 o 0 13 1 0.60 0.07 0.73 o 1 13 1 23.75 29.89 1.24 o 2 13 1 0.38 0.00 0.93 o 3 13 1 3.28 0.00 1.43 o 4 13 1 29.58 26.32 1.79 o -4 14 1 13.08 8.28 1.59 o -3 14 1 16.87 21.98 1.67 o -2 14 1 67.66 68.45 2.22 o -1 14 1 248.57 234.42 4.73 o 0 14 1 249.55 259.54 3.33 o 1 14 1 196.89 205.64 4.43 o 2 14 1 89.09 88.72 2.68 o 3 14 1 3.70 6.41 2.20 o 4 14 1 10.48 11.27 1.47 o -4 15 1 11.59 11.29 1.42 o -3 15 1 0.34 0.00 0.41 o -2 15 1 14.66 15.85 1.58 o -1 15 1 446.19 447.26 6.71 o 0 15 1 11.66 7.74 0.87 o 1 15 1 49.50 58.18 1.80 o 2 15 1 12.78 9.12 1.54 o 3 15 1 4.37 7.48 2.15 o 4 15 1 0.01 0.00 1.54 o -4 16 1 7.89 7.33 1.21 o -3 16 1 12.43 12.15 1.78 o -2 16 1 104.00 101.64 2.95 o -1 16 1 63.41 63.50 2.01 o 0 16 1 181.91 182.19 3.10 o 1 16 1 7.34 9.54 1.23 o 2 16 1 347.28 342.48 6.77 o 3 16 1 61.98 58.25 2.42 o -3 17 1 15.86 20.08 1.64 o -2 17 1 206.23 210.89 5.54 o -1 17 1 66.85 60.56 2.02 o 0 17 1 0.71 0.85 1.05 o 1 17 1 69.55 65.66 2.11 o 2 17 1 27.20 31.33 1.82 o 3 17 1 2.09 3.35 1.86 o -3 18 1 10.19 12.04 1.41 o -2 18 1 31.53 35.41 1.93 o -1 18 1 755.60 776.44 9.76 o 0 18 1 7.04 9.81 0.87 o 1 18 1 23.40 25.41 1.60 o 2 18 1 13.79 13.49 1.61 o 3 18 1 11.15 11.18 1.49 o -3 19 1 18.11 18.20 1.52 o -2 19 1 25.15 30.16 1.78 o -1 19 1 512.08 517.55 8.14 o 0 19 1 0.13 0.66 1.30 o 1 19 1 0.11 2.78 1.54 o 2 19 1 33.11 34.54 1.81 o 3 19 1 42.48 48.75 1.87 o -3 20 1 2.91 3.47 1.53 o -2 20 1 10.38 10.12 1.52 o -1 20 1 183.06 174.57 5.04 o 0 20 1 71.65 73.49 1.67 o 1 20 1 0.91 2.54 1.59 o 2 20 1 6.13 7.20 2.13 o 3 20 1 8.62 10.46 1.47 o -3 21 1 13.04 18.40 1.25 o -2 21 1 40.03 34.07 1.80 o -1 21 1 3.92 3.76 1.75 o 0 21 1 189.11 194.22 4.41 o 1 21 1 97.13 97.98 2.97 o 2 21 1 46.29 44.53 2.06 o 3 21 1 25.44 24.28 1.36 o -2 22 1 28.17 26.11 1.58 o -1 22 1 11.99 12.18 1.42 o 0 22 1 587.45 573.82 5.93 o 1 22 1 0.33 0.22 1.77 o 2 22 1 0.18 0.78 1.21 o -2 23 1 13.69 12.99 1.38 o -1 23 1 1.32 0.00 1.58 o 0 23 1 46.19 47.50 1.40 o 1 23 1 0.93 1.49 1.40 o 2 23 1 3.52 1.03 1.19 o -2 24 1 39.47 38.72 1.62 o -1 24 1 0.00 0.00 0.50 o 0 24 1 60.31 57.90 2.16 o 1 24 1 0.33 2.48 1.32 o 2 24 1 13.59 16.08 1.24 o -1 25 1 2.00 1.71 1.18 o 0 25 1 0.00 1.40 0.80 o 1 25 1 5.48 17.92 1.34 o -1 26 1 9.27 9.07 1.10 o 0 26 1 0.69 1.73 0.78 o 1 26 1 9.75 8.16 1.04 o -5 0 2 2.96 3.73 1.29 o -4 0 2 36.79 43.13 2.03 o -3 0 2 80.15 93.76 2.67 o -2 0 2 680.46 669.34 6.12 o -1 0 2 3.39 2.23 0.81 o 0 0 2 6352.72 6146.17 72.49 o 1 0 2 23784.98 28693.54 167.43 o 2 0 2 752.51 792.92 6.89 o 3 0 2 37.57 35.22 1.73 o 4 0 2 2.26 2.57 1.93 o -5 1 2 14.53 10.81 1.28 o -4 1 2 62.60 62.47 2.31 o -3 1 2 36.88 45.79 1.87 o -2 1 2 51.86 69.33 1.96 o -1 1 2 6742.93 6606.80 70.89 o 0 1 2 2467.11 2352.24 105.30 o 1 1 2 5966.57 6240.27 70.32 o 2 1 2 97.34 98.17 2.66 o 3 1 2 70.33 74.28 2.17 o 4 1 2 17.46 16.47 1.68 o -4 2 2 4.03 4.80 1.80 o -3 2 2 45.71 44.21 1.89 o -2 2 2 41.07 37.03 1.09 o -1 2 2 1551.38 1524.05 6.76 o 0 2 2 3635.37 3327.19 27.56 o 1 2 2 8072.21 8364.30 84.19 o 2 2 2 244.87 256.17 4.03 o 3 2 2 15.91 18.44 1.57 o 4 2 2 1.79 0.00 1.33 o -4 3 2 40.41 39.28 2.04 o -3 3 2 269.50 274.47 5.65 o -2 3 2 529.08 526.72 5.61 o -1 3 2 1063.54 1087.94 5.68 o 0 3 2 598.87 540.82 6.28 o 1 3 2 2279.53 2334.89 8.80 o 2 3 2 381.69 407.85 5.09 o 3 3 2 2.85 6.56 2.10 o 4 3 2 0.88 4.22 2.05 o -4 4 2 17.90 16.80 1.73 o -3 4 2 149.09 163.45 4.47 o -2 4 2 475.95 476.75 5.51 o -1 4 2 2639.41 2680.57 9.46 o 0 4 2 369.88 357.73 4.55 o 1 4 2 2069.93 1962.53 8.41 o 2 4 2 447.19 458.41 5.58 o 3 4 2 1.30 0.00 0.75 o 4 4 2 1.83 0.58 2.03 o -4 5 2 1.57 0.00 2.24 o -3 5 2 24.72 26.78 1.68 o -2 5 2 5.38 7.71 0.88 o -1 5 2 4582.17 4563.03 13.07 o 0 5 2 480.32 432.27 4.07 o 1 5 2 101.27 96.93 2.08 o 2 5 2 846.38 876.66 7.73 o 3 5 2 31.95 32.52 1.90 o 4 5 2 1.88 4.20 2.36 o -4 6 2 0.49 1.85 1.83 o -3 6 2 25.16 26.91 1.77 o -2 6 2 0.67 0.00 1.02 o -1 6 2 1394.19 1364.41 7.27 o 0 6 2 153.46 109.74 1.38 o 1 6 2 2226.46 2308.16 9.91 o 2 6 2 3.98 6.31 1.02 o 3 6 2 28.12 30.03 1.96 o 4 6 2 0.34 1.77 1.94 o -4 7 2 0.01 0.00 4.53 o -3 7 2 109.01 110.00 3.49 o -2 7 2 851.38 886.34 8.01 o -1 7 2 3.94 2.91 0.95 o 0 7 2 15.16 16.72 0.45 o 1 7 2 458.39 501.81 4.74 o 2 7 2 1.63 0.14 2.23 o 3 7 2 67.05 65.53 2.43 o 4 7 2 11.04 29.05 2.06 o -4 8 2 21.51 15.92 1.81 o -3 8 2 236.79 235.34 5.48 o -2 8 2 374.47 386.88 5.60 o -1 8 2 56.08 43.36 1.34 o 0 8 2 308.67 283.77 3.29 o 1 8 2 894.95 916.97 6.92 o 2 8 2 313.09 342.85 5.42 o 3 8 2 0.03 3.38 2.10 o 4 8 2 40.66 34.88 2.30 o -4 9 2 7.25 5.69 2.15 o -3 9 2 303.11 279.11 6.25 o -2 9 2 0.02 0.00 2.98 o -1 9 2 389.87 343.70 4.37 o 0 9 2 144.68 123.40 1.75 o 1 9 2 1283.16 1384.56 8.83 o 2 9 2 38.24 49.83 1.66 o 3 9 2 24.99 25.62 1.93 o 4 9 2 5.80 6.48 2.38 o -4 10 2 38.05 30.03 1.96 o -3 10 2 1.08 3.17 1.89 o -2 10 2 202.37 227.77 4.66 o -1 10 2 100.91 123.44 2.89 o 0 10 2 489.20 424.09 32.86 o 1 10 2 181.33 229.76 3.94 o 2 10 2 2.39 3.31 1.64 o 3 10 2 51.94 54.28 2.27 o 4 10 2 0.06 2.45 1.96 o -4 11 2 135.13 121.21 3.49 o -3 11 2 0.00 0.00 0.55 o -2 11 2 74.23 88.03 2.59 o -1 11 2 0.01 1.63 1.03 o 0 11 2 78.92 88.51 3.29 o 1 11 2 328.61 341.92 4.96 o 2 11 2 116.63 119.32 3.28 o 3 11 2 10.16 10.52 1.74 o 4 11 2 202.66 189.65 4.81 o -4 12 2 9.55 10.31 1.46 o -3 12 2 99.62 109.73 3.40 o -2 12 2 34.51 37.42 1.74 o -1 12 2 37.71 49.89 1.49 o 0 12 2 2247.72 2347.14 12.54 o 1 12 2 218.97 231.66 4.33 o 2 12 2 113.99 119.13 3.37 o 3 12 2 35.37 32.89 2.00 o 4 12 2 0.82 3.44 1.90 o -4 13 2 17.47 16.57 1.49 o -3 13 2 252.49 252.62 6.07 o -2 13 2 361.87 354.87 6.43 o -1 13 2 27.10 25.25 1.22 o 0 13 2 641.78 626.05 12.02 o 1 13 2 9.42 7.71 1.04 o 2 13 2 18.86 15.44 1.59 o 3 13 2 13.73 11.27 1.66 o 4 13 2 0.43 2.61 1.70 o -4 14 2 0.06 0.86 1.30 o -3 14 2 14.76 16.70 1.66 o -2 14 2 16.44 15.66 1.57 o -1 14 2 232.60 232.52 4.71 o 0 14 2 7.12 8.85 0.95 o 1 14 2 19.88 19.00 1.31 o 2 14 2 237.11 243.39 5.58 o 3 14 2 1.38 0.00 0.89 o 4 14 2 0.42 0.33 1.49 o -4 15 2 1.87 1.12 1.24 o -3 15 2 11.74 17.41 1.63 o -2 15 2 46.09 50.00 2.07 o -1 15 2 26.61 27.93 1.50 o 0 15 2 12.97 11.91 0.78 o 1 15 2 13.79 14.16 1.28 o 2 15 2 114.72 120.37 3.74 o 3 15 2 192.15 170.75 5.10 o 4 15 2 0.07 0.23 1.54 o -3 16 2 26.25 25.13 1.99 o -2 16 2 193.29 206.64 5.37 o -1 16 2 777.54 776.09 9.30 o 0 16 2 159.53 144.88 2.87 o 1 16 2 27.54 31.24 1.59 o 2 16 2 123.35 134.68 3.96 o 3 16 2 195.39 204.09 5.34 o -3 17 2 19.59 19.93 1.67 o -2 17 2 223.92 231.45 5.81 o -1 17 2 331.84 323.47 6.43 o 0 17 2 0.97 1.39 0.90 o 1 17 2 0.08 0.00 2.11 o 2 17 2 163.01 153.34 4.22 o 3 17 2 29.20 23.57 1.81 o -3 18 2 6.41 7.57 1.38 o -2 18 2 69.96 71.64 2.34 o -1 18 2 75.67 70.35 2.32 o 0 18 2 110.75 108.98 2.40 o 1 18 2 7.43 10.89 1.39 o 2 18 2 28.84 21.67 1.63 o 3 18 2 223.23 209.79 4.83 o -3 19 2 1.33 2.03 1.43 o -2 19 2 185.95 185.04 4.97 o -1 19 2 692.31 667.34 9.25 o 0 19 2 597.24 586.49 6.21 o 1 19 2 0.08 1.46 1.62 o 2 19 2 29.94 22.75 1.70 o 3 19 2 18.35 14.99 1.51 o -3 20 2 5.84 3.17 1.56 o -2 20 2 5.21 9.19 1.45 o -1 20 2 0.03 0.00 1.38 o 0 20 2 93.88 99.27 2.17 o 1 20 2 38.35 44.37 1.95 o 2 20 2 30.41 25.29 1.88 o 3 20 2 0.58 0.97 1.19 o -3 21 2 1.23 1.79 1.12 o -2 21 2 8.14 8.49 1.28 o -1 21 2 87.81 101.13 2.78 o 0 21 2 137.70 140.37 2.79 o 1 21 2 17.96 16.41 1.51 o 2 21 2 7.93 6.56 1.89 o -2 22 2 4.93 5.35 1.60 o -1 22 2 24.72 22.67 1.66 o 0 22 2 354.87 362.50 10.06 o 1 22 2 138.01 139.07 3.83 o 2 22 2 1.46 1.09 1.32 o -2 23 2 1.40 3.49 1.42 o -1 23 2 25.19 27.63 1.66 o 0 23 2 24.08 25.65 1.13 o 1 23 2 99.77 95.75 2.70 o 2 23 2 26.80 29.32 1.58 o -2 24 2 0.00 0.00 0.59 o -1 24 2 136.70 130.05 3.61 o 0 24 2 61.56 62.35 1.45 o 1 24 2 95.09 100.58 2.85 o 2 24 2 16.09 19.39 1.29 o -1 25 2 4.45 6.05 1.10 o 0 25 2 10.09 11.29 0.79 o 1 25 2 61.66 70.01 2.04 o 0 26 2 23.63 22.96 0.93 o -4 1 3 4.15 0.24 2.18 o -3 1 3 0.60 1.41 1.41 o -2 1 3 10.84 7.02 0.77 o -1 1 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