#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:58:37 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180934 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/14/2201443.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201443_Fobs loop_ _publ_author_name 'Willett, Roger D.' 'Awwadi, Firas F.' _publ_section_title ; Tris(propane-1,3-diamine)nickel(II) bis(tetrafluoroborate) ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m471 _journal_page_last m472 _journal_volume 58 _journal_year 2002 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 15.2751 _cell_length_b 15.4983 _cell_length_c 16.8355 _exptl_crystal_F_000 1888.00 _reflns_d_resolution_high 0.8307 _cod_data_source_file cv6130Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' fa in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 346.92 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 585.77 688.65 25.98 o 4 0 0 120350.48 118882.70 716.86 o 6 0 0 7524.07 8710.91 232.42 o 8 0 0 8822.37 9263.00 251.06 o 10 0 0 825.54 810.28 69.32 o 12 0 0 7668.84 8197.15 239.12 o 14 0 0 97.27 42.33 97.95 o 16 0 0 4765.06 4828.44 209.56 o 18 0 0 32.25 110.58 120.43 o 2 1 0 51985.87 49048.26 1519.37 o 4 1 0 12953.29 13000.09 667.43 o 6 1 0 26120.89 26618.54 722.37 o 8 1 0 21.85 40.33 34.44 o 10 1 0 8228.67 8232.74 340.22 o 12 1 0 147.15 75.61 49.51 o 14 1 0 3215.18 3294.81 187.17 o 16 1 0 0.51 161.57 78.63 o 18 1 0 542.10 671.08 128.18 o 0 2 0 29480.24 24500.15 251.71 o 2 2 0 5140.25 5577.22 141.56 o 4 2 0 29.27 34.45 32.08 o 6 2 0 9856.08 9586.80 242.07 o 8 2 0 2500.34 2769.01 97.48 o 10 2 0 33.32 14.31 52.50 o 12 2 0 500.49 685.80 74.33 o 14 2 0 120.38 167.65 94.08 o 16 2 0 741.34 617.05 122.68 o 18 2 0 34.08 -127.37 128.58 o 2 3 0 16364.31 17607.39 282.78 o 4 3 0 12106.61 12820.36 266.23 o 6 3 0 584.90 561.39 46.39 o 8 3 0 587.41 610.44 54.73 o 10 3 0 512.47 513.06 62.04 o 12 3 0 28.24 87.47 62.31 o 14 3 0 100.93 145.80 90.37 o 16 3 0 2.98 -109.17 109.17 o 18 3 0 0.17 -29.34 129.60 o 0 4 0 173.88 193.81 38.03 o 2 4 0 602.71 624.87 42.47 o 4 4 0 159.26 131.92 34.78 o 6 4 0 4857.41 5095.13 188.44 o 8 4 0 6227.78 6319.84 221.62 o 10 4 0 1019.22 1092.14 72.81 o 12 4 0 55.16 -13.18 64.68 o 14 4 0 66.10 101.12 95.11 o 16 4 0 148.24 184.16 106.62 o 2 5 0 583.05 537.36 42.55 o 4 5 0 8524.22 9547.65 252.68 o 6 5 0 15556.53 15834.57 324.06 o 8 5 0 15.39 13.13 51.31 o 10 5 0 1374.26 1264.71 77.63 o 12 5 0 271.32 285.05 69.47 o 14 5 0 471.18 321.23 113.09 o 16 5 0 48.09 -26.62 110.13 o 0 6 0 710.77 712.77 48.99 o 2 6 0 569.62 518.32 47.45 o 4 6 0 4718.16 3861.51 174.86 o 6 6 0 2576.27 2618.39 100.66 o 8 6 0 10972.74 10798.65 272.44 o 10 6 0 38.94 53.78 60.95 o 12 6 0 5331.51 5093.42 188.02 o 14 6 0 186.28 153.91 109.41 o 16 6 0 527.89 551.26 128.15 o 2 7 0 16865.42 17435.30 352.88 o 4 7 0 510.41 476.99 54.34 o 6 7 0 7560.76 7431.72 240.04 o 8 7 0 128.74 216.52 62.20 o 10 7 0 4626.21 4710.51 187.70 o 12 7 0 488.66 510.12 99.39 o 14 7 0 1750.67 1702.66 144.20 o 16 7 0 7.40 4.83 117.14 o 0 8 0 7315.32 7677.59 243.17 o 2 8 0 536.11 642.16 58.38 o 4 8 0 13847.88 13493.47 321.38 o 6 8 0 854.58 701.59 67.27 o 8 8 0 4395.00 4460.76 187.96 o 10 8 0 518.37 521.43 72.95 o 12 8 0 2291.49 2158.63 140.08 o 14 8 0 46.83 63.64 106.87 o 16 8 0 181.19 202.65 125.45 o 2 9 0 592.61 597.85 66.83 o 4 9 0 10221.00 10834.73 285.12 o 6 9 0 946.75 876.13 75.72 o 8 9 0 279.72 63.47 67.06 o 10 9 0 27.67 61.00 65.78 o 12 9 0 62.32 112.50 106.52 o 14 9 0 64.19 49.20 113.98 o 16 9 0 9.71 -10.85 128.91 o 0 10 0 1528.44 1549.89 84.07 o 2 10 0 587.37 727.00 66.76 o 4 10 0 726.44 485.40 76.07 o 6 10 0 146.37 159.82 64.89 o 8 10 0 116.74 70.66 68.26 o 10 10 0 2.10 60.99 90.87 o 12 10 0 347.31 376.78 108.85 o 14 10 0 0.38 -27.58 109.08 o 2 11 0 3121.31 3289.19 117.56 o 4 11 0 74.41 130.28 65.14 o 6 11 0 1776.31 1596.11 90.08 o 8 11 0 5.70 -22.74 61.06 o 10 11 0 423.31 394.37 111.15 o 12 11 0 0.31 -47.80 106.37 o 14 11 0 262.30 229.89 136.50 o 0 12 0 5435.16 5114.31 208.85 o 2 12 0 348.34 353.30 72.59 o 4 12 0 5809.58 6536.91 212.04 o 6 12 0 250.73 217.16 64.79 o 8 12 0 1060.79 1282.19 124.40 o 10 12 0 61.99 -108.66 108.66 o 12 12 0 978.71 1096.03 140.89 o 2 13 0 1656.40 1476.91 90.57 o 4 13 0 0.33 -16.84 64.95 o 6 13 0 1540.96 1673.92 136.60 o 8 13 0 3.49 60.93 97.95 o 10 13 0 524.36 576.04 124.04 o 12 13 0 0.82 -38.15 114.47 o 0 14 0 1770.04 2083.53 145.12 o 2 14 0 1.51 -81.95 96.40 o 4 14 0 821.15 982.04 120.06 o 6 14 0 59.58 352.90 100.48 o 8 14 0 125.79 91.85 115.71 o 10 14 0 4.89 -20.25 123.86 o 2 15 0 11.67 39.69 107.01 o 4 15 0 39.23 160.53 110.21 o 6 15 0 68.80 57.31 117.01 o 8 15 0 0.17 45.25 115.50 o 10 15 0 45.76 -59.43 126.01 o 0 16 0 36.34 -66.20 113.13 o 2 16 0 35.11 23.99 105.54 o 4 16 0 28.40 157.77 113.54 o 6 16 0 7.42 81.00 116.75 o 8 16 0 12.43 -137.84 137.84 o 2 17 0 260.02 179.44 130.39 o 4 17 0 4.36 36.96 113.25 o 6 17 0 201.36 192.53 133.11 o 0 18 0 413.25 368.73 146.06 o 2 18 0 1.49 -127.65 127.65 o 1 1 1 19277.33 19330.89 231.61 o 2 1 1 2611.32 2312.63 45.76 o 3 1 1 5010.67 5760.63 179.28 o 4 1 1 161.57 203.26 18.44 o 5 1 1 4600.20 4583.63 94.59 o 6 1 1 8518.59 7804.81 144.52 o 7 1 1 765.68 786.74 37.51 o 8 1 1 174.83 186.47 26.03 o 9 1 1 271.69 320.19 28.11 o 10 1 1 1637.55 1710.26 40.30 o 11 1 1 4.05 -1.78 30.54 o 12 1 1 51.40 -7.97 33.87 o 13 1 1 159.39 162.59 36.28 o 14 1 1 331.91 428.06 58.06 o 15 1 1 293.16 344.71 57.45 o 16 1 1 26.09 87.62 54.94 o 17 1 1 53.85 16.24 60.35 o 18 1 1 218.17 196.57 68.00 o 0 2 1 27656.65 25234.25 746.24 o 1 2 1 2972.51 2759.20 63.80 o 2 2 1 3652.33 3845.63 84.64 o 3 2 1 2218.23 2237.88 56.91 o 4 2 1 10242.81 10522.46 365.26 o 5 2 1 1952.00 2052.39 133.19 o 6 2 1 793.72 839.12 35.33 o 7 2 1 8421.26 8184.26 210.43 o 8 2 1 19158.57 19605.21 248.30 o 9 2 1 2616.78 2826.15 75.07 o 10 2 1 2.10 -6.89 39.13 o 11 2 1 270.81 290.65 45.62 o 12 2 1 1413.17 1367.55 58.45 o 13 2 1 48.53 71.07 46.84 o 14 2 1 24.90 -60.48 81.05 o 15 2 1 91.06 -18.84 74.30 o 16 2 1 1057.36 1086.45 98.81 o 17 2 1 163.80 110.64 124.59 o 18 2 1 6.06 30.71 86.38 o 1 3 1 2851.47 3083.14 67.67 o 2 3 1 101198.88 100755.29 1434.65 o 3 3 1 7334.94 7646.14 145.87 o 4 3 1 580.19 535.75 28.44 o 5 3 1 9992.05 9549.23 173.19 o 6 3 1 5926.77 6009.30 273.28 o 7 3 1 3388.92 3330.24 85.09 o 8 3 1 55.03 54.96 33.84 o 9 3 1 1339.09 1228.93 50.37 o 10 3 1 5716.50 5545.99 171.46 o 11 3 1 165.36 163.42 62.71 o 12 3 1 238.53 280.18 47.89 o 13 3 1 512.12 513.61 119.75 o 14 3 1 2359.65 2294.09 108.15 o 15 3 1 268.89 289.32 75.94 o 16 3 1 2.66 -2.06 78.40 o 17 3 1 264.27 293.07 185.63 o 18 3 1 436.90 440.37 94.47 o 0 4 1 2978.90 2711.29 67.73 o 1 4 1 9848.91 10103.40 121.60 o 2 4 1 602.47 668.63 62.93 o 3 4 1 259.92 346.67 52.14 o 4 4 1 373.93 385.41 31.58 o 5 4 1 2129.14 2019.26 71.83 o 6 4 1 732.99 736.03 62.25 o 7 4 1 3968.69 4059.48 128.64 o 8 4 1 2687.50 2792.46 75.94 o 9 4 1 2542.70 2567.27 142.66 o 10 4 1 168.39 127.24 45.07 o 11 4 1 600.14 670.79 53.77 o 12 4 1 1187.38 1159.53 58.05 o 13 4 1 51.13 3.02 45.49 o 14 4 1 85.08 8.28 83.30 o 15 4 1 24.82 -13.93 75.20 o 16 4 1 660.65 615.86 92.94 o 17 4 1 33.28 -48.01 83.94 o 1 5 1 928.30 879.82 23.87 o 2 5 1 552.32 648.00 31.78 o 3 5 1 5322.40 5491.75 150.03 o 4 5 1 1023.08 1023.16 40.73 o 5 5 1 1228.56 1297.76 41.31 o 6 5 1 2002.68 2198.21 63.11 o 7 5 1 1043.12 1063.12 44.57 o 8 5 1 124.97 78.39 36.58 o 9 5 1 1542.85 1484.80 87.51 o 10 5 1 1173.81 1119.60 53.95 o 11 5 1 19.76 64.33 42.67 o 12 5 1 109.93 125.87 46.18 o 13 5 1 218.43 127.59 65.84 o 14 5 1 219.13 241.69 203.88 o 15 5 1 0.90 -59.07 74.93 o 16 5 1 27.35 -81.48 81.48 o 17 5 1 81.26 -17.00 89.36 o 0 6 1 49.56 57.97 65.17 o 1 6 1 1272.63 1194.22 27.97 o 2 6 1 7354.55 7314.12 162.94 o 3 6 1 162.48 210.33 30.33 o 4 6 1 1466.80 1470.95 46.18 o 5 6 1 41.58 61.07 61.07 o 6 6 1 120.76 174.72 33.34 o 7 6 1 236.63 139.19 36.23 o 8 6 1 626.34 551.29 84.62 o 9 6 1 624.33 767.69 69.75 o 10 6 1 698.83 609.38 48.96 o 11 6 1 66.26 55.60 46.51 o 12 6 1 12.19 16.61 47.43 o 13 6 1 119.85 87.99 68.81 o 14 6 1 25.46 93.78 71.59 o 15 6 1 23.76 -73.38 78.48 o 16 6 1 6.01 74.17 150.60 o 17 6 1 7.19 -84.43 90.12 o 1 7 1 1.61 -26.99 32.28 o 2 7 1 743.70 756.66 40.42 o 3 7 1 597.34 609.91 38.51 o 4 7 1 307.48 251.67 48.19 o 5 7 1 620.99 586.53 42.00 o 6 7 1 407.55 426.81 39.34 o 7 7 1 493.26 509.55 43.93 o 8 7 1 208.71 175.25 41.34 o 9 7 1 161.25 103.26 45.11 o 10 7 1 311.97 265.94 48.97 o 11 7 1 691.58 640.58 62.80 o 12 7 1 71.99 -5.75 68.62 o 13 7 1 127.07 93.83 79.28 o 14 7 1 75.84 79.53 75.38 o 15 7 1 19.42 144.52 78.57 o 16 7 1 7.63 20.95 145.56 o 0 8 1 2459.01 2435.43 115.62 o 1 8 1 1700.82 1626.39 36.75 o 2 8 1 99.35 56.02 35.24 o 3 8 1 904.51 851.37 44.51 o 4 8 1 9961.02 9889.03 321.33 o 5 8 1 1615.07 1630.43 73.31 o 6 8 1 1206.58 1150.82 86.90 o 7 8 1 234.91 290.97 48.46 o 8 8 1 1890.66 1850.40 61.68 o 9 8 1 687.72 801.01 54.90 o 10 8 1 58.36 165.45 99.21 o 11 8 1 535.17 529.05 68.80 o 12 8 1 679.84 712.08 85.69 o 13 8 1 62.77 104.45 75.06 o 14 8 1 24.69 -61.00 92.09 o 15 8 1 47.81 -47.55 83.21 o 16 8 1 170.08 236.52 92.08 o 1 9 1 1113.14 1068.87 34.98 o 2 9 1 7923.61 8110.52 308.32 o 3 9 1 6095.37 6183.29 165.10 o 4 9 1 81.70 71.90 41.75 o 5 9 1 1284.71 1325.54 56.10 o 6 9 1 9011.54 9581.43 187.43 o 7 9 1 876.44 889.53 53.34 o 8 9 1 150.69 82.52 45.66 o 9 9 1 1512.78 1711.60 89.64 o 10 9 1 4044.18 4287.15 126.37 o 11 9 1 433.40 476.16 73.18 o 12 9 1 93.82 53.22 167.11 o 13 9 1 482.35 461.92 83.89 o 14 9 1 855.62 998.22 126.29 o 15 9 1 100.46 160.09 82.27 o 0 10 1 5762.32 5516.33 223.40 o 1 10 1 933.23 926.09 39.62 o 2 10 1 6.11 20.77 46.66 o 3 10 1 3562.03 3723.17 103.29 o 4 10 1 10948.78 10555.84 302.48 o 5 10 1 1041.37 1081.70 100.96 o 6 10 1 17.21 50.37 61.17 o 7 10 1 239.84 213.29 48.68 o 8 10 1 3305.80 3380.04 95.13 o 9 10 1 299.01 338.90 98.00 o 10 10 1 1.19 148.49 66.31 o 11 10 1 273.06 107.43 90.89 o 12 10 1 1954.06 1538.49 107.09 o 13 10 1 156.92 71.35 83.09 o 14 10 1 0.89 189.89 79.00 o 15 10 1 37.68 -91.53 91.53 o 1 11 1 1005.83 982.61 39.21 o 2 11 1 2424.44 2471.29 72.56 o 3 11 1 1281.56 1300.53 59.72 o 4 11 1 19.39 -44.66 58.99 o 5 11 1 1126.14 1095.21 57.32 o 6 11 1 1776.96 1676.64 63.14 o 7 11 1 219.40 184.71 58.04 o 8 11 1 17.07 103.42 43.52 o 9 11 1 190.72 170.55 71.68 o 10 11 1 601.01 585.94 211.45 o 11 11 1 3.73 -72.95 75.08 o 12 11 1 14.04 -54.94 77.76 o 13 11 1 94.19 0.46 83.84 o 14 11 1 228.33 309.85 89.49 o 0 12 1 129.51 119.07 98.11 o 1 12 1 42.78 45.50 33.68 o 2 12 1 37.54 11.34 44.75 o 3 12 1 27.38 25.30 45.99 o 4 12 1 18.87 92.47 45.46 o 5 12 1 14.67 13.59 45.37 o 6 12 1 29.94 41.31 56.88 o 7 12 1 48.12 153.91 63.34 o 8 12 1 29.47 -66.70 66.70 o 9 12 1 52.83 56.18 67.91 o 10 12 1 4.55 -4.96 70.83 o 11 12 1 18.09 68.23 134.31 o 12 12 1 23.39 179.22 76.88 o 13 12 1 8.70 34.22 201.57 o 1 13 1 11.40 78.28 32.84 o 2 13 1 326.04 334.75 51.91 o 3 13 1 6.02 -9.14 45.01 o 4 13 1 9.82 -20.91 107.96 o 5 13 1 101.67 107.43 76.04 o 6 13 1 64.07 81.95 65.88 o 7 13 1 5.87 22.66 94.33 o 8 13 1 0.17 -68.93 68.93 o 9 13 1 5.19 22.98 72.48 o 10 13 1 61.52 41.35 132.91 o 11 13 1 29.89 -7.16 112.07 o 12 13 1 0.05 -55.49 81.82 o 0 14 1 409.34 433.60 70.56 o 1 14 1 69.54 4.17 47.25 o 2 14 1 3.24 -51.68 67.47 o 3 14 1 273.88 249.58 78.82 o 4 14 1 472.25 444.39 84.38 o 5 14 1 59.96 42.21 72.79 o 6 14 1 43.31 172.31 72.95 o 7 14 1 4.29 -48.73 129.32 o 8 14 1 96.45 4.84 78.20 o 9 14 1 30.58 -43.06 160.67 o 10 14 1 0.70 82.76 95.79 o 11 14 1 22.08 100.87 88.32 o 1 15 1 247.51 154.92 56.46 o 2 15 1 943.74 758.95 92.72 o 3 15 1 176.60 112.93 111.20 o 4 15 1 4.91 24.36 109.83 o 5 15 1 289.80 298.41 85.98 o 6 15 1 484.92 436.78 90.04 o 7 15 1 45.33 -2.33 118.94 o 8 15 1 0.28 -56.17 82.75 o 9 15 1 80.80 142.73 89.37 o 10 15 1 312.45 317.14 101.57 o 0 16 1 473.98 576.16 86.24 o 1 16 1 116.55 132.84 61.95 o 2 16 1 5.32 -21.82 77.55 o 3 16 1 63.37 11.96 79.66 o 4 16 1 639.81 609.77 97.23 o 5 16 1 98.92 195.79 86.56 o 6 16 1 0.01 2.03 82.29 o 7 16 1 46.07 -23.93 89.27 o 8 16 1 345.46 362.41 102.27 o 1 17 1 39.83 36.73 59.02 o 2 17 1 484.44 662.02 95.93 o 3 17 1 95.81 213.67 88.60 o 4 17 1 0.93 93.78 86.46 o 5 17 1 66.69 80.98 89.26 o 6 17 1 267.88 233.87 94.59 o 0 18 1 96.50 22.75 86.59 o 1 18 1 11.34 161.14 60.08 o 2 18 1 5.16 103.21 109.13 o 0 0 2 64596.27 63575.36 392.76 o 1 0 2 73001.56 72449.01 1109.39 o 2 0 2 217.98 214.31 25.08 o 3 0 2 31903.32 32207.66 358.25 o 4 0 2 27414.65 31124.31 384.45 o 5 0 2 3225.08 3121.44 151.33 o 6 0 2 3388.88 3997.32 166.26 o 7 0 2 23780.22 24810.82 394.22 o 8 0 2 5593.77 5688.24 210.62 o 9 0 2 5490.21 5867.61 203.56 o 10 0 2 1400.49 1302.05 76.17 o 11 0 2 1130.07 1108.35 80.19 o 12 0 2 1387.14 1466.20 87.88 o 13 0 2 1403.35 1189.01 87.18 o 14 0 2 2.20 7.31 92.56 o 15 0 2 1501.00 1328.45 127.46 o 16 0 2 433.82 717.75 128.27 o 17 0 2 565.74 741.06 141.51 o 18 0 2 8.50 -67.48 133.72 o 1 1 2 12598.41 12647.69 149.09 o 2 1 2 17423.66 17942.02 845.85 o 3 1 2 6416.83 7199.10 354.52 o 4 1 2 8886.63 9198.51 325.19 o 5 1 2 10737.05 11687.97 333.56 o 6 1 2 305.22 301.24 38.41 o 7 1 2 13395.93 13097.38 208.27 o 8 1 2 140.68 191.92 32.32 o 9 1 2 5008.57 5105.92 144.02 o 10 1 2 706.42 721.87 79.06 o 11 1 2 4151.42 4336.92 178.70 o 12 1 2 239.96 265.69 49.20 o 13 1 2 794.72 734.40 85.20 o 14 1 2 352.52 451.53 91.18 o 15 1 2 917.03 996.55 124.74 o 16 1 2 1.33 -5.75 81.35 o 17 1 2 415.42 484.56 94.06 o 18 1 2 154.37 162.10 97.26 o 0 2 2 3416.40 4132.30 126.78 o 1 2 2 13016.91 13614.32 426.77 o 2 2 2 2116.89 2155.09 75.61 o 3 2 2 11074.18 11295.59 230.05 o 4 2 2 7398.46 7631.28 199.05 o 5 2 2 7940.87 8504.90 223.69 o 6 2 2 1427.19 1370.43 59.58 o 7 2 2 6141.31 6573.97 214.59 o 8 2 2 394.72 429.83 54.17 o 9 2 2 1533.12 1495.25 72.16 o 10 2 2 259.44 314.97 61.81 o 11 2 2 2468.88 2430.75 95.55 o 12 2 2 71.05 -3.61 64.84 o 13 2 2 353.31 420.05 72.42 o 14 2 2 24.22 114.08 92.24 o 15 2 2 498.91 341.80 118.41 o 16 2 2 83.63 0.00 112.97 o 17 2 2 56.18 55.60 116.15 o 18 2 2 4.04 -24.87 124.37 o 1 3 2 4002.06 3810.21 141.87 o 2 3 2 1.20 20.38 33.56 o 3 3 2 118.36 117.16 34.32 o 4 3 2 2553.20 2976.43 143.47 o 5 3 2 245.94 222.98 38.73 o 6 3 2 116.98 192.57 39.93 o 7 3 2 149.65 184.72 44.71 o 8 3 2 1.29 -8.27 48.39 o 9 3 2 523.39 473.73 61.59 o 10 3 2 349.39 266.36 63.02 o 11 3 2 283.26 275.89 65.69 o 12 3 2 204.61 292.78 66.00 o 13 3 2 45.09 22.91 66.33 o 14 3 2 3.56 24.24 93.34 o 15 3 2 29.37 54.85 103.60 o 16 3 2 13.00 -118.90 118.90 o 17 3 2 34.78 199.77 110.98 o 18 3 2 0.40 70.73 129.06 o 0 4 2 26258.85 25794.87 387.99 o 1 4 2 11036.64 11425.26 237.92 o 2 4 2 8.88 4.83 32.64 o 3 4 2 73.32 51.38 33.46 o 4 4 2 2839.18 2748.65 100.83 o 5 4 2 871.26 871.04 48.46 o 6 4 2 99.90 138.11 44.86 o 7 4 2 1644.82 1488.22 68.50 o 8 4 2 1316.56 1500.33 70.99 o 9 4 2 792.07 664.35 65.25 o 10 4 2 74.63 55.94 60.71 o 11 4 2 55.69 -37.04 65.71 o 12 4 2 169.99 184.75 68.38 o 13 4 2 367.39 232.59 68.69 o 14 4 2 9.24 -101.71 101.71 o 15 4 2 364.17 133.89 119.29 o 16 4 2 1.50 -8.57 105.24 o 17 4 2 97.22 180.93 121.85 o 1 5 2 5121.87 5222.00 253.87 o 2 5 2 1467.50 1495.08 65.53 o 3 5 2 1243.95 1114.50 54.11 o 4 5 2 2347.61 2530.02 96.71 o 5 5 2 4223.59 4558.82 191.39 o 6 5 2 3396.97 3495.48 123.36 o 7 5 2 2612.15 2693.48 100.77 o 8 5 2 270.25 333.39 55.76 o 9 5 2 2399.33 2601.72 102.21 o 10 5 2 977.23 917.49 70.30 o 11 5 2 823.60 760.20 74.11 o 12 5 2 32.11 32.40 65.98 o 13 5 2 615.48 579.38 108.40 o 14 5 2 128.51 280.69 96.79 o 15 5 2 70.03 138.59 104.55 o 16 5 2 0.10 97.75 114.87 o 17 5 2 76.95 208.87 115.49 o 0 6 2 54.43 50.56 40.70 o 1 6 2 12914.08 12077.41 922.32 o 2 6 2 0.50 -30.39 40.12 o 3 6 2 3952.06 3595.10 174.93 o 4 6 2 2135.96 1850.19 70.75 o 5 6 2 12552.72 11853.80 285.33 o 6 6 2 403.46 460.79 51.20 o 7 6 2 4248.97 4334.93 186.72 o 8 6 2 2306.69 2241.94 92.76 o 9 6 2 2602.43 2488.43 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