#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2201444.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201444_Fobs loop_ _publ_author_name 'Flippen-Anderson, Judith L.' 'Deschamps, Jeffrey R.' 'George, Clifford' 'Gilardi, Richard D.' _publ_section_title ; 4,4,8,8-Tetranitro-2,6-dioxabicyclo[3.3.0]octane ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1018 _journal_page_last o1020 _journal_volume 58 _journal_year 2002 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.546 _cell_angle_gamma 90.000 _cell_length_a 9.5746 _cell_length_b 11.3472 _cell_length_c 29.2411 _exptl_crystal_F_000 1800.00 _reflns_d_resolution_high 0.7490 _[local]_cod_data_source_file cv6131Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' tnbo try snb' _shelx_refln_list_code 4 _shelx_f_calc_maximum 350.14 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 5 -13 0 264.78 312.69 71.12 o 6 -13 0 210.68 204.26 65.53 o 5 -12 0 380.72 331.94 65.27 o 6 -12 0 35.97 103.62 49.93 o 7 -12 0 256.66 225.45 55.65 o 5 -11 0 1113.90 1057.57 83.34 o 6 -11 0 235.80 246.26 60.98 o 7 -11 0 146.00 206.08 53.44 o 8 -11 0 297.01 378.35 57.86 o 5 -10 0 126.03 129.50 45.51 o 6 -10 0 1351.31 1239.60 91.27 o 7 -10 0 55.75 79.44 46.29 o 8 -10 0 66.09 20.54 41.09 o 9 -10 0 41.14 67.87 51.88 o 4 -9 0 360.87 357.03 39.01 o 5 -9 0 295.45 330.36 29.01 o 6 -9 0 2350.77 2185.09 117.93 o 7 -9 0 350.14 324.35 54.80 o 8 -9 0 57.71 33.41 29.85 o 9 -9 0 502.64 459.67 42.42 o 10 -9 0 36.88 3.51 49.28 o 3 -8 0 2400.46 2477.03 72.50 o 4 -8 0 1090.97 1085.02 44.12 o 5 -8 0 244.31 253.27 20.31 o 6 -8 0 269.36 311.22 23.66 o 7 -8 0 690.20 695.50 41.59 o 8 -8 0 109.65 123.97 32.82 o 9 -8 0 1139.16 1164.45 81.91 o 10 -8 0 44.17 -46.16 50.58 o 1 -7 0 28.88 66.05 21.58 o 2 -7 0 1075.18 1039.41 38.62 o 3 -7 0 2105.23 2122.95 63.10 o 4 -7 0 430.26 488.27 28.64 o 5 -7 0 614.78 642.38 27.76 o 6 -7 0 2186.94 2247.27 75.60 o 7 -7 0 10.64 37.57 21.51 o 8 -7 0 178.24 246.63 30.23 o 9 -7 0 2331.56 2200.30 115.85 o 10 -7 0 60.40 91.53 42.91 o 11 -7 0 41.44 147.18 54.87 o 0 -6 0 913.67 1088.12 47.98 o 1 -6 0 313.88 309.23 13.33 o 2 -6 0 720.55 784.80 30.39 o 3 -6 0 1994.65 2158.60 62.63 o 4 -6 0 75.75 90.36 26.59 o 5 -6 0 326.94 287.84 35.10 o 6 -6 0 3266.28 3121.60 94.42 o 7 -6 0 81.76 103.28 23.57 o 9 -6 0 31.18 25.87 33.54 o 10 -6 0 291.71 258.09 45.25 o 11 -6 0 87.39 45.51 47.72 o 1 -5 0 1564.59 1583.80 27.28 o 2 -5 0 46.06 61.20 9.11 o 3 -5 0 942.68 988.42 37.42 o 4 -5 0 1645.65 1771.62 56.37 o 5 -5 0 80.26 94.37 32.89 o 6 -5 0 8311.65 8569.34 212.14 o 7 -5 0 183.98 213.06 24.17 o 8 -5 0 369.15 369.51 39.92 o 9 -5 0 4492.77 3962.70 162.39 o 10 -5 0 44.30 39.40 36.02 o 11 -5 0 5.63 26.00 37.32 o 0 -4 0 28184.76 33201.06 744.51 o 1 -4 0 5519.07 5300.92 88.87 o 2 -4 0 5371.42 5430.34 214.28 o 3 -4 0 112.20 116.36 11.49 o 4 -4 0 1603.82 1567.54 40.93 o 5 -4 0 831.85 834.05 33.63 o 6 -4 0 72.10 115.46 23.01 o 7 -4 0 783.99 737.72 47.98 o 8 -4 0 58.52 47.33 24.57 o 9 -4 0 2462.76 2373.23 109.48 o 10 -4 0 157.31 196.07 39.14 o 11 -4 0 5.11 -3.90 31.59 o 1 -3 0 231.68 227.58 12.74 o 2 -3 0 978.75 1017.48 31.76 o 3 -3 0 22353.22 24485.56 517.04 o 4 -3 0 19.31 19.01 8.54 o 5 -3 0 466.77 429.16 18.43 o 6 -3 0 7734.25 8367.08 280.19 o 7 -3 0 279.90 296.70 29.51 o 8 -3 0 288.98 285.52 32.63 o 9 -3 0 2367.64 2227.09 100.89 o 10 -3 0 229.29 311.52 39.53 o 11 -3 0 132.47 118.71 36.28 o 12 -3 0 71.21 151.73 41.61 o 0 -2 0 63853.98 71374.92 1608.53 o 1 -2 0 729.29 659.39 31.33 o 2 -2 0 123.72 101.51 9.65 o 3 -2 0 19932.26 21141.49 489.43 o 4 -2 0 672.39 512.53 17.59 o 5 -2 0 163.87 160.34 11.30 o 6 -2 0 148.62 170.84 21.97 o 7 -2 0 225.44 231.17 25.87 o 8 -2 0 85.01 73.20 24.70 o 9 -2 0 498.93 463.78 40.31 o 10 -2 0 9.92 16.51 27.56 o 11 -2 0 35.08 36.67 31.33 o 12 -2 0 310.01 311.52 43.69 o 1 -1 0 134.57 98.42 4.60 o 2 -1 0 740.72 617.42 30.76 o 3 -1 0 11272.61 11726.40 214.81 o 4 -1 0 184.90 188.33 9.29 o 5 -1 0 2383.25 2271.57 58.01 o 6 -1 0 925.07 1102.30 53.44 o 7 -1 0 35.07 46.68 24.18 o 8 -1 0 94.92 48.24 26.00 o 9 -1 0 5701.85 5060.71 187.23 o 10 -1 0 70.80 61.24 28.47 o 11 -1 0 127.13 178.65 33.15 o 12 -1 0 134.81 214.27 42.26 o 1 0 0 0.18 -1.46 1.46 o 2 0 0 147.39 117.29 6.72 o 3 0 0 82887.40 85938.57 1966.93 o 4 0 0 200.87 180.34 8.78 o 5 0 0 472.01 515.76 20.27 o 6 0 0 3235.63 3472.69 175.39 o 7 0 0 1.20 7.41 16.51 o 8 0 0 101.63 113.64 25.87 o 9 0 0 3327.23 2647.70 110.52 o 10 0 0 0.07 -1.82 24.44 o 11 0 0 32.50 57.60 28.47 o 12 0 0 961.30 882.18 61.63 o 1 1 0 134.61 112.23 4.90 o 2 1 0 740.60 653.05 16.68 o 3 1 0 11273.53 11598.07 216.36 o 4 1 0 184.74 187.00 21.26 o 5 1 0 2382.48 2234.06 57.64 o 6 1 0 923.47 1072.83 37.84 o 7 1 0 34.97 48.65 12.53 o 8 1 0 94.72 104.48 18.66 o 9 1 0 5696.77 5190.99 183.98 o 10 1 0 70.92 68.00 30.94 o 11 1 0 127.30 192.82 39.01 o 12 1 0 135.14 149.91 37.06 o 0 2 0 63849.43 70267.06 2153.89 o 1 2 0 729.76 735.94 19.11 o 2 2 0 123.42 102.21 8.52 o 3 2 0 19934.24 21606.57 375.44 o 4 2 0 673.38 525.31 21.28 o 5 2 0 164.04 163.07 10.09 o 6 2 0 149.39 133.37 11.59 o 7 2 0 225.41 196.09 16.06 o 8 2 0 85.03 81.00 24.31 o 9 2 0 499.46 456.88 34.58 o 10 2 0 10.01 38.23 24.31 o 11 2 0 35.09 38.62 33.54 o 12 2 0 308.89 315.16 39.40 o 1 3 0 231.98 251.81 11.21 o 2 3 0 978.10 1021.27 27.94 o 3 3 0 22318.66 25056.85 533.54 o 4 3 0 19.39 34.13 8.37 o 5 3 0 465.24 455.77 18.68 o 6 3 0 7732.63 8434.17 200.94 o 7 3 0 280.37 305.94 19.39 o 8 3 0 288.55 260.56 24.31 o 9 3 0 2369.63 2154.41 91.40 o 10 3 0 229.15 230.91 28.47 o 11 3 0 131.98 178.91 33.28 o 12 3 0 70.38 119.23 42.13 o 0 4 0 28172.49 31723.47 995.81 o 1 4 0 5519.12 5412.17 121.30 o 2 4 0 5371.45 5476.76 123.95 o 3 4 0 111.29 152.34 10.75 o 4 4 0 1605.64 1568.98 47.00 o 5 4 0 831.86 779.69 27.82 o 6 4 0 70.83 100.21 15.01 o 7 4 0 783.95 731.35 38.36 o 8 4 0 58.43 43.95 20.15 o 9 4 0 2462.47 2425.63 95.95 o 10 4 0 157.49 175.92 35.24 o 11 4 0 5.15 4.81 23.66 o 12 4 0 515.36 550.11 49.02 o 1 5 0 1565.61 1569.30 42.93 o 2 5 0 46.12 58.09 9.51 o 3 5 0 941.72 1002.89 65.46 o 4 5 0 1644.34 1771.55 49.04 o 5 5 0 80.59 97.36 18.07 o 6 5 0 8316.96 8386.36 195.52 o 7 5 0 184.21 175.63 18.19 o 8 5 0 369.16 333.24 28.86 o 9 5 0 4494.88 3919.15 142.37 o 10 5 0 44.50 104.53 27.04 o 11 5 0 5.61 13.26 23.92 o 12 5 0 47.92 104.27 34.58 o 0 6 0 912.67 1052.37 48.11 o 1 6 0 313.49 273.09 15.49 o 2 6 0 721.11 806.02 29.03 o 3 6 0 1992.28 2179.30 61.17 o 4 6 0 75.64 98.31 13.98 o 5 6 0 327.20 339.32 18.22 o 6 6 0 3266.97 3137.70 81.87 o 7 6 0 81.81 82.37 15.55 o 8 6 0 295.01 275.14 23.92 o 9 6 0 30.86 40.83 26.00 o 10 6 0 291.57 282.40 30.03 o 11 6 0 87.28 114.81 38.36 o 1 7 0 29.01 27.60 11.61 o 2 7 0 1073.79 1109.30 45.83 o 3 7 0 2106.62 2128.49 59.84 o 4 7 0 430.29 441.08 22.67 o 5 7 0 615.38 657.23 39.92 o 6 7 0 2187.65 2217.29 63.82 o 7 7 0 10.70 23.66 14.53 o 8 7 0 178.02 169.72 24.28 o 9 7 0 2332.87 2399.10 93.48 o 10 7 0 60.57 76.32 23.66 o 11 7 0 41.42 85.42 32.11 o 0 8 0 1392.19 1385.09 64.49 o 1 8 0 240.07 232.26 31.33 o 2 8 0 50.08 51.45 16.54 o 3 8 0 2404.69 2495.69 69.12 o 4 8 0 1090.38 1048.84 39.34 o 5 8 0 244.38 275.58 39.07 o 6 8 0 268.35 296.04 22.45 o 7 8 0 689.36 666.46 33.22 o 8 8 0 110.08 106.99 21.75 o 9 8 0 1139.50 1179.92 57.47 o 10 8 0 44.05 83.21 34.84 o 1 9 0 535.93 547.08 28.68 o 2 9 0 31.86 38.38 20.17 o 3 9 0 962.58 976.51 37.89 o 4 9 0 361.28 364.57 23.08 o 5 9 0 295.51 301.54 25.25 o 6 9 0 2353.44 2353.53 68.71 o 7 9 0 350.12 357.34 24.46 o 8 9 0 57.81 118.95 48.17 o 0 10 0 1200.26 1045.22 57.60 o 1 10 0 91.53 96.34 22.13 o 2 10 0 166.77 156.33 20.19 o 3 10 0 2326.37 2207.18 68.27 o 4 10 0 389.90 371.79 25.93 o 5 10 0 126.45 157.91 24.90 o 6 10 0 1347.40 1322.57 64.81 o 7 10 0 55.63 92.87 49.41 o 8 10 0 66.26 60.59 44.86 o 1 11 0 28.15 68.37 19.83 o 2 11 0 1965.82 1824.11 61.36 o 3 11 0 1125.97 1039.00 51.42 o 4 11 0 615.27 575.65 47.65 o 5 11 0 1112.21 1036.17 66.05 o 6 11 0 235.91 251.36 38.29 o 7 11 0 145.56 106.75 60.46 o 8 11 0 297.31 421.13 71.25 o 0 12 0 357.01 399.29 49.41 o 1 12 0 12.35 22.06 58.83 o 2 12 0 385.81 386.05 29.93 o 3 12 0 973.78 1043.78 46.76 o 4 12 0 51.08 105.70 25.80 o 5 12 0 381.19 438.06 31.49 o 6 12 0 36.34 38.64 25.76 o 7 12 0 256.64 241.31 59.55 o 1 13 0 125.26 117.62 64.49 o 2 13 0 254.58 265.39 28.25 o 3 13 0 7.52 15.97 26.00 o 4 13 0 23.68 69.56 27.93 o 5 13 0 265.33 289.19 31.55 o 6 13 0 210.83 294.36 61.50 o 0 14 0 21.82 60.98 43.30 o 1 14 0 101.17 89.88 31.43 o 2 14 0 482.34 427.05 40.52 o 3 14 0 621.86 573.34 41.05 o 4 14 0 295.95 333.63 49.02 o -6 -13 1 64.30 86.33 52.92 o -5 -13 1 490.83 469.76 73.72 o 5 -13 1 119.30 88.28 55.52 o 6 -13 1 1.24 -22.36 59.68 o -7 -12 1 36.66 56.17 44.60 o -6 -12 1 33.53 -3.12 42.26 o -5 -12 1 219.30 254.32 60.85 o 5 -12 1 1090.15 1079.28 83.99 o 6 -12 1 67.26 104.79 57.34 o 7 -12 1 254.77 310.35 62.80 o -8 -11 1 320.30 268.49 52.01 o -7 -11 1 368.65 374.58 55.13 o -6 -11 1 13.88 6.11 44.21 o -5 -11 1 708.23 693.26 70.86 o 5 -11 1 929.91 847.33 74.50 o 6 -11 1 148.68 205.69 59.81 o 7 -11 1 28.00 7.41 45.77 o 8 -11 1 389.28 401.89 60.98 o -9 -10 1 222.38 305.67 72.42 o -8 -10 1 54.70 27.56 42.13 o -7 -10 1 304.45 342.21 56.56 o -6 -10 1 189.70 133.66 49.41 o -5 -10 1 171.12 125.73 48.24 o -4 -10 1 2926.35 3212.11 128.46 o 5 -10 1 147.95 175.52 41.22 o 6 -10 1 540.42 521.37 62.93 o 7 -10 1 54.97 25.61 48.50 o 8 -10 1 113.76 112.86 48.89 o 9 -10 1 149.08 168.11 54.87 o -10 -9 1 9.66 70.08 50.32 o -9 -9 1 24.13 29.53 32.81 o -8 -9 1 75.60 122.73 32.32 o -7 -9 1 180.95 216.88 35.48 o -6 -9 1 283.86 294.88 26.95 o -5 -9 1 58.87 72.98 25.74 o -4 -9 1 17.14 10.79 29.25 o -3 -9 1 79.49 85.42 29.38 o 4 -9 1 60.24 78.14 27.95 o 5 -9 1 486.09 487.31 47.33 o 6 -9 1 539.57 531.65 53.05 o 7 -9 1 652.53 679.87 68.65 o 8 -9 1 139.83 145.75 54.74 o 9 -9 1 124.84 110.39 49.80 o -10 -8 1 92.34 70.21 49.15 o -9 -8 1 71.24 90.79 31.17 o -8 -8 1 853.81 895.33 51.81 o -7 -8 1 1031.78 1038.13 41.72 o -6 -8 1 404.29 408.91 25.91 o -5 -8 1 1115.26 1085.25 56.17 o -4 -8 1 1485.87 1589.60 71.71 o -3 -8 1 673.67 701.25 33.38 o -2 -8 1 303.95 354.82 34.19 o 3 -8 1 148.18 125.74 18.45 o 4 -8 1 502.24 565.71 31.74 o 5 -8 1 172.04 215.58 19.71 o 6 -8 1 13.37 4.71 18.75 o 7 -8 1 189.39 157.17 41.74 o 8 -8 1 125.82 164.77 34.84 o 9 -8 1 30.62 57.21 45.12 o 10 -8 1 104.11 227.66 54.74 o -11 -7 1 95.16 117.80 54.35 o -10 -7 1 237.77 350.14 51.49 o -9 -7 1 158.70 145.10 41.22 o -8 -7 1 619.67 574.28 40.31 o -7 -7 1 1649.68 1435.48 91.66 o -6 -7 1 163.08 164.42 34.39 o -5 -7 1 617.07 643.69 27.83 o -4 -7 1 5098.19 5478.54 138.73 o -3 -7 1 966.75 926.25 36.83 o -2 -7 1 825.61 739.77 25.75 o -1 -7 1 3714.76 4187.38 145.49 o 0 -7 1 1129.01 1088.94 35.65 o 1 -7 1 418.41 396.82 31.59 o 2 -7 1 11866.89 12908.35 295.07 o 3 -7 1 8.71 3.54 22.10 o 4 -7 1 23.52 23.78 12.75 o 5 -7 1 3539.48 3612.32 83.58 o 6 -7 1 553.33 506.06 33.58 o 7 -7 1 204.23 204.83 27.11 o 8 -7 1 70.06 20.77 63.38 o 9 -7 1 40.53 51.62 35.50 o 10 -7 1 195.31 223.24 51.75 o 11 -7 1 216.78 223.89 58.51 o -11 -6 1 47.51 -40.83 41.74 o -10 -6 1 446.96 453.11 54.35 o -9 -6 1 32.89 68.52 36.15 o -8 -6 1 40.99 47.63 22.89 o -7 -6 1 1348.37 1393.93 57.77 o -6 -6 1 470.92 433.02 31.27 o -5 -6 1 843.28 822.10 38.89 o -4 -6 1 10005.41 10662.45 183.40 o -3 -6 1 1011.34 925.78 38.90 o -2 -6 1 1332.46 1320.03 50.73 o -1 -6 1 65.25 97.86 13.47 o 0 -6 1 305.36 318.69 14.43 o 1 -6 1 663.00 637.90 18.78 o 2 -6 1 13188.20 14637.81 332.02 o 3 -6 1 1106.12 1009.23 49.08 o 4 -6 1 69.10 101.80 18.26 o 5 -6 1 924.00 1023.17 41.29 o 6 -6 1 40.99 43.71 18.11 o 7 -6 1 48.81 36.69 22.02 o 8 -6 1 495.69 498.49 45.90 o 9 -6 1 60.94 43.04 34.19 o 10 -6 1 30.21 3.25 38.10 o 11 -6 1 1118.51 1170.04 83.21 o -11 -5 1 5.94 14.43 40.70 o -10 -5 1 721.84 699.37 57.34 o -9 -5 1 632.78 552.45 49.02 o -8 -5 1 927.90 834.46 57.99 o -7 -5 1 3032.04 3049.79 137.56 o -6 -5 1 931.85 928.87 67.54 o -5 -5 1 118.39 106.81 14.41 o -4 -5 1 4413.36 4954.60 106.19 o -3 -5 1 1188.98 1167.21 32.24 o -2 -5 1 1168.88 1126.97 29.78 o -1 -5 1 4428.50 5047.19 100.64 o 0 -5 1 799.24 788.99 21.70 o 1 -5 1 1964.96 1976.15 43.24 o 2 -5 1 3214.41 3357.16 84.20 o 3 -5 1 426.52 391.36 30.68 o 4 -5 1 1016.12 1029.03 40.10 o 5 -5 1 301.32 316.98 24.70 o 6 -5 1 855.15 850.45 39.57 o 7 -5 1 189.25 189.40 21.74 o 8 -5 1 5031.71 4596.80 177.87 o 9 -5 1 1129.53 1063.29 66.44 o 10 -5 1 30.59 86.46 37.19 o 11 -5 1 52.75 119.36 41.87 o -12 -4 1 22.76 24.05 42.00 o -11 -4 1 29.19 78.40 37.84 o -10 -4 1 678.60 705.48 56.30 o -9 -4 1 262.90 232.21 34.84 o -8 -4 1 126.66 179.17 30.16 o -7 -4 1 1199.15 1180.96 64.62 o -6 -4 1 349.52 335.59 19.31 o -5 -4 1 918.95 912.71 34.96 o -4 -4 1 4693.99 5112.59 106.80 o -3 -4 1 283.13 235.09 20.13 o -2 -4 1 6393.03 6743.98 154.22 o -1 -4 1 25670.98 28362.28 522.42 o 0 -4 1 4349.67 4029.58 78.61 o 1 -4 1 4138.72 4052.67 59.88 o 2 -4 1 23845.79 26610.86 583.00 o 3 -4 1 135.72 122.45 14.31 o 4 -4 1 2151.65 2175.44 103.69 o 5 -4 1 2935.73 3193.03 88.52 o 6 -4 1 543.51 508.46 27.90 o 7 -4 1 452.82 436.73 37.71 o 8 -4 1 306.73 310.35 34.71 o 9 -4 1 401.40 404.10 41.87 o 10 -4 1 201.25 223.11 43.17 o 11 -4 1 10.98 85.42 36.28 o 12 -4 1 52.81 43.95 39.66 o -12 -3 1 7.94 40.57 35.76 o -11 -3 1 2.68 -0.13 30.29 o -10 -3 1 132.84 86.20 31.20 o -9 -3 1 971.11 754.76 53.57 o -8 -3 1 59.99 74.89 27.56 o -7 -3 1 2770.70 2682.67 108.70 o -6 -3 1 224.92 254.62 19.71 o -5 -3 1 401.36 373.92 17.49 o -4 -3 1 328.61 335.23 15.79 o -3 -3 1 713.69 594.52 19.74 o -2 -3 1 1583.15 1493.64 74.96 o -1 -3 1 2265.67 2462.66 51.33 o 0 -3 1 843.67 758.01 18.62 o 1 -3 1 1573.13 1457.80 31.59 o 2 -3 1 17131.96 19507.19 594.70 o 3 -3 1 3152.93 3196.26 85.11 o 4 -3 1 626.01 533.55 40.11 o 5 -3 1 3345.66 3432.79 92.80 o 6 -3 1 877.21 827.96 46.55 o 7 -3 1 70.10 105.31 23.53 o 8 -3 1 817.46 737.85 49.93 o 9 -3 1 365.40 372.24 38.23 o 10 -3 1 39.46 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