#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2201460.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201460_Fobs loop_ _publ_author_name 'Lee, Uk' 'Joo, Hea-Chung' 'Cho, Mi-Ae' _publ_section_title ; Hexaaquacobalt(II) tetrapotassium diethylenediaminetetraacetato(4--)cobaltate(III) \b-octamolybdate hexahydrate ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m599 _journal_page_last m601 _journal_volume 58 _journal_year 2002 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 90.320 _cell_angle_beta 95.860 _cell_angle_gamma 100.790 _cell_length_a 8.3607 _cell_length_b 10.6850 _cell_length_c 16.9220 _exptl_crystal_F_000 1097.00 _reflns_d_resolution_high 0.7707 _[local]_cod_data_source_file cv6148Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' EDTACOCOMO8O40 POM' _shelx_refln_list_code 4 _shelx_f_calc_maximum 352.36 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 13202.24 12365.48 79.66 o 2 0 0 557.52 724.77 44.36 o 3 0 0 641.11 748.14 48.65 o 4 0 0 3268.30 3475.04 91.34 o 5 0 0 1.00 -38.40 38.40 o 6 0 0 6769.79 6296.38 149.18 o 7 0 0 2241.04 2064.01 99.09 o 8 0 0 12.60 43.29 57.00 o 9 0 0 5187.84 5003.64 177.20 o 10 0 0 4178.70 4150.56 173.50 o -10 1 0 3559.60 3049.81 145.36 o -9 1 0 5.53 17.89 56.05 o -8 1 0 1239.29 1120.67 87.41 o -7 1 0 55.81 63.92 43.88 o -6 1 0 6913.18 6383.07 144.64 o -5 1 0 2478.50 2348.05 83.23 o -4 1 0 98.92 84.43 35.06 o -3 1 0 2748.29 2951.91 77.87 o -2 1 0 8463.94 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