#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2201468.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201468_Fobs loop_ _publ_author_name 'Rei\&s, Guido J.' 'Koppelhuber-Bitschnau, Brigitte' _publ_section_title ; Diisopropylammonium chloride hemihydrate, a combined single-crystal and powder diffraction study ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1309 _journal_page_last o1311 _journal_volume 58 _journal_year 2002 _space_group_IT_number 68 _symmetry_space_group_name_Hall '-C 2a 2ac' _symmetry_space_group_name_H-M 'C c c a :2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.2888 _cell_length_b 15.7228 _cell_length_c 11.5900 _exptl_crystal_F_000 648.00 _reflns_d_resolution_high 0.8403 _[local]_cod_data_source_file cv6156Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' nbisoc in Ccca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 213.19 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z' '-x, y, -z+1/2' 'x+1/2, -y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1, -y+1/2, z' '-x+1/2, y+1/2, -z+1/2' 'x+1, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z' 'x, -y, z-1/2' '-x-1/2, y, z-1/2' '-x+1/2, -y+1/2, -z' 'x, y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' '-x, y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 10042.51 9402.39 514.08 o 6 0 0 5461.43 4554.65 226.00 o 8 0 0 672.74 605.72 47.00 o 10 0 0 480.78 520.37 24.17 o 12 0 0 123.15 122.26 31.26 o 2 2 0 1284.31 1152.28 47.79 o 4 2 0 7095.45 6176.64 234.30 o 6 2 0 552.39 420.33 16.69 o 8 2 0 486.57 463.03 19.19 o 10 2 0 223.52 250.21 17.25 o 12 2 0 71.86 66.73 14.98 o 0 4 0 10007.83 11275.65 1311.59 o 2 4 0 3956.27 4898.92 286.35 o 4 4 0 2619.44 2764.06 105.27 o 6 4 0 1175.40 1170.91 60.80 o 8 4 0 398.61 387.20 16.92 o 10 4 0 65.20 40.27 11.29 o 0 6 0 6161.97 7117.51 853.91 o 2 6 0 4877.68 5177.18 352.28 o 4 6 0 2032.73 2008.31 93.54 o 6 6 0 2317.49 2342.90 91.12 o 8 6 0 28.78 31.36 10.79 o 10 6 0 988.20 1107.74 53.53 o 0 8 0 146.75 190.64 21.30 o 2 8 0 4958.69 5341.72 392.59 o 4 8 0 1331.31 1451.05 82.38 o 6 8 0 1426.09 1486.42 66.66 o 8 8 0 120.05 132.67 13.88 o 10 8 0 668.89 696.20 28.78 o 0 10 0 1204.92 1261.12 165.67 o 2 10 0 3372.08 3486.06 275.80 o 4 10 0 30.36 22.82 14.11 o 6 10 0 1310.61 1222.58 59.57 o 8 10 0 169.15 174.24 16.67 o 10 10 0 42.55 53.38 16.04 o 0 12 0 451.65 549.62 68.98 o 2 12 0 221.92 215.88 17.54 o 4 12 0 359.74 322.94 22.91 o 6 12 0 29.01 35.96 12.81 o 8 12 0 0.07 0.00 13.19 o 0 14 0 1475.34 1535.53 183.01 o 2 14 0 0.26 11.19 11.34 o 4 14 0 187.72 193.45 17.29 o 6 14 0 159.09 163.77 13.65 o 8 14 0 101.43 109.22 20.93 o 0 16 0 882.80 846.71 98.69 o 2 16 0 196.98 214.90 16.39 o 4 16 0 494.78 494.23 32.42 o 6 16 0 55.28 32.91 16.11 o 0 18 0 49.26 23.27 21.91 o 2 18 0 33.23 15.36 16.05 o 3 1 1 10951.99 10343.88 227.36 o 5 1 1 323.60 255.51 9.21 o 7 1 1 193.72 180.03 8.69 o 9 1 1 152.37 175.22 10.80 o 11 1 1 36.00 40.05 9.56 o 2 2 1 1638.52 1554.50 43.84 o 4 2 1 44.23 49.68 9.24 o 6 2 1 54.67 28.27 8.23 o 8 2 1 48.47 53.90 8.28 o 10 2 1 0.08 0.00 8.84 o 12 2 1 0.00 0.00 11.21 o 1 3 1 2464.54 2824.97 135.81 o 3 3 1 11767.12 11912.35 318.13 o 5 3 1 1346.06 1154.52 33.37 o 7 3 1 1421.27 1431.03 37.32 o 9 3 1 530.57 596.93 20.88 o 11 3 1 154.71 166.72 10.04 o 2 4 1 0.14 1.20 11.87 o 4 4 1 88.08 106.45 9.00 o 6 4 1 280.03 273.19 8.12 o 8 4 1 79.69 74.28 8.00 o 10 4 1 8.07 12.26 8.76 o 1 5 1 16076.31 19751.30 1036.62 o 3 5 1 2650.38 2748.24 96.14 o 5 5 1 2695.03 2616.26 97.32 o 7 5 1 1838.52 1941.06 66.55 o 9 5 1 267.89 290.32 12.48 o 11 5 1 115.57 134.64 10.51 o 2 6 1 242.84 274.39 14.01 o 4 6 1 219.45 221.09 8.72 o 6 6 1 387.14 414.77 15.84 o 8 6 1 139.64 148.93 8.48 o 10 6 1 7.55 6.60 9.46 o 1 7 1 499.03 537.43 27.84 o 3 7 1 80.56 63.61 8.42 o 5 7 1 342.51 432.35 15.51 o 7 7 1 85.25 90.45 8.38 o 9 7 1 54.14 63.21 8.88 o 11 7 1 25.83 22.57 10.67 o 2 8 1 206.11 263.36 13.74 o 4 8 1 74.63 64.13 7.52 o 6 8 1 26.81 13.11 8.54 o 8 8 1 31.24 22.29 8.95 o 10 8 1 0.21 5.14 10.70 o 1 9 1 371.96 370.59 19.38 o 3 9 1 21.81 43.40 7.90 o 5 9 1 53.20 67.06 9.43 o 7 9 1 293.45 340.80 15.72 o 9 9 1 7.63 11.36 10.59 o 2 10 1 224.43 211.99 11.95 o 4 10 1 438.18 435.59 20.26 o 6 10 1 338.63 337.39 12.11 o 8 10 1 72.39 60.89 8.65 o 10 10 1 0.05 3.02 11.41 o 1 11 1 1569.34 1718.87 92.11 o 3 11 1 1938.30 1990.09 91.60 o 5 11 1 560.80 543.53 21.49 o 7 11 1 316.67 309.41 13.47 o 9 11 1 202.35 179.05 11.17 o 2 12 1 550.23 494.93 25.58 o 4 12 1 435.01 438.36 17.77 o 6 12 1 84.06 84.88 8.79 o 8 12 1 0.97 0.00 10.53 o 1 13 1 418.31 396.85 18.80 o 3 13 1 876.44 838.92 38.50 o 5 13 1 387.41 442.85 19.38 o 7 13 1 100.23 96.86 9.59 o 2 14 1 2.46 5.29 9.68 o 4 14 1 21.92 0.52 8.40 o 6 14 1 20.33 12.38 9.41 o 8 14 1 4.74 0.00 11.18 o 1 15 1 195.78 190.27 12.37 o 3 15 1 16.97 0.00 8.63 o 5 15 1 87.44 69.82 10.66 o 7 15 1 42.24 44.34 10.50 o 2 16 1 172.46 165.41 9.66 o 4 16 1 220.41 180.24 9.72 o 6 16 1 46.27 29.80 9.97 o 1 17 1 27.26 26.88 9.77 o 3 17 1 77.53 63.43 11.15 o 5 17 1 17.26 10.51 11.04 o 2 18 1 5.52 10.01 11.79 o 2 0 2 45448.88 44842.78 1264.58 o 8 0 2 2044.19 1867.50 61.21 o 10 0 2 54.14 68.45 11.71 o 12 0 2 252.84 276.93 21.63 o 1 1 2 9537.44 8815.54 359.22 o 3 1 2 785.45 689.15 17.32 o 5 1 2 1.65 0.31 7.68 o 7 1 2 96.02 82.09 9.27 o 9 1 2 38.58 41.04 9.17 o 11 1 2 67.33 79.75 10.12 o 0 2 2 125.39 138.13 18.23 o 2 2 2 12528.97 12749.79 364.25 o 4 2 2 1651.82 1480.73 44.93 o 6 2 2 1019.66 910.78 22.93 o 8 2 2 714.88 699.92 19.22 o 10 2 2 80.36 85.69 8.66 o 12 2 2 86.10 88.47 10.24 o 1 3 2 52.94 24.65 13.01 o 3 3 2 3582.29 3719.58 119.40 o 5 3 2 2150.10 1987.94 47.19 o 7 3 2 266.52 263.82 9.38 o 9 3 2 0.01 0.00 8.87 o 11 3 2 0.93 0.24 10.38 o 0 4 2 4360.63 4817.47 386.68 o 2 4 2 1482.07 1607.37 62.49 o 4 4 2 19.49 17.46 7.63 o 6 4 2 156.36 134.80 9.75 o 8 4 2 128.19 141.52 8.36 o 10 4 2 58.10 44.26 9.10 o 1 5 2 1443.49 1733.25 90.16 o 3 5 2 1188.77 1277.82 48.98 o 5 5 2 488.63 508.84 12.33 o 7 5 2 140.16 138.37 8.95 o 9 5 2 62.20 59.89 8.75 o 11 5 2 16.71 10.58 9.59 o 0 6 2 4.23 0.00 11.62 o 2 6 2 8167.08 9754.20 433.07 o 4 6 2 1170.45 1001.42 33.91 o 6 6 2 198.92 195.36 9.57 o 8 6 2 1050.53 1157.46 38.87 o 10 6 2 1.53 1.90 9.89 o 1 7 2 2140.79 2236.67 119.21 o 3 7 2 4.39 0.89 8.12 o 5 7 2 10.63 9.90 8.62 o 7 7 2 18.06 7.82 8.37 o 9 7 2 299.95 289.02 9.12 o 11 7 2 88.14 73.73 11.05 o 0 8 2 2726.66 2743.36 218.60 o 2 8 2 2943.14 3271.44 165.50 o 4 8 2 2479.07 2853.85 113.84 o 6 8 2 850.07 916.06 33.70 o 8 8 2 675.59 736.14 29.86 o 10 8 2 92.18 101.36 11.13 o 1 9 2 3.36 16.67 8.65 o 3 9 2 37.47 42.96 9.65 o 5 9 2 211.01 195.58 10.05 o 7 9 2 124.58 121.84 8.83 o 9 9 2 104.00 99.49 10.53 o 0 10 2 2320.35 2707.82 214.65 o 2 10 2 327.02 296.34 15.11 o 4 10 2 1001.57 1003.16 40.95 o 6 10 2 435.76 442.04 17.30 o 8 10 2 99.31 80.95 8.47 o 10 10 2 82.42 77.25 11.67 o 1 11 2 7.17 5.61 9.12 o 3 11 2 210.94 213.09 10.07 o 5 11 2 435.52 438.86 15.79 o 7 11 2 66.36 70.62 8.25 o 9 11 2 1.22 2.86 10.32 o 0 12 2 58.07 70.25 12.85 o 2 12 2 39.61 44.95 8.15 o 4 12 2 17.03 23.73 8.40 o 6 12 2 0.63 0.00 8.28 o 8 12 2 5.51 0.00 10.01 o 1 13 2 642.30 616.60 35.11 o 3 13 2 219.31 229.69 13.61 o 5 13 2 0.18 0.00 8.98 o 7 13 2 0.10 6.82 9.29 o 0 14 2 189.68 213.19 15.71 o 2 14 2 391.83 426.31 19.39 o 4 14 2 142.12 149.58 8.84 o 6 14 2 141.90 122.08 10.04 o 1 15 2 314.86 322.24 13.16 o 3 15 2 52.45 43.79 9.13 o 5 15 2 0.22 5.71 10.07 o 7 15 2 2.48 14.07 10.54 o 0 16 2 194.63 210.90 18.12 o 2 16 2 444.23 433.89 22.26 o 4 16 2 184.88 126.18 10.14 o 6 16 2 147.06 113.98 10.93 o 1 17 2 8.18 6.92 10.26 o 3 17 2 24.71 21.87 10.52 o 0 18 2 60.59 59.59 14.89 o 2 18 2 99.24 75.44 11.01 o 1 1 3 4490.39 5189.09 214.77 o 3 1 3 1400.59 1303.46 39.64 o 5 1 3 1685.63 1450.33 46.73 o 7 1 3 118.66 83.69 9.22 o 9 1 3 58.79 50.56 8.60 o 11 1 3 31.68 37.30 9.32 o 2 2 3 2953.83 3012.80 96.08 o 4 2 3 190.48 166.05 9.10 o 6 2 3 7.90 2.23 7.83 o 8 2 3 132.86 125.14 8.59 o 10 2 3 0.09 10.69 8.05 o 1 3 3 16699.70 20078.40 854.08 o 3 3 3 216.49 162.24 10.10 o 5 3 3 8454.64 7912.36 200.85 o 7 3 3 453.72 425.41 11.52 o 9 3 3 462.11 522.98 15.73 o 11 3 3 202.44 222.99 11.14 o 2 4 3 1165.77 1353.13 52.66 o 4 4 3 829.60 898.41 33.34 o 6 4 3 7.44 14.25 9.48 o 8 4 3 32.01 33.75 8.58 o 10 4 3 8.01 9.27 9.76 o 1 5 3 2594.39 3118.12 154.01 o 3 5 3 3855.93 3823.84 147.11 o 5 5 3 2420.65 2135.37 78.89 o 7 5 3 287.15 247.40 11.44 o 9 5 3 519.98 584.14 24.98 o 11 5 3 179.25 210.20 10.77 o 2 6 3 2463.53 2963.22 129.32 o 4 6 3 1156.33 1173.23 42.15 o 6 6 3 3.98 6.05 8.02 o 8 6 3 2.83 1.62 8.61 o 10 6 3 8.30 9.82 10.04 o 1 7 3 720.73 682.43 33.72 o 3 7 3 1660.85 1867.91 69.22 o 5 7 3 10.84 28.16 8.76 o 7 7 3 299.64 284.97 10.32 o 9 7 3 43.98 48.40 8.65 o 11 7 3 9.81 15.77 10.72 o 2 8 3 88.10 83.17 9.90 o 4 8 3 76.93 88.74 9.27 o 6 8 3 1.21 2.84 9.45 o 8 8 3 7.58 0.00 8.53 o 10 8 3 0.05 0.49 10.22 o 1 9 3 534.36 558.74 28.78 o 3 9 3 258.39 294.68 11.38 o 5 9 3 587.39 657.80 26.94 o 7 9 3 4.66 5.20 8.19 o 9 9 3 79.18 69.32 10.67 o 2 10 3 456.56 466.84 23.11 o 4 10 3 368.04 390.82 16.83 o 6 10 3 50.41 41.96 9.44 o 8 10 3 24.38 24.28 9.48 o 10 10 3 0.89 0.00 10.88 o 1 11 3 1131.73 1222.70 66.97 o 3 11 3 442.94 477.13 20.33 o 5 11 3 678.59 703.86 29.94 o 7 11 3 296.71 304.66 11.59 o 9 11 3 92.44 92.48 10.63 o 2 12 3 2.51 0.00 8.54 o 4 12 3 46.56 59.05 9.54 o 6 12 3 48.49 39.58 8.69 o 8 12 3 88.06 62.21 10.16 o 1 13 3 968.04 906.73 42.65 o 3 13 3 461.79 490.33 21.47 o 5 13 3 299.20 337.34 17.68 o 7 13 3 335.03 332.32 15.44 o 2 14 3 10.68 12.94 8.40 o 4 14 3 5.93 2.37 8.69 o 6 14 3 9.04 13.70 9.32 o 1 15 3 10.97 6.84 9.01 o 3 15 3 152.96 141.45 10.44 o 5 15 3 5.61 0.00 9.15 o 2 16 3 0.76 0.00 9.11 o 4 16 3 19.75 12.85 9.26 o 1 17 3 41.48 42.68 9.87 o 3 17 3 0.05 0.00 11.02 o 2 18 3 9.62 5.10 10.56 o 0 0 4 954.86 1272.55 174.95 o 2 0 4 6945.13 6626.00 275.02 o 6 0 4 1926.16 1888.86 76.78 o 8 0 4 84.32 90.54 13.03 o 10 0 4 1244.67 1314.22 55.58 o 1 1 4 4.49 7.86 13.19 o 3 1 4 26.97 31.22 8.44 o 5 1 4 159.46 144.44 7.91 o 7 1 4 11.18 5.80 9.20 o 9 1 4 13.49 24.72 8.51 o 11 1 4 20.49 15.70 9.46 o 0 2 4 6446.82 7440.08 801.78 o 2 2 4 6914.44 6941.81 251.22 o 4 2 4 586.78 503.57 16.42 o 6 2 4 2328.05 2267.83 56.01 o 8 2 4 83.52 81.03 8.14 o 10 2 4 378.41 406.12 11.83 o 1 3 4 1679.32 2017.74 102.98 o 3 3 4 698.48 710.04 25.88 o 5 3 4 219.18 194.71 7.86 o 7 3 4 0.01 3.07 8.22 o 9 3 4 2.42 0.84 8.14 o 11 3 4 0.63 0.00 10.05 o 0 4 4 1449.15 1464.34 112.91 o 2 4 4 420.48 482.08 21.64 o 4 4 4 1808.50 1763.53 57.15 o 6 4 4 317.38 332.00 10.59 o 8 4 4 3.72 1.42 8.76 o 10 4 4 7.72 3.00 11.02 o 1 5 4 241.55 244.34 10.20 o 3 5 4 17.37 14.30 8.40 o 5 5 4 17.91 8.14 9.39 o 7 5 4 72.78 77.13 9.51 o 9 5 4 8.04 3.41 7.99 o 11 5 4 18.28 7.44 11.27 o 0 6 4 11332.75 12154.38 914.22 o 2 6 4 316.65 351.11 16.13 o 4 6 4 1427.95 1392.31 51.28 o 6 6 4 478.99 437.01 14.37 o 8 6 4 307.69 341.14 16.85 o 10 6 4 42.24 50.28 10.31 o 1 7 4 650.83 704.83 35.34 o 3 7 4 19.52 25.14 7.74 o 5 7 4 0.01 0.00 8.36 o 7 7 4 213.85 233.15 12.69 o 9 7 4 41.16 24.24 10.05 o 0 8 4 8450.48 8645.29 664.20 o 2 8 4 1051.13 1016.51 44.33 o 4 8 4 2189.54 2496.72 102.55 o 6 8 4 726.64 738.73 27.10 o 8 8 4 699.19 692.98 25.66 o 10 8 4 42.13 29.75 11.14 o 1 9 4 242.18 255.04 12.99 o 3 9 4 1.03 11.17 8.72 o 5 9 4 0.99 6.59 7.65 o 7 9 4 143.26 138.37 8.52 o 9 9 4 26.06 26.99 10.46 o 0 10 4 199.50 216.45 13.93 o 2 10 4 401.51 405.35 19.41 o 4 10 4 1206.37 1244.13 49.60 o 6 10 4 1.36 7.34 8.46 o 8 10 4 335.13 326.46 10.47 o 1 11 4 55.76 45.98 8.26 o 3 11 4 30.98 26.90 8.54 o 5 11 4 1.63 6.92 8.86 o 7 11 4 4.91 15.37 9.73 o 9 11 4 0.89 3.26 10.77 o 0 12 4 115.50 83.72 12.28 o 2 12 4 11.00 14.49 7.71 o 4 12 4 126.43 131.16 8.97 o 6 12 4 40.57 26.27 8.20 o 8 12 4 25.16 16.01 10.48 o 1 13 4 340.13 353.45 17.68 o 3 13 4 108.89 97.55 9.56 o 5 13 4 12.01 6.03 8.41 o 7 13 4 17.47 27.17 9.13 o 0 14 4 7.12 0.00 12.96 o 2 14 4 662.30 676.94 33.20 o 4 14 4 227.35 243.20 11.85 o 6 14 4 77.04 53.71 10.24 o 1 15 4 143.42 127.45 9.26 o 3 15 4 35.44 33.53 9.83 o 5 15 4 10.39 12.02 10.17 o 0 16 4 198.80 171.66 14.81 o 2 16 4 234.52 216.18 10.80 o 4 16 4 75.74 49.82 11.05 o 1 17 4 0.70 16.78 10.61 o 3 17 4 0.96 13.77 10.19 o 1 1 5 228.50 209.05 13.92 o 3 1 5 678.15 635.50 21.29 o 5 1 5 37.36 39.86 9.57 o 7 1 5 748.60 705.84 21.41 o 9 1 5 4.26 0.00 9.30 o 11 1 5 4.86 0.00 11.19 o 2 2 5 323.51 352.42 14.03 o 4 2 5 236.29 250.91 9.12 o 6 2 5 130.58 101.05 9.68 o 8 2 5 15.12 7.41 8.97 o 10 2 5 27.56 23.69 11.65 o 1 3 5 3440.13 3463.05 186.53 o 3 3 5 8952.42 9188.16 359.23 o 5 3 5 6.62 14.59 10.20 o 7 3 5 2439.93 2443.14 80.49 o 9 3 5 167.45 165.41 9.26 o 11 3 5 45.32 46.94 10.88 o 2 4 5 617.88 676.78 34.12 o 4 4 5 3.85 4.59 7.59 o 6 4 5 23.77 23.33 8.87 o 8 4 5 32.97 53.39 9.64 o 10 4 5 27.08 29.61 8.98 o 1 5 5 640.39 614.51 28.36 o 3 5 5 5049.97 5068.15 220.53 o 5 5 5 387.90 412.66 16.78 o 7 5 5 536.99 568.80 21.68 o 9 5 5 369.49 404.39 13.62 o 2 6 5 578.65 632.25 28.43 o 4 6 5 154.84 171.00 10.01 o 6 6 5 12.67 12.60 8.80 o 8 6 5 48.32 54.64 8.71 o 10 6 5 5.10 0.00 9.88 o 1 7 5 951.33 1001.37 45.22 o 3 7 5 19.51 9.41 9.24 o 5 7 5 956.97 978.18 36.60 o 7 7 5 3.16 13.95 10.31 o 9 7 5 56.79 40.00 9.97 o 2 8 5 58.15 60.68 9.40 o 4 8 5 20.58 22.84 8.47 o 6 8 5 2.79 0.00 9.51 o 8 8 5 3.14 1.60 9.09 o 10 8 5 0.17 4.49 11.22 o 1 9 5 18.21 9.29 9.61 o 3 9 5 1715.76 1874.84 82.94 o 5 9 5 8.37 4.73 8.08 o 7 9 5 101.98 74.10 9.09 o 9 9 5 40.32 32.50 9.02 o 2 10 5 166.49 159.89 8.64 o 4 10 5 65.26 71.51 8.10 o 6 10 5 42.91 46.17 8.15 o 8 10 5 2.93 15.73 10.25 o 1 11 5 688.90 687.98 36.33 o 3 11 5 385.97 390.33 14.88 o 5 11 5 328.97 350.35 16.46 o 7 11 5 307.65 311.97 12.87 o 2 12 5 0.03 0.00 9.43 o 4 12 5 1.90 5.29 10.42 o 6 12 5 59.04 52.31 9.73 o 8 12 5 1.97 0.00 11.02 o 1 13 5 838.38 920.59 49.22 o 3 13 5 143.39 126.43 8.89 o 5 13 5 366.51 374.92 20.36 o 7 13 5 193.42 174.59 11.38 o 2 14 5 0.08 0.00 8.54 o 4 14 5 9.80 5.63 10.14 o 6 14 5 1.57 0.38 12.00 o 1 15 5 15.99 14.63 10.69 o 3 15 5 47.55 33.90 9.98 o 5 15 5 32.90 27.22 12.39 o 2 16 5 5.49 4.92 9.82 o 4 16 5 0.00 9.60 11.26 o 1 17 5 14.08 4.27 10.67 o 0 0 6 3090.99 3211.96 781.04 o 2 0 6 1935.62 1663.02 121.61 o 4 0 6 3366.42 3144.18 129.67 o 6 0 6 594.06 606.55 29.64 o 8 0 6 749.58 812.43 33.31 o 10 0 6 116.68 154.09 15.91 o 1 1 6 999.25 962.31 56.48 o 3 1 6 25.89 26.28 8.79 o 5 1 6 56.72 46.05 9.47 o 7 1 6 1.92 3.16 7.93 o 9 1 6 309.74 311.14 11.37 o 11 1 6 23.63 18.04 11.66 o 0 2 6 2518.09 3016.32 333.72 o 2 2 6 775.26 786.63 29.10 o 4 2 6 1924.81 1831.24 57.31 o 6 2 6 296.18 253.71 9.09 o 8 2 6 357.62 371.24 14.22 o 10 2 6 42.75 49.05 9.87 o 1 3 6 255.32 312.64 19.07 o 3 3 6 74.46 56.68 9.05 o 5 3 6 765.37 716.72 28.01 o 7 3 6 172.69 176.05 9.75 o 9 3 6 55.66 51.74 9.51 o 0 4 6 237.12 240.49 15.67 o 2 4 6 115.83 118.31 9.60 o 4 4 6 21.05 31.49 9.33 o 6 4 6 30.11 28.68 9.04 o 8 4 6 14.45 20.40 8.67 o 10 4 6 7.88 0.64 9.40 o 1 5 6 73.01 98.35 9.84 o 3 5 6 218.43 272.53 13.91 o 5 5 6 114.07 104.77 8.76 o 7 5 6 92.01 111.45 10.39 o 9 5 6 0.00 9.18 10.74 o 0 6 6 620.87 624.22 45.31 o 2 6 6 1047.57 1130.44 55.00 o 4 6 6 329.55 331.19 14.62 o 6 6 6 731.05 770.86 28.32 o 8 6 6 45.75 48.26 8.25 o 10 6 6 118.80 137.07 11.15 o 1 7 6 2509.84 2706.35 119.67 o 3 7 6 549.57 609.60 26.49 o 5 7 6 63.63 57.07 8.02 o 7 7 6 0.01 0.00 9.15 o 9 7 6 16.18 13.21 10.20 o 0 8 6 1477.09 1585.38 112.98 o 2 8 6 1697.37 1783.66 78.64 o 4 8 6 471.52 432.12 19.14 o 6 8 6 910.73 933.20 36.93 o 8 8 6 109.69 110.69 10.00 o 1 9 6 776.81 830.93 40.78 o 3 9 6 596.17 571.53 26.24 o 5 9 6 15.55 3.71 9.17 o 7 9 6 18.96 18.10 9.87 o 9 9 6 33.81 34.98 11.10 o 0 10 6 115.82 122.82 13.58 o 2 10 6 750.97 767.32 32.77 o 4 10 6 165.71 216.94 11.45 o 6 10 6 277.31 295.82 14.45 o 8 10 6 46.38 48.94 9.89 o 1 11 6 17.18 8.86 9.36 o 3 11 6 62.80 60.18 9.61 o 5 11 6 129.04 139.64 9.23 o 7 11 6 77.51 66.11 10.60 o 0 12 6 60.44 55.77 14.59 o 2 12 6 49.08 38.88 9.02 o 4 12 6 6.34 2.04 8.60 o 6 12 6 4.04 5.80 10.09 o 1 13 6 40.01 32.67 10.48 o 3 13 6 26.55 17.41 9.10 o 5 13 6 3.02 0.00 10.35 o 7 13 6 39.35 38.88 10.45 o 0 14 6 223.37 193.84 15.92 o 2 14 6 90.70 95.36 9.61 o 4 14 6 156.41 149.39 10.79 o 6 14 6 35.78 13.26 11.32 o 1 15 6 0.03 0.67 11.00 o 3 15 6 12.55 14.76 9.62 o 5 15 6 6.67 3.46 10.97 o 0 16 6 160.41 164.33 17.81 o 2 16 6 133.36 103.75 12.66 o 1 1 7 547.39 472.68 30.27 o 3 1 7 86.99 76.25 11.78 o 5 1 7 880.67 861.31 33.55 o 7 1 7 14.02 10.05 10.71 o 9 1 7 91.73 95.88 9.75 o 2 2 7 76.39 62.47 10.67 o 4 2 7 127.34 101.16 9.62 o 6 2 7 65.93 66.46 8.43 o 8 2 7 0.36 7.29 9.74 o 10 2 7 7.37 9.67 11.74 o 1 3 7 2391.12 2560.06 169.46 o 3 3 7 97.48 101.33 10.56 o 5 3 7 2824.88 2677.48 92.68 o 7 3 7 12.31 4.86 9.41 o 9 3 7 315.59 315.42 12.73 o 2 4 7 56.24 67.03 12.47 o 4 4 7 0.47 2.44 10.28 o 6 4 7 75.87 91.09 9.48 o 8 4 7 76.94 54.42 9.82 o 10 4 7 5.91 10.53 11.49 o 1 5 7 2269.63 2357.32 121.56 o 3 5 7 421.70 473.24 24.45 o 5 5 7 1140.01 1208.34 53.85 o 7 5 7 399.61 477.10 23.50 o 9 5 7 139.09 123.69 10.19 o 2 6 7 92.37 79.70 9.96 o 4 6 7 9.90 15.21 8.72 o 6 6 7 15.02 13.14 9.29 o 8 6 7 44.10 26.76 9.14 o 1 7 7 13.34 15.67 10.80 o 3 7 7 582.65 607.83 31.00 o 5 7 7 5.69 9.87 9.68 o 7 7 7 172.52 145.57 9.22 o 9 7 7 13.18 21.99 12.67 o 2 8 7 58.78 49.51 8.95 o 4 8 7 27.96 22.42 9.05 o 6 8 7 4.18 4.63 9.39 o 8 8 7 11.87 13.00 11.01 o 1 9 7 301.09 288.05 12.62 o 3 9 7 80.31 98.89 10.53 o 5 9 7 328.34 300.34 15.60 o 7 9 7 8.06 8.96 12.38 o 2 10 7 25.46 24.47 10.22 o 4 10 7 0.03 0.00 10.38 o 6 10 7 10.58 6.70 10.73 o 8 10 7 14.41 23.68 11.49 o 1 11 7 439.81 484.22 20.14 o 3 11 7 403.09 411.31 18.90 o 5 11 7 321.23 354.17 15.26 o 7 11 7 72.50 64.66 11.04 o 2 12 7 19.26 14.98 9.88 o 4 12 7 23.87 19.32 10.51 o 6 12 7 41.63 42.09 10.56 o 1 13 7 149.63 164.06 9.88 o 3 13 7 351.94 332.29 16.57 o 5 13 7 124.81 93.79 10.50 o 2 14 7 0.41 0.28 10.09 o 4 14 7 3.11 1.45 11.09 o 1 15 7 50.72 40.48 10.13 o 3 15 7 12.48 15.18 12.11 o 2 0 8 1597.94 1619.60 127.45 o 4 0 8 637.59 615.11 35.74 o 6 0 8 555.71 647.05 43.38 o 8 0 8 816.66 909.27 40.53 o 1 1 8 0.07 3.54 17.52 o 3 1 8 81.44 98.31 11.62 o 5 1 8 1.00 0.00 9.18 o 7 1 8 203.87 197.91 9.43 o 9 1 8 2.37 0.00 10.01 o 0 2 8 567.27 631.77 62.73 o 2 2 8 333.66 364.07 20.80 o 4 2 8 734.18 705.67 27.50 o 6 2 8 27.83 25.18 9.03 o 8 2 8 376.44 381.72 11.58 o 1 3 8 0.00 0.00 13.55 o 3 3 8 49.00 41.54 10.05 o 5 3 8 28.42 23.87 8.17 o 7 3 8 107.60 120.99 9.61 o 9 3 8 19.50 11.57 10.01 o 0 4 8 128.64 130.15 18.93 o 2 4 8 81.11 67.81 12.25 o 4 4 8 438.78 439.79 19.40 o 6 4 8 121.44 97.14 10.04 o 8 4 8 1.63 0.00 9.73 o 1 5 8 47.66 38.99 14.04 o 3 5 8 19.27 15.20 10.15 o 5 5 8 93.02 104.82 9.92 o 7 5 8 12.55 11.03 8.64 o 9 5 8 21.03 24.68 11.08 o 0 6 8 16.53 16.40 16.96 o 2 6 8 1934.97 1859.51 101.36 o 4 6 8 206.78 246.49 11.67 o 6 6 8 134.66 138.41 9.95 o 8 6 8 131.40 118.31 10.01 o 1 7 8 430.24 432.42 21.58 o 3 7 8 134.91 126.20 10.64 o 5 7 8 137.04 139.62 9.40 o 7 7 8 17.65 12.00 9.42 o 0 8 8 34.95 33.90 12.85 o 2 8 8 1189.77 1218.71 55.67 o 4 8 8 354.29 379.49 19.72 o 6 8 8 209.89 214.26 11.40 o 8 8 8 111.28 101.46 12.63 o 1 9 8 521.45 563.01 21.68 o 3 9 8 123.03 108.38 10.09 o 5 9 8 67.97 49.04 10.00 o 7 9 8 27.74 35.06 11.55 o 0 10 8 728.27 770.31 44.85 o 2 10 8 216.44 251.86 13.74 o 4 10 8 27.53 27.91 9.50 o 6 10 8 362.71 403.04 25.28 o 1 11 8 12.81 17.90 10.68 o 3 11 8 2.49 3.20 9.87 o 5 11 8 15.46 11.02 9.93 o 0 12 8 7.59 2.11 14.49 o 2 12 8 2.85 4.59 10.69 o 4 12 8 27.34 16.41 10.60 o 6 12 8 36.56 42.94 11.84 o 1 13 8 89.70 78.58 11.27 o 3 13 8 6.30 4.27 10.45 o 5 13 8 6.56 5.98 11.72 o 0 14 8 273.09 270.52 22.34 o 2 14 8 7.48 3.22 11.05 o 1 15 8 12.69 15.76 11.34 o 1 1 9 54.01 35.79 21.36 o 3 1 9 756.85 743.92 38.47 o 5 1 9 0.71 0.00 10.44 o 7 1 9 68.19 61.26 11.55 o 9 1 9 30.12 29.18 11.58 o 2 2 9 43.73 37.65 16.03 o 4 2 9 6.85 13.18 11.03 o 6 2 9 0.24 3.33 8.97 o 8 2 9 43.86 38.44 10.14 o 1 3 9 258.56 270.25 16.47 o 3 3 9 1612.29 1601.30 88.28 o 5 3 9 19.57 29.88 10.11 o 7 3 9 432.91 439.25 17.62 o 9 3 9 80.99 99.80 11.50 o 2 4 9 4.65 5.48 13.24 o 4 4 9 128.85 142.94 11.81 o 6 4 9 6.95 8.56 10.05 o 8 4 9 27.32 29.16 10.10 o 1 5 9 939.17 928.02 54.53 o 3 5 9 337.74 373.72 16.85 o 5 5 9 299.27 312.75 13.67 o 7 5 9 398.31 403.43 16.82 o 2 6 9 17.93 12.28 12.82 o 4 6 9 114.89 122.79 10.90 o 6 6 9 1.35 3.24 9.45 o 8 6 9 9.91 14.77 11.30 o 1 7 9 115.79 132.16 12.68 o 3 7 9 0.35 1.40 11.46 o 5 7 9 145.27 137.28 9.34 o 7 7 9 5.71 15.31 9.59 o 2 8 9 20.98 20.59 11.17 o 4 8 9 9.04 7.76 10.25 o 6 8 9 0.29 3.83 10.10 o 1 9 9 56.98 52.22 9.80 o 3 9 9 18.61 11.69 10.35 o 5 9 9 1.16 5.62 11.12 o 7 9 9 88.27 79.35 11.49 o 2 10 9 29.03 18.46 9.70 o 4 10 9 107.89 88.10 11.34 o 6 10 9 4.73 4.61 11.51 o 1 11 9 201.30 188.66 11.56 o 3 11 9 256.03 259.36 13.34 o 5 11 9 97.16 78.79 11.47 o 2 12 9 0.60 1.74 10.00 o 4 12 9 44.28 37.83 12.22 o 1 13 9 74.00 55.97 12.34 o 3 13 9 168.45 157.73 13.54 o 2 0 10 185.40 172.88 58.92 o 4 0 10 392.23 401.02 27.03 o 6 0 10 765.18 819.46 47.34 o 8 0 10 1.51 0.00 18.37 o 1 1 10 100.10 77.21 58.28 o 3 1 10 99.14 80.87 15.46 o 5 1 10 10.34 11.63 10.04 o 7 1 10 56.50 52.58 11.22 o 0 2 10 305.22 274.76 28.84 o 2 2 10 262.03 274.10 19.56 o 4 2 10 89.64 103.87 12.33 o 6 2 10 349.20 405.82 18.27 o 8 2 10 0.05 0.00 11.06 o 1 3 10 12.76 6.84 16.80 o 3 3 10 105.63 92.02 14.19 o 5 3 10 55.31 46.57 10.69 o 7 3 10 29.96 17.83 10.38 o 0 4 10 341.50 360.84 30.05 o 2 4 10 289.71 279.05 16.45 o 4 4 10 78.30 68.25 11.78 o 6 4 10 7.44 9.71 11.78 o 8 4 10 0.00 1.85 11.70 o 1 5 10 20.96 28.28 16.27 o 3 5 10 9.44 11.85 13.68 o 5 5 10 27.29 24.66 11.69 o 7 5 10 0.01 0.00 13.40 o 0 6 10 1224.39 1258.55 135.88 o 2 6 10 11.46 18.64 15.65 o 4 6 10 457.93 412.00 15.69 o 6 6 10 58.48 40.37 10.46 o 1 7 10 14.82 10.61 14.77 o 3 7 10 31.50 24.21 11.42 o 5 7 10 0.94 4.32 10.80 o 7 7 10 2.29 0.00 12.03 o 0 8 10 606.73 606.97 66.47 o 2 8 10 78.45 75.56 13.34 o 4 8 10 386.41 375.66 17.32 o 6 8 10 76.13 72.44 13.72 o 1 9 10 15.05 17.09 16.66 o 3 9 10 6.99 7.78 13.29 o 5 9 10 51.51 51.01 11.97 o 0 10 10 92.48 75.74 17.51 o 2 10 10 94.48 96.20 12.11 o 4 10 10 126.42 116.36 13.19 o 1 11 10 0.42 0.00 11.07 o 3 11 10 16.18 19.79 13.28 o 0 12 10 3.43 0.00 17.39 o 2 12 10 0.01 0.00 12.22 o 3 1 11 0.56 1.91 19.26 o 5 1 11 62.48 50.40 13.09 o 7 1 11 18.68 19.69 13.13 o 2 2 11 54.34 52.08 20.53 o 4 2 11 5.65 4.72 16.12 o 6 2 11 15.49 6.56 12.36 o 1 3 11 399.17 371.44 21.09 o 3 3 11 102.38 87.31 15.92 o 5 3 11 283.89 289.85 16.94 o 7 3 11 68.94 79.95 12.41 o 2 4 11 13.32 8.90 15.57 o 4 4 11 0.05 0.00 14.15 o 6 4 11 94.07 91.13 14.46 o 1 5 11 158.45 166.82 16.32 o 3 5 11 280.45 257.96 19.07 o 5 5 11 149.41 122.21 12.66 o 2 6 11 2.81 0.00 15.99 o 4 6 11 0.89 0.00 13.60 o 6 6 11 76.30 78.11 12.53 o 1 7 11 26.79 22.52 15.34 o 3 7 11 53.29 55.19 17.79 o 5 7 11 13.59 19.24 13.29 o 2 8 11 6.77 0.00 14.35 o 4 8 11 1.60 0.00 15.35 o 1 9 11 7.73 6.22 16.32 o 3 9 11 59.34 53.82 15.69 o 2 10 11 20.08 21.56 14.91 o 1 11 11 75.06 60.80 19.76 o 4 0 12 73.95 67.66 29.61 o 6 0 12 26.77 28.28 18.98 o 3 1 12 11.73 10.84 38.69 o 5 1 12 119.97 119.11 15.92 o 2 2 12 320.28 351.51 50.96 o 4 2 12 18.57 16.60 18.34 o 1 3 12 68.79 53.11 24.81 o 3 3 12 27.54 19.29 19.83 o 5 3 12 28.41 17.44 17.37 o 0 4 12 107.69 99.31 27.06 o 2 4 12 43.62 33.00 18.54 o 4 4 12 9.32 12.37 17.74 o 1 5 12 34.77 26.37 17.72 o 3 5 12 32.17 18.74 16.48 o 5 5 12 1.82 0.00 16.53 o 0 6 12 1.26 0.00 24.84 o 2 6 12 182.66 143.60 18.14 o 4 6 12 19.06 21.12 17.50 o 1 7 12 2.05 1.32 16.39 o 3 7 12 24.06 33.30 19.69 o 0 8 12 185.44 166.48 33.04 o 2 8 12 92.39 68.49 18.93 o 1 9 12 4.31 14.74 16.49 o 3 3 13 33.24 23.23 30.77 o 2 4 13 0.04 0.82 26.04 o 1 5 13 59.88 63.66 22.21 o