#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2201489.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201489_Fobs loop_ _publ_author_name 'Olmstead, Marilyn M.' 'By, Kolbot' 'Nantz, Michael H.' _publ_section_title ; A long thin molecule, 2,6-dimethyl-6-tetradecyl-2-tetradecyloxy-1,3,6-dioxazocan-6-ium iodide ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1323 _journal_page_last o1324 _journal_volume 58 _journal_year 2002 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 85.527 _cell_angle_beta 88.810 _cell_angle_gamma 87.880 _cell_length_a 6.0194 _cell_length_b 7.2183 _cell_length_c 42.3836 _exptl_crystal_F_000 732.00 _reflns_d_resolution_high 0.7107 _[local]_cod_data_source_file fl6005Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mn1259 in P-1; Kolbot's' _shelx_refln_list_code 4 _shelx_f_calc_maximum 371.38 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 77.64 93.92 13.63 o 3 0 0 1747.47 1650.32 48.38 o 4 0 0 3171.72 3267.83 80.59 o 5 0 0 32.42 24.72 15.43 o 6 0 0 242.59 277.57 32.96 o 7 0 0 859.47 899.08 78.34 o -8 1 0 121.42 118.34 50.78 o -7 1 0 234.69 261.55 57.22 o -6 1 0 1673.35 1744.69 65.61 o 0 1 0 506.79 537.92 12.13 o 3 1 0 665.59 733.71 35.05 o 4 1 0 404.99 388.72 29.96 o 5 1 0 1773.83 1714.73 60.67 o 6 1 0 1773.40 1797.27 68.46 o 7 1 0 118.05 172.12 46.44 o -8 2 0 222.64 148.30 57.67 o -7 2 0 176.99 189.19 56.47 o -6 2 0 1.55 5.54 39.10 o -5 2 0 3138.62 3033.70 85.08 o -4 2 0 2491.61 2364.25 51.83 o -3 2 0 1345.25 1633.39 46.74 o -1 2 0 8240.13 8720.16 106.81 o 0 2 0 367.94 365.96 15.13 o 4 2 0 2263.90 2273.03 65.16 o 5 2 0 1493.69 1549.65 59.32 o 6 2 0 224.93 250.16 27.11 o 7 2 0 1256.79 1335.29 59.62 o -7 3 0 531.52 529.23 75.50 o -6 3 0 1020.63 1009.78 86.28 o -5 3 0 201.78 214.36 29.81 o -4 3 0 666.21 591.55 36.10 o -2 3 0 2979.90 3008.08 56.02 o -1 3 0 0.78 3.15 9.14 o 0 3 0 956.49 940.88 24.42 o 1 3 0 3669.67 3565.78 70.25 o 3 3 0 724.19 736.70 23.97 o 4 3 0 882.78 761.42 28.91 o 5 3 0 896.73 996.90 47.64 o 6 3 0 401.31 544.21 41.79 o 7 3 0 320.98 290.31 35.50 o -7 4 0 60.47 149.05 59.02 o -6 4 0 192.63 143.21 49.58 o -5 4 0 1908.86 1913.96 71.75 o -3 4 0 618.32 639.04 39.25 o -2 4 0 1355.80 1275.82 36.10 o -1 4 0 4615.53 4788.87 71.75 o 0 4 0 3004.81 3129.27 52.73 o 1 4 0 104.75 143.81 15.88 o 3 4 0 2322.87 2230.78 49.88 o 4 4 0 239.63 285.21 30.71 o 5 4 0 271.86 302.89 28.01 o 6 4 0 1099.18 1094.72 53.78 o 7 4 0 336.30 305.29 57.37 o -7 5 0 820.62 849.65 101.41 o -6 5 0 677.79 713.04 88.08 o -5 5 0 214.08 195.04 55.87 o -4 5 0 773.59 760.82 47.19 o -3 5 0 4130.03 4123.77 106.51 o -2 5 0 414.13 456.28 26.51 o -1 5 0 317.66 327.76 23.97 o 0 5 0 2565.62 2578.31 55.87 o 1 5 0 3507.78 3471.70 65.61 o 2 5 0 217.74 264.84 29.36 o 3 5 0 771.19 699.85 42.69 o 4 5 0 2098.84 1954.56 69.96 o 5 5 0 788.59 718.28 74.45 o 6 5 0 0.42 -0.15 40.15 o 7 5 0 262.36 267.39 60.82 o -6 6 0 3015.13 3129.87 165.38 o -5 6 0 592.88 740.30 87.93 o -4 6 0 475.95 403.40 42.99 o -3 6 0 267.55 316.07 38.50 o -2 6 0 1058.68 1178.31 56.47 o -1 6 0 1594.52 1667.84 63.96 o 0 6 0 64.38 95.57 17.98 o 1 6 0 990.29 924.70 49.28 o 2 6 0 1516.52 1321.51 57.97 o 3 6 0 674.23 738.20 46.29 o 4 6 0 9.23 -17.83 37.30 o 5 6 0 1039.59 887.40 82.69 o 6 6 0 464.20 442.95 69.51 o -5 7 0 199.88 241.47 64.71 o -4 7 0 959.64 1011.13 94.52 o -3 7 0 878.13 902.68 58.57 o -2 7 0 5.62 -0.90 27.41 o -1 7 0 874.29 827.93 52.43 o 0 7 0 680.06 711.69 51.08 o 1 7 0 850.90 819.84 51.98 o 2 7 0 45.80 58.57 28.31 o 3 7 0 473.34 429.77 70.11 o 4 7 0 666.43 632.00 75.65 o 5 7 0 177.26 148.60 51.38 o 6 7 0 118.40 147.25 58.27 o -4 8 0 0.75 60.67 56.62 o -3 8 0 767.13 825.53 58.57 o -2 8 0 1178.22 1201.52 65.91 o -1 8 0 350.91 294.35 41.34 o 0 8 0 131.23 157.29 35.50 o 1 8 0 999.53 923.05 59.17 o 2 8 0 499.92 540.32 50.03 o 3 8 0 186.25 153.54 52.28 o 4 8 0 70.64 124.93 54.68 o 5 8 0 1057.43 954.96 102.16 o -3 9 0 190.99 139.91 58.42 o -2 9 0 94.63 101.56 35.65 o -1 9 0 625.80 719.48 60.37 o 0 9 0 1138.53 1213.66 69.21 o 1 9 0 0.35 38.65 32.96 o 2 9 0 149.25 159.98 57.97 o 3 9 0 1267.04 1272.38 110.40 o 4 9 0 492.36 547.06 88.68 o -1 10 0 21.15 52.88 33.11 o 0 10 0 189.64 236.08 44.64 o 1 10 0 658.62 707.79 94.37 o -1 -10 1 54.10 35.50 52.88 o 0 -10 1 298.94 354.12 73.85 o -4 -9 1 147.50 179.91 68.01 o -3 -9 1 31.04 66.51 49.88 o -2 -9 1 656.51 664.65 88.08 o -1 -9 1 759.65 795.42 93.17 o 0 -9 1 2069.09 2082.18 87.63 o 1 -9 1 27.04 35.50 30.71 o 2 -9 1 645.24 640.53 58.12 o 3 -9 1 613.89 722.62 91.08 o -5 -8 1 14.81 -28.46 41.34 o -4 -8 1 529.21 507.36 74.90 o -3 -8 1 975.53 990.01 90.78 o -2 -8 1 556.87 651.62 80.59 o -1 -8 1 90.07 92.72 32.36 o 0 -8 1 982.72 1025.36 61.27 o 1 -8 1 1976.92 1971.33 80.59 o 2 -8 1 455.63 421.98 46.89 o 3 -8 1 93.43 118.34 34.60 o 4 -8 1 769.35 909.87 100.51 o -6 -7 1 585.86 614.02 85.68 o -5 -7 1 420.33 393.82 72.35 o -4 -7 1 336.89 285.36 61.57 o -3 -7 1 181.93 182.00 50.63 o -2 -7 1 1531.49 1559.99 66.36 o -1 -7 1 1365.46 1385.18 63.51 o 0 -7 1 317.40 377.79 41.19 o 1 -7 1 128.16 155.64 33.55 o 2 -7 1 894.03 875.27 54.68 o 3 -7 1 1397.44 1407.95 67.41 o 4 -7 1 21.90 35.80 50.18 o 5 -7 1 1118.59 1165.42 104.71 o -6 -6 1 20.40 46.74 49.13 o -5 -6 1 299.43 253.61 54.98 o -4 -6 1 1156.10 984.02 84.19 o -3 -6 1 829.98 899.38 50.93 o -2 -6 1 57.05 41.79 21.57 o -1 -6 1 515.95 618.96 44.19 o 0 -6 1 4073.22 4007.08 79.39 o 1 -6 1 285.68 281.47 34.30 o 2 -6 1 114.72 96.02 27.86 o 3 -6 1 765.90 843.81 51.23 o 4 -6 1 1692.24 1639.98 70.70 o 5 -6 1 52.24 38.20 48.38 o 6 -6 1 5.31 12.43 48.53 o -7 -5 1 284.12 341.99 66.51 o -6 -5 1 774.78 706.29 80.59 o -5 -5 1 337.27 348.28 59.02 o -4 -5 1 88.49 91.98 25.32 o -3 -5 1 518.47 519.35 38.20 o -1 -5 1 1511.96 1425.92 38.65 o 0 -5 1 39.80 28.01 14.23 o 1 -5 1 2116.75 2004.74 42.69 o 2 -5 1 9322.16 9834.50 153.84 o 3 -5 1 30.58 33.70 23.22 o 4 -5 1 10.96 13.78 16.33 o 5 -5 1 1090.70 1040.94 89.13 o 6 -5 1 545.67 602.93 79.39 o 7 -5 1 0.57 -42.09 41.49 o -7 -4 1 144.35 160.73 31.46 o -6 -4 1 2.42 44.04 24.57 o -5 -4 1 1336.69 1295.60 45.24 o -4 -4 1 3372.35 3363.40 89.43 o -3 -4 1 883.02 855.94 31.01 o -2 -4 1 3.60 41.19 11.83 o -1 -4 1 4256.14 4482.24 76.10 o 0 -4 1 5544.34 5765.85 81.94 o 1 -4 1 949.79 932.94 28.91 o 2 -4 1 998.55 975.63 32.06 o 3 -4 1 1290.48 1294.70 50.93 o 4 -4 1 2003.34 1943.02 67.11 o 5 -4 1 87.92 157.59 29.06 o 6 -4 1 404.75 438.61 70.40 o 7 -4 1 1812.07 1863.33 124.03 o -7 -3 1 483.12 582.71 45.54 o -6 -3 1 5092.92 5240.21 122.23 o -5 -3 1 561.57 528.64 25.77 o -4 -3 1 854.55 860.14 28.31 o -3 -3 1 4897.03 5077.98 72.65 o -2 -3 1 1003.55 1039.74 30.41 o 0 -3 1 3481.56 3546.45 52.73 o 1 -3 1 4637.39 4658.55 66.06 o 2 -3 1 3381.09 3354.56 60.82 o 3 -3 1 92.47 88.98 17.08 o 4 -3 1 944.42 994.36 45.69 o 5 -3 1 2256.57 2225.99 73.40 o 6 -3 1 1039.82 914.81 83.44 o 7 -3 1 696.15 633.19 83.89 o -7 -2 1 74.93 74.15 27.11 o -6 -2 1 99.36 112.65 22.47 o -5 -2 1 3719.31 3660.75 94.52 o -3 -2 1 345.64 411.04 23.07 o -2 -2 1 14.61 1.50 8.54 o -1 -2 1 10795.09 11359.44 155.04 o 0 -2 1 6299.79 6577.45 82.09 o 1 -2 1 320.66 367.60 15.28 o 3 -2 1 6529.15 6737.89 105.91 o 4 -2 1 406.33 439.06 24.27 o 5 -2 1 483.39 485.79 38.50 o 6 -2 1 780.30 719.63 77.89 o 7 -2 1 818.10 799.62 88.08 o 8 -2 1 64.16 121.79 54.68 o -7 -1 1 1032.40 980.87 55.43 o -6 -1 1 1013.55 977.73 52.43 o -5 -1 1 869.99 858.94 45.39 o -4 -1 1 641.09 620.16 36.40 o -3 -1 1 5628.54 5886.74 115.34 o -1 -1 1 32004.21 34089.69 440.70 o 0 -1 1 141.07 154.44 7.94 o 1 -1 1 9886.73 10542.74 143.96 o 2 -1 1 526.51 522.49 19.92 o 3 -1 1 1691.25 1822.73 41.19 o 4 -1 1 93.76 106.66 15.73 o 5 -1 1 627.75 619.41 30.26 o 6 -1 1 233.53 259.60 32.66 o 7 -1 1 338.81 387.08 62.77 o 8 -1 1 927.03 1027.46 92.72 o -7 0 1 72.48 116.39 41.49 o -6 0 1 1421.04 1490.48 61.87 o -5 0 1 3212.98 3253.30 87.03 o -4 0 1 1684.46 1726.41 56.17 o -3 0 1 287.16 303.34 23.97 o -2 0 1 9474.47 9985.04 171.67 o 1 0 1 471.14 449.99 16.93 o 4 0 1 415.42 520.85 51.38 o 5 0 1 786.43 813.10 43.14 o 7 0 1 665.71 657.61 73.70 o 8 0 1 1.99 37.75 39.40 o -8 1 1 682.42 700.90 82.84 o -7 1 1 871.90 851.75 78.49 o -6 1 1 130.34 46.59 18.57 o -5 1 1 45.68 40.30 19.02 o -4 1 1 13652.07 13990.93 202.83 o -3 1 1 5276.32 5434.50 87.33 o -2 1 1 214.73 306.04 29.66 o -1 1 1 6547.21 6714.97 115.19 o 0 1 1 288.12 306.93 10.19 o 2 1 1 1222.22 1367.95 39.25 o 3 1 1 2826.25 2952.96 69.96 o 4 1 1 2674.46 2534.57 68.91 o 5 1 1 773.72 736.85 42.69 o 6 1 1 562.87 541.67 43.44 o 7 1 1 883.00 922.45 79.09 o -8 2 1 86.47 22.17 45.99 o -7 2 1 208.95 211.96 56.77 o -6 2 1 1238.38 1172.61 55.57 o -4 2 1 284.43 336.00 25.47 o -3 2 1 5232.23 5216.24 102.61 o -2 2 1 3217.06 3063.96 53.33 o -1 2 1 4082.41 4467.86 69.21 o 0 2 1 497.70 508.56 17.68 o 1 2 1 4692.60 4771.65 71.30 o 2 2 1 992.97 886.05 24.42 o 3 2 1 3755.50 4131.71 70.70 o 4 2 1 770.54 781.64 40.00 o 5 2 1 3234.32 3303.78 89.43 o 6 2 1 766.80 796.17 37.45 o 7 2 1 80.63 76.85 44.49 o -7 3 1 817.45 740.90 85.08 o -6 3 1 256.27 286.41 59.02 o -5 3 1 1121.93 1080.64 50.93 o -3 3 1 1162.09 1121.68 31.61 o -2 3 1 598.60 609.97 24.87 o -1 3 1 2848.59 2846.00 53.03 o 0 3 1 5519.04 5800.30 77.15 o 1 3 1 3691.42 4439.40 70.25 o 5 3 1 0.16 8.69 14.98 o 6 3 1 66.46 90.33 20.52 o 7 3 1 708.32 783.29 50.93 o -7 4 1 802.48 720.83 87.18 o -6 4 1 1001.62 987.46 90.03 o -5 4 1 206.45 185.00 29.51 o -4 4 1 618.48 600.69 41.49 o -3 4 1 525.85 536.27 38.35 o -2 4 1 3468.05 3460.47 65.61 o -1 4 1 49.20 41.64 16.03 o 0 4 1 2728.43 2821.28 56.62 o 1 4 1 5206.11 5314.51 85.68 o 2 4 1 1080.21 1095.32 30.86 o 3 4 1 114.55 79.84 19.92 o 4 4 1 2089.12 2058.82 102.76 o 5 4 1 1807.82 1737.80 64.71 o 6 4 1 272.11 289.41 52.58 o 7 4 1 1.93 35.95 38.65 o -7 5 1 119.69 174.96 58.72 o -6 5 1 375.09 389.17 69.06 o -5 5 1 1176.38 1015.63 89.58 o -4 5 1 470.05 479.95 42.39 o -3 5 1 319.81 359.81 37.45 o -2 5 1 680.52 745.69 43.59 o -1 5 1 4611.34 4674.28 109.05 o 0 5 1 1234.36 1206.17 36.85 o 1 5 1 121.15 100.66 15.28 o 2 5 1 2786.56 2687.66 77.15 o 4 5 1 328.96 289.56 33.11 o 5 5 1 12.38 33.70 40.15 o 6 5 1 771.77 694.46 78.04 o 7 5 1 783.87 919.91 91.08 o -6 6 1 434.29 484.00 80.74 o -5 6 1 58.21 42.09 48.68 o -4 6 1 1425.84 1473.86 68.16 o -3 6 1 1386.39 1492.28 65.16 o -2 6 1 1514.59 1527.33 63.96 o -1 6 1 187.77 170.32 29.66 o 0 6 1 3916.81 3949.56 102.76 o 1 6 1 1334.32 1282.86 56.47 o 2 6 1 489.52 569.38 43.74 o 3 6 1 747.66 689.67 69.81 o 4 6 1 1400.24 1368.40 62.47 o 5 6 1 1064.16 1076.89 89.88 o 6 6 1 104.62 153.24 53.33 o 7 6 1 307.04 201.63 61.87 o -5 7 1 735.98 645.48 86.58 o -4 7 1 113.49 140.81 34.60 o -3 7 1 174.82 193.24 37.45 o -2 7 1 547.95 679.63 52.28 o -1 7 1 589.11 684.42 51.38 o 0 7 1 39.82 32.51 26.96 o 1 7 1 589.14 693.26 51.23 o 2 7 1 1617.94 1699.00 71.15 o 4 7 1 9.68 -1.95 39.25 o 5 7 1 152.06 140.81 54.98 o 6 7 1 960.39 1013.53 100.21 o -4 8 1 675.21 651.17 89.73 o -3 8 1 476.25 519.35 51.38 o -2 8 1 96.09 105.31 34.30 o -1 8 1 556.51 618.36 52.73 o 0 8 1 1177.44 1253.50 65.61 o 1 8 1 802.70 791.23 58.42 o 2 8 1 34.67 65.91 32.51 o 3 8 1 578.97 747.64 87.63 o 4 8 1 539.44 699.85 86.88 o 5 8 1 156.66 143.06 61.42 o -3 9 1 411.55 440.10 52.43 o -2 9 1 1125.86 1087.08 67.71 o -1 9 1 439.75 454.04 50.48 o 0 9 1 43.26 58.12 32.06 o 1 9 1 901.40 988.81 65.76 o 2 9 1 1150.92 1107.45 99.17 o 3 9 1 1.56 35.20 50.48 o 4 9 1 48.83 0.15 51.23 o -1 10 1 545.13 565.78 57.07 o 0 10 1 943.66 973.08 69.96 o 1 10 1 43.10 37.15 56.17 o -1 -10 2 676.48 591.10 86.43 o 0 -10 2 660.77 734.31 90.63 o -4 -9 2 101.69 51.98 59.77 o -3 -9 2 827.81 828.38 97.52 o -2 -9 2 545.40 519.35 80.89 o -1 -9 2 111.77 103.36 59.02 o 0 -9 2 47.26 90.48 33.85 o 1 -9 2 529.63 580.91 53.63 o 2 -9 2 480.30 587.95 57.22 o 3 -9 2 4.81 -16.03 47.19 o -5 -8 2 755.82 678.88 88.23 o -4 -8 2 4764.44 4816.44 203.87 o -3 -8 2 0.37 39.40 49.88 o -2 -8 2 149.39 195.04 58.27 o -1 -8 2 1308.22 1303.24 67.11 o 0 -8 2 315.36 313.53 43.74 o 1 -8 2 7.88 -0.75 28.76 o 2 -8 2 907.11 902.38 59.47 o 3 -8 2 1040.94 943.57 60.52 o 4 -8 2 246.98 215.41 63.21 o -6 -7 2 387.96 347.08 68.76 o -5 -7 2 16.48 -10.64 41.19 o -4 -7 2 93.24 12.88 38.80 o -3 -7 2 1710.60 1550.10 102.91 o -2 -7 2 609.14 661.80 73.10 o -1 -7 2 2.52 -0.45 25.17 o 0 -7 2 418.42 416.44 41.79 o 1 -7 2 4406.76 4263.23 115.64 o 2 -7 2 298.27 305.74 39.55 o 3 -7 2 240.06 258.70 37.90 o 4 -7 2 667.25 816.55 93.02 o 5 -7 2 1492.04 1641.48 120.44 o -6 -6 2 294.77 313.53 62.32 o -5 -6 2 1447.10 1222.95 93.62 o -4 -6 2 188.99 159.98 48.98 o -3 -6 2 19.98 40.45 24.42 o -2 -6 2 755.08 737.75 72.95 o -1 -6 2 2872.91 2842.71 83.44 o 0 -6 2 437.75 463.62 29.06 o 1 -6 2 4214.97 4276.57 86.13 o 2 -6 2 2124.70 2138.06 74.60 o 3 -6 2 863.17 884.85 52.13 o 4 -6 2 11.25 39.40 20.82 o 5 -6 2 159.86 165.38 55.13 o 6 -6 2 108.83 85.98 53.78 o -7 -5 2 414.92 435.76 70.55 o -6 -5 2 330.31 377.04 66.51 o -5 -5 2 173.61 191.29 53.18 o -4 -5 2 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