#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/15/2201518.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2201518_Fobs
loop_
_publ_author_name
'Lee, Uk'
_publ_section_title
;
 Pentapotassium trihydrogenhexatungstoplatinate(IV) hexahydrate,
 K~5~[H~3~PtW~6~O~24~]·6H~2~O
;
_journal_issue                   12
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              i130
_journal_page_last               i132
_journal_volume                  58
_journal_year                    2002
_space_group_IT_number           12
_symmetry_space_group_name_Hall  '-C 2y'
_symmetry_space_group_name_H-M   'C 1 2/m 1'
_cell_angle_alpha                90.000
_cell_angle_beta                 101.429
_cell_angle_gamma                90.000
_cell_length_a                   11.4491
_cell_length_b                   19.8290
_cell_length_c                   13.6884
_exptl_crystal_F_000             3488.00
_reflns_d_resolution_high        0.7692
_[local]_cod_data_source_file    mg6017Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' KPtW6 POM'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            1774.23
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z'
'-x, -y, -z'
'x, -y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 3147903.75 3050677.25 13233.51 o
4 0 0 1510298.50 1535886.13 6049.85 o
6 0 0 418530.28 438914.63 3248.17 o
8 0 0 160668.11 168296.23 2351.12 o
10 0 0 4721.52 5224.83 669.53 o
12 0 0 6651.58 9172.21 944.93 o
14 0 0 23114.50 22850.46 1405.47 o
1 1 0 46289.82 51454.46 483.41 o
3 1 0 369834.50 400968.06 2240.90 o
5 1 0 349291.84 354575.13 2650.51 o
7 1 0 386697.72 398235.41 3444.48 o
9 1 0 346134.59 379390.56 3892.22 o
11 1 0 154974.50 167887.78 3005.53 o
13 1 0 30493.20 35147.14 1640.09 o
0 2 0 338167.53 368222.38 1764.60 o
2 2 0 374761.84 368406.72 1926.96 o
4 2 0 60760.02 56991.54 974.97 o
6 2 0 23589.34 25458.71 822.40 o
8 2 0 7656.66 5898.10 595.32 o
10 2 0 22189.92 24306.89 1128.65 o
12 2 0 24466.16 26864.04 1386.54 o
14 2 0 9993.83 9879.88 1073.09 o
1 3 0 5587.39 3379.32 299.28 o
3 3 0 1015.33 916.15 312.48 o
5 3 0 551.75 1038.39 335.48 o
7 3 0 11213.39 8889.00 585.13 o
9 3 0 17343.44 15637.32 889.70 o
11 3 0 34372.18 33833.00 1368.93 o
13 3 0 25101.03 21222.78 1295.61 o
0 4 0 149074.03 170415.03 1495.81 o
2 4 0 442896.22 469288.94 2481.23 o
4 4 0 54761.52 54108.62 991.46 o
6 4 0 130546.45 133954.80 1818.99 o
8 4 0 44752.00 31745.14 1078.02 o
10 4 0 37306.04 41564.63 1444.83 o
12 4 0 7844.04 9143.18 897.09 o
14 4 0 5982.39 4622.63 861.30 o
1 5 0 1787.31 4936.00 426.28 o
3 5 0 351.54 1352.54 333.70 o
5 5 0 5774.13 5781.13 469.17 o
7 5 0 1795.32 2394.96 413.66 o
9 5 0 7815.55 7720.24 692.96 o
11 5 0 25.58 -537.76 537.76 o
13 5 0 252.10 770.28 692.19 o
0 6 0 52649.37 61302.82 1128.13 o
2 6 0 20658.30 15440.26 561.14 o
4 6 0 25844.33 26136.81 759.22 o
6 6 0 8223.88 11975.92 645.28 o
8 6 0 20570.48 21084.91 949.02 o
10 6 0 510.57 1542.39 546.67 o
12 6 0 394.60 115.37 614.10 o
14 6 0 790.72 1315.22 768.54 o
1 7 0 13444.33 10470.46 547.23 o
3 7 0 1135.99 926.72 333.76 o
5 7 0 1069.56 355.04 353.26 o
7 7 0 21805.56 25308.89 974.38 o
9 7 0 123.48 79.87 433.06 o
11 7 0 117.43 465.00 521.79 o
13 7 0 565.15 -133.12 578.62 o
0 8 0 81901.98 79296.02 1446.27 o
2 8 0 208495.53 208084.73 2032.60 o
4 8 0 158170.20 171309.19 2014.04 o
6 8 0 188580.59 188397.58 2424.62 o
8 8 0 88754.81 60089.58 1587.79 o
10 8 0 49218.95 46331.74 1609.10 o
12 8 0 13473.77 14047.31 1169.57 o
1 9 0 2980.52 4971.42 484.89 o
3 9 0 6069.33 6179.40 542.05 o
5 9 0 2086.76 6700.68 575.26 o
7 9 0 234.92 768.51 324.80 o
9 9 0 5132.58 6478.89 706.85 o
11 9 0 8481.22 11588.45 1021.52 o
13 9 0 33391.68 36375.03 1797.02 o
0 10 0 270265.19 274990.47 2983.35 o
2 10 0 116542.41 120136.58 1738.42 o
4 10 0 44541.80 48223.14 1177.88 o
6 10 0 13222.21 13277.66 766.60 o
8 10 0 12238.42 14702.80 910.26 o
10 10 0 25659.16 27535.19 1303.23 o
12 10 0 34955.46 32416.99 1637.24 o
1 11 0 24725.77 32409.90 1027.64 o
3 11 0 230945.08 230450.61 2629.35 o
5 11 0 368359.31 385393.66 3690.16 o
7 11 0 328354.56 356239.44 3863.68 o
9 11 0 215920.95 159361.61 2953.57 o
11 11 0 66799.53 71362.98 2281.73 o
13 11 0 26265.90 25342.66 1722.61 o
0 12 0 1947908.75 2151097.75 10610.30 o
2 12 0 1548607.00 1647187.75 8049.88 o
4 12 0 858954.88 899180.44 5786.23 o
6 12 0 380234.09 389832.78 4025.73 o
8 12 0 88135.94 60534.98 1772.10 o
10 12 0 504.43 976.19 598.14 o
12 12 0 6111.27 6229.98 974.99 o
1 13 0 10757.70 13731.72 835.78 o
3 13 0 168676.27 179037.48 2495.10 o
5 13 0 144587.88 143101.77 2425.15 o
7 13 0 185477.31 146807.77 2636.06 o
9 13 0 142608.53 154680.06 3016.66 o
11 13 0 88413.48 98131.63 2657.34 o
0 14 0 345528.66 380398.81 4253.14 o
2 14 0 104050.88 112188.73 2043.57 o
4 14 0 15846.77 17757.39 937.60 o
6 14 0 1747.29 3632.09 585.82 o
8 14 0 10.50 488.07 537.76 o
10 14 0 1351.31 571.57 631.92 o
12 14 0 6051.74 7314.88 1049.55 o
1 15 0 144.98 120.69 573.27 o
3 15 0 4602.73 5825.37 653.58 o
5 15 0 9304.76 8563.86 764.15 o
7 15 0 15373.67 17053.50 1031.39 o
9 15 0 5744.03 6897.84 804.51 o
11 15 0 9994.68 12196.72 1113.96 o
0 16 0 62685.86 69867.36 1995.80 o
2 16 0 46248.33 50558.95 1549.25 o
4 16 0 38353.56 44171.57 1495.22 o
6 16 0 25912.47 21101.31 1125.40 o
8 16 0 22837.61 23822.85 1270.60 o
10 16 0 8187.53 8053.97 937.91 o
1 17 0 4182.06 4679.35 720.99 o
3 17 0 91.35 628.28 534.22 o
5 17 0 1686.16 3550.34 614.21 o
7 17 0 1063.93 1338.36 500.55 o
9 17 0 995.98 672.72 557.34 o
0 18 0 4442.76 4810.80 824.00 o
2 18 0 9790.40 9017.07 892.11 o
4 18 0 239.45 -386.92 536.00 o
6 18 0 2319.50 484.65 608.92 o
8 18 0 387.26 -94.07 599.90 o
10 18 0 352.87 1327.59 640.72 o
1 19 0 117.10 733.00 647.81 o
3 19 0 3.98 468.54 532.44 o
5 19 0 926.25 1380.94 578.64 o
7 19 0 385.31 -502.29 621.20 o
9 19 0 174.70 -287.52 624.74 o
0 20 0 60804.81 56661.36 2152.94 o
2 20 0 50191.55 52924.23 1910.69 o
4 20 0 45099.43 45105.46 1780.67 o
6 20 0 35707.70 25709.03 1391.65 o
8 20 0 44255.49 40913.98 1964.93 o
1 21 0 107.91 161.51 688.63 o
3 21 0 4715.65 5655.79 841.71 o
5 21 0 1145.66 1759.04 649.65 o
7 21 0 212.44 -521.80 521.80 o
0 22 0 76161.05 81427.50 2735.49 o
2 22 0 28298.74 26550.61 1573.95 o
4 22 0 8084.10 8668.68 1001.87 o
6 22 0 768.52 667.37 694.00 o
1 23 0 8194.98 6885.30 1144.00 o
3 23 0 43388.15 40172.08 1943.61 o
5 23 0 86068.33 90288.38 2840.15 o
0 24 0 379952.31 400595.09 6576.06 o
2 24 0 317086.28 306536.19 5339.55 o
4 24 0 173229.64 172882.72 3945.25 o
1 25 0 2997.11 3062.46 1132.66 o
3 25 0 26400.99 26980.04 1909.48 o
-14 0 1 213677.97 221068.42 4231.11 o
-12 0 1 335447.03 359362.88 4569.05 o
-10 0 1 433342.97 466319.03 4683.79 o
-8 0 1 188586.91 187242.94 2443.29 o
-6 0 1 48524.14 56471.75 1144.72 o
-4 0 1 6097.62 8659.21 464.17 o
-2 0 1 214990.72 179922.00 2059.64 o
0 0 1 521599.16 455246.16 5046.37 o
2 0 1 556181.25 554959.56 2678.54 o
4 0 1 189860.92 182306.75 1768.24 o
6 0 1 15757.37 16472.43 712.32 o
8 0 1 14238.27 13034.52 770.29 o
10 0 1 7423.62 7475.84 769.26 o
12 0 1 7803.24 8922.87 927.28 o
14 0 1 26002.45 24824.91 1566.02 o
-13 1 1 13642.15 16413.35 1231.80 o
-11 1 1 105657.23 114413.37 2473.29 o
-9 1 1 315302.38 330103.88 3537.69 o
-7 1 1 586331.13 579400.50 4160.83 o
-5 1 1 392648.66 392103.84 2979.32 o
-3 1 1 1118154.25 1107020.88 4490.97 o
-1 1 1 800734.63 703945.63 3063.12 o
1 1 1 303295.97 312978.38 1665.45 o
3 1 1 71229.98 68485.70 1008.91 o
5 1 1 221.86 268.01 356.75 o
7 1 1 14184.21 11413.57 617.48 o
9 1 1 6930.48 7911.28 742.63 o
11 1 1 7180.72 6670.32 785.16 o
13 1 1 1190.86 51.48 612.38 o
-14 2 1 13509.57 13217.84 1233.45 o
-12 2 1 57698.06 67228.26 1992.44 o
-10 2 1 66057.15 67463.60 1771.35 o
-8 2 1 50851.12 54324.84 1337.22 o
-6 2 1 34230.48 33246.11 915.60 o
-4 2 1 1128.10 557.49 339.11 o
-2 2 1 19.51 578.59 287.52 o
0 2 1 55.53 385.15 347.88 o
2 2 1 26393.07 24209.05 580.95 o
4 2 1 5479.98 2600.81 382.21 o
6 2 1 313.02 363.86 342.56 o
8 2 1 77030.99 66551.03 1550.92 o
10 2 1 83566.78 89368.29 2085.51 o
12 2 1 73043.12 76954.96 2215.79 o
14 2 1 38670.67 50204.20 2074.10 o
-13 3 1 39637.61 44318.65 1795.06 o
-11 3 1 60325.07 61795.82 1827.73 o
-9 3 1 87555.16 92290.38 1904.32 o
-7 3 1 68497.34 69449.46 1404.05 o
-5 3 1 44283.56 47696.46 996.14 o
-3 3 1 41184.09 35831.82 719.38 o
-1 3 1 35800.82 34147.81 784.05 o
1 3 1 57750.62 49461.64 691.68 o
3 3 1 46634.61 47796.86 853.42 o
5 3 1 7018.45 7315.67 496.01 o
7 3 1 36775.37 38834.75 1093.43 o
9 3 1 12271.42 11736.48 862.32 o
11 3 1 3764.96 5600.29 699.59 o
13 3 1 32.72 70.99 637.15 o
-14 4 1 20746.82 17476.81 1403.34 o
-12 4 1 19822.67 20292.19 1223.90 o
-10 4 1 1215.93 122.48 516.55 o
-8 4 1 69.50 244.92 385.13 o
-6 4 1 21257.07 25820.08 821.86 o
-4 4 1 36100.68 37691.80 825.00 o
-2 4 1 35397.29 41692.50 726.20 o
0 4 1 12425.33 11812.47 428.83 o
2 4 1 1468.77 3065.11 358.72 o
4 4 1 13445.84 11137.12 550.44 o
6 4 1 6032.95 7052.75 604.17 o
8 4 1 44823.27 45001.95 1320.96 o
10 4 1 724.79 1267.32 489.89 o
12 4 1 266.26 -262.68 555.52 o
14 4 1 1624.80 1572.72 708.26 o
-13 5 1 27666.19 23916.57 1415.23 o
-11 5 1 42823.74 46969.36 1657.60 o
-9 5 1 67402.91 76908.71 1810.29 o
-7 5 1 14047.16 11681.17 670.80 o
-5 5 1 43462.88 45641.78 1032.71 o
-3 5 1 11428.94 16306.48 559.34 o
-1 5 1 24836.26 29149.35 685.19 o
1 5 1 107148.45 100360.05 1105.87 o
3 5 1 78580.04 78902.74 1139.30 o
5 5 1 5658.50 4766.03 458.48 o
7 5 1 2846.29 2171.64 381.77 o
9 5 1 22015.76 19090.99 988.11 o
11 5 1 59520.54 74296.80 2098.71 o
13 5 1 51303.72 51936.32 2089.73 o
-14 6 1 12974.67 12740.47 1160.49 o
-12 6 1 6717.15 8527.36 886.31 o
-10 6 1 5222.96 5679.72 678.44 o
-8 6 1 90.65 129.56 386.91 o
-6 6 1 10412.98 7905.16 604.67 o
-4 6 1 216.02 -344.33 344.33 o
-2 6 1 4972.19 4940.35 412.44 o
0 6 1 61018.07 73636.70 992.96 o
2 6 1 359540.31 371295.84 2456.43 o
4 6 1 386339.03 410255.31 2973.34 o
6 6 1 617046.69 623615.38 4352.73 o
8 6 1 539375.50 334121.31 3693.55 o
10 6 1 323702.50 342429.81 4226.34 o
12 6 1 143251.06 149575.27 3186.56 o
-13 7 1 15732.41 18510.42 1292.46 o
-11 7 1 46506.30 55147.92 1765.20 o
-9 7 1 57543.66 60270.75 1610.32 o
-7 7 1 37373.20 39345.80 1169.89 o
-5 7 1 92.23 -266.22 340.77 o
-3 7 1 196.62 796.92 342.55 o
-1 7 1 27417.97 24566.98 775.22 o
1 7 1 21283.52 22563.53 657.49 o
3 7 1 58809.90 64106.26 1127.83 o
5 7 1 5645.55 7853.61 586.36 o
7 7 1 16673.97 14030.95 763.48 o
9 7 1 38660.21 36603.92 1341.76 o
11 7 1 56872.44 66363.56 2028.02 o
13 7 1 52250.84 46119.21 1973.76 o
-12 8 1 14345.55 14946.58 1167.92 o
-10 8 1 4669.58 4743.30 685.48 o
-8 8 1 2958.02 3322.11 539.78 o
-6 8 1 10051.23 11018.45 666.76 o
-4 8 1 1263.77 1429.11 385.24 o
-2 8 1 22257.99 23652.55 1231.90 o
0 8 1 3852.92 4319.30 415.76 o
2 8 1 12002.95 12416.20 559.03 o
4 8 1 9147.04 11265.45 597.50 o
6 8 1 10041.77 8983.84 627.61 o
8 8 1 20404.87 19986.91 1005.75 o
10 8 1 301.55 -326.57 520.03 o
12 8 1 747.89 1018.81 481.01 o
-13 9 1 42160.06 39819.65 1800.50 o
-11 9 1 37949.01 39141.90 1609.82 o
-9 9 1 47047.30 48940.62 1550.32 o
-7 9 1 16493.64 18136.13 896.84 o
-5 9 1 113181.23 117250.66 1850.76 o
-3 9 1 33206.82 29809.91 983.47 o
-1 9 1 58952.57 60571.30 1314.93 o
1 9 1 43647.68 45804.27 977.84 o
3 9 1 55645.60 56401.20 1171.32 o
5 9 1 99725.85 107794.66 1796.40 o
7 9 1 75426.94 76104.27 1716.42 o
9 9 1 28547.96 31402.28 1286.23 o
11 9 1 10191.71 8662.30 922.20 o
13 9 1 138.11 1254.79 637.16 o
-12 10 1 30199.88 24906.23 1397.83 o
-10 10 1 47458.85 52131.03 1742.34 o
-8 10 1 27875.38 26178.44 1138.58 o
-6 10 1 11290.96 12096.55 780.59 o
-4 10 1 201.16 115.37 447.26 o
-2 10 1 17835.03 18680.68 2325.29 o
0 10 1 18109.84 21431.89 746.77 o
2 10 1 15389.02 16899.40 678.47 o
4 10 1 4527.68 5378.69 520.46 o
6 10 1 2094.27 3385.66 479.35 o
8 10 1 24953.72 15958.90 913.62 o
10 10 1 61340.04 64129.75 1970.31 o
12 10 1 62263.17 66814.89 2263.73 o
-13 11 1 13064.50 13367.91 1228.03 o
-11 11 1 56174.07 60411.09 2023.71 o
-9 11 1 214065.61 223621.91 3422.11 o
-7 11 1 308936.72 306601.25 3634.32 o
-5 11 1 547373.06 562165.25 4645.69 o
-3 11 1 530944.38 541394.56 5728.10 o
-1 11 1 381965.88 393970.63 3730.33 o
1 11 1 31810.55 36954.25 1002.29 o
3 11 1 18771.55 16073.20 733.84 o
5 11 1 3269.01 2876.72 506.09 o
7 11 1 16711.12 17000.81 925.12 o
9 11 1 15147.74 14141.86 1027.79 o
11 11 1 3836.85 3966.58 747.51 o
-12 12 1 212208.03 233807.36 4191.53 o
-10 12 1 222472.98 220880.59 3662.04 o
-8 12 1 99224.52 100861.08 2260.34 o
-6 12 1 42919.66 43694.46 1407.65 o
-4 12 1 12443.62 14001.16 971.12 o
-2 12 1 58720.68 59289.22 2395.69 o
0 12 1 233437.59 246368.34 2711.30 o
2 12 1 220378.14 224585.69 2559.79 o
4 12 1 168915.67 162050.78 2326.80 o
6 12 1 68546.03 45269.35 1387.66 o
8 12 1 4927.22 5585.30 665.97 o
10 12 1 5648.55 5308.32 848.90 o
12 12 1 8707.58 7212.21 911.30 o
-11 13 1 67667.10 69784.14 2245.68 o
-9 13 1 139353.83 142750.78 2887.72 o
-7 13 1 267463.22 263989.13 3609.89 o
-5 13 1 221109.23 230226.47 3294.85 o
-3 13 1 457656.94 497427.19 9765.71 o
-1 13 1 366148.81 389830.38 4076.65 o
1 13 1 159945.58 161622.77 2268.87 o
3 13 1 16852.43 17454.77 841.86 o
5 13 1 2419.27 917.90 504.22 o
7 13 1 2873.89 3360.97 569.93 o
9 13 1 917.86 937.19 509.42 o
11 13 1 2275.73 3339.19 736.72 o
-12 14 1 24020.77 22659.67 1434.02 o
-10 14 1 44507.85 46521.12 1822.96 o
-8 14 1 34018.90 31358.90 1450.84 o
-6 14 1 24130.74 26109.75 1248.32 o
-4 14 1 18902.79 21128.29 1587.74 o
-2 14 1 6072.88 7687.25 1131.68 o
0 14 1 163.39 1251.26 486.30 o
2 14 1 7.31 321.24 401.10 o
4 14 1 10188.87 11230.51 755.46 o
6 14 1 31434.79 32955.71 1310.10 o
8 14 1 20628.54 23723.45 1156.55 o
10 14 1 33272.66 37729.18 1708.32 o
12 14 1 30517.91 30380.68 1719.76 o
-11 15 1 45626.42 46903.75 2038.36 o
-9 15 1 34163.96 35914.28 1641.05 o
-7 15 1 48737.93 50124.92 1734.05 o
-5 15 1 38174.81 41149.88 1718.30 o
-3 15 1 26554.28 18104.72 2811.93 o
-1 15 1 215.36 -612.32 612.32 o
1 15 1 1639.12 2378.83 500.62 o
3 15 1 1982.22 2396.68 518.39 o
5 15 1 4408.30 3573.05 609.12 o
7 15 1 903.55 -221.87 610.60 o
9 15 1 3131.34 3525.99 678.21 o
11 15 1 720.62 979.76 702.87 o
-10 16 1 0.75 301.71 725.89 o
-8 16 1 3702.70 4328.82 783.02 o
-6 16 1 19624.49 19385.35 1339.80 o
-4 16 1 17419.37 16517.30 2008.62 o
-2 16 1 35863.15 38850.87 1848.43 o
0 16 1 21129.18 19611.50 1059.36 o
2 16 1 358.61 -115.37 500.52 o
4 16 1 1020.36 784.57 520.09 o
6 16 1 6408.09 4948.59 701.61 o
8 16 1 3302.46 7078.79 797.19 o
10 16 1 1561.44 2321.81 788.14 o
-11 17 1 15329.79 15434.53 1441.60 o
-9 17 1 28784.19 29077.72 1581.01 o
-7 17 1 3881.23 4563.32 832.76 o
-5 17 1 1311.77 477.50 983.40 o
-3 17 1 8795.83 12246.63 2023.93 o
-1 17 1 19077.63 22663.25 1279.53 o
1 17 1 66491.39 69195.50 1805.80 o
3 17 1 35351.14 31479.45 1275.09 o
5 17 1 22039.01 23637.30 1188.90 o
7 17 1 479.35 3615.44 658.48 o
9 17 1 5718.03 5984.75 852.43 o
-10 18 1 191.10 117.14 718.80 o
-8 18 1 819.29 1766.07 768.55 o
-6 18 1 5437.03 7274.28 1076.22 o
-4 18 1 711.00 -2263.06 2263.06 o
-2 18 1 1175.18 1860.27 953.21 o
0 18 1 32764.44 34154.18 1467.14 o
2 18 1 99413.61 94570.34 2244.10 o
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