#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/15/2201556.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201556_Fobs loop_ _publ_author_name 'Chen, Chunlong' 'Su, Chengyong' 'Xu, Anwu' 'Zhang, Huaxin' 'Feng, Xiaolong' 'Kang, Beisheng' _publ_section_title ; 1,4-Bis(benzimidazol-2-yl)butane ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o916 _journal_page_last o917 _journal_volume 58 _journal_year 2002 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.7926 _cell_length_b 9.3664 _cell_length_c 17.8814 _exptl_crystal_F_000 616.00 _reflns_d_resolution_high 0.7765 _[local]_cod_data_source_file ob6151Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 04182M in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 160.14 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1921.17 1953.76 32.35 o 4 0 0 580.48 595.16 11.06 o 6 0 0 51.33 57.69 2.73 o 8 0 0 384.73 381.83 9.06 o 10 0 0 155.34 167.77 6.02 o 2 1 0 29.99 13.42 0.52 o 4 1 0 127.05 119.03 2.32 o 6 1 0 412.76 383.36 5.89 o 8 1 0 4.23 6.62 1.37 o 10 1 0 142.29 146.85 3.94 o 0 2 0 25644.73 22178.40 290.08 o 2 2 0 373.19 349.77 3.23 o 4 2 0 89.14 101.17 2.13 o 6 2 0 0.85 1.46 1.26 o 8 2 0 581.14 570.29 8.70 o 10 2 0 0.35 0.12 1.44 o 2 3 0 646.28 703.60 6.15 o 4 3 0 1422.68 1454.44 17.74 o 6 3 0 0.72 0.62 1.15 o 8 3 0 2.54 4.07 1.38 o 10 3 0 250.16 266.23 5.65 o 0 4 0 5301.29 5461.12 51.32 o 2 4 0 69.70 93.19 1.15 o 4 4 0 11.63 7.06 0.77 o 6 4 0 1.11 1.38 1.23 o 8 4 0 28.83 26.07 1.84 o 10 4 0 144.89 157.13 4.27 o 2 5 0 1587.02 1731.02 11.88 o 4 5 0 325.00 326.31 3.54 o 6 5 0 438.15 466.02 13.61 o 8 5 0 4.11 10.04 1.63 o 10 5 0 26.64 28.23 3.15 o 0 6 0 441.05 535.20 7.24 o 2 6 0 1227.48 1196.60 9.32 o 4 6 0 105.50 92.63 1.85 o 6 6 0 31.06 26.04 1.31 o 8 6 0 247.58 267.82 12.64 o 2 7 0 54.64 63.77 1.38 o 4 7 0 176.34 167.59 2.43 o 6 7 0 5.12 3.26 0.98 o 8 7 0 12.71 11.39 1.83 o 0 8 0 371.74 330.01 5.34 o 2 8 0 715.18 742.32 7.16 o 4 8 0 6.54 13.12 1.06 o 6 8 0 40.17 39.30 2.21 o 8 8 0 19.28 11.31 2.59 o 2 9 0 45.47 36.54 1.55 o 4 9 0 234.91 234.01 3.83 o 6 9 0 1.03 0.47 1.45 o 0 10 0 220.03 225.87 6.63 o 2 10 0 7.04 10.40 1.69 o 4 10 0 18.91 21.99 1.68 o 6 10 0 1.34 4.26 1.78 o 2 11 0 2.08 1.37 1.59 o 4 11 0 22.06 37.43 3.61 o 1 1 1 3927.82 3766.05 23.30 o 2 1 1 174.20 165.10 1.39 o 3 1 1 1239.74 1223.45 9.34 o 4 1 1 33.97 37.81 0.81 o 5 1 1 21.60 19.97 0.84 o 6 1 1 961.97 975.59 9.01 o 7 1 1 48.79 52.01 1.41 o 8 1 1 6.49 7.89 1.00 o 9 1 1 144.00 147.49 2.63 o 10 1 1 3.37 4.27 1.13 o 11 1 1 6.57 2.59 1.19 o 0 2 1 79.92 64.97 0.97 o 1 2 1 1442.66 1453.02 9.88 o 2 2 1 11.60 12.55 0.36 o 3 2 1 100.66 115.17 1.23 o 4 2 1 148.03 145.96 1.53 o 5 2 1 104.82 98.37 1.60 o 6 2 1 15.19 18.67 1.00 o 7 2 1 0.10 1.20 0.73 o 8 2 1 0.10 1.17 0.85 o 9 2 1 28.43 28.32 1.35 o 10 2 1 77.62 83.15 2.17 o 1 3 1 3568.49 3538.57 17.38 o 2 3 1 41.21 43.29 0.57 o 3 3 1 751.21 793.07 5.29 o 4 3 1 308.32 309.86 2.65 o 5 3 1 365.33 375.42 3.99 o 6 3 1 75.46 80.06 1.60 o 7 3 1 40.55 51.92 1.57 o 8 3 1 205.62 213.48 3.15 o 9 3 1 0.27 0.49 1.19 o 10 3 1 116.06 120.51 2.60 o 0 4 1 66.79 65.21 0.88 o 1 4 1 58.21 69.60 0.57 o 2 4 1 31.69 30.94 0.48 o 3 4 1 891.95 940.93 5.83 o 4 4 1 439.69 455.50 3.40 o 5 4 1 282.22 294.86 3.01 o 6 4 1 390.91 392.87 5.06 o 7 4 1 114.52 108.25 1.86 o 8 4 1 44.16 44.25 1.53 o 9 4 1 2.67 3.93 1.13 o 10 4 1 63.43 70.81 2.09 o 1 5 1 760.01 841.63 4.42 o 2 5 1 57.42 57.35 0.64 o 3 5 1 344.36 353.94 2.30 o 4 5 1 150.87 154.55 1.48 o 5 5 1 23.43 21.78 0.74 o 6 5 1 127.59 124.67 2.12 o 7 5 1 83.63 81.61 1.86 o 8 5 1 80.87 81.86 2.01 o 9 5 1 24.40 31.40 1.94 o 10 5 1 4.50 1.86 1.32 o 0 6 1 2.94 2.29 0.42 o 1 6 1 91.21 82.06 0.84 o 2 6 1 20.50 21.60 0.52 o 3 6 1 121.72 121.03 1.07 o 4 6 1 0.52 1.53 0.42 o 5 6 1 1.03 3.75 0.53 o 6 6 1 154.08 155.57 2.89 o 7 6 1 14.87 24.76 1.36 o 8 6 1 74.96 77.02 2.00 o 9 6 1 6.57 8.33 1.46 o 1 7 1 94.43 91.48 1.14 o 2 7 1 66.29 65.70 0.99 o 3 7 1 5.27 9.22 0.60 o 4 7 1 2.52 4.64 0.56 o 5 7 1 159.63 165.63 1.77 o 6 7 1 92.42 94.82 1.60 o 7 7 1 199.39 206.64 3.16 o 8 7 1 31.02 38.08 1.88 o 9 7 1 23.41 22.00 7.13 o 0 8 1 28.93 26.23 1.25 o 1 8 1 59.99 53.23 0.97 o 2 8 1 121.72 123.34 1.46 o 3 8 1 5.63 4.44 0.58 o 4 8 1 377.43 386.22 3.35 o 5 8 1 177.47 183.11 2.12 o 6 8 1 30.37 31.80 1.26 o 7 8 1 142.61 155.31 3.24 o 8 8 1 0.50 0.44 1.50 o 1 9 1 429.88 416.46 3.84 o 2 9 1 103.23 108.68 1.57 o 3 9 1 175.31 185.66 2.13 o 4 9 1 10.75 13.63 0.90 o 5 9 1 16.72 17.61 1.08 o 6 9 1 0.03 -0.71 1.02 o 7 9 1 73.94 80.32 3.08 o 0 10 1 11.75 14.02 1.79 o 1 10 1 65.36 61.68 1.55 o 2 10 1 5.21 3.91 0.92 o 3 10 1 26.95 21.79 1.77 o 4 10 1 11.98 8.68 1.07 o 5 10 1 11.51 10.22 1.30 o 6 10 1 0.32 -0.77 1.39 o 1 11 1 46.79 41.50 1.64 o 2 11 1 6.82 5.28 1.15 o 3 11 1 15.12 12.63 1.84 o 4 11 1 0.31 -0.25 1.16 o 1 0 2 2314.93 2307.07 22.11 o 2 0 2 5863.44 5567.88 52.61 o 3 0 2 39.84 52.09 1.06 o 4 0 2 726.36 682.92 7.22 o 5 0 2 215.17 226.54 4.66 o 6 0 2 44.72 54.43 1.96 o 7 0 2 172.95 164.45 3.49 o 8 0 2 471.47 472.83 7.52 o 9 0 2 8.94 11.89 1.58 o 10 0 2 37.06 38.86 2.20 o 1 1 2 458.50 470.25 4.46 o 2 1 2 238.93 257.26 1.99 o 3 1 2 529.88 557.57 5.09 o 4 1 2 457.36 483.11 4.15 o 5 1 2 312.52 294.75 2.93 o 6 1 2 27.54 25.99 1.04 o 7 1 2 0.44 1.36 0.76 o 8 1 2 1.26 1.35 0.79 o 9 1 2 0.23 0.85 0.91 o 10 1 2 43.44 44.65 1.66 o 11 1 2 23.27 12.09 1.91 o 0 2 2 2987.25 2783.07 22.61 o 1 2 2 302.83 280.50 1.80 o 2 2 2 5.09 4.58 0.31 o 3 2 2 12.59 13.90 0.50 o 4 2 2 1436.63 1516.71 11.65 o 5 2 2 135.45 153.05 2.74 o 6 2 2 0.87 -0.15 0.60 o 7 2 2 21.83 22.92 1.47 o 8 2 2 420.23 412.53 4.85 o 9 2 2 129.22 135.70 2.56 o 10 2 2 14.75 14.06 1.35 o 1 3 2 11.80 11.54 0.30 o 2 3 2 116.85 129.77 1.27 o 3 3 2 214.62 245.89 2.11 o 4 3 2 86.07 88.81 1.26 o 5 3 2 117.61 121.91 1.66 o 6 3 2 3.56 2.51 0.71 o 7 3 2 21.02 23.86 1.21 o 8 3 2 12.13 18.75 1.29 o 9 3 2 2.83 2.59 1.06 o 10 3 2 44.65 45.44 1.75 o 0 4 2 212.71 233.82 2.14 o 1 4 2 13.99 13.99 0.43 o 2 4 2 1967.73 2014.53 11.16 o 3 4 2 2.61 1.37 0.37 o 4 4 2 103.46 118.14 1.28 o 5 4 2 0.55 -0.24 0.48 o 6 4 2 181.97 169.28 2.20 o 7 4 2 104.12 106.76 2.07 o 8 4 2 17.32 22.09 1.38 o 9 4 2 189.57 203.56 3.30 o 10 4 2 2.95 4.48 1.22 o 1 5 2 408.05 402.75 2.47 o 2 5 2 55.85 62.62 0.72 o 3 5 2 412.19 440.66 2.90 o 4 5 2 50.81 50.03 0.82 o 5 5 2 696.49 674.71 4.88 o 6 5 2 7.51 10.95 0.85 o 7 5 2 221.49 226.00 3.21 o 8 5 2 2.72 2.29 0.91 o 9 5 2 2.59 1.79 1.09 o 10 5 2 1.51 0.84 1.16 o 0 6 2 38.76 38.69 0.99 o 1 6 2 42.94 47.53 0.65 o 2 6 2 667.09 687.18 4.17 o 3 6 2 4.19 4.56 0.41 o 4 6 2 348.74 348.63 2.41 o 5 6 2 286.92 288.80 2.43 o 6 6 2 220.20 205.95 2.58 o 7 6 2 187.48 192.72 2.98 o 8 6 2 101.77 109.43 2.35 o 9 6 2 30.61 32.11 1.95 o 1 7 2 110.81 110.05 1.26 o 2 7 2 549.94 491.88 3.52 o 3 7 2 169.38 161.91 1.64 o 4 7 2 4.03 5.71 0.58 o 5 7 2 45.98 49.57 1.00 o 6 7 2 4.16 2.49 0.96 o 7 7 2 69.58 71.84 2.19 o 8 7 2 0.58 0.49 1.21 o 9 7 2 21.17 12.43 2.06 o 0 8 2 261.92 262.24 3.22 o 1 8 2 397.36 379.29 3.19 o 2 8 2 159.59 151.73 1.76 o 3 8 2 126.60 135.94 1.70 o 4 8 2 5.07 4.61 0.69 o 5 8 2 49.07 46.90 1.12 o 6 8 2 2.28 -0.09 0.79 o 7 8 2 0.80 1.45 1.22 o 8 8 2 9.02 3.88 1.48 o 1 9 2 32.82 28.84 1.07 o 2 9 2 259.10 253.84 2.77 o 3 9 2 141.24 147.97 2.04 o 4 9 2 0.82 -0.68 0.68 o 5 9 2 95.40 97.82 1.92 o 6 9 2 1.16 1.79 0.94 o 7 9 2 1.63 4.22 1.72 o 0 10 2 12.50 15.37 1.48 o 1 10 2 100.04 99.95 1.73 o 2 10 2 57.61 54.93 1.37 o 3 10 2 7.27 8.81 1.02 o 4 10 2 15.81 19.16 1.84 o 5 10 2 0.05 0.01 1.03 o 6 10 2 14.52 18.86 4.04 o 1 11 2 1.18 1.18 1.06 o 2 11 2 9.24 12.83 1.37 o 3 11 2 5.00 5.69 1.99 o 4 11 2 0.82 0.82 1.05 o 1 1 3 19579.17 17839.89 183.15 o 2 1 3 23525.99 21734.38 211.10 o 3 1 3 674.59 666.92 4.47 o 4 1 3 55.63 35.18 0.73 o 5 1 3 243.70 254.07 2.63 o 6 1 3 399.46 392.73 3.82 o 7 1 3 29.95 28.76 1.14 o 8 1 3 38.14 36.24 1.33 o 9 1 3 113.48 116.55 2.34 o 10 1 3 0.22 -0.27 0.99 o 11 1 3 5.81 1.14 1.18 o 0 2 3 664.28 697.09 6.90 o 1 2 3 3550.09 3525.69 19.66 o 2 2 3 2948.38 2939.67 16.08 o 3 2 3 92.56 80.50 0.80 o 4 2 3 286.98 273.90 3.02 o 5 2 3 0.57 0.15 0.46 o 6 2 3 128.84 129.41 1.83 o 7 2 3 3.20 3.20 0.81 o 8 2 3 211.63 205.31 3.06 o 9 2 3 94.22 93.57 2.14 o 10 2 3 0.01 -0.24 1.05 o 1 3 3 255.72 240.46 1.81 o 2 3 3 13.38 12.29 0.35 o 3 3 3 157.56 162.27 1.58 o 4 3 3 11.98 12.41 0.51 o 5 3 3 228.58 255.73 2.69 o 6 3 3 431.86 437.71 4.21 o 7 3 3 0.31 0.22 0.77 o 8 3 3 5.47 8.11 1.07 o 9 3 3 52.34 56.37 1.75 o 10 3 3 39.86 36.54 1.63 o 0 4 3 2977.82 3143.39 22.96 o 1 4 3 339.79 371.36 2.25 o 2 4 3 581.18 590.66 3.58 o 3 4 3 614.57 604.11 3.95 o 4 4 3 645.22 691.88 4.81 o 5 4 3 66.16 61.96 0.98 o 6 4 3 43.69 48.06 1.19 o 7 4 3 1.06 3.58 0.83 o 8 4 3 2.04 1.35 0.92 o 9 4 3 108.00 114.85 2.44 o 10 4 3 12.13 16.67 3.00 o 1 5 3 166.11 198.87 1.43 o 2 5 3 213.16 219.81 1.57 o 3 5 3 12.41 8.42 0.45 o 4 5 3 60.77 54.81 0.86 o 5 5 3 6.19 8.24 0.60 o 6 5 3 181.91 175.64 2.09 o 7 5 3 0.21 -0.04 0.85 o 8 5 3 16.01 21.99 1.79 o 9 5 3 10.49 11.23 1.46 o 10 5 3 0.49 -0.47 1.37 o 0 6 3 1104.11 1150.36 8.96 o 1 6 3 65.27 69.69 0.79 o 2 6 3 24.31 27.07 0.56 o 3 6 3 1.98 2.35 0.39 o 4 6 3 157.49 170.28 1.56 o 5 6 3 15.44 17.03 0.72 o 6 6 3 0.26 -0.50 0.57 o 7 6 3 9.91 13.43 1.39 o 8 6 3 0.85 -1.05 1.09 o 9 6 3 0.03 -1.30 1.30 o 1 7 3 169.07 172.31 1.64 o 2 7 3 162.59 161.71 1.74 o 3 7 3 91.58 101.73 1.38 o 4 7 3 240.91 244.45 2.37 o 5 7 3 61.95 64.56 1.44 o 6 7 3 249.49 246.39 3.39 o 7 7 3 33.75 35.22 1.73 o 8 7 3 12.97 10.19 1.74 o 0 8 3 4.30 7.00 1.21 o 1 8 3 23.22 23.67 0.99 o 2 8 3 76.80 73.94 1.37 o 3 8 3 362.03 363.51 3.35 o 4 8 3 13.50 16.36 0.84 o 5 8 3 31.95 30.77 1.08 o 6 8 3 7.49 7.71 0.97 o 7 8 3 3.96 2.59 1.10 o 8 8 3 2.76 0.67 1.42 o 1 9 3 14.88 19.62 1.14 o 2 9 3 219.80 223.63 2.57 o 3 9 3 44.14 40.67 1.17 o 4 9 3 122.77 133.41 1.99 o 5 9 3 15.49 18.33 1.97 o 6 9 3 4.32 4.76 1.42 o 7 9 3 26.80 16.77 1.74 o 0 10 3 5.07 3.00 1.22 o 1 10 3 12.86 20.54 1.11 o 2 10 3 9.83 9.03 0.93 o 3 10 3 15.66 12.10 1.13 o 4 10 3 10.85 6.30 0.95 o 5 10 3 0.24 0.81 1.10 o 6 10 3 2.60 0.84 1.64 o 1 11 3 2.75 1.39 0.96 o 2 11 3 3.49 2.21 0.99 o 3 11 3 3.01 -0.03 1.00 o 4 11 3 9.79 5.78 1.25 o 0 0 4 351.90 302.10 6.62 o 1 0 4 13074.84 12106.79 98.99 o 2 0 4 6393.52 6230.58 58.80 o 3 0 4 542.22 531.97 5.66 o 4 0 4 323.38 357.96 3.72 o 5 0 4 904.34 920.89 13.53 o 6 0 4 111.86 107.98 2.13 o 7 0 4 368.29 363.70 6.20 o 8 0 4 3.54 3.83 1.30 o 9 0 4 100.01 101.15 3.52 o 10 0 4 1.55 2.09 1.45 o 1 1 4 1663.63 1668.22 9.88 o 2 1 4 277.34 252.45 1.75 o 3 1 4 3.77 0.62 0.28 o 4 1 4 301.91 311.02 2.67 o 5 1 4 10.14 16.47 0.66 o 6 1 4 10.94 11.90 0.80 o 7 1 4 108.78 101.65 1.92 o 8 1 4 123.62 117.65 2.23 o 9 1 4 124.36 128.88 2.48 o 10 1 4 13.21 10.20 1.23 o 0 2 4 1152.12 1063.14 8.98 o 1 2 4 800.94 756.11 4.44 o 2 2 4 289.05 308.19 1.96 o 3 2 4 748.13 795.32 5.29 o 4 2 4 9.14 11.50 0.46 o 5 2 4 156.66 155.97 2.25 o 6 2 4 38.27 41.13 1.07 o 7 2 4 62.91 61.58 1.38 o 8 2 4 0.21 0.35 0.83 o 9 2 4 8.79 10.98 1.22 o 10 2 4 1.99 1.54 1.11 o 1 3 4 0.67 0.75 0.18 o 2 3 4 212.23 202.74 1.43 o 3 3 4 59.85 67.65 0.79 o 4 3 4 225.01 229.29 1.93 o 5 3 4 9.33 13.96 0.59 o 6 3 4 44.22 45.77 1.19 o 7 3 4 8.76 12.82 0.90 o 8 3 4 428.77 434.86 5.10 o 9 3 4 89.70 91.75 2.15 o 10 3 4 37.18 35.53 1.60 o 0 4 4 262.53 263.49 2.39 o 1 4 4 334.59 319.89 2.25 o 2 4 4 727.39 748.57 4.43 o 3 4 4 1208.57 1235.23 7.54 o 4 4 4 104.47 104.73 1.12 o 5 4 4 126.92 133.91 1.62 o 6 4 4 6.21 6.85 0.77 o 7 4 4 103.35 110.02 1.85 o 8 4 4 0.21 -0.85 0.85 o 9 4 4 25.09 27.60 1.58 o 10 4 4 57.68 65.70 2.21 o 1 5 4 757.95 740.21 4.21 o 2 5 4 18.95 20.68 0.45 o 3 5 4 130.43 139.63 1.26 o 4 5 4 5.21 4.60 0.47 o 5 5 4 9.85 15.92 0.73 o 6 5 4 18.04 21.38 1.08 o 7 5 4 307.30 296.62 3.40 o 8 5 4 120.03 127.40 2.87 o 9 5 4 4.15 1.86 1.34 o 0 6 4 0.67 0.27 0.44 o 1 6 4 34.40 43.44 0.65 o 2 6 4 422.79 458.30 2.89 o 3 6 4 42.32 41.11 0.76 o 4 6 4 25.46 23.40 0.75 o 5 6 4 118.98 117.62 2.04 o 6 6 4 6.66 6.32 0.76 o 7 6 4 166.07 176.76 2.54 o 8 6 4 8.65 11.68 1.24 o 9 6 4 8.30 5.28 1.25 o 1 7 4 1.75 1.92 0.55 o 2 7 4 15.96 14.23 0.69 o 3 7 4 18.13 20.13 0.71 o 4 7 4 24.17 23.87 0.80 o 5 7 4 21.44 23.28 1.09 o 6 7 4 264.59 284.68 4.54 o 7 7 4 12.09 12.56 1.62 o 8 7 4 1.62 -1.19 1.19 o 0 8 4 27.91 24.34 1.42 o 1 8 4 302.17 278.81 2.82 o 2 8 4 126.33 129.80 1.80 o 3 8 4 38.51 39.60 1.09 o 4 8 4 4.70 9.42 0.83 o 5 8 4 1.70 2.61 0.95 o 6 8 4 39.70 36.66 1.48 o 7 8 4 72.42 75.99 2.33 o 8 8 4 17.58 10.26 2.04 o 1 9 4 12.25 10.18 0.96 o 2 9 4 27.07 26.83 1.10 o 3 9 4 37.38 31.88 1.09 o 4 9 4 61.48 61.66 1.55 o 5 9 4 23.83 26.07 1.95 o 6 9 4 82.54 84.08 2.13 o 7 9 4 47.67 46.11 4.37 o 0 10 4 118.38 118.61 3.71 o 1 10 4 217.76 222.05 2.69 o 2 10 4 17.08 16.46 1.06 o 3 10 4 1.33 1.51 0.81 o 4 10 4 22.79 21.93 1.62 o 5 10 4 3.64 3.29 1.12 o 1 11 4 41.88 40.42 1.34 o 2 11 4 5.94 6.41 1.01 o 3 11 4 2.64 1.79 1.03 o 4 11 4 8.08 1.08 1.38 o 1 1 5 296.33 285.61 1.92 o 2 1 5 1331.58 1306.96 7.37 o 3 1 5 10.40 11.06 0.44 o 4 1 5 1323.62 1422.07 10.05 o 5 1 5 105.39 114.45 1.44 o 6 1 5 515.41 493.85 4.20 o 7 1 5 233.49 229.36 2.78 o 8 1 5 120.35 115.01 2.20 o 9 1 5 69.86 67.34 1.82 o 10 1 5 7.74 5.20 1.42 o 0 2 5 180.61 154.33 2.75 o 1 2 5 370.41 378.72 2.66 o 2 2 5 193.70 174.11 1.18 o 3 2 5 723.95 732.94 4.33 o 4 2 5 8.50 8.12 0.38 o 5 2 5 55.29 55.33 1.02 o 6 2 5 0.95 0.29 0.58 o 7 2 5 6.74 7.84 0.83 o 8 2 5 271.00 269.47 3.65 o 9 2 5 339.27 341.94 4.47 o 10 2 5 0.06 -0.57 1.03 o 1 3 5 459.45 474.36 3.07 o 2 3 5 661.73 691.25 3.87 o 3 3 5 893.16 955.41 6.34 o 4 3 5 15.28 25.09 0.52 o 5 3 5 0.13 0.52 0.48 o 6 3 5 750.01 740.44 6.45 o 7 3 5 193.97 192.48 3.03 o 8 3 5 63.14 66.88 1.57 o 9 3 5 11.34 11.83 1.24 o 10 3 5 1.54 2.00 1.13 o 0 4 5 360.35 365.49 5.01 o 1 4 5 1049.16 1123.67 6.08 o 2 4 5 11.33 17.59 0.40 o 3 4 5 23.55 19.80 0.53 o 4 4 5 0.96 0.49 0.36 o 5 4 5 0.75 0.46 0.48 o 6 4 5 253.88 251.15 2.87 o 7 4 5 22.94 27.85 1.07 o 8 4 5 15.62 19.15 1.15 o 9 4 5 233.62 246.33 4.36 o 10 4 5 11.27 8.64 1.55 o 1 5 5 3.25 6.15 0.45 o 2 5 5 15.08 12.72 0.59 o 3 5 5 2.27 4.22 0.42 o 4 5 5 987.94 964.37 6.15 o 5 5 5 367.37 368.26 3.09 o 6 5 5 19.43 21.47 0.92 o 7 5 5 4.50 4.35 0.83 o 8 5 5 36.74 39.02 1.49 o 9 5 5 17.36 15.39 1.65 o 0 6 5 517.89 470.69 5.77 o 1 6 5 20.71 26.19 0.59 o 2 6 5 17.16 16.78 0.58 o 3 6 5 9.60 13.05 0.59 o 4 6 5 46.13 37.67 0.89 o 5 6 5 129.18 120.78 1.69 o 6 6 5 179.10 178.88 2.22 o 7 6 5 2.20 1.68 0.82 o 8 6 5 37.88 37.10 1.80 o 9 6 5 31.96 30.72 2.62 o 1 7 5 182.09 170.44 1.66 o 2 7 5 90.74 87.30 1.17 o 3 7 5 32.19 30.94 0.80 o 4 7 5 1180.12 1192.04 9.22 o 5 7 5 77.51 75.07 1.55 o 6 7 5 148.44 153.33 2.31 o 7 7 5 15.34 17.26 1.78 o 8 7 5 0.81 0.92 1.12 o 0 8 5 1018.70 964.82 10.43 o 1 8 5 184.29 186.38 2.20 o 2 8 5 71.18 66.99 1.30 o 3 8 5 25.65 25.20 1.15 o 4 8 5 9.89 10.11 0.98 o 5 8 5 74.00 74.60 1.87 o 6 8 5 18.60 23.48 1.84 o 7 8 5 5.25 5.41 1.36 o 1 9 5 6.03 4.95 0.78 o 2 9 5 24.90 26.86 1.00 o 3 9 5 34.14 38.41 1.17 o 4 9 5 156.92 151.93 2.39 o 5 9 5 90.37 114.84 2.39 o 6 9 5 0.07 -0.97 1.04 o 7 9 5 8.78 12.11 2.82 o 0 10 5 0.41 0.61 1.17 o 1 10 5 42.79 45.71 1.29 o 2 10 5 0.00 0.12 0.78 o 3 10 5 6.31 8.13 0.99 o 4 10 5 11.35 9.47 1.13 o 5 10 5 0.93 0.27 1.11 o 1 11 5 55.70 57.84 1.49 o 2 11 5 4.57 3.81 1.04 o 3 11 5 2.67 -0.34 0.96 o 0 0 6 94.07 99.45 1.70 o 1 0 6 1227.36 1154.65 10.31 o 2 0 6 2934.31 2945.33 24.44 o 3 0 6 6231.46 6362.79 74.88 o 4 0 6 711.63 629.16 6.83 o 5 0 6 414.60 452.11 4.64 o 6 0 6 5.87 5.72 0.88 o 7 0 6 96.37 92.50 2.14 o 8 0 6 54.82 53.30 2.22 o 9 0 6 0.94 0.94 1.36 o 10 0 6 1.42 -0.61 1.47 o 1 1 6 15.45 10.92 0.31 o 2 1 6 2431.49 2547.31 14.08 o 3 1 6 1064.36 1029.63 5.98 o 4 1 6 625.95 584.81 4.54 o 5 1 6 0.31 0.64 0.46 o 6 1 6 43.90 40.68 1.01 o 7 1 6 3.13 3.63 0.66 o 8 1 6 1.57 1.66 0.79 o 9 1 6 6.23 6.65 1.10 o 10 1 6 7.96 8.41 1.24 o 0 2 6 880.28 847.26 8.57 o 1 2 6 801.00 825.63 5.94 o 2 2 6 1.55 -0.11 0.22 o 3 2 6 3364.17 3643.40 18.98 o 4 2 6 49.43 61.29 0.83 o 5 2 6 99.45 98.52 1.35 o 6 2 6 29.54 30.34 0.92 o 7 2 6 2.22 1.60 0.71 o 8 2 6 3.65 4.87 0.82 o 9 2 6 17.22 23.87 1.49 o 10 2 6 7.47 6.32 1.76 o 1 3 6 81.02 91.64 0.98 o 2 3 6 0.43 1.41 0.91 o 3 3 6 1156.42 1188.04 8.22 o 4 3 6 388.63 378.03 2.75 o 5 3 6 63.61 54.52 0.88 o 6 3 6 18.61 18.99 1.04 o 7 3 6 81.50 71.70 1.51 o 8 3 6 1.50 2.03 0.74 o 9 3 6 4.39 5.01 1.08 o 10 3 6 0.38 -1.25 1.25 o 0 4 6 70.35 75.04 1.44 o 1 4 6 7.98 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1.10 o 4 8 6 5.30 11.12 1.71 o 5 8 6 11.47 16.53 1.29 o 6 8 6 0.16 0.22 1.41 o 7 8 6 17.97 15.30 2.02 o 1 9 6 38.54 36.43 1.11 o 2 9 6 22.79 26.46 1.13 o 3 9 6 6.34 7.94 0.87 o 4 9 6 10.09 8.03 1.13 o 5 9 6 43.58 38.17 1.61 o 6 9 6 2.15 -0.05 1.10 o 0 10 6 0.16 1.36 1.11 o 1 10 6 86.07 79.89 1.69 o 2 10 6 101.38 106.08 1.84 o 3 10 6 0.33 -0.88 0.89 o 4 10 6 30.33 31.48 1.49 o 5 10 6 20.73 15.87 1.51 o 1 11 6 42.06 53.23 1.61 o 2 11 6 4.41 1.84 0.94 o 3 11 6 3.67 2.36 1.35 o 1 1 7 355.73 322.45 2.21 o 2 1 7 436.22 467.08 3.11 o 3 1 7 4104.48 4111.85 22.59 o 4 1 7 936.93 935.54 6.62 o 5 1 7 36.63 35.07 0.87 o 6 1 7 270.38 265.34 2.76 o 7 1 7 35.29 34.97 1.04 o 8 1 7 2.06 1.87 0.80 o 9 1 7 10.51 13.99 1.26 o 10 1 7 16.47 12.96 1.34 o 0 2 7 0.06 0.30 0.39 o 1 2 7 4.71 4.38 0.39 o 2 2 7 73.20 76.12 0.89 o 3 2 7 1977.46 1930.71 10.87 o 4 2 7 776.49 747.18 4.92 o 5 2 7 17.15 19.70 0.72 o 6 2 7 782.35 775.81 6.14 o 7 2 7 705.26 688.13 5.71 o 8 2 7 21.95 20.17 1.17 o 9 2 7 7.28 6.11 1.07 o 10 2 7 7.31 5.15 1.21 o 1 3 7 37.58 34.57 0.57 o 2 3 7 59.27 61.09 0.65 o 3 3 7 12.12 12.74 0.42 o 4 3 7 101.37 99.13 1.10 o 5 3 7 327.98 331.73 2.83 o 6 3 7 84.46 79.86 1.27 o 7 3 7 0.05 0.04 0.66 o 8 3 7 6.38 10.57 0.97 o 9 3 7 40.31 36.47 1.54 o 10 3 7 6.63 1.87 1.33 o 0 4 7 124.99 122.81 1.99 o 1 4 7 1010.14 1045.64 6.06 o 2 4 7 3.49 2.41 0.41 o 3 4 7 1.68 5.35 0.40 o 4 4 7 26.85 26.15 0.68 o 5 4 7 233.91 230.69 2.40 o 6 4 7 48.53 48.91 1.26 o 7 4 7 135.26 132.63 2.14 o 8 4 7 0.07 -0.79 0.79 o 9 4 7 24.69 18.17 1.28 o 10 4 7 19.15 7.27 2.63 o 1 5 7 0.96 3.03 0.46 o 2 5 7 17.20 19.63 0.62 o 3 5 7 128.25 134.26 1.46 o 4 5 7 819.55 804.84 6.21 o 5 5 7 15.23 17.66 0.93 o 6 5 7 8.07 10.20 0.90 o 7 5 7 36.58 38.21 1.28 o 8 5 7 75.60 79.06 1.79 o 9 5 7 2.80 2.84 1.02 o 0 6 7 313.35 303.28 3.62 o 1 6 7 230.65 227.13 1.99 o 2 6 7 4.64 6.90 0.61 o 3 6 7 6.63 11.14 0.72 o 4 6 7 126.64 121.10 1.85 o 5 6 7 96.13 91.02 1.67 o 6 6 7 11.68 6.87 0.86 o 7 6 7 0.13 -0.71 0.79 o 8 6 7 7.47 13.28 1.84 o 9 6 7 0.01 -0.13 1.16 o 1 7 7 0.05 0.13 0.49 o 2 7 7 1.24 1.04 0.51 o 3 7 7 107.76 108.29 1.58 o 4 7 7 425.22 405.79 4.14 o 5 7 7 145.48 144.46 2.20 o 6 7 7 0.00 -0.67 0.87 o 7 7 7 7.75 9.36 1.54 o 8 7 7 110.69 132.02 3.91 o 0 8 7 213.96 194.56 3.28 o 1 8 7 24.81 31.58 1.01 o 2 8 7 0.37 -0.09 0.65 o 3 8 7 49.63 49.45 1.49 o 4 8 7 7.96 7.73 1.05 o 5 8 7 18.88 22.94 1.43 o 6 8 7 15.46 13.70 2.96 o 7 8 7 10.06 3.88 1.91 o 1 9 7 4.19 3.46 0.79 o 2 9 7 4.61 8.46 0.86 o 3 9 7 121.95 119.65 3.06 o 4 9 7 69.42 70.79 1.90 o 5 9 7 21.06 16.92 1.39 o 6 9 7 1.17 -0.43 1.34 o 0 10 7 17.52 15.26 1.77 o 1 10 7 1.41 1.73 0.82 o 2 10 7 34.88 35.63 1.23 o 3 10 7 10.00 8.26 1.12 o 4 10 7 0.04 -0.72 1.10 o 5 10 7 12.04 8.35 1.31 o 1 11 7 8.52 7.92 1.32 o 2 11 7 48.73 55.77 2.21 o 0 0 8 2530.06 2438.03 44.45 o 1 0 8 20.42 25.32 0.66 o 2 0 8 653.76 678.32 6.16 o 3 0 8 212.17 183.58 2.32 o 4 0 8 54.64 60.45 1.25 o 5 0 8 168.17 155.32 2.25 o 6 0 8 111.60 112.11 2.29 o 7 0 8 131.25 127.71 2.57 o 8 0 8 41.45 35.60 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159.31 1.80 o 6 4 8 27.92 30.07 1.08 o 7 4 8 0.10 0.09 0.77 o 8 4 8 22.54 23.30 1.32 o 9 4 8 7.78 9.41 1.04 o 1 5 8 1.44 0.04 0.45 o 2 5 8 40.34 39.16 0.90 o 3 5 8 19.75 26.83 0.92 o 4 5 8 305.98 287.01 3.10 o 5 5 8 389.91 351.23 3.68 o 6 5 8 37.02 30.53 1.11 o 7 5 8 11.03 14.82 1.10 o 8 5 8 20.92 21.20 2.21 o 9 5 8 69.12 77.08 3.08 o 0 6 8 544.19 527.27 5.33 o 1 6 8 32.15 33.75 0.80 o 2 6 8 661.97 614.68 4.95 o 3 6 8 218.92 216.77 2.60 o 4 6 8 10.15 8.23 0.84 o 5 6 8 52.00 59.10 1.40 o 6 6 8 25.07 25.59 1.24 o 7 6 8 65.32 67.76 1.87 o 8 6 8 39.63 39.84 1.65 o 1 7 8 237.21 229.25 2.13 o 2 7 8 160.51 154.25 1.79 o 3 7 8 50.00 49.95 1.29 o 4 7 8 184.46 177.92 2.43 o 5 7 8 24.10 26.09 1.21 o 6 7 8 3.14 4.55 1.18 o 7 7 8 5.25 10.17 1.24 o 8 7 8 1.34 2.98 1.45 o 0 8 8 1.04 1.80 0.98 o 1 8 8 41.43 40.08 1.12 o 2 8 8 266.11 245.29 2.71 o 3 8 8 15.04 14.55 1.18 o 4 8 8 0.93 -0.28 0.90 o 5 8 8 32.19 35.79 1.76 o 6 8 8 79.45 82.09 3.01 o 7 8 8 0.97 2.15 1.88 o 1 9 8 53.42 51.05 1.29 o 2 9 8 10.66 14.40 0.98 o 3 9 8 50.72 55.80 1.69 o 4 9 8 1.04 0.56 0.98 o 5 9 8 69.97 76.38 2.39 o 6 9 8 2.74 3.47 1.41 o 0 10 8 178.59 186.09 3.53 o 1 10 8 20.00 19.97 1.58 o 2 10 8 2.44 2.33 0.93 o 3 10 8 11.53 15.61 1.73 o 4 10 8 13.65 8.76 1.33 o 1 11 8 0.10 -0.93 0.93 o 2 11 8 6.25 2.74 1.43 o 1 1 9 269.57 268.26 1.97 o 2 1 9 857.04 941.93 5.92 o 3 1 9 77.20 94.39 0.95 o 4 1 9 194.00 198.56 1.78 o 5 1 9 427.35 442.52 3.60 o 6 1 9 386.87 363.98 2.99 o 7 1 9 5.91 8.89 0.73 o 8 1 9 0.65 0.64 0.67 o 9 1 9 41.48 47.03 1.34 o 10 1 9 7.29 6.93 1.44 o 0 2 9 27.79 38.86 1.17 o 1 2 9 35.06 30.69 0.55 o 2 2 9 8.32 8.43 0.50 o 3 2 9 281.44 285.72 2.05 o 4 2 9 554.41 584.51 4.92 o 5 2 9 412.61 395.31 3.12 o 6 2 9 5.08 5.54 0.62 o 7 2 9 105.89 102.12 1.54 o 8 2 9 0.57 0.39 0.71 o 9 2 9 3.33 3.31 0.90 o 10 2 9 0.56 0.48 1.15 o 1 3 9 1893.53 1930.00 14.75 o 2 3 9 484.49 514.83 3.51 o 3 3 9 0.63 2.00 0.40 o 4 3 9 191.58 182.68 1.87 o 5 3 9 159.36 167.55 1.87 o 6 3 9 0.88 0.25 0.57 o 7 3 9 21.90 26.54 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2 8 9 17.56 16.57 1.21 o 3 8 9 114.79 108.84 2.20 o 4 8 9 36.67 37.81 1.71 o 5 8 9 26.25 32.58 2.27 o 6 8 9 8.61 5.19 1.69 o 7 8 9 8.45 1.23 1.77 o 1 9 9 77.60 87.03 1.81 o 2 9 9 40.02 42.63 1.57 o 3 9 9 1.07 0.13 0.92 o 4 9 9 1.46 -0.04 1.02 o 5 9 9 21.59 8.61 1.53 o 0 10 9 0.00 -0.90 1.16 o 1 10 9 3.18 0.99 0.84 o 2 10 9 23.92 28.37 1.73 o 3 10 9 7.02 5.66 1.20 o 4 10 9 14.46 10.28 1.35 o 0 0 10 1267.32 1235.77 15.18 o 1 0 10 1818.78 1754.91 14.94 o 2 0 10 95.78 100.82 1.50 o 3 0 10 8.66 7.68 0.65 o 4 0 10 22.82 19.92 0.92 o 5 0 10 750.90 734.23 7.15 o 6 0 10 26.53 23.37 0.99 o 7 0 10 40.15 40.59 1.36 o 8 0 10 34.56 39.70 1.50 o 9 0 10 12.56 13.81 1.83 o 10 0 10 26.12 33.57 2.27 o 1 1 10 5.86 7.19 0.38 o 2 1 10 2.85 4.31 0.38 o 3 1 10 44.61 45.59 0.75 o 4 1 10 38.44 37.79 0.79 o 5 1 10 1576.41 1514.78 9.55 o 6 1 10 13.91 20.63 0.84 o 7 1 10 17.69 22.65 0.91 o 8 1 10 0.03 -0.16 0.63 o 9 1 10 9.01 10.38 0.94 o 10 1 10 5.16 2.08 1.08 o 0 2 10 3.72 1.94 0.39 o 1 2 10 140.94 133.52 1.97 o 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62.52 60.64 1.40 o 3 5 12 70.53 60.72 1.37 o 4 5 12 264.20 252.83 4.39 o 5 5 12 33.49 39.21 1.77 o 6 5 12 28.37 30.23 1.38 o 7 5 12 0.39 -0.42 1.23 o 8 5 12 0.74 -0.28 1.14 o 0 6 12 633.48 638.24 7.58 o 1 6 12 0.48 -0.67 0.67 o 2 6 12 57.05 59.58 1.41 o 3 6 12 246.58 247.63 3.02 o 4 6 12 3.55 6.17 1.01 o 5 6 12 17.79 18.73 1.34 o 6 6 12 0.07 -0.33 0.98 o 7 6 12 70.47 79.74 3.01 o 1 7 12 139.57 156.77 2.13 o 2 7 12 156.85 159.33 2.36 o 3 7 12 28.10 30.47 1.21 o 4 7 12 87.47 81.84 2.00 o 5 7 12 24.81 25.87 1.97 o 6 7 12 28.55 34.22 1.79 o 7 7 12 1.06 3.21 1.73 o 0 8 12 90.90 84.16 2.30 o 1 8 12 8.56 6.58 0.86 o 2 8 12 0.07 -0.73 0.73 o 3 8 12 7.26 7.04 1.13 o 4 8 12 0.02 -1.15 1.15 o 5 8 12 15.75 13.45 4.49 o 1 9 12 89.51 94.18 2.23 o 2 9 12 1.83 1.88 1.07 o 3 9 12 17.13 12.65 1.71 o 4 9 12 9.94 2.79 1.73 o 1 10 12 0.10 -0.88 1.17 o 1 1 13 74.32 63.04 0.98 o 2 1 13 4.16 4.92 0.50 o 3 1 13 216.16 205.41 2.04 o 4 1 13 72.22 64.88 1.14 o 5 1 13 20.60 23.56 0.79 o 6 1 13 2.19 5.87 0.83 o 7 1 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21.00 24.98 1.74 o 3 3 19 3.32 5.85 1.74 o 4 3 19 0.93 -0.71 1.20 o 5 3 19 2.14 0.25 1.32 o 0 4 19 124.23 131.37 4.45 o 1 4 19 0.28 -0.63 0.98 o 2 4 19 49.00 51.19 1.74 o 3 4 19 20.08 19.27 2.22 o 4 4 19 37.56 39.31 4.80 o 5 4 19 6.73 0.88 1.74 o 1 5 19 4.18 5.60 1.18 o 2 5 19 0.63 -1.06 1.06 o 3 5 19 35.79 40.31 2.31 o 4 5 19 5.21 3.92 1.88 o 0 6 19 44.28 42.46 2.38 o 1 6 19 0.31 -0.20 1.16 o 2 6 19 0.62 0.06 1.14 o 0 0 20 1177.68 1292.80 24.94 o 1 0 20 5.01 1.80 1.57 o 2 0 20 90.33 90.67 3.15 o 3 0 20 8.41 5.92 1.67 o 4 0 20 1.93 3.68 1.63 o 5 0 20 12.63 9.97 3.11 o 1 1 20 7.72 7.86 1.22 o 2 1 20 2.85 2.46 1.09 o 3 1 20 0.13 -0.73 1.07 o 4 1 20 6.52 2.99 1.24 o 5 1 20 24.78 22.57 3.64 o 0 2 20 143.58 160.70 4.10 o 1 2 20 8.20 7.09 1.28 o 2 2 20 2.58 0.96 1.02 o 3 2 20 7.34 6.76 1.21 o 4 2 20 0.51 0.29 1.36 o 5 2 20 28.43 30.54 6.23 o 1 3 20 0.47 0.78 1.45 o 2 3 20 28.58 25.48 5.96 o 3 3 20 29.79 31.58 2.14 o 0 4 20 69.67 70.28 3.97 o 1 4 20 0.00 -1.25 1.25 o 2 4 20 9.09 9.54 3.35 o 3 4 20 14.95 18.43 4.06 o 4 4 20 1.53 1.21 1.74 o 1 5 20 5.09 5.58 1.64 o 2 5 20 29.48 30.32 5.74 o 1 1 21 174.66 191.46 7.15 o 2 1 21 11.91 12.90 1.40 o 3 1 21 2.49 1.48 1.19 o 4 1 21 0.90 -0.96 1.21 o 0 2 21 9.66 16.83 2.77 o 1 2 21 0.01 -1.17 1.17 o 2 2 21 11.14 8.63 1.33 o 3 2 21 1.15 1.88 1.24 o 4 2 21 6.05 2.81 1.78 o 1 3 21 39.41 36.70 3.66 o 2 3 21 23.35 18.34 2.17 o 3 3 21 17.89 8.29 2.03 o 0 4 21 9.03 12.72 2.70 o 1 4 21 28.65 15.52 3.20 o 2 4 21 1.32 1.41 1.57 o 0 0 22 95.96 101.03 4.97 o 1 0 22 6.38 7.02 1.91 o 2 0 22 1.91 1.98 1.79 o 3 0 22 20.72 14.51 2.25 o 1 1 22 0.17 3.13 1.69 o 2 1 22 0.02 -0.60 1.23 o 3 1 22 3.66 2.54 1.31 o 0 2 22 1.41 -0.30 2.20 o 1 2 22 0.01 1.33 2.82 o 2 2 22 0.17 -0.80 1.74 o 1 3 22 0.43 1.16 1.75 o